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On the Cover: Plasticity Bridges Microscale Martensitic Shear Bands in Superelastic Nitinol 封面:超弹性镍钛诺中微尺度马氏体剪切带的塑性桥梁
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-30 DOI: 10.1007/s11340-025-01188-9
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引用次数: 0
Improving Reversed Three-Point Bending Tests for Characterising the Fatigue Life of Polymers 改进了表征聚合物疲劳寿命的反向三点弯曲试验
IF 2.4 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-23 DOI: 10.1007/s11340-025-01184-z
S. Baril-Gosselin

Background

Cyclic loading is a leading cause of material failure and accurate testing methods are required to predict the life of components.

Objective

This work investigated the challenges of performing reversed three-point bending experiments for characterising the fatigue life of polymers and composites, and sought to develop guidelines for improving the testing method.

Methods

Testing was performed with polypropylene (PP) and glass-fibre reinforced PP on a test fixture that featured double-sided supports. Monotonic and fully reversed (i.e. stress ratio R = - 1) cyclic bending experiments were conducted to characterise the effects that the test conditions, including the type of supports and level of contact between the specimens and anvils, have on the measurements.

Results

Stresses generated during reversed bending are highly dependent on the type of fixture configuration used. Most configurations that were tested led to mechanical interlocking that altered the bending moments and generated membrane stresses. In this work, the purest form of reversed bending was achieved using double-sided pivoting supports, and a 0.35 mm gap between specimens and anvils to allow sliding in the supports.

Conclusions

This configuration provided the most similar stress state to that obtained from the standardised simply-supported beam experiments that are used for characterising the quasi-static flexural properties of materials, and was ultimately the configuration that provided the most reliable fatigue data.

循环载荷是导致材料失效的主要原因,因此需要精确的测试方法来预测部件的寿命。目的:本研究探讨了进行反向三点弯曲实验表征聚合物和复合材料疲劳寿命的挑战,并寻求制定改进测试方法的指导方针。方法采用聚丙烯(PP)和玻璃纤维增强PP在双面支撑的测试夹具上进行测试。进行单调和完全反向(即应力比R = - 1)循环弯曲实验,以表征测试条件的影响,包括支撑的类型和试件与砧之间的接触水平,对测量结果的影响。结果在反向弯曲过程中产生的应力高度依赖于所使用的夹具配置类型。大多数被测试的结构都会导致机械联锁,从而改变弯矩并产生膜应力。在这项工作中,最纯粹的反向弯曲形式是使用双面旋转支架实现的,样品和砧之间有0.35毫米的间隙,允许在支架中滑动。该配置提供了与标准化简支梁实验中获得的应力状态最相似的状态,用于表征材料的准静态弯曲性能,并且最终是提供最可靠的疲劳数据的配置。
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引用次数: 0
Mechanical Characterization of Additive-Manufactured Ti-6Al-4V Processed via Bound Metal Deposition 结合金属沉积增材制造Ti-6Al-4V的力学特性
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-23 DOI: 10.1007/s11340-025-01178-x
E. Devine, M. Lester, T. McElroy, T. Valenzuela, W. LePage

Background

Additive manufacturing (AM) is rapidly growing, with new AM methods continually in development. Alloys processed with novel methods require systematic characterization to understand and validate the materials, especially for demanding fields.

Objective

This study characterized the mechanical properties and failure mechanisms of a Ti-6Al-4V alloy manufactured with bound metal deposition (BMD), a form of metal extrusion (MEX) AM.

Methods

Specimens made of Ti64 were printed via Desktop Metal’s Studio System 2 through a printing, debinding, and sintering process. The microstructure was analyzed with optical metallography and a newly developed open-source porosity analysis tool. Scanning electron microscopy (SEM), optical microscopy, and compositional analysis of green, brown, and sintered parts were conducted to study the material and its failure modes. Sintered specimens were tensile and hardness tested.

Results

As-sintered specimens exhibited ductility more than 10 times lower than wrought Ti64, partially due to contamination/impurity that formed brittle (alpha )-case titanium. Sources of contamination may have included the sacrificial Al(_2)O(_3) interlayer, the wax/polymer binder, and/or impurity introduction from the furnace. Fractography imaging found quasi-cleavage fracture initiating at areas of high surface roughness along the ceramic interlayer surface of the parts and transitioning into dimple rupture and intergranular decohesion.

