Pub Date : 2023-10-17DOI: 10.1007/s11340-023-01005-1
Y. Zhang, Y. Duan, P. Fu, S. Qi, J. Zhao
{"title":"On Orthotropic Elastic Constitutive Modeling for Springback Prediction","authors":"Y. Zhang, Y. Duan, P. Fu, S. Qi, J. Zhao","doi":"10.1007/s11340-023-01005-1","DOIUrl":"https://doi.org/10.1007/s11340-023-01005-1","url":null,"abstract":"","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-10-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136032873","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-10-13DOI: 10.1007/s11340-023-00997-0
M. Grédiac, X. Balandraud, B. Blaysat, T. Jailin, R. Langlois, F. Sur, A. Vinel
Background
Reliably measuring sharp details in displacement and strain maps returned by full-field measurement techniques remains an open question in the photomechanics community.
Objective
The primary objective of this study is to improve and fine-tune a deconvolution algorithm in order to limit the blur that obscures the details in displacement and strain maps.
Methods
Checkerboard patterns are used and processed with a spectral method, namely the Localized Spectrum Analysis (LSA), and the raw maps returned by this technique are deconvolved. The influence of various settings on the quality of the results is studied by using synthetic images deformed through a well-vetted reference displacement field.
Results
It is shown that linking the size of the analysis window used in LSA on the one hand, and the size of the second derivative kernel employed in the deconvolution algorithm on the other hand, ensures the convergence of the deconvolution algorithm in all cases. This was not the case with the initial version. The ratio between these sizes, which optimizes the metrological performance of LSA followed by deconvolution, is identified. The influence of the sampling density of the checkerboard pattern in the images is also examined. The efficiency of the deconvolution algorithm employed with optimized settings is illustrated with strain maps obtained on two specimens, one in shape memory alloy, and the other in wood.
Conclusions
It is shown in this study that deconvolution with optimized settings is an effective tool to enhance small and sharp details in strain maps obtained with LSA.
{"title":"Fine-Tuning a Deconvolution Algorithm to Restore Displacement and Strain Maps Obtained with LSA","authors":"M. Grédiac, X. Balandraud, B. Blaysat, T. Jailin, R. Langlois, F. Sur, A. Vinel","doi":"10.1007/s11340-023-00997-0","DOIUrl":"10.1007/s11340-023-00997-0","url":null,"abstract":"<div><h3>Background</h3><p>Reliably measuring sharp details in displacement and strain maps returned by full-field measurement techniques remains an open question in the photomechanics community.</p><h3>Objective</h3><p>The primary objective of this study is to improve and fine-tune a deconvolution algorithm in order to limit the blur that obscures the details in displacement and strain maps.</p><h3>Methods</h3><p>Checkerboard patterns are used and processed with a spectral method, namely the Localized Spectrum Analysis (LSA), and the raw maps returned by this technique are deconvolved. The influence of various settings on the quality of the results is studied by using synthetic images deformed through a well-vetted reference displacement field.</p><h3>Results</h3><p>It is shown that linking the size of the analysis window used in LSA on the one hand, and the size of the second derivative kernel employed in the deconvolution algorithm on the other hand, ensures the convergence of the deconvolution algorithm in all cases. This was not the case with the initial version. The ratio between these sizes, which optimizes the metrological performance of LSA followed by deconvolution, is identified. The influence of the sampling density of the checkerboard pattern in the images is also examined. The efficiency of the deconvolution algorithm employed with optimized settings is illustrated with strain maps obtained on two specimens, one in shape memory alloy, and the other in wood.</p><h3>Conclusions</h3><p>It is shown in this study that deconvolution with optimized settings is an effective tool to enhance small and sharp details in strain maps obtained with LSA.</p></div>","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2023-10-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135855628","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-10-13DOI: 10.1007/s11340-023-01003-3
S. S. Chen, D. Cai, J. J. Cui, G. Y. Li, H. Jiang
{"title":"Optimization on Cruciform Specimen Geometries of AA5052 Under Equi-Biaxial Loading: Acquisition of Ultimate Fracture Strain","authors":"S. S. Chen, D. Cai, J. J. Cui, G. Y. Li, H. Jiang","doi":"10.1007/s11340-023-01003-3","DOIUrl":"https://doi.org/10.1007/s11340-023-01003-3","url":null,"abstract":"","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-10-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135855028","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-10-13DOI: 10.1007/s11340-023-01004-2
H. Koruk, H. O. Koc, S. B. Yurdaer, A. Besli, A. N. Pouliopoulos
