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Optimization of self-compacting mortars with olive pomace bottom ash using central composite design approach 橄榄渣底灰自密实砂浆的中心复合设计优化
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-12 DOI: 10.1007/s43452-025-01327-y
Besma Belaidi, Cherif Belebchouche, Abdelkader Hammoudi, Abdellah Douadi, Kamel Hebbache, Mourad Boutlikht, Adrian Chajec, Slawomir Czarnecki

This study investigates the potential use of Olive Pomace Bottom Ash (OPBA) as a partial cement replacement in self-compacting mortars (SCMs) to enhance sustainability in construction while addressing environmental concerns. A Central Composite Design (CCD) approach was used to investigate the effect of OPBA content (0–20%), limestone filler content (10–20%), and water-to-binder (W/B) ratio (0.4–0.5) on fresh properties, mechanical behavior, and water absorption potential of SCM. The results indicate that increasing the OPBA content typically decreased workability and strength while at the same time increasing water absorption potential. However, this effect can be mitigated by optimizing the filler content and W/B ratio. With low additions of OPBA (up to 10%), incorporating limestone filler showed a regular increase in strength. Statistical analyses using the central composite design method confirm that complex non-linear relationships among variables exist and that advanced optimization techniques are needed in mix design. An optimal mix was found to have 6.66% OPBA, 20% filler, and a W/B ratio of 0.42, with a desirability value of 0.927. This optimal mixture recorded a slump of 26.3 cm, flow time of 11.85 s, compressive strength of 48.66 MPa, flexural strength of 5.47 MPa, and water absorption of 11%. The above study indicates that OPBA is feasible in SCMs and could improve sustainability in the construction industry without compromising performance. These findings highlight OPBA feasibility in SCMs, promoting waste valorization and reducing cement consumption without compromising performance.

本研究探讨了橄榄渣底灰(OPBA)作为自密实砂浆(SCMs)中部分水泥替代品的潜在用途,以提高建筑的可持续性,同时解决环境问题。采用中心复合设计(CCD)方法研究了OPBA含量(0-20%)、石灰石填料含量(10-20%)和水胶比(W/B)(0.4-0.5)对SCM新鲜性能、力学行为和吸水势的影响。结果表明,增加OPBA含量会降低材料的和易性和强度,同时提高材料的吸水势。然而,这种影响可以通过优化填料含量和W/B比来缓解。在OPBA掺量较低(10%)的情况下,石灰石填料的强度有规律地增加。采用中心组合设计方法进行的统计分析证实了变量之间存在复杂的非线性关系,混合设计需要先进的优化技术。优选出的最佳配合比为:OPBA 6.66%,填料20%,W/B比0.42,理想值为0.927。该混合料坍落度为26.3 cm,流动时间为11.85 s,抗压强度为48.66 MPa,抗折强度为5.47 MPa,吸水率为11%。上述研究表明,OPBA在scm中是可行的,可以在不影响绩效的情况下提高建筑业的可持续性。这些发现强调了OPBA在scm中的可行性,在不影响性能的情况下促进废物增值和减少水泥消耗。
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引用次数: 0
The role of particle size optimisation of waste granite powder in cementitious composites 花岗石废粉粒度优化在胶凝复合材料中的作用
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-12 DOI: 10.1007/s43452-025-01330-3
Adrian Chajec

