首页 > 最新文献

Journal of Adhesive Dentistry最新文献

英文 中文
24-Month Clinical Performance of a Universal Adhesive on Non-Carious Cervical Lesions: Self-Etch and Etch-and-Rinse Techniques. 一种通用黏合剂治疗宫颈非龋齿病变的24个月临床表现:自蚀刻和蚀刻-冲洗技术。
IF 3.3 3区 医学 Q1 Dentistry Pub Date : 2021-10-01 DOI: 10.3290/j.jad.b2000173
Joana Cruz, Ana Luisa Silva, Raquel Eira, Catarina Coito, Bernardo Romão Sousa, Maria Manuela Lopes, Alexandre Cavalheiro

Purpose: To evaluate the 24-month clinical performance of Adhese Universal (ADH) (Ivoclar Vivadent) using two different application modes (etch-and-rinse vs self-etch) when restoring non-carious cervical lesions.

Materials and methods: Twenty-six patients participated in this study. A total of 117 non-carious cervical lesion restorations (N = 117) were assigned to two groups: 1) ADH in the etch-and-rinse mode (n = 59) and 2) ADH in the self-etch mode (n = 58). The same resin composite (Tetric EvoCeram, Ivoclar Vivadent) was used for all restorations. The restorations were evaluated at baseline and at 24 months using the World Dental Federation (FDI) criteria. The results were analyzed statistically using the McNemar test (α = 0.05) and a generalized estimating equation.

Results: In self-etch mode, significant differences were found for marginal coloring (p = 0.002), marginal adaptation (p = 0.031), and hypersensitivity (p = 0.031) between baseline and the end of the 24-month period. In the etch-and-rinse mode, significant differences were found for marginal coloring (p = 0.004), fractures/retention (p = 0.002), marginal adaptation (p = 0.002), and hypersensitivity (p = 0.000). Significant differences were also detected between groups at 24 months for fractures/retention (p = 0.001). At 24 months, 10 restorations of the etch-and-rinse group were lost and 2 restorations of the self-etch group were lost.

Conclusion: In terms of fractures and retention criteria, this universal adhesive obtained better results when applied in self-etch mode than in etch-and-rinse mode.

目的:评价Adhese Universal (ADH) (Ivoclar Vivadent)采用两种不同的应用模式(蚀刻冲洗与自蚀刻)修复宫颈非龋齿病变24个月的临床表现。材料与方法:26例患者参与本研究。117例非龋齿宫颈病变修复体(N = 117)分为两组:1)蚀刻冲洗模式ADH (N = 59)和2)自蚀刻模式ADH (N = 58)。所有修复体均使用相同的树脂复合材料(Tetric EvoCeram, Ivoclar Vivadent)。根据世界牙科联合会(FDI)的标准在基线和24个月时对修复体进行评估。采用McNemar检验(α = 0.05)和广义估计方程对结果进行统计学分析。结果:在自蚀刻模式下,在基线和24个月结束时,边缘着色(p = 0.002)、边缘适应(p = 0.031)和超敏(p = 0.031)方面存在显著差异。在蚀刻-冲洗模式下,在边缘着色(p = 0.004)、骨折/固位(p = 0.002)、边缘适应(p = 0.002)和超敏(p = 0.000)方面发现了显著差异。两组在24个月时骨折/潴留的发生率也有显著差异(p = 0.001)。24个月时,蚀刻冲洗组丢失10个修复体,自蚀刻组丢失2个修复体。结论:就骨折和固位标准而言,该通用胶粘剂在自蚀刻模式下比在蚀刻-冲洗模式下应用效果更好。