Abstract Background There are several techniques to characterize the mechanical properties of soft materials, such as the indentation method and the method based on the application of a spherical object placed inside the sample. The indentation systems usually yield the elastic properties of materials and their mathematical models do not consider the inertia of the sample involved in motion and radiation damping, while placing an object inside the sample is not practical and this procedure can alter the mechanical properties of the sample for the method based on the application of a bubble/sphere placed inside the sample. Objective A new approach for the identification of the viscoelastic properties of soft materials using the dynamic response of a spherical object placed at the sample interface was proposed. Methods The spherical object placed at the sample interface was pressed using an electromagnet and the dynamic response of the spherical object was tracked using a high-speed camera, while the dynamic response of the spherical object placed at the sample interface was estimated using a comprehensive analytical model. The effects of the shear modulus, viscosity, Poisson’s ratio and density of the soft sample, the radius and density of the spherical object and the damping due to radiation were considered in this mathematical model. The shear modulus and viscosity of the soft sample were determined by matching the experimentally identified and theoretically estimated responses of the spherical object. Results The shear moduli and viscosities of the three phantoms with the gelatin mass ratios of 0.20, 0.25 and 0.29 were measured to be 3450, 4300 and 4950 Pa and 12.5, 14.0 and 15.0 Pa⋅s, respectively. The shear modulus and viscosity of the phantom increases as the gelatin mass ratio increases. The frequency of oscillations of the hemisphere placed at the phantom interface increases as the gelatin mass ratio increases due to stiffness increase. Conclusions After matching the experimental and theoretical steady-state displacements and amplitudes of oscillations of the hemisphere at the sample interface, the comparison of the experimentally identified and theoretically predicted frequency of oscillations further confirmed the identified material properties of the samples. The approach presented here is expected to provide valuable information on material properties in biomedical and industrial applications.
{"title":"A New Approach for Measuring Viscoelastic Properties of Soft Materials Using the Dynamic Response of a Spherical Object Placed at the Sample Interface","authors":"H. Koruk, H. O. Koc, S. B. Yurdaer, A. Besli, A. N. Pouliopoulos","doi":"10.1007/s11340-023-01004-2","DOIUrl":"https://doi.org/10.1007/s11340-023-01004-2","url":null,"abstract":"Abstract Background There are several techniques to characterize the mechanical properties of soft materials, such as the indentation method and the method based on the application of a spherical object placed inside the sample. The indentation systems usually yield the elastic properties of materials and their mathematical models do not consider the inertia of the sample involved in motion and radiation damping, while placing an object inside the sample is not practical and this procedure can alter the mechanical properties of the sample for the method based on the application of a bubble/sphere placed inside the sample. Objective A new approach for the identification of the viscoelastic properties of soft materials using the dynamic response of a spherical object placed at the sample interface was proposed. Methods The spherical object placed at the sample interface was pressed using an electromagnet and the dynamic response of the spherical object was tracked using a high-speed camera, while the dynamic response of the spherical object placed at the sample interface was estimated using a comprehensive analytical model. The effects of the shear modulus, viscosity, Poisson’s ratio and density of the soft sample, the radius and density of the spherical object and the damping due to radiation were considered in this mathematical model. The shear modulus and viscosity of the soft sample were determined by matching the experimentally identified and theoretically estimated responses of the spherical object. Results The shear moduli and viscosities of the three phantoms with the gelatin mass ratios of 0.20, 0.25 and 0.29 were measured to be 3450, 4300 and 4950 Pa and 12.5, 14.0 and 15.0 Pa⋅s, respectively. The shear modulus and viscosity of the phantom increases as the gelatin mass ratio increases. The frequency of oscillations of the hemisphere placed at the phantom interface increases as the gelatin mass ratio increases due to stiffness increase. Conclusions After matching the experimental and theoretical steady-state displacements and amplitudes of oscillations of the hemisphere at the sample interface, the comparison of the experimentally identified and theoretically predicted frequency of oscillations further confirmed the identified material properties of the samples. The approach presented here is expected to provide valuable information on material properties in biomedical and industrial applications.","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-10-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135854834","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-10-10DOI: 10.1007/s11340-023-01001-5