The utilisation of granite powder (GP) waste in cementitious composites is limited by its low reactivity and adverse effects on mechanical performance. This study investigates the mechanical activation of GP through grinding (GP-M) and sieving (GP-S) to optimise its physical properties and sustainability potential. The modified powders were characterised in terms of specific surface area (SSA), reactivity, loss on ignition, and alkali leachability. Cementitious composites were prepared with 20% and 40% cement replacement and evaluated for slump flow, setting time, strength development, and bulk density. Results show that grinding increases the SSA from 2890 cm2/g (raw GP) to 4290 cm2/g (GP-M), improving particle packing and enhancing compressive strength by up to 20% compared to unprocessed GP. Despite its low pozzolanic reactivity, GP-M acts as an effective filler, improving microstructure and maintaining compressive strengths above 40 MPa at 28 days for 20% replacement. Alkali leachability was also reduced, supporting long-term durability. A Life Cycle Assessment (LCA) indicates that replacing 40% of cement with GP-M reduces CO2 emissions by over 50%, while maintaining acceptable mechanical properties. The proposed Mechanical Performance Ratio (MPR) and Environmental Performance Ratio (EPR) demonstrate that the most balanced performance was achieved in the GP-M20 and GP-S20 series, offering up to 12% CO2 savings with minimal strength reduction. This study confirms that mechanically valorised granite powder is a viable, sustainable SCM, capable of reducing cement content while satisfying structural and environmental requirements in construction applications.

花岗岩粉(GP)废料在胶凝复合材料中的利用受到其低反应性和对力学性能不利影响的限制。本研究通过研磨(GP- m)和筛分(GP- s)对GP进行机械活化,以优化其物理性能和可持续性潜力。改性粉末在比表面积(SSA)、反应性、着火损失和碱浸出性方面进行了表征。分别以20%和40%的水泥替代量制备了胶凝复合材料,并对坍落度流动、凝结时间、强度发展和容重进行了评价。结果表明,与未加工的GP相比,磨削使SSA从2890 cm2/g(粗GP)增加到4290 cm2/g (GP- m),改善颗粒堆积,抗压强度提高20%。尽管GP-M的火山灰反应性较低,但它可以作为有效的填料,改善微观结构,并在更换20%后的28天内保持40 MPa以上的抗压强度。碱浸出性也降低了,支持长期耐用性。生命周期评估(LCA)表明,用GP-M替代40%的水泥可减少50%以上的二氧化碳排放,同时保持可接受的机械性能。建议的机械性能比(MPR)和环境性能比(EPR)表明,GP-M20和GP-S20系列实现了最平衡的性能,在最小强度降低的情况下可节省高达12%的二氧化碳。这项研究证实,机械增值花岗岩粉是一种可行的、可持续的SCM,能够减少水泥含量,同时满足建筑应用中的结构和环境要求。
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引用次数: 0
The effect of annealing on the growth of Al3Ni and Al3Ni2 intermetallics at the interface of explosively welded Al/Ni clads 退火对爆炸焊接Al/Ni包层界面Al3Ni和Al3Ni2金属间化合物生长的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-12 DOI: 10.1007/s43452-025-01325-0
Izabella Kwiecien, Sylwia Terlicka, Agnieszka Bigos, Katarzyna Stan-Glowinska, Anna Wierzbicka-Miernik, Zygmunt Szulc, Joanna Wojewoda-Budka

Explosive welding is an effective method for joining metals with dissimilar physicochemical properties. The Al/Ni system is particularly interesting due to the formation of intermetallic phases with unique mechanical and thermal properties, which makes these welds potentially applicable in industries, such as aerospace, energy, and chemical. Diffusion processes occurring at the interface between these metals play a significant role and can impact the durability of the connections. Therefore, this research focuses on the analysis of diffusion phenomena in Al/Ni welds formed by explosive welding and subjected to further annealing. It was investigated whether the technological parameters of the joining process, such as detonation velocity, which varied from 2000 to 2800 m/s or mutual localization of the colliding plates during the explosion, influence post-annealing interface transformations, in particular the sequence of the intermetallic phase formation, their thickness and growth mechanism. Welded clads underwent annealing at 500 °C for periods ranging from 0.5 to 168 h. After the heat treatment, microstructure and phase characterization of the interface zone were performed, with scanning and transmission electron microscopy, thanks to which the mechanisms and growth kinetics of the forming phases were determined. Additionally, for the first time, the anisotropy of the thermal expansion in explosively welded Al/Ni was examined with respect to the shock wave propagation and the accompanying microstructure evolution, providing a significant contribution to the engineering design of welds subjected to the thermal cycling. The thermal expansion coefficient was measured over the temperature range from ambient temperature to 500 °C and analyzed in relation to the welding conditions. Differences in the thickness of the two forming Al3Ni and Al3Ni2 layers and their dominant growth mechanisms were observed for the individual clads. The effect of detonation velocity was particularly significant at 2000 m/s, where prolonged annealing led to weld degradation, thus limiting strength due to unfavorable welding conditions. The presence of porosity identified at the Al1050/Al3Ni2 interface was attributed to the Kirkendall effect accompanying the annealing procedure. Measurements of the thermal expansion coefficient revealed minor differences between samples, with the largest discrepancies observed for clads produced at 2400 m/s, which may be due to the less uniform initial microstructure of the interface. The obtained results indicate a relationship between explosive welding conditions and changes in the microstructure and physical properties of Al/Ni welds after heat treatment.