{"title":"24-Month Clinical Performance of a Universal Adhesive on Non-Carious Cervical Lesions: Self-Etch and Etch-and-Rinse Techniques.","authors":"Joana Cruz,&nbsp;Ana Luisa Silva,&nbsp;Raquel Eira,&nbsp;Catarina Coito,&nbsp;Bernardo Romão Sousa,&nbsp;Maria Manuela Lopes,&nbsp;Alexandre Cavalheiro","doi":"10.3290/j.jad.b2000173","DOIUrl":"https://doi.org/10.3290/j.jad.b2000173","url":null,"abstract":"<p><strong>Purpose: </strong>To evaluate the 24-month clinical performance of Adhese Universal (ADH) (Ivoclar Vivadent) using two different application modes (etch-and-rinse vs self-etch) when restoring non-carious cervical lesions.</p><p><strong>Materials and methods: </strong>Twenty-six patients participated in this study. A total of 117 non-carious cervical lesion restorations (N = 117) were assigned to two groups: 1) ADH in the etch-and-rinse mode (n = 59) and 2) ADH in the self-etch mode (n = 58). The same resin composite (Tetric EvoCeram, Ivoclar Vivadent) was used for all restorations. The restorations were evaluated at baseline and at 24 months using the World Dental Federation (FDI) criteria. The results were analyzed statistically using the McNemar test (α = 0.05) and a generalized estimating equation.</p><p><strong>Results: </strong>In self-etch mode, significant differences were found for marginal coloring (p = 0.002), marginal adaptation (p = 0.031), and hypersensitivity (p = 0.031) between baseline and the end of the 24-month period. In the etch-and-rinse mode, significant differences were found for marginal coloring (p = 0.004), fractures/retention (p = 0.002), marginal adaptation (p = 0.002), and hypersensitivity (p = 0.000). Significant differences were also detected between groups at 24 months for fractures/retention (p = 0.001). At 24 months, 10 restorations of the etch-and-rinse group were lost and 2 restorations of the self-etch group were lost.</p><p><strong>Conclusion: </strong>In terms of fractures and retention criteria, this universal adhesive obtained better results when applied in self-etch mode than in etch-and-rinse mode.</p>","PeriodicalId":55604,"journal":{"name":"Journal of Adhesive Dentistry","volume":null,"pages":null},"PeriodicalIF":3.3,"publicationDate":"2021-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39438179","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
Influence of Different Application Methods on the Bonding Effectiveness of Universal Adhesives to Dentin in the Early Phase. 不同应用方法对Dentin早期通用胶粘剂粘接效果的影响。
IF 3.3 3区 医学 Q1 Dentistry Pub Date : 2021-10-01 DOI: 10.3290/j.jad.b2000257
Munenori Yokoyama, Toshiki Takamizawa, Tomohiko Tamura, Yoshihiro Namura, Akimasa Tsujimoto, Wayne W Barkmeier, Mark A Latta, Masashi Miyazaki

