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Duplex stainless steel 2209 with excellent properties deposited by plasma arc additive manufacturing without post heat-treatment: favorable phase ratio and no σ-phase 通过等离子弧增材制造技术沉积出具有优异性能的双相不锈钢 2209,无需后热处理:相比值良好且无σ相
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2024-06-11 DOI: 10.1007/s43452-024-00907-8
Haoquan Zhang, Kang Peng, Xizhang Chen

This paper utilizes the plasma arc as the heat source to successfully fabricate well-formed thin-walled parts using combined cable wire duplex stainless steel 2209. Microstructure of parts exhibited the favorable two-phase ratio and the absence of σ-phase. It was found that appropriate heat input (1.68 kJ/cm) and cooling rate (5 °C/s) can effectively avoid the precipitation of σ-phase. Furthermore, the properties of the as-deposited samples were comparable to those of the samples heat-treated at 1300 °C, proving that no subsequent heat treatment was required for 2209 stainless steel fabricated by plasma arc additive manufacture. The samples showed excellent properties, in which the ultimate tensile strength and yield strength were improved by about 7% and 24% compared with GB/T4237-2015. The impact toughness meets the requirements of EN10028-7-2016, which is about 35% higher than that of the cold metal transfer samples, and the corrosion resistance is comparable to that of hot rolled 2205.

本文利用等离子弧作为热源,成功地使用组合电缆线双相不锈钢 2209 制成了成型良好的薄壁零件。零件的微观结构显示出良好的两相比例,且没有σ相。研究发现,适当的热输入(1.68 kJ/cm)和冷却速度(5 °C/s)可有效避免σ相的析出。此外,沉积样品的性能与在 1300 ℃ 下热处理的样品相当,证明等离子弧添加剂制造的 2209 不锈钢无需后续热处理。样品表现出优异的性能,其中极限抗拉强度和屈服强度与 GB/T4237-2015 相比分别提高了约 7% 和 24%。冲击韧性符合 EN10028-7-2016 的要求,比冷金属转移样品高出约 35%,耐腐蚀性与热轧 2205 相当。
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引用次数: 0
Numerical analysis of soil–steel composite structure performance at ultimate load: impact of stiffening ribs and geotextile reinforcement 土钢复合结构极限荷载性能数值分析:加劲肋和土工织物加固的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2024-06-10 DOI: 10.1007/s43452-024-00986-7
Alemu Mosisa Legese, Adrian Różański, Maciej Sobótka, Adam Wysokowski

This study investigates soil–steel composite structures, emphasizing the role of stiffening ribs and geotextile reinforcement through comprehensive numerical modeling. This study presents a two-dimensional finite element analysis (FEA) and compares the influence of stiffening rib and geotextile on the ultimate bearing capacity of the soil–steel composite structures. The results of this study demonstrate a significant enhancement in load capacity. Specifically, a notable 47% improvement was observed with a stiffening rib, and a 26% increase was noted with the use of a single layer of geotextile. Under peak load, the vertical displacement at the crown exceeds the permissible standard for all models except for one model, while bending moments reach their limits, marking a failure mode of composite system considered. Structures with stiffened ribs reach their load capacity due to the creation of a plastic hinge around the shoulder and haunch of the shell. On the other hand, in structures without stiffening ribs, the crown and haunch section of the shell becomes fully plastic under peak load. The maximum axial thrust is shown in geotextile-reinforced structure, reaching 78% of the shell maximum capacity due to compression. Eventually, stiffening rib substantially improves overall load-bearing capacity of the soil–steel composite structures, and geotextile placement in the upper part of the backfill reduces shell deflection due to bending.

