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Influence of selected technological parameters of hot rolling process and heat treatment on the microstructure and mechanical properties of high-strength S355J2/NANOS-BA® clad plates 热轧工艺和热处理工艺参数对高强度S355J2/NANOS-BA®复合板组织和力学性能的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-10-02 DOI: 10.1007/s43452-025-01337-w
Bartłomiej Walnik, Dariusz Woźniak, Aleksandra Bagińska, Mariusz Adamczyk

The article describes to design the parameters of hot rolling and heat treatment technology in a way that would allow for permanent bonding of S355J2 and NANOS-BA® steel into one high-strength clad plates. In the article, guidelines for the hot rolling process of clad plates with two-stage heat treatment were described, which were then verified in a semi-industrial technological line. The materials obtained in this way in different initial states were subjected to metallographic and strength tests. Based on three technological variants of the process, S355J2/ NANOS-BA® clad plates were produced. After additional heat treatment, a nanobainitic microstructure of high strength and ballistic and abrasion resistance was created in the applied layer, which indicates the possibility of using this type of clad plate in the armaments, machine building, or construction industry.

本文介绍了如何设计热轧参数和热处理技术,使S355J2和NANOS-BA®钢永久结合成一个高强度复合板。本文介绍了两段热处理复合板热轧工艺的指导原则,并在半工业化工艺生产线上进行了验证。用这种方法得到的材料在不同初始状态下进行了金相和强度试验。基于该工艺的三种技术变体,生产了S355J2/ NANOS-BA®复合板。经过额外的热处理后,在涂层中产生了高强度、抗弹道和耐磨性的纳米贝氏体微观结构,这表明在军备、机械制造或建筑行业中使用这种类型的复合板的可能性。
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引用次数: 0
Establishment of electroplastic constitutive equation and study of deformation mechanism during cutting Inconel718 Inconel718切削过程电塑性本构方程的建立及变形机理研究
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-29 DOI: 10.1007/s43452-025-01344-x
ZhaoPeng Hao, Yongshou Xu, YiHang Fan, Dongliang Zhu

In this paper, a pulse current assisted compression test platform is built to investigate the effects of temperature, strain rate, and current density on flow stress. Based on the Johnson-Cook model and considering the physical mechanism of the electroplastic effect, the constitutive equation for Inconel718 under pulsed current is constructed. By compiling the user subroutine Vumat and importing it into Abaqus for simulation, and comparing it with the electric pulse assisted turning experiment, the influence of electroplastic parameters (0–100 A) on chip morphology and cutting force is explored. The research results are expected to provide technical guidance for expanding the application field of Inconel718.

本文建立了脉冲电流辅助压缩试验平台,研究了温度、应变速率和电流密度对流动应力的影响。基于Johnson-Cook模型,考虑电塑性效应的物理机理,建立了脉冲电流作用下Inconel718的本构方程。通过编写用户子程序Vumat并导入Abaqus进行仿真,并与电脉冲辅助车削实验进行对比,探讨了电塑性参数(0 ~ 100 A)对切屑形貌和切削力的影响。研究成果有望为拓展Inconel718的应用领域提供技术指导。
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引用次数: 0
Influence of friction stir welding parameters on mechanical and electrochemical performance of EN AW-6082-T651 alloy butt joints 搅拌摩擦焊参数对EN AW-6082-T651合金对接接头力学和电化学性能的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-29 DOI: 10.1007/s43452-025-01336-x
Aleksandra Mirowska, Marek Szkodo, Łukasz Pawłowski, Dorota Moszczyńska, Jarosław Mizera

