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Seismic fragility assessment model for regional building structures considering multivariate intensity measures 考虑多变量烈度指标的区域建筑结构地震易损性评价模型
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2026-01-22 DOI: 10.1007/s43452-025-01402-4
Si-Qi Li

Seismic intensity measures are the core indicators for determining the distribution of seismic risk and the vulnerability of buildings in large-scale zones. As traditional intensity measures, macroscopic and instrumental seismic intensities are widely used worldwide. However, the quantification methods for macroseismic and instrument intensities are limited by the fuzziness of evaluation scales and the uneven distribution of seismic stations, resulting in an urgent need to improve the accuracy of evaluation scales. This study combines Chinese seismic design standards with macroscopic and instrumental intensity scales, and an evaluation method that considers multivariate intensity measures was proposed. Using nonlinear and response spectrum theory, nonlinear dynamic and spectral analyses were conducted on 360,000 accelerations monitored by 12 stations during the 2022 Luding earthquake in Sichuan Province, China. The time history and response spectrum curves were generated by considering the influence of different earthquake directions. An optimized seismic vulnerability level assessment method is proposed. A vulnerability assessment was conducted on four typical buildings (81239,407 m2 and 938,636 m2) subjected to two destructive earthquakes (the Shidian (SD) earthquake on April 10, 2001, and the Ninger (NR) earthquake on June 3, 2007) in Yunnan Province, China. A seismic damage probability matrix and surface model considering multivariate intensity measures were established. Using an updated nonlinear fitting algorithm, a seismic vulnerability curve for four types of buildings was generated on the basis of an optimized seismic vulnerability level. A seismic risk index model considering the coupling effect of adjacent vulnerability levels is proposed via a fuzzy set and probability theory. Combined with four types of structural damage data from two typical destructive earthquakes, seismic risk membership comparison curves considering multivariate intensity measures are generated.

地震烈度测度是确定大面积地震危险性分布和建筑物易损性的核心指标。宏观地震烈度和仪器地震烈度作为传统的烈度测量方法,在世界范围内得到了广泛的应用。然而,由于评价尺度的模糊性和台站分布的不均匀性,限制了宏观地震和仪器烈度的量化方法,迫切需要提高评价尺度的准确性。本研究将中国抗震设计标准与宏观烈度和仪器烈度尺度相结合,提出了一种考虑多变量烈度指标的评价方法。利用非线性和响应谱理论,对2022年四川泸定地震12个台站监测的36万个加速度进行了非线性动力学和谱分析。考虑不同地震方向的影响,生成了地震时程和反应谱曲线。提出了一种优化的地震易损性等级评价方法。对云南省石甸地震(2001年4月10日)和宁格尔地震(2007年6月3日)发生的4座典型建筑(81239、407 m2和938636 m2)进行了易损性评价。建立了考虑多变量烈度的地震损伤概率矩阵和表面模型。采用改进的非线性拟合算法,在优化的地震易损性等级基础上,生成了四种类型建筑物的地震易损性曲线。利用模糊集和概率论,建立了考虑相邻易损性等级耦合效应的地震风险指数模型。结合2次典型破坏性地震的4类结构损伤数据,生成考虑多变量烈度指标的地震风险隶属度对比曲线。
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引用次数: 0
Exploring the mechanical behavior of the spinal dura mater: experimental insights and measurement dilemmas 探索硬脑膜的力学行为:实验见解和测量困境
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2026-01-20 DOI: 10.1007/s43452-025-01395-0
Radosław Wolny, Tomasz Wiczenbach, Magdalena Rucka, Wojciech Witkowski, Jan Henryk Spodnik, Edyta Spodnik, Lukasz Pachocki