爆炸焊接是连接物理化学性质不同的金属的一种有效方法。Al/Ni体系特别有趣,因为它形成了具有独特机械和热性能的金属间相,这使得这些焊缝在航空航天、能源和化工等行业中具有潜在的应用前景。在这些金属之间的界面上发生的扩散过程起着重要的作用,并且会影响连接的耐久性。因此,本研究重点分析了爆炸焊接形成的Al/Ni焊缝中进一步退火后的扩散现象。研究了连接过程的工艺参数(如爆轰速度(2000 ~ 2800 m/s)或爆炸过程中碰撞板的相互局部化)对退火后界面转变的影响,特别是金属间相形成的顺序、厚度和生长机制。焊接熔覆层在500℃下退火0.5 ~ 168 h。热处理后,使用扫描电镜和透射电镜对界面区进行微观组织和相表征,从而确定形成相的机制和生长动力学。此外,首次研究了爆炸焊接Al/Ni中热膨胀的各向异性,以及冲击波传播和伴随的微观组织演变,为热循环焊缝的工程设计提供了重要贡献。在从环境温度到500°C的温度范围内测量了热膨胀系数,并分析了与焊接条件的关系。观察了不同覆层形成的Al3Ni和Al3Ni2层的厚度差异及其主要生长机制。爆轰速度的影响在2000 m/s时尤为显著,长时间的退火导致焊缝退化,从而由于不利的焊接条件而限制了强度。在Al1050/Al3Ni2界面上发现孔隙度的存在归因于退火过程中的Kirkendall效应。热膨胀系数的测量显示样品之间的差异很小,在2400 m/s的速度下产生的包层差异最大,这可能是由于界面的初始微观结构不均匀所致。结果表明,爆炸焊接条件与热处理后Al/Ni焊缝组织和物理性能的变化存在一定的关系。
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引用次数: 0
Thermo-dependent dynamic analysis of imperfect shear-deformable nanocomposite conical micro shells 不完全剪切变形纳米复合材料锥形微壳热相关动力学分析
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-11 DOI: 10.1007/s43452-025-01328-x
Ehsan Arshid, Saeed Amir, Iman Dadoo, Ömer Civalek

In the present research, free vibration of a truncated conical shell is investigated. The shell consists of three layers: a porous core and two carbon nanotube-reinforced nanocomposite (CNTs-RNC) facesheets. The structure is inserted in a thermal environment and also, is also subjected to a longitudinal magnetic field. The structure’s kinematics is modelled based on the first-order shear deformation theory (FSDT), and the modified coupled stress theory (MCST) is used to consider the scale effect. The equations of motion are derived using Hamilton’s principle, and then, the generalized differential quadrature method (GDQM) is employed to solve them under various combinations of boundary conditions. The effects of several parameters, including geometry, porosity coefficient, porosity distribution patterns, CNTs’ mass fraction and types, agglomeration coefficients, boundary conditions, and small-scale parameter are investigated. The results demonstrate that the natural frequency increases with increasing CNTs’ mass fraction and decreases with increasing porosity. These structures have a wide range of potential applications and can be used in microelectromechanical and nanoelectromechanical systems.