This study investigates the influence of friction stir welding parameters, specifically tool rotational speed and linear speed, on the electrochemical and mechanical properties of EN AW-6082-T651 butt joints. The research encompassed microstructural analysis, surface roughness measurements, potentiodynamic corrosion tests, hardness profile measurement, and static tensile testing. Results revealed that decreasing the linear speed or increasing the rotational speed during welding intensified heat input, leading to grain growth in the weld nugget zone. The smallest grain size of 3.46 ± 1.11 µm was achieved at 1000 rpm and 250 mm/min. Surface roughness was minimized at 1250 rpm and 200 mm/min, as excessive tool feed caused irregularities. Corrosion resistance improved compared to the parent material, attributed to fine-grained structures promoting compact passive layer formation. Hardness profiling indicated the lowest values in the heat-affected zone, particularly for joints produced at 1250 rpm and 200 mm/min due to the highest heat input and precipitate dissolution. Tensile testing confirmed fracture locations in the heat-affected zone, with maximum tensile strength reaching 69% of the base material and elongation approximately 30%.

研究了搅拌摩擦焊接参数,特别是刀具转速和线速度对EN AW-6082-T651对接接头电化学性能和力学性能的影响。研究内容包括微观结构分析、表面粗糙度测量、动电位腐蚀测试、硬度剖面测量和静态拉伸测试。结果表明,降低线速度或提高焊接转速均能增强热输入,导致焊缝熔核区晶粒长大;在转速为1000 rpm,转速为250 mm/min时,晶粒尺寸最小,为3.46±1.11µm。在1250 rpm和200 mm/min的转速下,由于刀具进给过大导致不规则,表面粗糙度最小。与母材相比,耐腐蚀性有所提高,这是由于细晶结构促进了致密被动层的形成。硬度分布表明,在热影响区,特别是在1250转/分钟和200毫米/分钟的速度下生产的接头,由于最高的热量输入和沉淀溶解,硬度值最低。拉伸测试确认断裂位置位于热影响区,最大抗拉强度达到母材的69%,延伸率约为30%。
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引用次数: 0
Correction: Effect of continuous annealing process on various structure parameters of martensite of dual-phase steels 修正:连续退火工艺对双相钢马氏体各组织参数的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-25 DOI: 10.1007/s43452-025-01314-3
Nemai Chandra Gorain, Mahesh Gulab Walunj, Manish Kumar Soni, B. Ravi Kumar
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引用次数: 0
Probabilistic approach to concrete durability based on combined stochastic differential equations and Monte Carlo method 基于随机微分方程和蒙特卡罗方法的混凝土耐久性概率分析
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-25 DOI: 10.1007/s43452-025-01335-y
Marcin Koniorczyk, Dalia Bednarska, Alicja Wieczorek, Kalina Materak

Cementitious materials are often exposed to aggressive environments, which have a significant impact on their durability. Proper prediction of concrete corrosion helps to apply the right measures and technologies, to extend the service life of structures. Carbonation and cyclic freezing are recognized among the most common corrosive factors for concrete. Their progress is linked to the penetration of CO2 and water into the concrete structure. Due to the random arrangement of aggregates and cement paste, concrete is an inhomogeneous material. Therefore, the progress of carbonation and frost-induced damage should be treated as random variables with appropriate probabilistic parameters. Experimental studies on concrete carbonation and freezing were conducted in accordance with the standards EN 12390–12 and EN 12390–9. As observed in the experiments, the progress of carbonation and frost damage of concrete could be described by zigzag, not necessarily monotonic functions. Stochastic differential equations (SDE) were employed to predict the behavior of concrete exposed to elevated CO2 concentrations and cyclic freezing. The stochastic model consisted of a drift term, which described the general trend of concrete durability exposed to carbonation and frost cycles, as well as a diffusion term, which accounted for the stochastic features of inhomogeneous concrete microstructure. The Euler–Maruyama approximation with Milstein improvement was applied to model the realization of the stochastic changes in concrete microstructure/durability. The proposed approach predicted experimental results with high accuracy. The application of the Monte Carlo (MC) method with 100,000 SDE realizations allowed to calculate the statistical parameters of the processes, such as concrete carbonation and freezing cycles. The probabilistic parameters, such as expected values and standard deviations, calculated using the SDE_MC approach, were in good agreement with experimental results for both problems, i.e. decelerating concrete carbonation and accelerating concrete scaling.