Purpose: To investigate the changes in the dentin bond strengths of universal adhesives during the early phase and evaluate the effect of a double-layer adhesive application on the performance of the dentin bond.

Materials and methods: Three universal adhesives and a two-step self-etch adhesive were employed to ascertain the shear bond strengths (SBS) of specimens to bovine dentin with the use of the etch-and-rinse or self-etch mode. The specimens were further divided into two groups based on adhesive application in a single or a double layer. The bonded specimens were stored in distilled water at 37°C for 5 min or 1, 6, 12, or 24 h prior to SBS measurement and the adhesives' Knoop hardness number (KHN).

Results: All the adhesives showed increased SBS with prolonged storage periods regardless of the adhesive layer (single or double) or etching mode. Most universal adhesives in the double adhesive layer groups showed significantly higher SBS than single adhesive layer groups for the same storage period. All the adhesives also showed increased KHN with increased storage period.

Conclusion: The SBS and KHN values of the adhesives increased with increasing storage duration over a 24-h period. Double adhesive layer application mediated increased dentin bond strength in the early phase.

目的:探讨通用胶粘剂早期牙本质粘结强度的变化,并评价双层adhesive应用on对牙本质粘结性能的影响。材料和方法:采用三种通用胶粘剂和一种两步自蚀刻胶粘剂,采用蚀刻-冲洗或自蚀刻方式测定试样与牛牙本质的剪切粘接强度(SBS)。根据adhesive应用[in]将样品进一步分为单层或双层两组。粘合后的样品在37°C的蒸馏水中保存5分钟或1、6、12或24小时,然后SBS测量and胶粘剂的努氏硬度值(KHN)。结果:所有胶粘剂的SBS均增加with,无论胶粘剂单层或双层或蚀刻方式均延长了储存时间。双胶层组中大多数通用胶粘剂的SBS均显著高于than单胶粘剂组for。所有胶粘剂also的KHN均随贮存时间的延长而增加。结论:increasing储存时间≥24h时,黏合剂的SBS和KHN值≥increased。双胶层应用mediated增加了the前期牙本质结合强度。
{"title":"Influence of Different Application Methods on the Bonding Effectiveness of Universal Adhesives to Dentin in the Early Phase.","authors":"Munenori Yokoyama,&nbsp;Toshiki Takamizawa,&nbsp;Tomohiko Tamura,&nbsp;Yoshihiro Namura,&nbsp;Akimasa Tsujimoto,&nbsp;Wayne W Barkmeier,&nbsp;Mark A Latta,&nbsp;Masashi Miyazaki","doi":"10.3290/j.jad.b2000257","DOIUrl":"https://doi.org/10.3290/j.jad.b2000257","url":null,"abstract":"<p><strong>Purpose: </strong>To investigate the changes in the dentin bond strengths of universal adhesives during the early phase and evaluate the effect of a double-layer adhesive application on the performance of the dentin bond.</p><p><strong>Materials and methods: </strong>Three universal adhesives and a two-step self-etch adhesive were employed to ascertain the shear bond strengths (SBS) of specimens to bovine dentin with the use of the etch-and-rinse or self-etch mode. The specimens were further divided into two groups based on adhesive application in a single or a double layer. The bonded specimens were stored in distilled water at 37°C for 5 min or 1, 6, 12, or 24 h prior to SBS measurement and the adhesives' Knoop hardness number (KHN).</p><p><strong>Results: </strong>All the adhesives showed increased SBS with prolonged storage periods regardless of the adhesive layer (single or double) or etching mode. Most universal adhesives in the double adhesive layer groups showed significantly higher SBS than single adhesive layer groups for the same storage period. All the adhesives also showed increased KHN with increased storage period.</p><p><strong>Conclusion: </strong>The SBS and KHN values of the adhesives increased with increasing storage duration over a 24-h period. Double adhesive layer application mediated increased dentin bond strength in the early phase.</p>","PeriodicalId":55604,"journal":{"name":"Journal of Adhesive Dentistry","volume":null,"pages":null},"PeriodicalIF":3.3,"publicationDate":"2021-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39440590","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 9
Bulk-fill Composites Compared to a Nanohybrid Composite in Class-II Cavities - A Two-year Follow-Up Study. 体填充复合材料与纳米复合材料在ii类空腔中的比较——一项为期两年的随访研究。
IF 3.3 3区 医学 Q1 Dentistry Pub Date : 2021-10-01 DOI: 10.3290/j.jad.b2000185
Lea Hoffmann, Cornelia Neuerer, Katrin Heck, Karl-Heinz Kunzelmann

Purpose: To compare different concepts of direct composite restorations in class-II cavities using bulk-fill composites and a conventional composite with different layer thicknesses in a clinical study over a period of 2 years.

Materials and methods: A low-viscosity (SDR), a high-viscosity bulk-fill (Tetric EvoCeram Bulk Fill) and a conventional nanohybrid composite (Tetric EvoCeram) were randomly assigned and placed in different layer thicknesses up to 4 mm in 160 class-II cavities in 94 patients. Restorations were clinically examined at baseline (n = 160), after 12 (n = 150) and 24 months (n = 148) and evaluated according to eight selected FDI criteria. In case of complete loss of the restoration or irreversible pulpitic symptoms, the restoration was rated as failure; repair was considered as relative failure.

Results: The materials investigated showed no significant differences regarding the FDI scores and failure rate during the entire follow-up. After 12 months, 7 failures and after 24 months a total of 8 failures were observed. After 2 years, Tetric EvoCeram Bulk Fill with a 4-mm layer thickness and SDR in combination with Tetric EvoCeram Bulk Fill with a 2-mm layer thickness exhibited a non-significant tendency towards increased hypersensitivity (FDI score 5) as compared to the reference material Tetric EvoCeram with a 2-mm layer thickness (p = 0.051; Kruskal-Wallis test).

Conclusion: The clinical stability of bulk-fill materials in layers up to 4 mm is comparable to nanohybrid composites after 2 years.