本研究探讨了钢土复合结构,通过全面的数值建模强调了加劲肋和土工织物加固的作用。本研究采用二维有限元分析(FEA),比较了加劲肋和土工织物对钢土复合结构极限承载能力的影响。研究结果表明,钢土复合结构的承载能力显著提高。具体来说,使用加劲肋可显著提高 47%,使用单层土工织物可提高 26%。在峰值荷载下,除一个模型外,所有模型的冠部垂直位移都超过了允许的标准,同时弯矩也达到了极限,这标志着复合材料系统出现了失效模式。由于在壳体的肩部和后部产生了塑性铰链,带有加劲肋的结构达到了其承载能力。另一方面,在没有加劲肋的结构中,壳体的冠部和尾部在峰值载荷作用下会完全塑化。土工织物加固结构的最大轴向推力达到了壳体最大承载力的 78%。最终,加劲肋大大提高了土钢复合结构的整体承载能力,而在回填土上部铺设土工织物则减少了壳体因弯曲而产生的挠度。
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引用次数: 0
Seismic performance of a new type of prefabricated bridge pier with cast-in-place UHPC jacketing 采用现浇超高性能混凝土护筒的新型预制桥墩的抗震性能
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2024-06-10 DOI: 10.1007/s43452-024-00982-x
Zhe Zhang, Pan Zou, En-Feng Deng, Shi-Bo Wang, Yu-Yang Pang, Hong-Tao Xue, Shao-Rong Men, Dong-Xu Liu

Accelerated bridge construction (ABC) is prevalent all over the world attributable to its technical advantages including the higher construction efficiency, less traffic disruption, and higher construction quality. Grouting sleeves (GS) and grouting corrugated pipes (GCP) are the traditional connection methods of ABC in high seismic regions, with the disadvantages of uncompacted grouting and high requirement of construction accuracy. To this end, this paper developed a new type of prefabricated concrete bridge pier connected with ultra-high performance concrete (PCBP–UHPC) jacketing to solve the problems. To validate the seismic performance of the proposed innovative bridge pier, quasi-static tests on three full-scale specimens PCBP–UHPC, PCBP–GS, and PCBP–GCP were carried out. The results indicated that the failure mode of specimen PCBP–UHPC was similar to that of specimens PCBP–GS and PCBP–GCP with the characteristics of longitudinal steel yielding and concrete crushing at the base of the hollow pier. The obvious plastic hinge outward shifting could be observed during the loading for specimen PCBP–UHPC. The positive ultimate load of specimen PCBP–UHPC was 636.33 kN, which was 14.8% and 13.3% higher than those of specimens PCBP–GS and PCBP–GCP, respectively. In addition, a refined finite element model (FEM) was established by ABAQUS to provide an in-depth understanding on the failure mechanism of the proposed PCBP–UHPC. The parametric analyses were conducted to reveal the influence of the socket depth and axial compression ratio on seismic performance of the proposed PCBP–UHPC. The results indicated that the socket depth had little effect on seismic performance of the prefabricated pier, while the ultimate load bearing capacity of specimen PCBP–UHPC increased to some extent as the increase of the axial compression ratio. The present research work provides an innovative prefabricated bridge pier and a comprehensive experimental–numerical understanding on its seismic performance, which is beneficial for its engineering application.