胶凝材料经常暴露在腐蚀性环境中,这对其耐久性有重大影响。正确的混凝土腐蚀预测有助于采取正确的措施和技术,延长结构的使用寿命。碳化和循环冻结是混凝土最常见的腐蚀因素。它们的进展与二氧化碳和水渗透到混凝土结构中有关。由于骨料和水泥浆的随机排列,混凝土是一种非均质材料。因此,应将碳酸化过程和冻害过程视为具有适当概率参数的随机变量。混凝土碳化和冻结的试验研究按照标准EN 12390-12和EN 12390-9进行。从试验中可以看出,混凝土的碳化和冻损过程可以用之字形函数来描述,而不一定是单调函数。采用随机微分方程(SDE)来预测混凝土暴露于高CO2浓度和循环冻结下的行为。随机模型包括一个漂移项和一个扩散项,前者描述了碳化和霜冻循环下混凝土耐久性的总体趋势,后者考虑了混凝土微观结构非均匀性的随机性特征。采用Milstein改进的Euler-Maruyama近似来模拟混凝土微观结构/耐久性随机变化的实现。该方法对实验结果的预测精度较高。应用蒙特卡罗(MC)方法与100,000 SDE实现允许计算过程的统计参数,如混凝土碳化和冻结循环。采用SDE_MC方法计算的概率参数,如期望值和标准差,与实验结果吻合良好,即减缓混凝土碳化和加速混凝土结垢。
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引用次数: 0
Experimental study and numerical simulation on the penetration mechanisms of La-modified 93W alloy based on adaptive FEM–SPH method 基于自适应FEM-SPH方法的la改性93W合金侵彻机理实验研究与数值模拟
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-24 DOI: 10.1007/s43452-025-01342-z
Jun Fang, Dongsheng Han, Yawen Liao, Mingchuan Wang, Chengxin Du, Zhonghua Du, Cai Chen

High-speed penetration experiments were performed on traditional sintered 93W alloy (93W–5.4Ni–1.6Fe) and a novel 93W–La alloy (93W–5.5Ni–1.1Fe–0.4La) containing 0.4% La, to impact a 30CrMnMo target at a velocity of 1650 m/s. The results indicated that the incorporation of La enhanced the mechanical properties of the 93W alloy, resulting in an 8.41% increase in the penetration depth of the 93W–La alloy compared with the sintered 93W alloy. The parameters for the Johnson–Cook constitutive equations of the two types of penetrator materials were determined through quasi-static tensile tests and Split-Hopkinson Pressure Bar (SHPB) experiments. Numerical simulations of the high-speed penetration tests were conducted on the LS-DYNA platform using FEM and adaptive FEM–SPH methods. The simulation results were compared with experimental target impact test data, demonstrating that the adaptive FEM–SPH method had superior computational accuracy. The penetration characteristics of both penetrators were analyzed throughout the crater formation, stable penetration, and plugging stages. The 93W alloy penetrator retained a “mushroom head” shape at the tip throughout the penetration process, whereas the 93W–La alloy penetrator exhibited significant adiabatic shear sensitivity, leading to adiabatic shear failure and “self-sharpening” characteristics.

采用传统烧结93W合金(93W - 5.4 ni - 1.6 fe)和新型含有0.4% La的93W - La合金(93W - 5.5 ni - 1.1 fe - 0.4La),以1650 m/s的速度冲击30CrMnMo靶材。结果表明:La的加入增强了93W合金的力学性能,使93W - La合金的渗深比烧结93W合金提高了8.41%;通过准静态拉伸试验和Split-Hopkinson压杆(SHPB)试验确定了两种侵彻材料的Johnson-Cook本构方程参数。采用有限元法和自适应FEM - sph方法,在LS-DYNA平台上对高速侵彻试验进行了数值模拟。仿真结果与实验目标冲击试验数据进行了比较,表明自适应FEM-SPH方法具有较好的计算精度。分析了两种侵彻器在整个弹坑地层、稳定侵彻和封堵阶段的侵彻特性。在侵彻过程中,93W合金侵彻头部呈“蘑菇头”形状,而93W - la合金侵彻头部表现出明显的绝热剪切敏感性,导致绝热剪切破坏和“自锐化”特征。
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引用次数: 0
Biaxial stress state deformation behavior and constitutive modeling of Ti65 sheets under superplastic forming conditions Ti65板材在超塑性成形条件下的双轴应力状态变形行为及本构建模
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-24 DOI: 10.1007/s43452-025-01322-3
Lihua Du, Zixuan Wang, Zhiqiang Li, Dechong Li, Yong Li, Kailun Zheng