目的:在一项为期2年的临床研究中,比较不同概念的ii类直接复合材料cavities使用块体填充复合材料和不同层厚的常规复合材料。材料和方法:将低粘度(SDR)、高粘度填充材料(Tetric EvoCeram Bulk Fill)和传统的纳米混合复合材料(Tetric EvoCeram)随机分配到94例患者的160个ii类腔中,并将其放置在不同厚度的层中,厚度可达4mm。在基线(n = 160)、12个月(n = 150)和24个月(n = 148)后对修复体进行临床检查,并根据8个选定的FDI标准进行评估。如果修复体完全丧失或出现不可逆的牙髓炎症状,则判定修复失败;修复被认为是相对失败。结果:调查资料显示,在整个随访期间,FDI得分和失败率无显著差异。12个月后观察到7例失败,24个月后观察到8例失败。2年后,与标准材料2毫米厚度的Tetric EvoCeram相比,层厚为4毫米的Tetric EvoCeram Bulk Fill和SDR结合层厚为2毫米的Tetric EvoCeram Bulk Fill表现出不显著的超敏性增加趋势(FDI得分5)(p = 0.051;克鲁斯卡尔-沃利斯测试)。结论:厚度达4 mm的块状填充材料的临床稳定性与纳米杂化复合材料相当。
{"title":"Bulk-fill Composites Compared to a Nanohybrid Composite in Class-II Cavities - A Two-year Follow-Up Study.","authors":"Lea Hoffmann,&nbsp;Cornelia Neuerer,&nbsp;Katrin Heck,&nbsp;Karl-Heinz Kunzelmann","doi":"10.3290/j.jad.b2000185","DOIUrl":"https://doi.org/10.3290/j.jad.b2000185","url":null,"abstract":"<p><strong>Purpose: </strong>To compare different concepts of direct composite restorations in class-II cavities using bulk-fill composites and a conventional composite with different layer thicknesses in a clinical study over a period of 2 years.</p><p><strong>Materials and methods: </strong>A low-viscosity (SDR), a high-viscosity bulk-fill (Tetric EvoCeram Bulk Fill) and a conventional nanohybrid composite (Tetric EvoCeram) were randomly assigned and placed in different layer thicknesses up to 4 mm in 160 class-II cavities in 94 patients. Restorations were clinically examined at baseline (n = 160), after 12 (n = 150) and 24 months (n = 148) and evaluated according to eight selected FDI criteria. In case of complete loss of the restoration or irreversible pulpitic symptoms, the restoration was rated as failure; repair was considered as relative failure.</p><p><strong>Results: </strong>The materials investigated showed no significant differences regarding the FDI scores and failure rate during the entire follow-up. After 12 months, 7 failures and after 24 months a total of 8 failures were observed. After 2 years, Tetric EvoCeram Bulk Fill with a 4-mm layer thickness and SDR in combination with Tetric EvoCeram Bulk Fill with a 2-mm layer thickness exhibited a non-significant tendency towards increased hypersensitivity (FDI score 5) as compared to the reference material Tetric EvoCeram with a 2-mm layer thickness (p = 0.051; Kruskal-Wallis test).</p><p><strong>Conclusion: </strong>The clinical stability of bulk-fill materials in layers up to 4 mm is comparable to nanohybrid composites after 2 years.</p>","PeriodicalId":55604,"journal":{"name":"Journal of Adhesive Dentistry","volume":null,"pages":null},"PeriodicalIF":3.3,"publicationDate":"2021-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39438180","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Microtensile Bond Strength, Bonding Interface Morphology, Adhesive Resin Infiltration, and Marginal Adaptation of Bulk-fill Composites Placed Using Different Adhesives. 微拉伸键合强度,键合界面形态,胶粘剂树脂渗透性和填充复合材料的边际适应性Using不同胶粘剂。
IF 3.3 3区 医学 Q1 Dentistry Pub Date : 2021-10-01 DOI: 10.3290/j.jad.b2000221
Maicon Sebold, Rodrigo Barros Esteves Lins, Beatriz Ometto Sahadi, Marina Rodrigues Santi, Luís Roberto Marcondes Martins, Marcelo Giannini

Purpose: This study evaluated dentin bond strength, failure mode, interface morphology, adhesive infiltration into dentin, and marginal adaptation of bulk-fill composites used with different adhesives.

Materials and methods: Third molars received occlusal class I cavities (4 mm x 4 mm x 4 mm) that were bulk-filled with Admira Fusion x-tra (Voco) or SonicFill 2 (Kerr) using four adhesives (Scotchbond Multipurpose, 3M Oral Care; Clearfil SE Bond, Kuraray Noritake; OptiBond All-In-One, Kerr; Futurabond U, Voco). Scotchbond was used with acid-etching, while the remaining adhesives were applied in self-etch mode. Sixty-four teeth were selected for the microtensile bond strength test (n = 8). Failure modes were analyzed with scanning electron microscopy (SEM). Interface morphology and adhesive infiltration (n = 3) were investigated using confocal laser scanning microscopy (CLSM). Marginal adaptation (n = 3) was also evaluated using SEM. Bond strength, failure mode, and adhesive infiltration data were analyzed for distribution and homocedasticity, followed by appropriate statistical analyses (α = 0.05).