Spinal dura mater provides essential structural protection for the spinal cord and helps maintain cerebrospinal fluid pressure, yet its mechanical characterization remains challenging because of its thinness and anisotropy. This study investigated the uniaxial tensile behavior of spinal dura mater and examined how speckle-paint application, the strain-measurement method (Digital Image Correlation (DIC)-derived strain vs. crosshead displacement), preconditioning, and donor demographics affect measured mechanical parameters. Samples were harvested postmortem from seven donors and assigned to three groups: painted & not preconditioned, unpainted & preconditioned, and unpainted & not preconditioned. A 3D-printed adapter was used to standardize sample geometry. Tests were conducted at a crosshead displacement rate of 5 mm·min⁻¹ (strain rate of 0.0042 s⁻¹), with some specimens undergoing cyclic preloading. Speckle paint increased stiffness but did not affect failure stress or stretch. DIC-derived elastic moduli were higher than those from crosshead displacement. After correcting for paint- and method-induced effects, the mean elastic moduli in the longitudinal and circumferential directions were ~ 283 MPa and ~ 16 MPa, respectively. Both orientations exhibited a failure stretch of ~ 1.10–1.12. The apparent Poisson function (Hencky form) ranged from 1.57 to 4.84 (longitudinal) and 2.91 to 6.29 (circumferential), indicating volumetric changes that challenge near-incompressibility assumptions. These findings emphasize the importance of standardized protocols and data normalization when investigating soft tissue mechanics. The higher DIC-based moduli arise primarily from local, gauge-region strain measurement and stiffening induced by the acrylic speckle coating, while the elevated apparent Poisson’s ratios likely reflect fluid redistribution and collagen-fiber reorientation under tensile loading in this highly anisotropic tissue.

硬脑膜为脊髓提供必要的结构保护,并有助于维持脑脊液压力,但由于其薄且各向异性,其力学特性仍然具有挑战性。本研究研究了脊髓硬脑膜的单轴拉伸行为,并研究了斑点涂料应用、应变测量方法(数字图像相关(DIC)衍生应变与十字位移)、预处理和供体人口统计学对测量力学参数的影响。从7个捐献者身上采集尸体样本,并将其分为三组:涂上颜料和未预处理的,未涂上颜料和未预处理的,以及未涂上颜料和未预处理的。使用3d打印适配器来标准化样品几何形状。试验以5 mm·min - 1(应变速率0.0042 s - 1)的十字位移速率进行,并对部分试样进行循环预压。斑点漆增加了刚度,但不影响失效应力或拉伸。dic导出的弹性模量高于十字头位移导出的弹性模量。在校正油漆和方法引起的影响后,纵向和周向的平均弹性模量分别为~ 283 MPa和~ 16 MPa。两个方向的破坏拉伸均为~ 1.10 ~ 1.12。表观泊松函数(Hencky形式)范围为1.57至4.84(纵向)和2.91至6.29(周向),表明体积变化挑战了近乎不可压缩的假设。这些发现强调了在研究软组织力学时标准化方案和数据规范化的重要性。较高的dic基模量主要来自局部应变测量和丙烯酸斑点涂层引起的硬化,而表观泊松比的升高可能反映了这种高度各向异性组织在拉伸载荷下的流体重新分配和胶原纤维重新取向。
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引用次数: 0
Bayesian identification of anisotropy rotation angle and principal scales of fluctuation for soils with rotated anisotropy based on limited CPTu soundings 基于有限CPTu测深的各向异性旋转土壤各向异性旋转角和主要波动尺度的贝叶斯识别
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2026-01-19 DOI: 10.1007/s43452-025-01398-x
Marek Kawa, Irena Bagińska