To precisely elucidate the deformation characteristics of Ti65 sheets under uniaxial and biaxial stress states during the superplastic forming (SPF) process, a series of uniaxial hot tensile and biaxial bulging tests were conducted to explore the superplastic deformation behavior within a temperature range of 900–960 °C and a strain rate range of 0.001–0.03 s⁻1. The deformation behavior and uniform strain under uniaxial stress states were characterized through the DIC real-time strain measurement system. In addition, the key microstructures evolutions during different stress states were characterized and analyzed to determine the deformation mechanisms. Based on the test results, the constitutive model for both uniaxial and biaxial behavior of Ti65 sheets was developed and calibrated. The results of this research indicated that Ti65 exhibited superplastic deformation at 940 °C—0.0014 s⁻1 and 960 °C—0.0075 s⁻1, which led to an enlargement of its forming limit. Simultaneously, the evolution mechanism of the microstructure under biaxial stress was revealed. As the temperature increased, the proportion of high angle grain boundaries rose, the grain size decreased, and the forming limit increased accordingly. The established constitutive model, which takes into account the evolution of the microstructure, successfully captured the forming limit points. The accuracy of the predicted uniaxial stress–strain and the bulging grain size reached 91.2% and 96.24%, respectively. This research provides theoretical guidance for the selection of the process window of titanium alloys.

为准确阐明Ti65板材在超塑性成形(SPF)过程中单轴和双轴应力状态下的变形特征,进行了一系列的单轴热拉伸和双轴胀形试验,探讨了温度900 ~ 960℃、应变速率0.001 ~ 0.03 s⁻1范围内的超塑性变形行为。通过DIC实时应变测量系统对单轴应力状态下的变形行为和均匀应变进行了表征。此外,对不同应力状态下的关键组织演变进行了表征和分析,以确定变形机制。基于试验结果,建立了Ti65板的单轴和双轴本构模型并进行了标定。研究结果表明,Ti65在940°C-0.0014 s毒血症和960°C-0.0075 s毒血症时表现出超塑性变形,导致其形成极限增大。同时,揭示了双轴应力作用下的微观组织演化机制。随着温度的升高,高角度晶界比例增加,晶粒尺寸减小,成形极限相应增大。所建立的本构模型考虑了微观组织的演变,成功地捕获了成形极限点。预测的单轴应力应变和胀形晶粒尺寸精度分别达到91.2%和96.24%。该研究为钛合金工艺窗口的选择提供了理论指导。
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引用次数: 0
Research on dry micro-milling performance and tool wear of EDM-fabricated polycrystalline diamond micro-end mill 电火花加工聚晶金刚石微立铣刀干式微铣削性能及刀具磨损研究
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-23 DOI: 10.1007/s43452-025-01315-2
Siqian Gong, Yao Sun, X. M. Zhu