Conclusions

Elevated contamination levels, high surface roughness, and internal porosity led to low elongation and ultimate strength in the Ti64 BMD alloy. With the processing route presented here, BMD for Ti64 may not be suitable for applications that demand high ductility and strength with minimal impurities, although with process refinement, the method may be promising for certain applications

随着新的增材制造方法的不断发展,增材制造(AM)正在迅速发展。用新方法加工的合金需要系统的表征来理解和验证材料,特别是在要求苛刻的领域。目的研究结合金属沉积法(BMD)制备的Ti-6Al-4V合金的力学性能和失效机理。方法采用Desktop Metal 's Studio System 2对Ti64试样进行打印、脱脂和烧结处理。利用光学金相学和新开发的开源孔隙度分析工具对其微观结构进行了分析。通过扫描电子显微镜(SEM)、光学显微镜以及对绿色、棕色和烧结件的成分分析来研究材料及其失效模式。对烧结试样进行拉伸和硬度测试。结果as -烧结试样的延展性比变形Ti64低10倍以上,部分原因是污染/杂质形成了脆性(alpha ) -case钛。污染源可能包括牺牲的Al (_2) O (_3)中间层、蜡/聚合物粘合剂和/或从炉中引入的杂质。断口成像发现,准解理断裂始于零件沿陶瓷层间表面的高表面粗糙度区域,然后转变为韧窝断裂和晶间脱黏。结论高污染水平、高表面粗糙度和内部孔隙率导致Ti64 BMD合金伸长率和极限强度较低。根据本文提出的工艺路线,Ti64的BMD可能不适合要求高延展性和强度且杂质最少的应用,尽管经过工艺改进,该方法可能对某些应用有希望
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引用次数: 0
Mechanics of Additively Manufactured Materials 增材制造材料力学
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-23 DOI: 10.1007/s11340-025-01181-2
L.R. Xu, G. J. Pataky
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引用次数: 0
4D Porosity Evolution in Additively Manufactured 316L Stainless Steel through In-Situ Tensile Testing and X-Ray Computed Tomography 通过原位拉伸测试和x射线计算机断层扫描,增材制造316L不锈钢的4D孔隙演化
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-17 DOI: 10.1007/s11340-025-01180-3
D. Hertz-Eichenrode, H. Talebinezhad, A. Shmatok, R.D. Fischer, S. Bremen, W. Reichert, B.C. Prorok

Background

Many aspects of ductile failure through microvoid coalescence remain elusive due to the challenging spatial and temporal scales it operates on. Experimentally resolving all aspects of the process remains a significant goal of researchers. Much of the current understanding has been derived from post-mortem metallography, leaving key aspects of its evolution undocumented.

Objective

This work builds on efforts using X-ray computed tomography (XCT) characterize voids and their evolution under loading.

Methods

It employs in-situ XCT tensile testing on 316L Stainless Steel samples that were constructed by laser powder bed fusion that contain tailored, pre-existing voids with a spatial scale relevant to the growth and evolution stages of microvoid coalescence. Pre-existing voids extended the observation window for monitoring void growth and interaction under loading. They also enhanced fiducial correlation of voids during deformation.

Results

Void populations were found to increase under loading as their deformed dimensions rendered them detectable by the XCT algorithm. Neighboring voids underwent interconnection events by a cleavage process when stress concentrations between them exceeded the macroscopic yield stress. Pores that did not undergo interconnection events were found to revert to their initial size and population after unloading. Finally, the porosity structure before failure was correlated to features on the fracture surface with high fidelity.

Conclusions

This unique combination of in-situ XCT tensile testing on samples with tailored void structure enabled new visualization and quantification of void evolution under load as well as strong correlation to the observed stress–strain behavior and post-mortem fracture characteristics.