本文研究了截顶锥形壳的自由振动问题。外壳由三层组成:多孔核心和两个碳纳米管增强纳米复合材料(CNTs-RNC)表面。该结构被插入热环境中,也受到纵向磁场的影响。基于一阶剪切变形理论(FSDT)对结构进行运动学建模,并采用修正耦合应力理论(MCST)考虑尺度效应。利用Hamilton原理推导了运动方程,然后利用广义微分正交法(GDQM)在各种边界条件组合下求解了运动方程。研究了几何形状、孔隙率系数、孔隙率分布模式、CNTs的质量分数和类型、团聚系数、边界条件和小尺度参数等参数的影响。结果表明:固有频率随CNTs质量分数的增加而增加,随孔隙率的增加而降低;这些结构具有广泛的潜在应用,可用于微机电和纳米微机电系统。
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引用次数: 0
Tensile strength-ductility properties of face-centered cubic deformation twin/matrix structures 面心立方变形孪晶/基体组织的抗拉强度-延性
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-11 DOI: 10.1007/s43452-025-01324-1
M. S. Szczerba, M. Kowalska, S. Kopacz, M. J. Szczerba

Large anisotropy of the tensile strength-ductility combination of the laminated twin/matrix (T/M) structure was found by studying the mechanical response of pre-twinned Cu-8at.%Al crystal structures, subjected to plastic tension under the different loading conditions. Three resolved shear stress-driven mechanisms, M1, M2, M3, were introduced to describe the deformation properties of the bimodal T/M structure. The “zero” tensile ductility (εT) accompanied by the tensile strength σT about 550 MPa or above 900 MPa was established when the T/M structure was loaded almost parallel (M3) or perpendicular (M1) to the T/M interface. Consequently, the T/M structure revealed the minimal (“zero”) tensile strength-ductility combination (σT × εT), when plastic yielding was initiated by M1 or M3 mechanism; both connected with T/M lattice shears occurring across the T/M interface. However, the T/M structure loaded at an angle about π/4 to the T/M interface revealed exceptionally large ductility (true strain equal to unity) accompanied by true stress of 850 MPa, i.e., the maximal combination σT × εT of 850 MPa, projected to about 1500 MPa for an analogous T/M structure of high manganese steels. All the “non-zero” cases of σT × εT were determined by activity of M2 mechanism, i.e., T/M lattice shear parallel to the T/M interface. The σT × εT values depended on the length of M2 deformation path terminated by a sudden entry of M3 (M1) mechanism. The entry, governed by the Schmid–Boas law, occurred always well before the Considère condition was met. The physical reasons of the observed anisotropy of the T/M structure are discussed.

通过对预孪晶Cu-8at的力学响应研究,发现层合孪晶/基体(T/M)组织的抗拉强度-塑性组合具有较大的各向异性。Al晶体结构,在不同的加载条件下受到塑性拉伸。引入三种分解剪切应力驱动机制M1、M2、M3来描述双峰T/M结构的变形特性。当T/M结构几乎与T/M界面平行(M3)或垂直(M1)加载时,其抗拉塑性εT为零,抗拉强度σT约为550 MPa或900 MPa以上。因此,当塑性屈服由M1或M3机制引发时,T/M组织表现出最小(“零”)抗拉强度-塑性组合(σT × εT);两者都与发生在T/M界面上的T/M晶格剪切有关。然而,当T/M结构与T/M界面呈π/4角加载时,在850 MPa的真实应力下显示出异常大的塑性(真应变等于1),即高锰钢的类似T/M结构的最大组合σT × εT为850 MPa,预估为1500 MPa左右。所有σT × εT的“非零”情况均由平行于T/M界面的M2机制(即T/M晶格剪切)的活度决定。σT × εT值与M3 (M1)机制突然进入所终止的M2变形路径长度有关。受施密德-鲍亚士定律支配的进入,总是发生在相当大的条件得到满足之前。讨论了观察到的T/M结构各向异性的物理原因。
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引用次数: 0
The effects of process parameters and heat treatment on microstructure evolution and mechanical properties of 7A85 aluminum alloy friction stir welded joints 工艺参数和热处理对7A85铝合金搅拌摩擦焊接接头组织演变和力学性能的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-10 DOI: 10.1007/s43452-025-01329-w
Yu Juan, Congcong Zhu, Fan Zhenzhong, Wu Zhigang, Tong Gaungze, Gao Wenli