加速桥梁施工(Accelerated Bridge Construction,ABC)因其具有施工效率高、对交通影响小、施工质量高等技术优势而在全球盛行。灌浆套筒(GS)和灌浆波纹管(GCP)是高震区 ABC 的传统连接方法,存在灌浆不密实、施工精度要求高等缺点。为此,本文开发了一种新型预制混凝土桥墩连接超高性能混凝土(PCBP-UHPC)护筒,以解决上述问题。为了验证所提出的创新桥墩的抗震性能,对三个全尺寸试件 PCBP-UHPC、PCBP-GS 和 PCBP-GCP 进行了准静力试验。结果表明,PCBP-UHPC 试件的破坏模式与 PCBP-GS 和 PCBP-GCP 试件相似,都具有纵向钢筋屈服和空心墩底部混凝土破碎的特点。在加载过程中,PCBP-UHPC 试件出现了明显的塑性铰外移现象。PCBP-UHPC 试件的正极限荷载为 636.33 kN,分别比 PCBP-GS 和 PCBP-GCP 试件高出 14.8%和 13.3%。此外,还利用 ABAQUS 建立了精细的有限元模型(FEM),以深入了解拟议的 PCBP-UHPC 的失效机理。参数分析揭示了插座深度和轴向压缩比对 PCBP-UHPC 抗震性能的影响。结果表明,承台深度对预制墩的抗震性能影响较小,而随着轴压比的增加,PCBP-UHPC 试件的极限承载力有一定程度的提高。本研究工作提供了一种创新的预制桥墩,并对其抗震性能有了全面的实验-数值认识,有利于其工程应用。
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引用次数: 0
Effect of heat input in dissimilar friction stir welding of A390-10 wt.% SiC composite–AA2024 aluminum alloy A390-10 wt.% SiC 复合材料-AA2024 铝合金异种摩擦搅拌焊中输入热量的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2024-06-09 DOI: 10.1007/s43452-024-00957-y
Hamed Jamshidi Aval

This study investigates the impact of heat input, generated during friction stir welding, on the microstructure, mechanical properties, and corrosion resistance of dissimilar joints between A390-10 wt.% SiC composite and AA2024-T6 aluminum alloy. Welds were created using two rotational speeds: 600 rpm and 1600 rpm, while maintaining a constant traverse speed of 60 mm/min and employing a triangular pin tool. The results reveal that increasing the heat input from 125 to 354 J/mm leads to enhanced mixing in the stir zone, resulting in the formation of a layered structure. The stir zone area increases by 23% with the rise in heat input from 125 to 354 J/mm. Moreover, as the heat input and plastic strain in the stir zone increase, the particle size decreases by 31%, and their distribution becomes more uniform. Furthermore, an increase in heat input leads to the formation of coarser precipitates and particles on both the advancing and retreating sides, regardless of the type of precipitates formed. Conversely, reducing the heat input from 354 to 125 J/mm results in achieving maximum hardness (165.3 ± 2.3 HV0.1), yield strength (410.3 ± 11.3 MPa), ultimate tensile strength (514.5 ± 10.4 MPa), and minimum corrosion rate (0.41 mm/year).

本研究探讨了搅拌摩擦焊接过程中产生的热量对 A390-10 wt.% SiC 复合材料和 AA2024-T6 铝合金异种接头的微观结构、机械性能和耐腐蚀性能的影响。焊接采用两种转速:600 rpm 和 1600 rpm:600 rpm 和 1600 rpm,同时保持 60 mm/min 的恒定移动速度,并使用三角销工具。结果表明,将输入热量从 125 焦耳/毫米增加到 354 焦耳/毫米会加强搅拌区的混合,从而形成分层结构。随着热输入从 125 焦耳/毫米增加到 354 焦耳/毫米,搅拌区面积增加了 23%。此外,随着热输入和搅拌区塑性应变的增加,颗粒尺寸减小了 31%,其分布也变得更加均匀。此外,无论形成的沉淀类型如何,热输入的增加都会导致在前进和后退两侧形成更粗的沉淀和颗粒。相反,将热输入从 354 焦耳/毫米减少到 125 焦耳/毫米,可获得最大硬度(165.3 ± 2.3 HV0.1)、屈服强度(410.3 ± 11.3 兆帕)、极限抗拉强度(514.5 ± 10.4 兆帕)和最小腐蚀率(0.41 毫米/年)。
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引用次数: 0
Structural characteristics and corrosion properties of Cu/Sn–Pb composite produced by accumulative roll bonding process 采用累积辊粘工艺制作的铜/锡-铅复合材料的结构特性和腐蚀性能
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2024-06-07 DOI: 10.1007/s43452-024-00981-y
Narges Malmir, Morteza Alizadeh, Shima Pashangeh, Ahmad Ostovari Moghaddam