Sapphire, known for its high hardness and excellent optical properties, is widely used in fields such as aerospace, optoelectronics and defense. Micro-milling technology for sapphire demonstrates significant potential in the field of sapphire surface processing due to its efficiency, high quality, low loss and flexibility. In this study, a double-edged helical polycrystalline diamond (PCD) micro-end mill with a diameter of 1 mm is designed and fabricated by electrical discharge machining (EDM). Then, the micro-slots on sapphire material are prepared with EDM-fabricated micro-end mills, and the surface quality, surface morphology, micro-milling forces and tool wear involved in micro-milling process are investigated. Experimental results indicate that three types of damages are observed on sapphire micro-slot surface including wavy cracks, individual small cracks and layered tear structures. The minimum surface roughness Sa for sapphire micro-slot obtained with PCD micro-end mill can reach to 0.73 µm. In addition, the major wear forms of PCD micro-end mill when machining sapphire include mechanical wear, thermal chemical wear, adhesive wear, and micro-chipping. The research of adopting PCD micro-end mills for sapphire holds significant application value, which can advance technological progress in machining efficiency and surface quality of hard brittle material.

蓝宝石以其高硬度和优异的光学性能而闻名,广泛应用于航空航天、光电子和国防等领域。蓝宝石微铣削技术以其高效、高质量、低损耗和柔韧性等优点,在蓝宝石表面加工领域显示出巨大的潜力。设计并制造了直径为1 mm的双刃螺旋聚晶金刚石(PCD)微立铣刀。然后,利用电火花加工的微型立铣刀在蓝宝石材料上制备了微槽,研究了微铣削过程中所涉及的表面质量、表面形貌、微铣削力和刀具磨损。实验结果表明,蓝宝石微槽表面存在波状裂纹、单个小裂纹和层状撕裂结构三种损伤类型。PCD微立铣刀加工蓝宝石微槽的最小表面粗糙度Sa可达0.73µm。此外,PCD微立铣刀加工蓝宝石时的主要磨损形式包括机械磨损、热化学磨损、粘着磨损和微切屑。采用PCD微立铣刀加工蓝宝石具有重要的应用价值,可以促进硬脆材料加工效率和表面质量的技术进步。
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引用次数: 0
Microstructural evolution and enhanced wear resistance of laser-clad IN718/h-BN composite coatings on H13 tool steel H13工具钢激光熔覆IN718/h-BN复合涂层的组织演变及耐磨性增强
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-22 DOI: 10.1007/s43452-025-01318-z
Jiahao Sun, Weizhou Gu, Yang Bu, Jianhua Zhang, Qinhe Zhang, Enfu Zhang, Yonghui Wang

H13 steel is a key material in the field of hot work dies. Despite its excellent strength and toughness, surface coatings are often needed to improve its hardness and wear resistance in high-temperature environments. In this research, laser cladding of Inconel 718 (IN718)/hexagonal boron nitride (h-BN) composite coatings on H13 steel is investigated to enhance its performance. The effect of process parameters on the macroscopic morphology, represented by the width-to-height ratio and dilution rate, is investigated to obtain coatings with enhanced interfacial bonding strength and improved metallurgical compatibility. The powder composition is determined by characterizing the microstructure, surface hardness, wear resistance, and other properties of composite coatings with varying h-BN content. Additionally, the roles of solution treatment and age hardening as post-treatment methods in further improving coating performance are evaluated. The results indicate that the composite coatings prepared under the applied laser cladding parameters exhibit no significant defects. The 35 wt.% h-BN composite coating (the optimal composition) demonstrates superior ambient/elevated-temperature hardness, 35.4% lower friction coefficient, and 76.8% reduced wear loss compared to the H13 steel substrate. As h-BN content increases, the volume of nitrides and borides in the coatings also rises. Precipitates such as alumina, Metal Carbide (MC), Metal Nitride (MN), and Laves phases are observed both inside and outside the grains, with grain sizes ranging from 5 to 100 µm. After solution treatment, the dissolution and diffusion of intergranular precipitates are evident. Following age hardening, hard phases enriched with B and N fully diffuse and precipitate at the grain boundaries. Post-treatment effectively releases residual stress in the coating, resulting in enhanced material properties. This research provides a novel strategy for surface strengthening of H13 steel in high-temperature applications.