A. Greco, E. Sgambitterra, F. Furgiuele, D. Furfari
Background
The accurate measurement of residual stresses (RS) is crucial for predicting the performance of mechanical components, as RS can significantly impact fatigue life, fracture, corrosion, and wear resistance. Different experimental methods were developed to measure RS, including non-destructive techniques. Among these methods, instrumented nanoindentation has emerged as a promising approach to assess equi- or non-equi-biaxial RS states. This technique analyzes variations in the mechanical response of indentation on a stressed or stress-free component to estimate residual stresses. Previous studies proposed different approaches to establish a relationship between RS and indentation parameters, such as contact area, peak load, mean contact pressure, indentation work, etc. However, the correlation between RS and peak load variation, commonly assumed to be linear, showed limitations, particularly when dealing with compressive RS.
Objective
The aim of this work is to develop a hybrid procedure, based on finite element (FEM) simulations and experimental analyses, to measure the equi-biaxial residual stresses. In particular, it is based on the analysis of the nanoindentation peak load variation generated by the presence of residual stresses on a component.
Methods
To overcome the limitations of the linear assumption, nanoindentation experiments were combined with finite element analyses (FEA). FEA simulations were used to estimate the correlation between RS and peak load variation, providing a better understanding of the non-linear relationship. A proper experimental setup, consisting in a stress generating jig, was designed and manufactured to perform nanoindentations on a sample, made by aluminium alloy AA 7050 T451, subjected to external mechanical stress with the aim to validate the FEA model. FEA and the digital image correlation (DIC) technique were also used to verify that the induced stress field was the expected one.
Results
Obtained results revealed that the proposed method is a valid way to measure residual stresses. In fact, it offers an improved correlation between RS and peak load variation. In addition, by integrating nanoindentation experiments and FEA, a more accurate assessment of RS can be also achieved.
Conclusions
This research contributes to the development of a consistent methodology for RS measurement using instrumented nanoindentation.
{"title":"A Novel Method to Measure Equi-Biaxial Residual Stress by Nanoindentation","authors":"A. Greco, E. Sgambitterra, F. Furgiuele, D. Furfari","doi":"10.1007/s11340-023-01001-5","DOIUrl":"10.1007/s11340-023-01001-5","url":null,"abstract":"<div><h3>Background</h3><p>The accurate measurement of residual stresses (RS) is crucial for predicting the performance of mechanical components, as RS can significantly impact fatigue life, fracture, corrosion, and wear resistance. Different experimental methods were developed to measure RS, including non-destructive techniques. Among these methods, instrumented nanoindentation has emerged as a promising approach to assess equi- or non-equi-biaxial RS states. This technique analyzes variations in the mechanical response of indentation on a stressed or stress-free component to estimate residual stresses. Previous studies proposed different approaches to establish a relationship between RS and indentation parameters, such as contact area, peak load, mean contact pressure, indentation work, etc. However, the correlation between RS and peak load variation, commonly assumed to be linear, showed limitations, particularly when dealing with compressive RS.</p><h3>Objective</h3><p>The aim of this work is to develop a hybrid procedure, based on finite element (FEM) simulations and experimental analyses, to measure the equi-biaxial residual stresses. In particular, it is based on the analysis of the nanoindentation peak load variation generated by the presence of residual stresses on a component.</p><h3>Methods</h3><p>To overcome the limitations of the linear assumption, nanoindentation experiments were combined with finite element analyses (FEA). FEA simulations were used to estimate the correlation between RS and peak load variation, providing a better understanding of the non-linear relationship. A proper experimental setup, consisting in a stress generating jig, was designed and manufactured to perform nanoindentations on a sample, made by aluminium alloy AA 7050 T451, subjected to external mechanical stress with the aim to validate the FEA model. FEA and the digital image correlation (DIC) technique were also used to verify that the induced stress field was the expected one.</p><h3>Results</h3><p>Obtained results revealed that the proposed method is a valid way to measure residual stresses. In fact, it offers an improved correlation between RS and peak load variation. In addition, by integrating nanoindentation experiments and FEA, a more accurate assessment of RS can be also achieved.</p><h3>Conclusions</h3><p>This research contributes to the development of a consistent methodology for RS measurement using instrumented nanoindentation.</p></div>","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2023-10-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s11340-023-01001-5.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136294507","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-10-03DOI: 10.1007/s11340-023-01002-4