由于微孔隙聚结作用的空间和时间尺度具有挑战性,许多方面的延性破坏仍然难以捉摸。通过实验解决这一过程的各个方面仍然是研究人员的一个重要目标。目前的认识大多来自于死后的金相学,对其演化的关键方面没有记载。目的利用x射线计算机断层扫描(XCT)表征孔隙及其在载荷作用下的演变。方法采用原位XCT拉伸测试方法对316L不锈钢试样进行拉伸测试。316L不锈钢试样采用激光粉末床熔融法制备,含有定制的预先存在的孔洞,其空间尺度与微孔洞合并的生长和演化阶段相关。预先存在的孔洞扩大了监测孔洞生长和在载荷作用下相互作用的观察窗口。它们还增强了变形过程中空洞的基准相关性。结果发现在载荷作用下,由于其变形的尺寸使其可以被XCT算法检测到,因此空洞种群增加。当相邻孔洞之间的应力集中超过宏观屈服应力时,邻近孔洞通过解理过程发生相互连接。未经历互连事件的孔隙在卸载后恢复到初始大小和数量。最后,将断裂前孔隙结构与断口特征进行了高保真关联。这种独特的原位XCT拉伸测试结合了定制的孔洞结构,使孔洞在载荷下的演变具有了新的可视化和量化,并且与观察到的应力-应变行为和死后断裂特征有很强的相关性。
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引用次数: 0
Estimation of Elastic Modulus with Multiple Indenters 多压头弹性模量的估计
IF 2.4 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-14 DOI: 10.1007/s11340-025-01173-2
Y. Yoon, G. Han, N. Kim, H. Lee

The conventional Oliver-Pharr method of estimating elastic modulus shows reasonably good accuracy, but errors occur due to inaccuracies in the actual contact area.

To resolve this issue, this study proposed a new method to estimate the elastic modulus using two different indenters without additional equipment or complicated calibration. We aimed to estimate the elastic modulus using the theoretical indentation depth, without the consideration of sink-in / pile-up effect.

A numerical indentation test was performed using Berkovich and spherical indenters, and the theoretical contact area and initial unloading slope of the indentation load-depth curve were calculated to derive c-ratio based on the correction factor c. Numerical validation using finite element analysis for various material properties of J2 and pressure-dependent hardening models showed that the method estimates the elastic modulus with R 2 = 98 %, outperforming the conventional method.

Microindentation tests were conducted on copper, Al1050, SS304 specimens for experimental validation. The estimated elastic moduli with proposed method showed good agreement with those from tensile tests with an error of 7 %.

This study proposed a new method for estimating elastic modulus that overcomes the limitations of the conventional method, which is difficult to accurately measure the actual contact area at maximum load, and has high applicability to various materials by using the correction factor c.

传统的估算弹性模量的oliver - farr方法具有较好的精度,但由于实际接触面积的不精确而产生误差。为了解决这一问题,本研究提出了一种利用两个不同的压头估算弹性模量的新方法,无需额外的设备或复杂的校准。我们的目标是使用理论压痕深度来估计弹性模量,而不考虑下沉/堆积效应。采用Berkovich和球形压头进行了数值压痕试验,计算了压痕载荷-深度曲线的理论接触面积和初始卸载斜率,并基于修正系数c推导出了c比。基于J2各种材料特性的有限元分析和压力相关硬化模型的数值验证表明,该方法估算的弹性模量r2 = 98%,优于传统方法。对铜、Al1050、SS304试样进行了微压痕实验验证。用该方法估算的弹性模量与拉伸试验结果吻合较好,误差为7%。本研究提出了一种估算弹性模量的新方法,克服了传统方法在最大载荷下难以准确测量实际接触面积的局限性,并利用修正系数c对各种材料具有较高的适用性。
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引用次数: 0
A Robust Deep Learning-Assisted Digital Image Correlation for Deformation Measurement at 1600 °C in Air 一种鲁棒深度学习辅助数字图像相关在1600°C空气中的变形测量
IF 2.4 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-14 DOI: 10.1007/s11340-025-01182-1
G. Niu, R. Zhu, Z. Qu, H. Lei, P. Wang, H. Yang, D. Fang

Digital image correlation (DIC) is an image-based deformation measurement method. However, problems such as heat haze, speckle oxidation and debonding, and image overexposure in ultra-high-temperature environments lead to image degradation and compromise the reliability of deformation measurement.

This study proposes a robust and high-precision DIC algorithm designed to measure deformation stably from low-quality speckle images by leveraging machine learning. An ultra-high-temperature in-situ X-ray imaging device addresses challenges like speckle instability and heat haze interference. The proposed algorithm and experimental device are combined to measure the deformation field at 1600 °C in air.

A novel image matching network-assisted digital image correlation (IMN-DIC) is proposed. This approach uses a deep learning-based image matching network to extract and match features for initial displacement estimation. Subsequently, an iterative algorithm based on the inverse compositional Gauss–Newton (IC-GN) method is applied to achieve sub-pixel accuracy in high-temperature deformation field measurements. Numerical experiments and real experiments of C/SiC composite samples under tension at 1600 °C in the air with optical and X-ray imaging were carried out to verify the effectiveness of the IMN-DIC.