Cu/Sn–Pb multilayer composite was fabricated by accumulative roll bonding (ARB) technique and its structural, mechanical, and corrosion properties were studied. Microstructural evolution revealed that distribution of Cu and Sn–Pb layers improves by increasing ARB passes and multilayer composite with wavy microstructure and formation of Cu6Sn5 intermetallic compound by solid-state reactions was achieved, while tensile test depicted that tensile strength and fracture strain decrease after the first ARB pass. However, the strength of the multilayered composite at the first pass (about 300 MPa) is much higher than that of the pure Cu (about 200 MPa). Electrochemical tests (potentiodynamic polarization) were conducted in 3.5 wt.% NaCl and boiler feed water (BFW) on the surface and cross-sectional areas. Open circuit potential (OCP) of the composite was lower than that of the pure and ARBed Cu (pure Cu was fabricated using ARB process after seven passes). The results demonstrated that corrosion resistance on the surface and cross-sectional area decreased with increasing ARB passes, indicating a growing susceptibility to corrosion on both surfaces. Besides, with increasing ARB passes a more uniform distribution of Sn–Pb within Cu matrix was realized and due to the conversion of galvanic coupling to micro-galvanic coupling corrosion occurs more uniformly.

采用累积辊粘合(ARB)技术制造了铜/锡-铅多层复合材料,并对其结构、机械和腐蚀特性进行了研究。微观结构演变表明,随着 ARB 层数的增加,铜层和锡铅层的分布得到改善,多层复合材料的微观结构呈波浪状,并通过固态反应形成了 Cu6Sn5 金属间化合物。不过,多层复合材料在第一道工序时的强度(约 300 兆帕)远高于纯铜(约 200 兆帕)。在 3.5 重量百分比的氯化钠和锅炉给水(BFW)中对表面和横截面积进行了电化学测试(电位极化)。复合材料的开路电位(OCP)低于纯铜和 ARBed 铜(纯铜是采用 ARB 工艺经过七道工序制成的)。结果表明,表面和横截面积的耐腐蚀性随着 ARB 通过次数的增加而降低,这表明两个表面的腐蚀敏感性都在增加。此外,随着 ARB 层数的增加,铜基体中锡铅的分布更加均匀,由于电偶耦合转变为微观电偶耦合,腐蚀发生得更加均匀。
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引用次数: 0
Role of layer thickness on the damage mechanism in the LPBFed copper alloy 层厚度对 LPBFed 铜合金损伤机制的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2024-06-07 DOI: 10.1007/s43452-024-00983-w
M. Saravana Kumar, N. Jeyaprakash, Che-Hua Yang

Parts with interior voids created by the LPBF process are known to have the potential to cause fracture when subjected to mechanical loading. In this research, the key process parameters such as laser thickness (LT), scanning speed (SS), and laser power (LP) were taken into consideration to avoid the void formations which was the major reason for affecting the structural integrity. So, void formations (V), ultimate tensile strength (UTS) and reduced modulus (RM) were considered as the response parameters in this study. The entropy-associated weighted aggregated sum product assessment (WASPAS) approach was implemented to examine the favorable conditions which substantiated that the LT is the most influential parameter in nucleation of voids. The verification experiments prove that the void formation was reduced by 98.6% and the UTS and RM were enhanced by 52.17 and 31.7%.

众所周知,LPBF 工艺产生内部空隙的零件在承受机械载荷时有可能导致断裂。在这项研究中,激光厚度(LT)、扫描速度(SS)和激光功率(LP)等关键工艺参数被纳入考虑范围,以避免出现空洞,因为空洞是影响结构完整性的主要原因。因此,本研究将空洞形成(V)、极限拉伸强度(UTS)和降低模量(RM)作为响应参数。采用熵相关加权聚合乘积评估(WASPAS)方法对有利条件进行检验,结果表明,LT 是对空洞成核影响最大的参数。验证实验证明,空洞的形成减少了 98.6%,而 UTS 和 RM 则分别提高了 52.17% 和 31.7%。
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引用次数: 0
Sub-global equilibrium method for identification of elastic parameters based on digital image correlation results 基于数字图像相关结果的次全局平衡法识别弹性参数
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2024-06-06 DOI: 10.1007/s43452-024-00979-6
Marcin Nowak, Paweł Szeptyński, Sandra Musiał, Michał Maj