This study successfully obtained 7A85 high-ribbed panels friction stir-welded (FSW) joints through proportional parameter changed (ω: 400–1200 rpm; v: 100–300 mm/min) and further optimized the mechanical properties of the FSW joints through artificial aging. The effects of welding process parameters and artificial aging on the microstructure and mechanical properties of the welded joint were investigated using OM, SEM, EBSD, TEM, tensile testing, and hardness testing. The results showed that the joint consists of the weld nucleus zone (NZ), thermomechanical influence zone (TMAZ), heat-affected zone (HAZ) and base metal (BM). Among these, the NZ undergoes significant dynamic recrystallization under thermomechanical coupling, with the degree of recrystallization increasing gradually from top to bottom along the thickness direction. When the welding pitch remains constant, increasing the welding speed reduces heat input and effectively suppresses the coarsening of precipitates in the HAZ. After aging, the GP zone in the NZ transforms into the strengthening η′ phase, while the coarsening in the HAZ is further suppressed. Mechanical tests indicate that increasing the parameters from ω = 400 rpm/v = 100 mm/min to ω = 1200 rpm/v = 300 mm/min can enhance tensile strength from 432 to 463 MPa, yield strength from 332 to 377 MPa, while reducing elongation from 6.2% to 5.2%. Increasing the proportional parameters enhances strength with limited loss of elongation, but expands the weakened zone of the TMAZ/HAZ. Therefore, welding process parameters of ω = 800 rpm and v = 200 mm/min yield excellent microstructural characteristics and optimal performance.

本研究通过改变比例参数(ω: 400 - 1200rpm; v: 100 - 300mm /min)成功获得7A85高肋板搅拌摩擦焊(FSW)接头,并通过人工时效进一步优化FSW接头的力学性能。采用OM、SEM、EBSD、TEM、拉伸试验和硬度试验研究了焊接工艺参数和人工时效对焊接接头组织和力学性能的影响。结果表明:该接头由焊缝核区(NZ)、热影响区(TMAZ)、热影响区(HAZ)和母材(BM)组成。其中,在热-机械耦合作用下,NZ发生了明显的动态再结晶,再结晶程度沿厚度方向从上到下逐渐增大。在焊接节距一定的情况下,提高焊接速度可以减少热输入,有效抑制热影响区析出相的粗化。时效后,NZ区的GP区转变为强化η′相,而HAZ区的粗化进一步受到抑制。力学试验表明,将参数从ω = 400 rpm/v = 100 mm/min提高到ω = 1200 rpm/v = 300 mm/min,抗拉强度从432提高到463 MPa,屈服强度从332提高到377 MPa,延伸率从6.2%降低到5.2%。增加比例参数可以在有限的伸长率损失下提高强度,但扩大了TMAZ/HAZ的弱化区。因此,ω = 800 rpm和v = 200 mm/min的焊接工艺参数可获得优异的显微组织特征和最佳性能。
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引用次数: 0
Microstructure, mechanical parameters, and corrosion resistance of austenitic ductile iron castings 奥氏体球墨铸铁铸件的显微组织、力学参数及耐蚀性
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-09 DOI: 10.1007/s43452-025-01331-2
M. Bork, M. Górny, G. Palumbo, G. Angella, J. Marosz