Interest in random fields (RFs) with rotated anisotropy has been growing, yet the identification of the anisotropy rotation angle has been mostly limited to rocks and soils with visible anisotropic structures. This paper presents a method for simultaneously determining the principal values of the scale of fluctuation (SOFs) and the anisotropy rotation angle based on limited CPTu soundings. The proposed method extends the approach of Ching et al. (2018, Geosci. Front., 9, 1597–1608) by including the identification of the rotation angle. The findings demonstrate that accurate and precise identification of the rotation angle is possible and that the identified values can be significant in some cases. Furthermore, it is shown that assuming an incorrect anisotropy rotation angle (e.g., commonly assumed α = 0°) can lead to two major problems: (1) loss of convergence when identifying SOF values (resulting in large coefficients of variation for the major SOF) when the difference between the true and assumed angles is large; and (2) incorrect identification of SOF values (with the error up to 80% or more) even when the difference is small (and convergence is not lost). Therefore, the proposed extended method, which reduces the error to approximately 10%, may be necessary for the accurate identification of RF parameters, even for soils with small anisotropy rotations, which are often neglected. Although small anisotropy rotations have little direct impact on probabilistic outcomes when the principal SOFs are correctly identified, they still influence the identification procedure itself, and therefore can have a significant indirect effect on the resulting probabilistic analyses.

随着各向异性旋转随机场的研究日益深入,各向异性旋转角的识别大多局限于具有可见各向异性结构的岩石和土壤。本文提出了一种基于有限CPTu测深同时确定波动尺度(SOFs)主值和各向异性旋转角的方法。本文提出的方法扩展了Ching et al. (2018, Geosci.)的方法。前面。(9,1597 - 1608),包括旋转角度的识别。研究结果表明,准确和精确地识别旋转角度是可能的,并且识别值在某些情况下可能是显著的。此外,研究表明,假设一个不正确的各向异性旋转角度(例如,通常假设α = 0°)会导致两个主要问题:(1)当真实角度与假设角度之间的差异较大时,识别SOF值时会失去收敛性(导致主要SOF的变异系数较大);(2)即使差异很小(且不会失去收敛性),也会错误地识别SOF值(误差高达80%以上)。因此,所提出的将误差降低到约10%的扩展方法可能是准确识别RF参数所必需的,即使是对于通常被忽略的具有小各向异性旋转的土壤也是如此。虽然在正确识别主要SOFs时,小的各向异性旋转对概率结果的直接影响很小,但它们仍然影响识别过程本身,因此可以对结果概率分析产生重大的间接影响。
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引用次数: 0
Fracture behavior of jointed rock under excavation unloading: laboratory testing 开挖卸载作用下节理岩体的断裂行为:室内试验
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2026-01-19 DOI: 10.1007/s43452-025-01407-z
Kaihui Li, Jiezhen Chen, Qingxiong Zhao, Ping Cao, Hang Lin, Rihong Cao

In deep-buried tunnel construction, the instability issues caused by excavation under high-stress conditions have been challenging. In this study, a series of true triaxial single-sided unloading tests were performed on jointed sandstone specimens with different joint inclinations to explore the fracture behavior of jointed rock at different burial depths under excavation unloading. The results show that the specimen under Loading Path I (unloading first and then loading) exhibits an unloading rebound phenomenon and a distinct yielding stage, reflecting a ductile failure. The specimen under Loading Path II (loading first and then unloading) shows a higher brittleness and greater susceptibility to failure, without an obvious yield stage. In the specimen under Loading Path I, the macroscopic failure forms a V-shaped notch due to buckling tensile cracks, whereas the failure of specimen under Loading Path II resembles the rockburst phenomenon with far-field tensile cracks. Additionally, the increased burial depth increases the yield and peak stresses of specimen and suppresses large-scale cracks but intensifies the crack propagation in specimen upon unloading, resulting in a more severe failure. The joint inclination affects the crack propagation and fragmentation characteristics of specimen, with the greatest influence occurring at 30°–45°. At joint inclinations of 0°–30°, the failure of specimen is dominated by shear cracks initiated from joint tips. At joint inclinations of 45°–60°, the failure of specimen involves mixed tensile-shear cracks, while at the joint inclination of 90°, the tensile cracks parallel to the joint dominate.