Results: Regarding bond strength, no differences were found among adhesives for SonicFill; Clearfil showed a significantly lower mean value than did Scotchbond (p ≤ 0.05) for Admira; the two composites did not differ. Adhesive and mixed failures were observed for all groups. Scotchbond led to thicker hybrid layers with deeper adhesive infiltration as opposed to Futurabond. The groups Admira+Futurabond, SonicFill+Clearfil, and SonicFill+Futurabond presented the highest marginal discontinuity.

Conclusion: The tested bulk-fill composites did not affect dentin bonding. Scotchbond and Clearfil seem to be reliable for bonding SonicFill 2 to dentin. The performance of Futurabond was questionable, given its poor-quality interface and higher percentages of marginal gaps.

目的:研究不同粘接剂对填充型复合材料的粘结强度、破坏模式、界面形态、粘接剂对牙本质的渗透及边际适应性。材料和方法:第三磨牙接受I类牙合腔(4mm x 4mm x 4mm),用Admira Fusion x-tra (Voco)或SonicFill 2 (Kerr)填充,使用四种粘合剂(Scotchbond Multipurpose, 3M Oral Care;Clearfil SE Bond, Kuraray Noritake;OptiBond All-In-One, Kerr;未来之路,未来之路。Scotchbond采用酸蚀方式,其余胶粘剂采用自蚀方式。选择64颗牙进行微拉伸粘结强度试验(n = 8),用扫描电镜(SEM)分析失效模式。用共聚焦激光扫描显微镜(CLSM)观察界面形貌和黏合剂的浸润情况(n = 3)。边际适应(n = 3)也使用扫描电镜进行评估。分析黏结强度、破坏模式和黏着物浸润数据的分布和均方差,并进行相应的统计分析(α = 0.05)。结果:不同粘结剂在粘结强度方面无差异;Clearfil的平均值显著低于Scotchbond (p≤0.05);这两种复合物没有差别。所有组均观察到粘接失败和混合失败。与Futurabond相反,Scotchbond导致更厚的杂化层和更深的粘合剂渗透。Admira+Futurabond、SonicFill+Clearfil和SonicFill+Futurabond组的边缘不连续程度最高。结论:块状填充复合材料对牙本质粘结无明显影响。Scotchbond和Clearfil似乎是可靠的粘合SonicFill 2牙本质。The Futurabond的性能was值得怀疑,因为它的界面质量差,边际差距的百分比更高。
{"title":"Microtensile Bond Strength, Bonding Interface Morphology, Adhesive Resin Infiltration, and Marginal Adaptation of Bulk-fill Composites Placed Using Different Adhesives.","authors":"Maicon Sebold,&nbsp;Rodrigo Barros Esteves Lins,&nbsp;Beatriz Ometto Sahadi,&nbsp;Marina Rodrigues Santi,&nbsp;Luís Roberto Marcondes Martins,&nbsp;Marcelo Giannini","doi":"10.3290/j.jad.b2000221","DOIUrl":"https://doi.org/10.3290/j.jad.b2000221","url":null,"abstract":"<p><strong>Purpose: </strong>This study evaluated dentin bond strength, failure mode, interface morphology, adhesive infiltration into dentin, and marginal adaptation of bulk-fill composites used with different adhesives.</p><p><strong>Materials and methods: </strong>Third molars received occlusal class I cavities (4 mm x 4 mm x 4 mm) that were bulk-filled with Admira Fusion x-tra (Voco) or SonicFill 2 (Kerr) using four adhesives (Scotchbond Multipurpose, 3M Oral Care; Clearfil SE Bond, Kuraray Noritake; OptiBond All-In-One, Kerr; Futurabond U, Voco). Scotchbond was used with acid-etching, while the remaining adhesives were applied in self-etch mode. Sixty-four teeth were selected for the microtensile bond strength test (n = 8). Failure modes were analyzed with scanning electron microscopy (SEM). Interface morphology and adhesive infiltration (n = 3) were investigated using confocal laser scanning microscopy (CLSM). Marginal adaptation (n = 3) was also evaluated using SEM. Bond strength, failure mode, and adhesive infiltration data were analyzed for distribution and homocedasticity, followed by appropriate statistical analyses (α = 0.05).</p><p><strong>Results: </strong>Regarding bond strength, no differences were found among adhesives for SonicFill; Clearfil showed a significantly lower mean value than did Scotchbond (p ≤ 0.05) for Admira; the two composites did not differ. Adhesive and mixed failures were observed for all groups. Scotchbond led to thicker hybrid layers with deeper adhesive infiltration as opposed to Futurabond. The groups Admira+Futurabond, SonicFill+Clearfil, and SonicFill+Futurabond presented the highest marginal discontinuity.</p><p><strong>Conclusion: </strong>The tested bulk-fill composites did not affect dentin bonding. Scotchbond and Clearfil seem to be reliable for bonding SonicFill 2 to dentin. The performance of Futurabond was questionable, given its poor-quality interface and higher percentages of marginal gaps.</p>","PeriodicalId":55604,"journal":{"name":"Journal of Adhesive Dentistry","volume":null,"pages":null},"PeriodicalIF":3.3,"publicationDate":"2021-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39438182","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Influence of Curing Mode and Layering Technique on the 3D Interfacial Gap of Bulk-fill Resin Composites in Deep Class-I Restorations: A Micro-CT Volumetric Study. 固化方式和分层技术对深度i类修复体填充树脂复合材料三维界面间隙的影响:微ct体积研究。
IF 3.3 3区 医学 Q1 Dentistry Pub Date : 2021-10-01 DOI: 10.3290/j.jad.b2000229
Allegra Comba, Andrea Baldi, Riccardo Michelotto Tempesta, Edoardo Alberto Vergano, Mario Alovisi, Damiano Pasqualini, Nicola Scotti