Austenitic ductile iron, also known as Ni-resist cast iron, belongs to the cast iron group, which is characterized by a high-nickel content ranging from 18% to 36% by weight. Although this level of nickel content significantly increases the production costs, it imparts numerous beneficial properties that justify the price. One notable property is its ability to operate across a wide temperature range, with a minimum service temperature of − 200 °C, and a maximum, depending on the grade, reaching up to 1050 °C. This family of high-quality alloys demonstrates mechanical properties, where grades without carbide-forming elements achieve elongation exceeding 40%. On the other hand, by adding Cr, which is a carbide-forming element, the Ni-resist cast iron’s plasticity decreases, while its corrosion resistance properties increase. However, a comprehensive investigation into the correlation between mechanical properties and corrosion resistance, particularly in relation to various nickel contents in the presence of Cr in high-nickel cast iron, is scarce. Therefore, the primary aim of this study was to elucidate the role of nickel content and chromium content in influencing the mechanical and corrosion resistance properties of austenitic ductile iron. The addition of 21, 25, 28, and 35 wt% of nickel with and without 2.5 wt% of chromium was investigated. Characterization of the materials was carried out using optical and scanning electron microscopy, static tensile tests, impact strength tests, and corrosion resistance assessments at room temperature in a 3.5 wt% NaCl solution. The investigation revealed a significant influence by changing the nickel and chromium content on the properties of high-nickel cast iron. In addition, it was proved that by controlling the content of these elements, the cast iron with establish properties can be achieved—depending on expected final properties, results show that it is possible to substitute part of the nickel content with smaller amount of chromium to get similar corrosion resistance properties and reduce the production costs, but it will influence to mechanical properties, which dependent on plasticity.

奥氏体球墨铸铁,又称抗镍铸铁,属于铸铁族,其特点是含镍量高,按重量计可达18% ~ 36%。尽管这种镍含量水平大大增加了生产成本,但它赋予了许多有益的特性,证明了价格的合理性。一个值得注意的特性是它能够在很宽的温度范围内工作,最低工作温度为- 200°C,根据等级不同,最高工作温度可达1050°C。该系列高质量合金具有良好的机械性能,其中不含碳化物形成元素的牌号伸长率超过40%。另一方面,加入碳化物形成元素Cr后,抗镍铸铁的塑性降低,耐腐蚀性能提高。然而,对机械性能和耐蚀性之间的关系的全面调查,特别是与高镍铸铁中存在Cr的各种镍含量的关系,很少。因此,本研究的主要目的是阐明镍含量和铬含量对奥氏体球墨铸铁力学性能和耐腐蚀性能的影响。研究了添加21,25,28,35 wt%镍和不添加2.5 wt%铬的情况。在3.5 wt% NaCl溶液中,通过光学和扫描电子显微镜、静态拉伸测试、冲击强度测试和室温耐腐蚀性评估对材料进行了表征。研究表明,改变镍和铬含量对高镍铸铁的性能有显著影响。此外,通过控制这些元素的含量,可以获得具有既定性能的铸铁,根据预期的最终性能,结果表明,用少量的铬代替部分镍含量可以获得相似的耐腐蚀性能并降低生产成本,但会影响力学性能,而力学性能取决于塑性。
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引用次数: 0
Thermo-mechanical processing of Al–Mg–Si(Cu) alloy extrusions based on dynamic stretching 基于动态拉伸的Al-Mg-Si (Cu)合金挤压件热机械加工
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-09 DOI: 10.1007/s43452-025-01323-2
Dariusz Leśniak, Antoni Woźnicki, Beata Leszczyńska-Madej, Grzegorz Włoch, Tomasz Latos, Jacek Madura, Marek Bogusz, Piotr Korczak, Bartłomiej Płonka

In the first part of the work, the 3-step homogenization procedure was carried out for AlMgSi(Cu) alloy, aimed at obtaining billets microstructure with numerous fine particles of strengthening phases and increased solidus temperature. In the second part of the work, an original on a global scale prototype device for the dynamic stretching of extruded profiles before artificial ageing, was proposed and tested in semi-industrial conditions. The thermo-mechanical treatment of extruded hollow profiles from AlMgSi(Cu) alloy with 1.22% content of copper was performed with dynamic deformation range: 0.25%, 0.5%, 1%, 1.5% and 2%. The microstructural inspection was performed in the welding area and outside the weld for variant after only extrusion and for variant after extrusion and dynamic stretching before artificial ageing. It was revealed that the designed three-stage homogenization treatment led to dissolution of soluble phases present in the as-cast billets microstructure, which caused significant increase in solidus temperature, from 509 °C in as-cast state to 573 °C after completed soaking. The application of dynamic deformation during the straightening of aluminium profiles after hot extrusion with water cooling on the press run, led to the induced favourable changes in the microstructure of the alloy, which translated into a significant increase in UTS of about 11%.