在深埋隧道施工中,高应力条件下开挖引起的失稳问题一直是一个难题。本研究通过对不同节理倾角节理砂岩试件进行真三轴单面卸荷试验,探讨不同埋深节理岩石在开挖卸荷作用下的断裂行为。结果表明:加载路径1(先卸荷后加荷)下试样出现卸荷回弹现象和明显的屈服阶段,表现为延性破坏;加载路径II(先加载后卸载)下的试样脆性更高,破坏易感性更强,没有明显的屈服阶段。加载路径1下试件的宏观破坏形式为屈曲拉伸裂纹导致的v形缺口,而加载路径2下试件的破坏形式类似于具有远场拉伸裂纹的岩爆现象。埋深的增加增加了试样的屈服应力和峰值应力,抑制了试样的大规模裂纹,但在卸荷时加剧了试样的裂纹扩展,导致破坏更加严重。节理倾角影响试样裂纹扩展和破碎特性,在30°~ 45°时影响最大。在节理倾角为0°~ 30°时,试样的破坏以节理尖端产生的剪切裂纹为主。节理倾角为45°~ 60°时,试件破坏以拉剪混合裂纹为主,节理倾角为90°时,试件破坏以平行于节理的拉伸裂纹为主。
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引用次数: 0
Dynamic evolution of austenite/ferrite grain boundary structure during in-situ tensile deformation in dss 2205 duplex steel dss2205双相钢原位拉伸变形过程中奥氏体/铁素体晶界组织的动态演变
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2026-01-16 DOI: 10.1007/s43452-025-01414-0
Juan Li, Chuanlong Han, Qingyao Tang, Guanghui Zhao, Huaying Li

The deformation behavior of 2205 duplex stainless steel was analyzed using in situ electron backscatter diffraction (EBSD) and scanning electron microscopy (SEM) to investigate phase-specific strain accommodation mechanisms. Results indicate that the slip deformation in the austenite and ferrite phases correlates with their mechanical property differences. In austenite, Σ3 boundaries enclosing twins demonstrated effective deformation compatibility. As strain increased, the slip systems activated remained consistent with those predicted by the maximum Schmid factor. In contrast, ferrite exhibited cross-slip behavior due to the simultaneous activation of {110} and {112} slip systems, deviating from the Schmid law. The evolution of low-angle grain boundaries (LAGBs) was a dominant deformation feature in ferrite, with the density of LAGBs increasing during tensile deformation. Additionally, preferential rotation of grain subdomains led to misorientation accumulation near original high-angle grain boundaries (HAGBs) and triple junctions, forming new HAGBs. These findings reveal coordinated deformation mechanisms involving grain rotation and slip interactions between the two phases.

采用原位电子背散射衍射(EBSD)和扫描电镜(SEM)分析了2205双相不锈钢的变形行为,探讨了相应变调节机制。结果表明,奥氏体和铁素体相的滑移变形与其力学性能的差异有关。在奥氏体中,Σ3包围孪晶的边界表现出有效的变形相容性。随着应变的增加,激活的滑移系统与最大施密德因子预测的滑移系统保持一致。相反,由于{110}和{112}滑移体系同时激活,铁氧体表现出偏离施密德定律的交叉滑移行为。低角晶界的演化是铁素体的主要变形特征,在拉伸变形过程中,低角晶界密度增大。此外,晶粒子域的优先旋转导致在原高角晶界(HAGBs)和三结附近的错取向积累,形成新的HAGBs。这些发现揭示了两相之间涉及晶粒旋转和滑移相互作用的协调变形机制。
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引用次数: 0
Influence of hot isostatic pressing on the microstructural and mechanical properties of Ti6Al4V produced via additive methods: laser powder bed fusion and cold spraying 热等静压对激光粉末床熔合和冷喷涂法制备Ti6Al4V合金组织和力学性能的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2026-01-14 DOI: 10.1007/s43452-025-01416-y
Bartosz Bucholc, Anna Dobkowska, Barbara Romelczyk-Baishya, Monika Wieczorek-Czarnocka, Szymon Nosewicz, Kamil Kaszyca, Bogusława Adamczyk-Cieślak, Wojciech Żórawski, Zbigniew Pakieła, Rafał Zybała