D. Long, Q. Chen, D. Xiang, M. Zhong, H. Zhang
Background
Rubber mounts are widely used to isolate vibrating components. Their complex stiffness characteristics, including dynamic stiffness and loss factors, are highly concerning in terms of vibration analysis and optimization. Rubber mounts show non-linear behavior with preload, leading to difficulty to predict their complex stiffness. Dynamic testing is generally necessary.
Objective
An approach to identify the complex stiffness of preloaded rubber mounts in both vertical and horizontal directions simultaneously is developed.
Methods
Tested Frequency Response Functions (FRF) of a mass suspended by rubber mounts are transformed to an FRF matrix of the mass center to decouple the Z Degrees of Freedom (DOF) and RZ DOF from other DOFs, which allows complex stiffness to be identified from the two decoupled DOFs. A software tool to implement automatically the FRF transformation and parameter identification is developed. An EPDM rubber mount is tested using the device and its complex stiffness is identified using the software to validate the proposed approach.
Results
The driving-point FRFs of the mass center calculated from the identified complex stiffness are very close to the corresponding FRFs determined from the test data. The comparison between the Finite-Element Analysis (FEA) results of the surficial FRFs and the test results shows good consistency as well. Therefore, the proposed approach and its supporting algorithm are validated.
Conclusion
the proposed approach allows for swift identification of high-accuracy complex stiffness of preloaded rubber mounts in both vertical and horizontal directions simultaneously.
{"title":"Simultaneous Identification of Vertical and Horizontal Complex Stiffness of Preloaded Rubber Mounts: Transformation of Frequency Response Functions and Decoupling of Degrees of Freedom","authors":"D. Long, Q. Chen, D. Xiang, M. Zhong, H. Zhang","doi":"10.1007/s11340-023-01002-4","DOIUrl":"10.1007/s11340-023-01002-4","url":null,"abstract":"<div><h3>Background</h3><p>Rubber mounts are widely used to isolate vibrating components. Their complex stiffness characteristics, including dynamic stiffness and loss factors, are highly concerning in terms of vibration analysis and optimization. Rubber mounts show non-linear behavior with preload, leading to difficulty to predict their complex stiffness. Dynamic testing is generally necessary.</p><h3>Objective</h3><p>An approach to identify the complex stiffness of preloaded rubber mounts in both vertical and horizontal directions simultaneously is developed.</p><h3>Methods</h3><p>Tested Frequency Response Functions (FRF) of a mass suspended by rubber mounts are transformed to an FRF matrix of the mass center to decouple the <i>Z</i> Degrees of Freedom (DOF) and <i>RZ</i> DOF from other DOFs, which allows complex stiffness to be identified from the two decoupled DOFs. A software tool to implement automatically the FRF transformation and parameter identification is developed. An EPDM rubber mount is tested using the device and its complex stiffness is identified using the software to validate the proposed approach.</p><h3>Results</h3><p>The driving-point FRFs of the mass center calculated from the identified complex stiffness are very close to the corresponding FRFs determined from the test data. The comparison between the Finite-Element Analysis (FEA) results of the surficial FRFs and the test results shows good consistency as well. Therefore, the proposed approach and its supporting algorithm are validated.</p><h3>Conclusion</h3><p>the proposed approach allows for swift identification of high-accuracy complex stiffness of preloaded rubber mounts in both vertical and horizontal directions simultaneously.</p></div>","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2023-10-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135696068","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-09-28DOI: 10.1007/s11340-023-00996-1
I. Levin, D. Rittel
Objective
Validate and assess the limitations of the Shear Compression 0 Specimen (SCS0) as a simple shear specimen for quasi-static and dynamic large strain loading conditions. Propose a simple data reduction procedure, using a simple, back of the envelope method, as a first approximation for the strain, as opposed to cumbersome numerical simulations and avoid the use of ad-hoc data reduction factors.