在第一部分工作中,对AlMgSi(Cu)合金进行了三步均匀化工艺,旨在获得具有大量强化相细颗粒和提高固相温度的坯料组织。在工作的第二部分,一个原始的在全球范围内的原型装置,挤出型材的动态拉伸前人工老化,提出并在半工业条件下进行了测试。对含铜量为1.22%的AlMgSi(Cu)合金挤压中空型材进行了动态变形范围为0.25%、0.5%、1%、1.5%和2%的热处理。在焊接区和焊缝外进行了仅挤压变形和挤压变形和人工时效前动态拉伸变形的显微组织检测。结果表明,三段均质处理导致铸态方坯组织中可溶相的溶解,导致固相温度从铸态509℃显著升高到完全浸泡后的573℃。在热挤压后的铝型材矫直过程中应用动态变形,在压机运行中进行水冷却,导致合金的微观组织发生了有利的变化,这转化为UTS显著增加了约11%。
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引用次数: 0
Elevated temperature response and fire resistance considerations of 3D-printed concrete: small- to medium-scale wall experiments 3d打印混凝土的高温响应和耐火考虑:中小规模墙体实验
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-08 DOI: 10.1007/s43452-025-01321-4
Pawel Sikora, Szymon Skibicki, Jakub Bielawski, Mateusz Techman, Karol Federowicz, Wojciech Węgrzyński

3D printing introduces unique challenges in construction, particularly regarding fire safety. The layer-by-layer deposition leads to potential weaknesses such as interlayer debonding, spalling, and cracking when exposed to elevated temperatures and thermal gradients. Despite growing interest, large-scale fire performance of 3D-printed concrete (3DPC) remains underexplored. This study investigates the thermal and fire behaviour of 3DPC, both material wise and of printed full scale. Laboratory tests on small specimens (160 × 40 × 40 mm) assessed the mechanical performance of 3D-printed concrete exposed to temperatures up to 800 °C. The results show that over 80% of compressive strength was retained after heating the samples to 450 °C. Full-scale wall segments (500 mm × 180 mm × 500 mm) with three different internal topologies (hollow, triangular, and sinusoidal) were subjected to standard fire resistance tests. Elements with attached thermocouples were fixed in the oven without a load and exposed to ISO 834 temperature–time profile. The occurring damage on the exposed and unexposed surface was evaluated using optical measurements. Results has shown that the elements maintained integrity (E) and insulation (I) criteria up to 450 °C at 1 cm depth for 19–25 min, and at 2 cm for 45–65 min. Tests revealed extensive surface cracking in all samples, with the most significant damage observed in hollow-core elements. In contrast, samples with triangular and sinusoidal infill exhibited lower thermal penetration and reduced structural degradation. The findings indicate promising thermal insulating performance of 3DPC and highlight the critical role of internal geometry in fire response. However, further research is required to assess fire behaviour under mechanical loading and to validate performance across a wider range of infill designs and real-scale conditions.