Although intensively researched in the last decade, additive manufacturing techniques are still subject to certain shortcomings, such as internal porosity or anisotropy of properties. In this work, we investigate the effects of postprocessing via hot isostatic pressing (HIP) on the properties of the titanium alloy Ti6Al4V produced via two various additive manufacturing methods: laser powder bed fusion (LPBF) and cold spray (CS). The LPBF produced a microstructure composed of a mixture of hcp-structured α(Ti) and α’(Ti), whereas α(Ti) and bcc-structured β(Ti) were recognized in the CS-ed materials. The subsequent HIP treatment did not cause reformation of the LPBF microstructure. This process had a significant effect on the densification of the CS-ed samples. To study the anisotropy of the material properties, the tensile and compressive strengths of the materials were determined in the planes parallel and perpendicular to the building (LPBF) and spraying (CS) directions. The LPBF materials exhibited significantly better mechanical properties stemming from the typical α/α’ martensitic microstructure, whereas the CS-ed materials presented a high number of pores and smooth and textured regions composed of recrystallized grains and grains with a high number of dislocations, respectively. The HIP treatment led to a reduction in porosity, causing a significant increase in the mechanical properties (UTS by 132%) and a reduction in the UTS anisotropy in the CS-ed materials.

尽管在过去十年中进行了深入的研究,但增材制造技术仍然存在某些缺点,例如内部孔隙度或性能的各向异性。在这项工作中,我们研究了热等静压后处理(HIP)对两种不同的增材制造方法:激光粉末床熔合(LPBF)和冷喷涂(CS)生产的Ti6Al4V钛合金性能的影响。LPBF产生了由hcp结构的α(Ti)和α ' (Ti)混合组成的微观结构,而在CS-ed材料中可以识别α(Ti)和bcc结构的β(Ti)。随后的HIP处理没有引起LPBF组织的改变。该过程对CS-ed样品的致密化有显著影响。为了研究材料性能的各向异性,测定了材料在平行和垂直于建筑(LPBF)和喷涂(CS)方向上的抗拉和抗压强度。LPBF材料具有典型的α/α′马氏体微观结构,具有较好的力学性能,而CS-ed材料则具有大量的孔隙和由再结晶晶粒组成的光滑织构区,以及具有大量位错的晶粒。HIP处理降低了孔隙率,显著提高了CS-ed材料的力学性能(UTS提高了132%),降低了UTS的各向异性。
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引用次数: 0
An exact closed-form solution for buckling of an elastically connected nano-size multi-bonded system subjected to axial load 弹性连接纳米多粘结体系在轴向载荷作用下屈曲的精确封闭解
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2026-01-14 DOI: 10.1007/s43452-025-01409-x
M. Soltani, M. H. Momenian, O. Civalek

This work’s primary objective is to create and demonstrate a low-cost computational technique and an easy-to-implement formulation for estimating buckling capacity of multiple parallel nano-scale elements elastically connected by a Kerr-type foundation subjected to axial load. To accomplish this goal, the system of governing equilibrium equations of the considered multi-bonded structure, which includes n coupled linear differential equations of order 8th, is extracted using the calculus of variations approach and after eliminating the deformation of the inner shear spring layers. A set of explicit and parametric formulas for predicting the stability strength of the system under-investigation, focusing on the double-bond system, is ultimately obtained after the resulting system of equations is solved using trigonometric functions for simply-supported boundary conditions. The attained closed-form formulations require a minimal computational cost, which greatly decrease the central processing unit time, and the extracted expressions, along with their correctness and precision, can be used to achieve the critical loads associated with both in-phase and out-of-phase buckling mode deflections. An exhaustive parametric study is conducted to precisely examine the sensitivity of endurable buckling loads of double-bonded nano-scale elements after the accuracy of the extracted closed-form solution formulations is evaluated. This study considers the effects of various parameters, including the non-locality parameter, the shear layer stiffness constant, the stiffness of Winkler-type elastic medium, including the top and bottom layers, mode number, and axial load ratio, taking into account the effects of applying compressive and/or tensile axial force.