For high-quality optical speckle images, IMN-DIC achieved comparable measurement accuracy but with greater computational efficiency than previous feature-based DIC methods. In X-ray images captured at 1600 °C in air, the traditional DIC method successfully processed only 50.17% of points of interest (POIs), whereas IMN-DIC achieved 98.96%, demonstrating superior robustness.

The IMN-DIC method exhibits high robustness, reliably capturing deformation data from low-quality speckle images with weak textures and high noise levels. This approach holds significant promise for applications in extreme environments where artificial speckle generation is challenging and image quality is compromised.

数字图像相关(DIC)是一种基于图像的变形测量方法。然而,在超高温环境下,热雾、斑点氧化和脱粘、图像过度曝光等问题导致图像退化,影响变形测量的可靠性。本研究提出了一种鲁棒的高精度DIC算法,旨在利用机器学习稳定地测量低质量散斑图像的变形。一种超高温原位x射线成像设备解决了散斑不稳定性和热雾干扰等挑战。将该算法与实验装置相结合,测量了空气中1600℃时的变形场。提出了一种新的图像匹配网络辅助数字图像相关(IMN-DIC)。该方法使用基于深度学习的图像匹配网络来提取和匹配初始位移估计的特征。随后,采用基于逆成分高斯-牛顿(IC-GN)法的迭代算法,实现了高温变形场测量的亚像素精度。为了验证IMN-DIC的有效性,对C/SiC复合材料样品在1600℃空气中拉伸的光学和x射线成像进行了数值实验和实际实验。对于高质量的光学散斑图像,IMN-DIC获得了相当的测量精度,但比以前基于特征的DIC方法具有更高的计算效率。在1600°C空气中捕获的x射线图像中,传统DIC方法成功处理了50.17%的兴趣点(poi),而IMN-DIC方法成功处理了98.96%,显示出优越的鲁棒性。IMN-DIC方法具有很高的鲁棒性,能够可靠地捕获纹理弱、噪声水平高的低质量散斑图像的形变数据。这种方法对于极端环境中的应用具有重要的前景,在极端环境中,人工散斑产生具有挑战性,图像质量受到损害。
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引用次数: 0
Evaluation of an Improved Filtering Method for Strain Measurement at High Temperatures Using 2D-DIC 基于2D-DIC的高温应变测量改进滤波方法的评价
IF 2.4 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-12 DOI: 10.1007/s11340-025-01174-1
L. P. Luong, G. Alonso Aruffo, R. Bonnaire, L. Penazzi

Background

The Two-Dimensional Digital Image Correlation (2D-DIC) method is widely used as a non-contact full-field kinematic measurement, but it presents significant errors related to temperature effects including the image con- trast and heat waves. Consequently, results of mechanical displacement or strain measured by the 2D-DIC method, especially strains in the elastic domain of materials, is significantly dispersed.

Objective

The aim of this study is to propose a very simple 2D-DIC method, using commercial DIC software with no need of additional storage to accurately measure strain and displacements at high temperatures, typically at the hot metal forming temperatures, from 400 C to 750 C.

Methods

This study demonstrates the influence of temperature effects (radiation and heat waves) on strain measurements obtained with the 2D-DIC method in the elastic regime (ε < 0.05) of the TA6V titanium alloy material at high temperatures. Furthermore, the strain measurement errors at different temperatures were characterized by the Background Oriented Schlieren technique (BOS). Correction methods using temperature-dependent low-pass filters for strain measurement errors are suggested.

Results

The correction methods allow separating mechanical strain fields and strain measurement errors caused by temperature effects. The efficiency of the correction methods is demonstrated by identifying the Young’s modulus (E) and the Thermal Expansion Coefficient (TEC) of the TA6V. After corrections, E and the TEC of the TA6V are close to the reference values found in the literature. Conclusion: The coefficient R2 from the linear regression method to determine the Young’s modulus from tensile test at 600 C increases from 0.783 to 0.989, revealing the great potential of using the improved-2D-DIC method for full-field kinematic measurements of mechanical tests at high temperatures.