Methods
Static and dynamic finite elements simulations were performed in which the large deformation options was turned on and off. Assessment of the Lode parameter in each case and evaluation of the accuracy of the specimen’s strains and stresses as determined through simple data reduction and full numerical simulations.
Results
The SCS0 was shown to undergo simple shear, both statically and dynamically, as evidenced from the very low values of the Lode parameter. The calculated stress is in excellent agreement with the measured one, determined using simple strength of materials definitions. When assuming the corresponding kinematics, it is observed that the calculated and the measured strain diverge to an extent of about 25%. This discrepancy is shown to result from the assumption of large geometrical deformations in the numerical model as opposed to the simple analytical kinematics.
Conclusion
The conclusion is that the SCS0 is now fully validated, and the experimentalist will decide which strain approximation is suitable, between analytical and numerical.
目标 验证和评估剪切压缩 0 号试样(SCS0)作为准静态和动态大应变加载条件下的简单剪切试样的局限性。提出一种简单的数据还原程序,使用简单的包络后退法作为应变的第一近似值,而不是繁琐的数值模拟,并避免使用临时数据还原因子。对每种情况下的 Lode 参数进行评估,并对通过简单数据缩减和完全数值模拟确定的试样应变和应力的准确性进行评估。计算得出的应力与使用简单材料强度定义确定的测量应力非常吻合。假设采用相应的运动学原理,可以发现计算应变和测量应变的偏差约为 25%。结论是 SCS0 现在已得到充分验证,实验人员将决定在分析和数值之间选择哪种应变近似方法更合适。
{"title":"Making Shear Simple – Validation of the Shear Compression Specimen 0 (SCS0) for Shear Testing","authors":"I. Levin, D. Rittel","doi":"10.1007/s11340-023-00996-1","DOIUrl":"10.1007/s11340-023-00996-1","url":null,"abstract":"<div><h3>Objective</h3><p>Validate and assess the limitations of the Shear Compression 0 Specimen (SCS0) as a simple shear specimen for quasi-static and dynamic large strain loading conditions. Propose a simple data reduction procedure, using a simple, back of the envelope method, as a first approximation for the strain, as opposed to cumbersome numerical simulations and avoid the use of ad-hoc data reduction factors.</p><h3>Methods</h3><p>Static and dynamic finite elements simulations were performed in which the large deformation options was turned on and off. Assessment of the Lode parameter in each case and evaluation of the accuracy of the specimen’s strains and stresses as determined through simple data reduction and full numerical simulations.</p><h3>Results</h3><p>The SCS0 was shown to undergo simple shear, both statically and dynamically, as evidenced from the very low values of the Lode parameter. The calculated stress is in excellent agreement with the measured one, determined using simple strength of materials definitions. When assuming the corresponding kinematics, it is observed that the calculated and the measured strain diverge to an extent of about 25%. This discrepancy is shown to result from the assumption of large geometrical deformations in the numerical model as opposed to the simple analytical kinematics.</p><h3>Conclusion</h3><p>The conclusion is that the SCS0 is now fully validated, and the experimentalist will decide which strain approximation is suitable, between analytical and numerical.</p></div>","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2023-09-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135385082","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-09-19DOI: 10.1007/s11340-023-00999-y
L. Summey, J. Zhang, A.K. Landauer, J. Sergay, J. Yang, A. Daul, J. Tao, J. Park, A. McGhee, C. Franck
Background
Intermediate-strain-rate mechanical testing of soft and biological materials is important when designing, measuring, predicting, or manipulating an object or system’s response to common impact scenarios. Open source micro-mechanical test instruments that provide high spatial and temporal resolution volumetric strain field measurements, non-destructive testing and gripping of soft materials with low elastic moduli, programmable strain rates spanning from (10^{-6}) s(^{-1}) to (10^{2}) s(^{-1}), and biocompatibility for living cell cultures and tissues in one instrument are lacking in the current literature.