这项工作的主要目标是创建和演示一种低成本的计算技术和易于实现的公式,用于估计由kerr型基础弹性连接的多个平行纳米级元件在轴向载荷下的屈曲能力。为了实现这一目标,采用变分法,在消除内部剪切弹簧层的变形后,提取了考虑的多键结构的控制平衡方程系统,该系统包括n个8阶的耦合线性微分方程。利用简支边界条件下的三角函数对所得到的方程组进行求解后,最终得到了一组用于预测所研究系统(重点是双键系统)稳定强度的显式和参数公式。所获得的封闭形式公式需要最小的计算成本,这大大减少了中央处理单元的时间,并且所提取的表达式,以及它们的正确性和精度,可以用于获得与相内和相外屈曲模式挠度相关的临界载荷。在对提取的闭式溶液公式的精度进行评估后,进行了详尽的参数化研究,以精确地检验双键纳米元件的耐久屈曲载荷敏感性。本研究考虑了非局域参数、剪切层刚度常数、winkler型弹性介质(包括顶层和底层)刚度、模态数、轴向载荷比等参数的影响,同时考虑了施加压缩和/或拉伸轴向力的影响。
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引用次数: 0
Influence of atmosphere and surface heterogeneity on high-temperature interaction between liquid magnesium and different types of cast irons 气氛和表面非均质性对液态镁与不同类型铸铁高温相互作用的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2026-01-12 DOI: 10.1007/s43452-025-01413-1
S. Terlicka, N. Sobczak, Y. Vronska, A. Korneva, K. Janus, M. Górny, J. J. Sobczak

This study focused on the high-temperature behavior of pure liquid Mg on three dissimilar types of cast iron substrates (Fe-C alloys with different morphologies, quantities, and distributions of the graphite phase). The experiments were performed using the sessile drop method under isothermal conditions at 715 °C in two different flowing gas atmospheres: (i) pure Ar and (ii) a mixture of Ar and 5 wt% H2. The tests were conducted using non-contact heating of a couple of dissimilar materials combined with capillary purification of Mg drops from a native oxide film directly at the test temperature in an experimental chamber by squeezing the drops from a graphite capillary placed above cast iron substrates. The high-temperature behavior of Mg/substrate couples was recorded with a high-speed CCD camera, and collected images were used for measurements of the contact angle values (θ) formed between the liquid Mg and selected substrates. The solidified Mg/substrate couples were subjected to detailed microstructural observations by scanning electron microscopy (SEM) coupled with energy-dispersive X-ray spectroscopy (EDS). The obtained results showed significant differences in the wetting behavior of Mg depending on the type of cast iron and the test atmosphere. In all cases, non-wetting behavior (θ > 90°) was observed in pure Ar, while the addition of hydrogen led to a reduction in contact angle values, especially for spheroidal graphite iron (SGI), where values decreased below 90°, commonly accepted as wetting behavior. In contrast, lamellar graphite iron (LGI) remained non-wettable under both atmospheres used in this study, although a decrease in contact angle (Δθ ~ 27°) was determined in the hydrogen-containing atmosphere, as compared to pure Ar. Compact graphite iron (CGI) also exhibited non-wetting behavior in both atmospheres; however, the values of contact angle were close to 90° in the Ar + 5 wt% H2 atmosphere. The SEM/EDS analysis of cross-sectioned solidified Mg/cast iron substrates revealed slight morphological differences. For SGI and CGI, localized interface areas containing Mg, O, and occasionally Si were observed, particularly after testing in the Ar + 5 wt% H2 atmosphere. These areas were generally thin and discontinuous, and no evidence of new phases was found. The presence of isolated Mg crystallites on the LGI surface was attributed to mechanical deposition or condensation of Mg during cooling.