Purpose: To three-dimensionally evaluate the interfacial gap of bulk-fill resin composites applied in deep Class-I restorations with different layering techniques and curing modes.

Materials and methods: Ninety-six (n = 96) samples were prepared with standardized deep Class-I cavities and adhesive procedures. Four materials were tested: SDR (SDR), SonicFill2 (SF), Admira Fusion X-Tra (AFXT), Filtek Supreme XTE (FS). Four subgroups (n = 6) were created according to layering and curing techniques: 2+2mm increments with soft start curing (SG1), 2+2 mm with conventional curing (SG2), a 4-mm increment with soft start curing (SG3), a 4-mm increment with conventional curing (SG4). All samples underwent micro-CT scans; afterwards, voids surrounding the restorations automatically underwent a thresholding procedure (Mimics, Materialise; Geomagic Studio 12, 3D Systems) to analyze the 3D interfacial gap. Statistical analysis was performed using three-way ANOVA with Tukey's test (significance p < 0.05).

Results: Statistically significant differences were reported between materials, layering techniques and their interaction. No statistically significant differences were reported for polymerisation mode. Bulk-fill materials showed average interfacial gap volumes ranging from 0.031 mm3 to 0.200 mm3, while FS showed volumes ranging from 0.416 mm3 to 1200 mm3.

Conclusions: All bulk-fill materials performed statistically significantly better than did FS (p < 0.05), with no statistically significant differences between them. Curing mode did not influence interfacial gap volume in any group (p > 0.05), while bulk-filling vs layering influenced the volume of interfacial gaps only in the FS group, which performied better when incrementally applied. Regarding gap localisation, the floor of the cavity was the area with the highest likelihood of gaps in all samples.