Methods
We introduce a micro-tensile testing device developed to meet all these criteria while being straightforwardly accessible to the end user. This device sits atop an inverted microscope stage, granting the researcher access to 3D spatial resolutions as low as 100 nm and frame rates only limited by the camera speed and availability of recordable photons. The micro-tensile specimen is attached to the test device by a specially designed fixture. This enables a material to be cast into the mold assembly and tested without being manually manipulated before or after testing. The tensile deformation is controlled by two voice-coil linear actuators synchronized to pull a specimen in opposing directions. A field of view focused centrally on the specimen experiences a highly-controllable uniform tensile strain with minimal rigid body motion.
Results
We validate the resulting in-plane strain fields on a 2D poly-dimethylsiloxane (PDMS) substrate and a heterogeneous polyurethane foam using Digital Image Correlation (DIC) and volumetrically on 3D polyacrylamide (PA) hydrogels using Digital Volume Correlation (DVC). High-Rate Volumetric Particle Tracking Microscopy (HR-VPTM) is used to quantify and validate the 3D volumetric strain fields at impact-relevant rates. The device can apply up to 200% engineering strain with peak strain rate up to approximately 240 s(^{-1}) to a 7 mm long dogbone specimen. Proof-of-concept biocompatibility was tested on 2D and 3D in vitro neural cell cultures, demonstrating the versatility and applicability for both soft materials and living biomaterials.
Conclusion
We demonstrate and validate a versatile micro-tensile impact device for soft materials and in vitro cellular biomechanics investigations. The achievable strain rates for such a design are some of the highest we have found reported to date and enable experiments that replicate the full range of observable large material deformations seen during real-world blunt impacts.
{"title":"Open Source, In-Situ, Intermediate Strain-Rate Tensile Impact Device for Soft Materials and Cell Culture Systems","authors":"L. Summey, J. Zhang, A.K. Landauer, J. Sergay, J. Yang, A. Daul, J. Tao, J. Park, A. McGhee, C. Franck","doi":"10.1007/s11340-023-00999-y","DOIUrl":"10.1007/s11340-023-00999-y","url":null,"abstract":"<div><h3>Background</h3><p>Intermediate-strain-rate mechanical testing of soft and biological materials is important when designing, measuring, predicting, or manipulating an object or system’s response to common impact scenarios. Open source micro-mechanical test instruments that provide high spatial and temporal resolution volumetric strain field measurements, non-destructive testing and gripping of soft materials with low elastic moduli, programmable strain rates spanning from <span>(10^{-6})</span> s<span>(^{-1})</span> to <span>(10^{2})</span> s<span>(^{-1})</span>, and biocompatibility for living cell cultures and tissues in one instrument are lacking in the current literature.</p><h3>Methods</h3><p>We introduce a micro-tensile testing device developed to meet all these criteria while being straightforwardly accessible to the end user. This device sits atop an inverted microscope stage, granting the researcher access to 3D spatial resolutions as low as 100 nm and frame rates only limited by the camera speed and availability of recordable photons. The micro-tensile specimen is attached to the test device by a specially designed fixture. This enables a material to be cast into the mold assembly and tested without being manually manipulated before or after testing. The tensile deformation is controlled by two voice-coil linear actuators synchronized to pull a specimen in opposing directions. A field of view focused centrally on the specimen experiences a highly-controllable uniform tensile strain with minimal rigid body motion.</p><h3>Results</h3><p>We validate the resulting in-plane strain fields on a 2D poly-dimethylsiloxane (PDMS) substrate and a heterogeneous polyurethane foam using Digital Image Correlation (DIC) and volumetrically on 3D polyacrylamide (PA) hydrogels using Digital Volume Correlation (DVC). High-Rate Volumetric Particle Tracking Microscopy (HR-VPTM) is used to quantify and validate the 3D volumetric strain fields at impact-relevant rates. The device can apply up to 200% engineering strain with peak strain rate up to approximately 240 s<span>(^{-1})</span> to a 7 mm long dogbone specimen. Proof-of-concept biocompatibility was tested on 2D and 3D <i>in vitro</i> neural cell cultures, demonstrating the versatility and applicability for both soft materials and living biomaterials.</p><h3>Conclusion</h3><p>We demonstrate and validate a versatile micro-tensile impact device for soft materials and <i>in vitro</i> cellular biomechanics investigations. The achievable strain rates for such a design are some of the highest we have found reported to date and enable experiments that replicate the full range of observable large material deformations seen during real-world blunt impacts.</p></div>","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2023-09-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135059301","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-09-15DOI: 10.1007/s11340-023-01000-6