H13钢是热作模具领域的关键材料。尽管其具有优异的强度和韧性,但在高温环境下,通常需要表面涂层来提高其硬度和耐磨性。为了提高H13钢的性能,研究了激光熔覆Inconel 718 (IN718)/六方氮化硼(h-BN)复合涂层。研究了工艺参数对宏观形貌(以宽高比和稀释率为代表)的影响,得到了界面结合强度增强、冶金相容性改善的涂层。通过表征不同h-BN含量的复合涂层的显微组织、表面硬度、耐磨性和其他性能来确定粉末成分。此外,还评价了固溶处理和时效硬化作为后处理方法在进一步提高涂层性能方面的作用。结果表明,在激光熔覆参数下制备的复合涂层无明显缺陷。与H13钢基体相比,35 wt.%的h-BN复合涂层(最佳成分)具有优异的室温/高温硬度,摩擦系数降低35.4%,磨损损失降低76.8%。随着h-BN含量的增加,涂层中氮化物和硼化物的体积也增加。晶粒内外均可观察到氧化铝、金属碳化物(MC)、金属氮化物(MN)和Laves相等析出相,晶粒尺寸为5 ~ 100 μ m。固溶处理后,晶间析出物的溶解和扩散较为明显。时效硬化后,富含B和N的硬相在晶界处充分扩散和析出。后处理有效地释放涂层中的残余应力,从而增强材料性能。本研究为高温应用中H13钢的表面强化提供了一种新的策略。
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引用次数: 0
The free vibration analysis of a GNP-reinforced deep thick cylindrical shell surrounded by an orthotropic medium subjected to thermal load 热载荷作用下由正交各向异性介质包围的gnp增强深厚圆柱壳的自由振动分析
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2025-09-22 DOI: 10.1007/s43452-025-01332-1
Javad Azimi, Abbas Loghman, Elyas Mohammad-Rezaei Bidgoli, Mohammad Arefi

In this article, the vibration analysis of a nanocomposite deep thick cylindrical shell surrounded by an orthotropic medium subjected to thermal load is studied. It is assumed that the shell is fabricated from a polymeric matrix reinforced with graphene nanoplatelets (GNPs) in which the volume fraction of the GNPs varies along the thickness based on several distribution patterns. The modeling of shell is carried out utilizing a quasi-3D shear theory which includes the thickness stretching. The modeling of the medium is conducted based on the orthotropic Pasternak model. The one-dimensional heat conduction equation is solved analytically to find the temperature profile through the thickness of the shell. Moreover, the dependency of properties of the materials on the temperature is considered. A semi-analytical solution is presented to determine the natural frequencies of the shell and associated mode shapes. The effects of several parameters on the natural frequencies are studied, including the mass fraction and distribution pattern of the GNPs, thermal loading, agglomeration parameters, boundary conditions, and characteristics of the orthotropic medium. Owing to considering the thickness stretching effect, removing shallow shell assumptions, and incorporating the agglomeration of the GNPs, the results of the presented work benefit from high accuracy and can be used in the design and analysis of thin to thick and shallow to deep nanocomposite cylindrical shells.

本文研究了纳米复合材料深厚圆柱壳在热载荷作用下的振动特性。假设壳是由石墨烯纳米片(GNPs)增强的聚合物基体制成的,其中GNPs的体积分数根据几种分布模式沿厚度变化。采用包含厚度拉伸的准三维剪切理论对壳体进行建模。介质的建模采用正交各向异性帕斯捷尔纳克模型。对一维热传导方程进行解析求解,求出随壳体厚度变化的温度分布。此外,还考虑了材料性能对温度的依赖关系。给出了确定壳体固有频率和相关模态振型的半解析解。研究了GNPs的质量分数和分布模式、热载荷、团聚参数、边界条件和正交各向异性介质特性等参数对固有频率的影响。由于考虑了厚度拉伸效应,消除了浅壳假设,并考虑了GNPs的团聚,所得结果具有较高的精度,可用于从薄到厚、从浅到深的纳米复合材料圆柱壳的设计和分析。
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