3D打印在建筑中引入了独特的挑战,特别是在消防安全方面。当暴露在高温和热梯度下时,逐层沉积会导致层间脱粘、剥落和开裂等潜在缺陷。尽管人们对3d打印混凝土(3DPC)的兴趣日益浓厚,但其大规模防火性能仍未得到充分探索。本研究考察了3d打印材料和全尺寸打印材料的热和燃烧行为。小样本(160 × 40 × 40 mm)的实验室测试评估了暴露在高达800°C温度下的3d打印混凝土的机械性能。结果表明,将试样加热至450℃后,试样的抗压强度保持在80%以上。具有三种不同内部拓扑结构(空心、三角形和正弦)的全尺寸墙段(500 mm × 180 mm × 500 mm)进行了标准的耐火测试。带有附加热电偶的元件在没有负载的情况下固定在烤箱中,并暴露在ISO 834温度时间曲线下。利用光学测量对暴露和未暴露表面上发生的损伤进行了评估。结果表明,元件保持完整性(E)和绝缘(I)标准高达450°C,在1厘米深度19-25分钟,在2厘米深度45-65分钟。测试显示,所有样品的表面都有广泛的开裂,在空心核心元素中观察到最显著的损伤。相反,三角形和正弦填充的样品表现出更低的热渗透和更少的结构降解。研究结果表明,3DPC具有良好的隔热性能,并强调了内部几何形状在火灾响应中的关键作用。然而,需要进一步的研究来评估机械载荷下的火灾行为,并验证在更大范围的填充设计和实际规模条件下的性能。
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引用次数: 0
Optimizing concrete properties with carbonated recycled concrete aggregate: a sustainable approach 用碳化再生混凝土骨料优化混凝土性能:一种可持续的方法
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-07 DOI: 10.1007/s43452-025-01319-y
Shimza Jamil, Maria Idrees, Arslan Akbar, Salim Barbhuiya

This study explores the potential of carbon dioxide sequestration to enhance the properties of recycled concrete aggregate (RCA) through accelerated carbonation techniques. Carbonated RCA (CRCA) was incorporated into concrete mixtures with two water–cement ratios (0.55 and 0.42), targeting compressive strengths of 30 MPa and 40 MPa, respectively. RCA particles (5–20 mm) were carbonated under 1 bar pressure for 2 and 3 h. Key physical properties including aggregate crushing value (ACV), aggregate impact value (AIV), and water absorption (WA), were evaluated for both RCA and CRCA. Results showed that CRCA significantly improved concrete workability and strength compared to untreated RCA. Specifically, CRCA reduced ACV, AIV, and WA by 2.8%, 2.3%, and 1.5%, respectively, indicating better aggregate quality. In 30 MPa concrete, compressive strength increased by 16% with 100% CRCA and by 9.6% with 50% CRCA; for 40 MPa concrete, the improvements were 18% and 12%, respectively. Similar trends were observed for split tensile strength. Microstructural analyses (XRD, FTIR, TGA, DSC, SEM) confirmed that carbonation at 1 bar for 2 h provided optimal RCA modification. These findings suggest that accelerated carbonation of RCA can substantially improve concrete performance, offering practical benefits for sustainable construction practices.

本研究探讨了二氧化碳封存的潜力,通过加速碳化技术提高再生混凝土骨料(RCA)的性能。碳化RCA (CRCA)掺入水灰比为0.55和0.42的混凝土混合料中,抗压强度分别为30 MPa和40 MPa。RCA颗粒(5-20 mm)在1 bar压力下碳化2和3小时。对RCA和CRCA的关键物理性能进行了评估,包括骨料破碎值(ACV)、骨料冲击值(AIV)和吸水率(WA)。结果表明,与未经处理的RCA相比,CRCA显著改善了混凝土的和易性和强度。具体而言,CRCA使ACV、AIV和WA分别降低2.8%、2.3%和1.5%,表明骨料质量较好。在30 MPa混凝土中,添加100% CRCA时抗压强度提高16%,添加50% CRCA时抗压强度提高9.6%;对于40mpa的混凝土,分别提高了18%和12%。在分裂拉伸强度方面也观察到类似的趋势。微观结构分析(XRD, FTIR, TGA, DSC, SEM)证实,在1 bar下碳化2 h提供了最佳的RCA改性。这些发现表明,RCA的加速碳化可以大大提高混凝土性能,为可持续建筑实践提供实际好处。
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Archives of Civil and Mechanical Engineering
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