M. Politi, O. Breuer, Y. Cohen
Background
Reliable numerical predictive tools are instrumental in the high-end and robust design of encapsulated electronic assemblies. Process optimization and residual stress calculations require a rigorous cure simulation, which considers the transient chemical, thermal and mechanical constitutive behavior of the curing resin. Though this subject has been widely studied for epoxy-based composite materials, fewer studies have been presented on a non-reinforced bulk of low glass-transition temperature (Tg) resin.
Objective
This research aims to numerically and experimentally study the cure behavior and the development of residual stresses and strains in such epoxy based encapsulants.
Methods
The computational study is performed using a commercially available finite element cure process analysis software, and the experimental study is performed by a specially designed test specimen, employing various strain sensing techniques.
Results
The results show good compatibility between experimental and numerical predictions of the thermal behavior and cure-induced residual stresses, which validates the use of the simulative tool for process design. Process induced stress relaxation in the resin is numerically and experimentally demonstrated, which enables a mapping of the process stages at which full viscoelastic modeling is required. The substantial effect of chain mobility on cure shrinkage and residual stress development in this type of materials is numerically demonstrated.
Conclusion
The extensive numerical and experimental investigation of the cure process performed in this study provided insights to both process modeling and design.
{"title":"Simulation and Experimental Validation of the Cure Process of an Epoxy-Based Encapsulant","authors":"M. Politi, O. Breuer, Y. Cohen","doi":"10.1007/s11340-023-01000-6","DOIUrl":"10.1007/s11340-023-01000-6","url":null,"abstract":"<div><h3>Background</h3><p>Reliable numerical predictive tools are instrumental in the high-end and robust design of encapsulated electronic assemblies. Process optimization and residual stress calculations require a rigorous cure simulation, which considers the transient chemical, thermal and mechanical constitutive behavior of the curing resin. Though this subject has been widely studied for epoxy-based composite materials, fewer studies have been presented on a non-reinforced bulk of low glass-transition temperature (Tg) resin.</p><h3>Objective</h3><p>This research aims to numerically and experimentally study the cure behavior and the development of residual stresses and strains in such epoxy based encapsulants.</p><h3>Methods</h3><p>The computational study is performed using a commercially available finite element cure process analysis software, and the experimental study is performed by a specially designed test specimen, employing various strain sensing techniques.</p><h3>Results</h3><p>The results show good compatibility between experimental and numerical predictions of the thermal behavior and cure-induced residual stresses, which validates the use of the simulative tool for process design. Process induced stress relaxation in the resin is numerically and experimentally demonstrated, which enables a mapping of the process stages at which full viscoelastic modeling is required. The substantial effect of chain mobility on cure shrinkage and residual stress development in this type of materials is numerically demonstrated.</p><h3>Conclusion</h3><p>The extensive numerical and experimental investigation of the cure process performed in this study provided insights to both process modeling and design.</p></div>","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2023-09-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135394492","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-09-11DOI: 10.1007/s11340-023-00995-2
S. Ricci, G. Zucca, G. Iannitti, A. Ruggiero, M. Sgambetterra, G. Rizzi, N. Bonora, G. Testa
Background
Understanding and predicting the behavior of additively manufactured (AM) parts in real-case scenarios is essential for optimizing the design process. Little literature presents a throughout investigation on the influence of the stress state on the anisotropic response of AM materials, and there has not been a great effort to validate the applicability of conventional material models for AM components.