In this work, a new, simple method is presented, which enables identification of material properties of solids basing on the digital image correlation (DIC) measurements. It may be considered as a simplified alternative of low computational complexity for the well-known finite element model updating (FEMU) method and virtual fields method (VFM). The idea of the introduced sub-global equilibrium (SGE) method is to utilize the fundamental concept and definition of internal forces and its equilibrium with appropriate set of external forces. This makes the method universal for the use in the description of a great variety of continua. The objective function is the measure of imbalance, namely the sum of squares of residua of equilibrium equations of external forces and internal forces determined for finite-sized part of the sample. It is then minimized with the use of the Nelder–Mead downhill simplex algorithm. The efficiency of the proposed SGE method is shown for two types of materials: 310 S austenitic steel and carbon-fiber-reinforced polymer (CFRP). The proposed method was also verified based on FE analysis showing error estimation.

本研究提出了一种简单的新方法,可根据数字图像相关(DIC)测量结果确定固体的材料属性。该方法可被视为众所周知的有限元模型更新法(FEMU)和虚拟场法(VFM)的简化替代方法,计算复杂度较低。所引入的次全局平衡(SGE)方法的理念是利用内力的基本概念和定义及其与适当外力的平衡。这使得该方法在描述各种连续体时具有通用性。目标函数是不平衡度量,即对样本的有限大小部分确定的外力和内力平衡方程残差的平方和。然后利用 Nelder-Mead 下坡单纯形算法将其最小化。针对两种材料,展示了所提出的 SGE 方法的效率:310 S 奥氏体钢和碳纤维增强聚合物 (CFRP)。基于误差估算的 FE 分析也验证了所提出的方法。
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引用次数: 0
Effect of Ti micro-addition on the hot tensile behaviour, microstructure and fractography of low-C high-manganese steels 微量添加钛对低碳高锰钢热拉伸性能、微观结构和断口形貌的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2024-06-05 DOI: 10.1007/s43452-024-00980-z
Gabriela Fojt-Dymara, Marek Opiela, Barbara Grzegorczyk, Klaudiusz Gołombek, Adam Grajcar

The aim of the work was to determine the effect of Ti micro-addition on the hot tensile behaviour, microstructure and fractography of two low-C high-manganese steels with additions of Si and Al. The hot tensile tests were performed using the Gleeble 3800 thermomechanical simulator. Samples were stretched at a temperature range from 1050 ℃ to 1200 ℃ at a strain rate of 2.5·10 3 s−1. The microstructure of the tested high-manganese steels under conditions of hot deformation was influenced by strain hardening and simultaneous dynamic recrystallization, as well as precipitation processes-depending on the chemical composition of the alloy and plastic deformation parameters. The analysis of the curves registered in the hot tensile tests indicated that a decrease of strain hardening was the result of the dynamic recrystallization. Hot tensile curves of the Ti-micro-alloyed steel were characterized by higher yield stress compared to the Ti-free steel. The Ti micro-addition with a concentration of 0.075 wt.% guaranteeing stable TiN-type nitrides eliminated the possibility of precipitating AlN-type nitrides and complex MnS-AlN type non-metallic inclusions, which are harmful to hot ductility. Fracture modes of the Ti-free steel showed a mixed nature from 1050 ℃ to 1150 °C, i.e. ductile fracture and numerous cavities and voids were identified. As the deformation temperature increased to 1200 °C, the fracture character was brittle with numerous inter-crystalline cracks along austenite grain boundaries. The addition of Ti improved significantly the hot ductility behaviour characterized by higher values of flow stress and reduction in area as well as ductile fracture modes in the entire high deformation temperature range.