目的:对不同铺层工艺和固化方式的体块填充树脂复合材料在ⅰ类深度修复体中的界面间隙进行三维评价。材料和方法:96个样品(n = 96)采用标准化的Class-I深腔和粘接程序制备。测试了四种材料:SDR (SDR)、SonicFill2 (SF)、Admira Fusion X-Tra (AFXT)、Filtek Supreme XTE (FS)。根据分层和固化技术创建了四个亚组(n = 6):软启动固化增量2+2mm (SG1),常规固化增量2+2mm (SG2),软启动固化增量4 mm (SG3),常规固化增量4 mm (SG4)。所有样本都进行了显微ct扫描;之后,修复体周围的空隙自动进行阈值处理(Mimics, Materialise;Geomagic Studio 12 (3D Systems)来分析三维界面间隙。统计学分析采用三向方差分析,采用Tukey检验(p < 0.05)。结果:材料、分层技术及其相互作用之间的差异有统计学意义。聚合方式的差异无统计学意义。块体填充材料的平均界面间隙体积在0.031 ~ 0.200 mm3之间,FS的平均界面间隙体积在0.416 ~ 1200 mm3之间。结论:所有体块填充材料的性能均优于FS (p < 0.05),两者之间无统计学差异。固化方式对两组的界面间隙体积均无影响(p > 0.05),而填充与分层只对FS组的界面间隙体积有影响,且FS组的效果更好。关于缝隙定位,空腔的地板是所有样品中缝隙可能性最高的区域。
{"title":"Influence of Curing Mode and Layering Technique on the 3D Interfacial Gap of Bulk-fill Resin Composites in Deep Class-I Restorations: A Micro-CT Volumetric Study.","authors":"Allegra Comba,&nbsp;Andrea Baldi,&nbsp;Riccardo Michelotto Tempesta,&nbsp;Edoardo Alberto Vergano,&nbsp;Mario Alovisi,&nbsp;Damiano Pasqualini,&nbsp;Nicola Scotti","doi":"10.3290/j.jad.b2000229","DOIUrl":"https://doi.org/10.3290/j.jad.b2000229","url":null,"abstract":"<p><strong>Purpose: </strong>To three-dimensionally evaluate the interfacial gap of bulk-fill resin composites applied in deep Class-I restorations with different layering techniques and curing modes.</p><p><strong>Materials and methods: </strong>Ninety-six (n = 96) samples were prepared with standardized deep Class-I cavities and adhesive procedures. Four materials were tested: SDR (SDR), SonicFill2 (SF), Admira Fusion X-Tra (AFXT), Filtek Supreme XTE (FS). Four subgroups (n = 6) were created according to layering and curing techniques: 2+2mm increments with soft start curing (SG1), 2+2 mm with conventional curing (SG2), a 4-mm increment with soft start curing (SG3), a 4-mm increment with conventional curing (SG4). All samples underwent micro-CT scans; afterwards, voids surrounding the restorations automatically underwent a thresholding procedure (Mimics, Materialise; Geomagic Studio 12, 3D Systems) to analyze the 3D interfacial gap. Statistical analysis was performed using three-way ANOVA with Tukey's test (significance p < 0.05).</p><p><strong>Results: </strong>Statistically significant differences were reported between materials, layering techniques and their interaction. No statistically significant differences were reported for polymerisation mode. Bulk-fill materials showed average interfacial gap volumes ranging from 0.031 mm3 to 0.200 mm3, while FS showed volumes ranging from 0.416 mm3 to 1200 mm3.</p><p><strong>Conclusions: </strong>All bulk-fill materials performed statistically significantly better than did FS (p < 0.05), with no statistically significant differences between them. Curing mode did not influence interfacial gap volume in any group (p > 0.05), while bulk-filling vs layering influenced the volume of interfacial gaps only in the FS group, which performied better when incrementally applied. Regarding gap localisation, the floor of the cavity was the area with the highest likelihood of gaps in all samples.</p>","PeriodicalId":55604,"journal":{"name":"Journal of Adhesive Dentistry","volume":null,"pages":null},"PeriodicalIF":3.3,"publicationDate":"2021-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39438183","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
Editorial: Universal adhesives - to etch or not to etch? 社论:通用粘合剂——蚀刻还是不蚀刻?
IF 3.3 3区 医学 Q1 Dentistry Pub Date : 2021-07-23 DOI: 10.3290/j.jad.b1764779
Lorenzo Breschi, Bart Van Meerbeek
{"title":"Editorial: Universal adhesives - to etch or not to etch?","authors":"Lorenzo Breschi,&nbsp;Bart Van Meerbeek","doi":"10.3290/j.jad.b1764779","DOIUrl":"https://doi.org/10.3290/j.jad.b1764779","url":null,"abstract":"","PeriodicalId":55604,"journal":{"name":"Journal of Adhesive Dentistry","volume":null,"pages":null},"PeriodicalIF":3.3,"publicationDate":"2021-07-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39190048","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Consideration of Dental Tissues and Composite Mechanical Properties in Secondary Caries Development: A Critical Review. 牙齿组织和复合力学性能的考虑in继发性龋齿的发展:一个重要的回顾。
IF 3.3 3区 医学 Q1 Dentistry Pub Date : 2021-07-23 DOI: 10.3290/j.jad.b1649941
Rémy Gauthier, Hazem Aboulleil, Jean-Marc Chenal, Jérôme Chevalier, Pierre Colon, Brigitte Grosgogeat