Objective
This work aims to assess the effect of building orientation and the stress state on the mechanical response of as-built laser powder bed fusion (L-PBF) AlSi10Mg and to propose, based on the experimental results, a material model able to represent its mechanical response thoroughly.
Methods
Several mechanical characterization tests, including uniaxial tensile and compressive tests, tensile tests on round-notched bars, and shear tests, were carried out for each investigated building direction (0°, 45°, 90°). The Cazacu-Barlat yield surface was selected to describe the mechanical behavior of the material. Material parameters were identified by inverse calibration and verified using finite element simulation of performed experimental tests.
Results
The results showed a more consistent effect of the building direction on ductility and maximum stress value, while the effect on yield stress was less significant. Under multiaxial stress states, the anisotropic behavior became less noticeable yet present. No anisotropic behavior was observed under shear conditions. In tension and compression, a slight asymmetry in response was noted. Computational results were found in agreement with the experimental data.
Conclusion
The influence of both stress state and of the building direction has been systematically investigated by performing several characterization tests on different sample geometries. In combination with mechanical testing, a material model has been proposed and validated to show the applicability of conventional modeling techniques to AM material.
{"title":"Characterization of Asymmetric and Anisotropic Plastic Flow of L-PBF AlSi10Mg","authors":"S. Ricci, G. Zucca, G. Iannitti, A. Ruggiero, M. Sgambetterra, G. Rizzi, N. Bonora, G. Testa","doi":"10.1007/s11340-023-00995-2","DOIUrl":"10.1007/s11340-023-00995-2","url":null,"abstract":"<div><h3>Background</h3><p>Understanding and predicting the behavior of additively manufactured (AM) parts in real-case scenarios is essential for optimizing the design process. Little literature presents a throughout investigation on the influence of the stress state on the anisotropic response of AM materials, and there has not been a great effort to validate the applicability of conventional material models for AM components.</p><h3>Objective</h3><p>This work aims to assess the effect of building orientation and the stress state on the mechanical response of as-built laser powder bed fusion (L-PBF) AlSi10Mg and to propose, based on the experimental results, a material model able to represent its mechanical response thoroughly.</p><h3>Methods</h3><p>Several mechanical characterization tests, including uniaxial tensile and compressive tests, tensile tests on round-notched bars, and shear tests, were carried out for each investigated building direction (0°, 45°, 90°). The Cazacu-Barlat yield surface was selected to describe the mechanical behavior of the material. Material parameters were identified by inverse calibration and verified using finite element simulation of performed experimental tests.</p><h3>Results</h3><p>The results showed a more consistent effect of the building direction on ductility and maximum stress value, while the effect on yield stress was less significant. Under multiaxial stress states, the anisotropic behavior became less noticeable yet present. No anisotropic behavior was observed under shear conditions. In tension and compression, a slight asymmetry in response was noted. Computational results were found in agreement with the experimental data.</p><h3>Conclusion</h3><p>The influence of both stress state and of the building direction has been systematically investigated by performing several characterization tests on different sample geometries. In combination with mechanical testing, a material model has been proposed and validated to show the applicability of conventional modeling techniques to AM material.</p></div>","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2023-09-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"134796064","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}