这项研究旨在确定微量添加 Ti 对两种添加了硅和铝的低碳高锰钢的热拉伸性能、微观结构和断口形貌的影响。热拉伸试验使用 Gleeble 3800 热机械模拟器进行。样品在 1050 ℃ 至 1200 ℃ 的温度范围内以 2.5-10 3 s-1 的应变速率拉伸。在热变形条件下,受测高锰钢的微观结构受到应变硬化和同步动态再结晶以及沉淀过程的影响,这取决于合金的化学成分和塑性变形参数。对热拉伸试验曲线的分析表明,应变硬化的降低是动态再结晶的结果。与无钛钢相比,微合金化钛钢的热拉伸曲线屈服应力更高。浓度为 0.075 wt.%的 Ti 微合金化保证了稳定的 TiN 型氮化物,消除了析出 AlN 型氮化物和复杂的 MnS-AlN 型非金属夹杂物的可能性,这些夹杂物对热延展性有害。从 1050 ℃ 到 1150 ℃,无钛钢的断裂模式呈现出混合性质,即韧性断裂和大量空洞和空隙。当变形温度升高到 1200 ℃ 时,断裂特征为脆性,沿奥氏体晶界出现大量晶间裂纹。钛的加入大大改善了热延展性能,在整个高变形温度范围内,热延展性能表现为流动应力值升高、面积减小以及韧性断裂模式。
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引用次数: 0
An experimental assessment on the seismic behaviour of precast hollowcore slab to beam connection with different connection details 不同连接细节下预制空心板与梁连接的抗震性能实验评估
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2024-06-03 DOI: 10.1007/s43452-024-00881-1
D. Vinutha, R. Vidjeapriya, K. P. Jaya

This study evaluates the cyclic response of the Precast Hollow Core Slab (PHCS) to the beam connection by proposing a novel connection detail. The evaluation involved, three different connection details, namely, (1) Continuity rebar and U-type Core Rebar Discrete with 100 mm ledge width (CUCRD_100); (2) continuity rebar and Core Rebar Combined with 100 mm ledge width (CCRC_100); and (3) continuity rebar and Core Rebar Combined with Ties along with 100 mm ledge width (CCRCT_100) were experimentally validated. These were validated through experimental testing, comparing their performance with a reference specimen that adhered to New Zealand guidelines using Continuity rebar and Core Rebar Discrete with 100 mm ledge width (CCRD_100). Displacement controlled reverse cyclic loading, following the ACI T1.1–0.1 protocol, was applied to the end of a hollow core slab for the experimental testing. The structural performance of all four connections considered failure pattern, strength, hysteretic behaviour, energy dissipation, displacement ductility, stiffness degradation, and equivalent viscous damping. The overall seismic efficiency of the connections was assessed using ACI 374.1–05 approval criteria. The experimental results proved that the peak load-carrying capacity for CCRCT_100 specimen was observed to be greater in both directions of loading (positive and negative) when compared with the other connection detailing. The presence of transverse reinforcement enhanced the confining capacity of the concrete in the joint region which substantially increased the ductility and dissipation of energy in CCRCT_100 specimen. The seismic performance of every connection specimen was favourable, and they all met the ACI 374.1–05 approval standards.