本研究的重点是纯液态Mg在三种不同类型的铸铁基体(具有不同形貌、数量和石墨相分布的Fe-C合金)上的高温行为。实验在715°C的等温条件下,在两种不同的流动气体气氛中(i)纯Ar和(ii) Ar和5 wt% H2的混合物中使用固定式滴法进行。试验采用非接触加热两种不同材料,并在实验室内直接在测试温度下从天然氧化膜中毛细管提纯Mg滴,方法是通过挤压放置在铸铁基体上方的石墨毛细管中的滴。利用高速CCD相机记录了Mg/衬底耦合的高温行为,并利用采集的图像测量了液态Mg与选定衬底之间形成的接触角值(θ)。利用扫描电子显微镜(SEM)和能谱仪(EDS)对凝固后的Mg/基体进行了详细的微观结构观察。所得结果表明,Mg的润湿行为因铸铁类型和试验气氛的不同而有显著差异。在所有情况下,在纯Ar中观察到非润湿行为(θ > 90°),而氢的加入导致接触角值降低,特别是对于球墨铁(SGI),其值降低到90°以下,通常被认为是润湿行为。相比之下,在本研究中使用的两种气氛下,层状石墨铁(LGI)保持不可润湿性,尽管在含氢气氛中与纯氩相比,接触角减小(Δθ ~ 27°)。致密石墨铁(CGI)在两种气氛下也表现出不可润湿性;而在Ar + 5 wt% H2气氛中,接触角接近90°。SEM/EDS分析表明,Mg/铸铁基体凝固后的横截面形貌存在细微差异。对于SGI和CGI,观察到含有Mg、O和偶尔含有Si的局部界面区域,特别是在Ar + 5 wt% H2气氛中测试后。这些区域通常很薄,不连续,没有发现新阶段的证据。在LGI表面存在分离的Mg晶体,这是由于Mg在冷却过程中的机械沉积或冷凝所致。
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引用次数: 0
Ambient-cured alkali-activated geopolymer mortars: influence of activator molarity and fly ash replacement on microstructure and mechanical performance 环境固化碱活化地聚合物砂浆:活化剂摩尔浓度和粉煤灰用量对其微观结构和力学性能的影响
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2026-01-12 DOI: 10.1007/s43452-025-01404-2
Kenan Toklu, Buğra Aydın, İlhami Demir, Şükrü Demir, Gazi Günel, Özer Sevim

This study investigates the mechanical and microstructural behavior of ambient-cured geopolymer mortars synthesized with ground granulated blast furnace slag (GBFS) and Class F fly ash (FA) as binder materials. Sodium hydroxide (NaOH) solutions at molarities of 4 M, 6 M, and 8 M were used as alkali activators, while GBFS was partially replaced with FA at ratios ranging from 0% to 25% by weight. The fresh and hardened properties of the mortars were evaluated through flow table tests, flexural and compressive strength measurements, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), and mercury intrusion porosimetry (MIP). Results indicated that higher activator molarity significantly enhanced both the flexural and compressive strengths, while increased FA content improved workability but adversely affected strength. Microstructural analyses revealed that greater FA replacement led to more microcracks and higher porosity, contributing to reduced mechanical performance. The formation of C-A-S-H and N-A-S-H gels was observed to be critical for strength development. The findings suggest that optimizing activator molarity and binder composition is essential for achieving durable, environmentally friendly geopolymer mortars under ambient curing conditions. Unlike most existing studies relying on elevated-temperature curing, this study offers a detailed analysis of ambient-cured systems using only industrial by-products, thus providing a novel framework for low-energy geopolymer mortar production suitable for real-world applications.