二维数字图像相关(2D-DIC)方法作为一种非接触式全场运动测量方法被广泛使用,但由于温度效应,包括图像对比度和热浪,该方法存在较大的误差。因此,用2D-DIC方法测量的机械位移或应变的结果,特别是材料弹性域中的应变,是明显分散的。本研究的目的是提出一种非常简单的2D-DIC方法,使用商业DIC软件,不需要额外的存储,在高温下精确测量应变和位移,通常在热金属成形温度,从400◦C到750◦C。方法研究了温度效应(辐射和热浪)对高温下TA6V钛合金材料弹性区(ε < 0.05) 2D-DIC法测量应变的影响。利用背景取向纹影技术(BOS)对不同温度下的应变测量误差进行了表征。提出了利用温度相关低通滤波器对应变测量误差进行校正的方法。结果校正方法可将机械应变场与温度效应引起的应变测量误差分离开来。通过确定TA6V的杨氏模量(E)和热膨胀系数(TEC),验证了修正方法的有效性。修正后,TA6V的E和TEC接近文献中的参考值。结论:线性回归法测定600℃拉伸试验杨氏模量的R2系数从0.783增加到0.989,揭示了使用改进的2d - dic方法进行高温力学试验的全场运动学测量的巨大潜力。
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引用次数: 0
A Strain Field Reconstruction Method Based on Digital Twin by Multi-Level Fusion of Multi-Type Data 基于数字孪生的多类型数据多级融合应变场重建方法
IF 2.4 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-11 DOI: 10.1007/s11340-025-01183-0
B. Wang, X. Ke, J. Wang, K. Liu, Z. Song, J. Zhou, C. Zhou

Background

Finite element analysis (FEA), digital image correlation (DIC), and strain gauge are usually used for test monitoring. Reconstructed by FEA strain field and strain gauges, the fusion field (DT-SFRM) has higher accuracy than FEA, and DT-SFRM accuracy is acceptable for small structural deformation. However, large deformation of thin-walled structures is accompanied by complex strain field, and the difference in strain distribution between FEA and strain gauges data increases sharply. The low-accuracy FEA strain field and small amount of strain gauges lead to insufficient accuracy of DT-SFRM.

Objective

This study aims to construct a high-accuracy strain field for test monitoring.

Methods

A strain field reconstruction method based on digital twin (DT) by multi-level fusion of multi-type data (DT-MFMD) is proposed. Large number of relatively high-accuracy DIC data is used to improve global FEA strain field accuracy. The high-accuracy strain gauges are used to further improve fusion field accuracy of FEA and DIC. A tensile test of large opening plate shell (LOPS) is performed to verify the advantage of DT-MFMD.

Results

The AvgErr (6.6%) and MaxErr (23.5%) of DT-MFMD are 16.0% and 58.8% lower than those of DT-SFRM, and the DT-MFMD is less affected by large deformation. In addition, the strain gauges number of DT-MFMD reduces by more than 62.5% under the same accuracy goal compared with that of DT-SFRM.

Conclusions

The DT-MFMD is validated to have a better application prospect for large deformation and complex strain field distribution.

试验监测通常采用有限元分析(FEA)、数字图像相关(DIC)和应变片等方法。通过有限元应变场和应变片重建,融合场(DT-SFRM)具有比有限元分析更高的精度,对于较小的结构变形,DT-SFRM精度可以接受。然而,薄壁结构的大变形伴随着复杂的应变场,有限元分析与应变片数据之间的应变分布差异急剧增大。由于有限元应变场精度低,应变片数量少,导致DT-SFRM精度不足。目的建立用于试验监测的高精度应变场。方法提出基于数字孪生(DT)的多类型数据多级融合应变场重建方法(DT- mfmd)。为了提高整体有限元应变场精度,采用了大量相对高精度的DIC数据。采用高精度应变片进一步提高了FEA和DIC的融合场精度。通过大开口板壳(LOPS)的拉伸试验,验证了DT-MFMD的优势。结果DT-MFMD的AvgErr(6.6%)和MaxErr(23.5%)分别比DT-SFRM低16.0%和58.8%,且DT-MFMD受大变形影响较小。在相同精度目标下,DT-MFMD的应变片数量比DT-SFRM减少了62.5%以上。结论DT-MFMD在大变形、复杂应变场分布等方面具有较好的应用前景。
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引用次数: 0
On the Cover: Fatigue Damage Evolution in SS316L Produced by Powder Bed Fusion in Different Orientations with Reused Powder Feedstock 封面:重复使用粉末原料不同取向粉末床熔合生产的SS316L疲劳损伤演化
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-04 DOI: 10.1007/s11340-025-01179-w
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引用次数: 0
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Experimental Mechanics
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