本研究通过提出一种新颖的连接细节,评估了预制空心板(PHCS)与梁连接的循环响应。评估涉及三种不同的连接细节,即:(1) 100 mm 壁架宽度的连续螺纹钢和 U 型核心螺纹钢离散连接(CUCRD_100);(2) 100 mm 壁架宽度的连续螺纹钢和核心螺纹钢组合连接(CCRC_100);以及 (3) 100 mm 壁架宽度的连续螺纹钢和核心螺纹钢与拉杆组合连接(CCRCT_100)。这些试验通过实验测试进行验证,并将其性能与符合新西兰准则的使用连续螺纹钢筋和带 100 毫米壁架宽度的离散核心螺纹钢筋(CCRD_100)的参考试样进行比较。在实验测试中,按照 ACI T1.1-0.1 协议对空心板的端部施加了位移控制反向循环荷载。所有四种连接件的结构性能均考虑了破坏模式、强度、滞后行为、能量耗散、位移延性、刚度退化和等效粘性阻尼。采用 ACI 374.1-05 批准标准对连接件的整体抗震效率进行了评估。实验结果证明,与其他连接细节相比,CCRCT_100 试件在两个加载方向(正向和负向)的峰值承载能力都更大。横向钢筋的存在增强了连接区域混凝土的约束能力,从而大大提高了 CCRCT_100 试件的延展性和能量消耗。每个连接试件的抗震性能都很好,均符合 ACI 374.1-05 批准标准。
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引用次数: 0
Mechanical and tribological properties of Ti1-xZrxB2 coatings deposited by magnetron sputtering on hot work steel 磁控溅射法沉积在热作钢上的 Ti1-xZrxB2 涂层的机械和摩擦学特性
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2024-05-31 DOI: 10.1007/s43452-024-00923-8
Łukasz Cieniek, Agnieszka Kopia, Marcin Kot, Grzegorz Cempura, Adam Gruszczyński, Mateusz Kopyściański, Jerzy Smolik, Joanna Kacprzyńska-Gołacka

Low fracture toughness is a common problem encountered by many researchers in the application of pure TiB2 coatings. To improve their properties, a convenient and useful method is the use of doping, so this study proposes the deposition of TiB2 enriched with Zr on a steel substrate. The objective of the research was to investigate the impact of Zr addition to TiB2 coatings on both their mechanical and tribological properties. Four coatings with varying compositions (pure TiB2; TiB2 doped with 3, 6, and 10 at.% Zr) were deposited using magnetron sputtering from TiB2 and Zr targets. The coating structures were analyzed by means of X-ray diffraction (XRD), transmission electron microscopy (TEM), and atomic force microscopy (AFM). Nanoindentation, scratch test, and ball-on-disk test were used to determine the mechanical and tribological properties. In most cases, only two factors have a significant impact on the mechanical and tribological properties of the Zr-doped coating. Firstly, a change in the preferred orientation of the coating from (102)(111) to (100) results in increased hardness and wear resistance. Secondly, a reduction in crystallite and column size enhances ductility and fracture toughness by impeding or altering the direction of crack propagation. Based on the study, one can conclude that the optimal Ti1-xZrxB2 properties were obtained for 6 at.% Zr content.

断裂韧性低是许多研究人员在应用纯 TiB2 涂层时遇到的共同问题。为了改善其性能,一种方便实用的方法是使用掺杂,因此本研究提出在钢基底上沉积富含 Zr 的 TiB2。研究的目的是调查在 TiB2 涂层中添加 Zr 对其机械和摩擦学性能的影响。研究人员使用磁控溅射技术从 TiB2 和 Zr 靶件上沉积出四种不同成分的涂层(纯 TiB2;掺杂 3、6 和 10 at.% Zr 的 TiB2)。涂层结构通过 X 射线衍射 (XRD)、透射电子显微镜 (TEM) 和原子力显微镜 (AFM) 进行了分析。纳米压痕、划痕测试和盘上球测试用于确定机械和摩擦学特性。在大多数情况下,只有两个因素会对掺锆涂层的机械和摩擦学性能产生重大影响。首先,将涂层的优先取向从(102)(111)改为(100)可提高硬度和耐磨性。其次,晶粒和晶柱尺寸的减小阻碍或改变了裂纹的扩展方向,从而提高了延展性和断裂韧性。根据这项研究,我们可以得出结论,当 Zr 含量为 6%时,Ti1-xZrxB2 的性能最佳。
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引用次数: 0
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Archives of Civil and Mechanical Engineering
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