研究了以磨碎的粒状高炉矿渣(GBFS)和F级粉煤灰(FA)为粘结剂合成的环境固化地聚合物砂浆的力学和微观结构行为。使用4、6、8 M摩尔浓度的氢氧化钠(NaOH)溶液作为碱活化剂,部分用FA代替GBFS,比例为0% ~ 25%。通过流动表测试、弯曲和抗压强度测量、扫描电子显微镜(SEM)、能量色散x射线光谱(EDX)和汞侵入孔隙度测定(MIP)来评估砂浆的新鲜和硬化性能。结果表明,较高的活化剂摩尔浓度可显著提高材料的抗折强度和抗压强度,而增加FA含量可提高材料的和易性,但对强度有不利影响。微观结构分析表明,FA含量越高,微裂纹越多,孔隙率越高,力学性能越差。C-A-S-H和N-A-S-H凝胶的形成对强度的发展至关重要。研究结果表明,优化活化剂的摩尔浓度和粘结剂的组成对于在环境养护条件下获得耐用、环保的地聚合物砂浆至关重要。与大多数依赖于高温固化的现有研究不同,本研究提供了仅使用工业副产品的环境固化系统的详细分析,从而为适合实际应用的低能耗地聚合物砂浆生产提供了新的框架。
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引用次数: 0
Optimizing FAST/SPS parameters for ultra-high SiC content Al–SiC composites: thermal performance and microstructural insights 优化超高SiC含量Al-SiC复合材料的FAST/SPS参数:热性能和微观结构见解
IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL Pub Date : 2026-01-12 DOI: 10.1007/s43452-025-01408-y
Anna Wąsik, Marcin Madej, Rafał Rubach, Agata Strojny-Nędza, Marcin Chmielewski, Dariusz Garbiec, Beata Leszczyńska-Madej

This study explores the influence of SiC weight fraction and Field-Assisted Sintering Technology/Spark Plasma Sintering (FAST/SPS) parameters on the microstructure and thermal performance of Al–SiC composites. Composites containing 70 wt% and 90 wt% SiC were consolidated at temperatures ranging from 600 °C to 2150 °C, under compaction pressures of 80–100 MPa and heating rates between 25 and 100 °C/min. X-ray diffraction revealed the presence of Al, SiC, Al₂O₃, and secondary phases such as Al₄C₃ and Si. The highest relative density (98.65%) was achieved in the 90 wt% SiC sample sintered at 2100 °C under 100 MPa. Microstructure analysis showed a heterogeneous microstructure with residual porosity. Thermal characterization indicated that increasing density improved thermal conductivity and specific heat capacity, while the coefficient of thermal expansion (CTE) decreased with increasing SiC content. The results demonstrate that precise control of FAST/SPS parameters enables optimization of densification and thermal properties in Al–SiC composites for potential use in high-performance structural applications.

本研究探讨了SiC重量分数和场辅助烧结技术/火花等离子烧结(FAST/SPS)参数对Al-SiC复合材料微观结构和热性能的影响。SiC含量为70% wt%和90% wt%的复合材料在温度为600°C至2150°C,压实压力为80-100 MPa,加热速率为25至100°C/min的条件下进行固结。x射线衍射显示了Al, SiC, Al₂O₃和Al₄C₃和Si等二次相的存在。在2100℃、100 MPa下烧结的90% SiC样品的相对密度最高(98.65%)。显微组织分析表明,该合金为非均质显微组织,存在残余孔隙。热特性分析表明,随着SiC含量的增加,材料的导热系数和比热容有所提高,而热膨胀系数(CTE)则随SiC含量的增加而降低。结果表明,精确控制FAST/SPS参数可以优化Al-SiC复合材料的致密化和热性能,从而在高性能结构应用中具有潜在的应用前景。
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引用次数: 0
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Archives of Civil and Mechanical Engineering
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