Different kinds of interactions between the restorative material and mineralized dental tissues result in secondary caries around dental composites. Of these, the mechanical interactions have to be carefully investigated. Due to the elastic mismatch between dental tissues and the composite restoration, complex stresses and strains develop at their interface. This complex mechanical environment disturbs the demineralization-remineralization equilibrium of dental hard tissues. The fluid flow both over and within enamel and dentin, associated with their complex ultrastructure and mechanical behavior, is a key factor. It is known that external mechanical loading can indirectly promote the dissolution of enamel and dentin through a pumping action of cariogenic fluids in and out of microgaps at the interface between mineralized tissues and composite. Mechanical loading can also directly influence the physicochemical behavior of dental hard tissues by inducing complex strain and stress fields on the crystal scale. It is important to consider both the direct and indirect paths by which mechanical loading can influence the apatite dissolution kinetics. Therefore, a systematic approach should be used to investigate the mechanism of secondary caries formation considering the tooth-composite interface as a unique complex in which each element has an influence on the other.

修复材料与矿化牙组织之间的不同种类的相互作用导致牙复合材料周围的继发性龋齿。其中,机械相互作用必须仔细研究。由于牙组织与复合修复体之间的弹性失配,在其界面处产生复杂的应力和应变。这种复杂的机械环境扰乱了牙齿硬组织的脱矿-再矿化equilibrium。牙釉质和牙本质表面和内部的流体流动,与它们复杂的超微结构和力学行为有关,是一个关键因素。众所周知,外部机械载荷可以间接促进牙釉质和牙本质的溶解,这是通过在矿化组织和复合材料界面的微间隙中泵送龋齿流体的作用来实现的。机械载荷还可以通过在晶体尺度上诱发复杂的应变和应力场,直接影响牙体硬组织的物理化学行为。考虑机械载荷影响磷灰石溶解动力学的直接和间接途径是很重要的。因此,考虑到牙齿-复合材料界面是一个独特的复合体,其中每个元素都对另一个元素有影响,应该使用systematic方法来研究次生龋形成的机制。
{"title":"Consideration of Dental Tissues and Composite Mechanical Properties in Secondary Caries Development: A Critical Review.","authors":"Rémy Gauthier,&nbsp;Hazem Aboulleil,&nbsp;Jean-Marc Chenal,&nbsp;Jérôme Chevalier,&nbsp;Pierre Colon,&nbsp;Brigitte Grosgogeat","doi":"10.3290/j.jad.b1649941","DOIUrl":"https://doi.org/10.3290/j.jad.b1649941","url":null,"abstract":"<p><p>Different kinds of interactions between the restorative material and mineralized dental tissues result in secondary caries around dental composites. Of these, the mechanical interactions have to be carefully investigated. Due to the elastic mismatch between dental tissues and the composite restoration, complex stresses and strains develop at their interface. This complex mechanical environment disturbs the demineralization-remineralization equilibrium of dental hard tissues. The fluid flow both over and within enamel and dentin, associated with their complex ultrastructure and mechanical behavior, is a key factor. It is known that external mechanical loading can indirectly promote the dissolution of enamel and dentin through a pumping action of cariogenic fluids in and out of microgaps at the interface between mineralized tissues and composite. Mechanical loading can also directly influence the physicochemical behavior of dental hard tissues by inducing complex strain and stress fields on the crystal scale. It is important to consider both the direct and indirect paths by which mechanical loading can influence the apatite dissolution kinetics. Therefore, a systematic approach should be used to investigate the mechanism of secondary caries formation considering the tooth-composite interface as a unique complex in which each element has an influence on the other.</p>","PeriodicalId":55604,"journal":{"name":"Journal of Adhesive Dentistry","volume":null,"pages":null},"PeriodicalIF":3.3,"publicationDate":"2021-07-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39190489","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
IAAD - The 4th Biennial Meeting of the International Academy for Adhesive Dentistry. IAAD -第四届两年一次的国际牙科粘接学会会议。
IF 3.3 3区 医学 Q1 Dentistry Pub Date : 2021-07-23
Marcelo Giannini
{"title":"IAAD - The 4th Biennial Meeting of the International Academy for Adhesive Dentistry.","authors":"Marcelo Giannini","doi":"","DOIUrl":"","url":null,"abstract":"","PeriodicalId":55604,"journal":{"name":"Journal of Adhesive Dentistry","volume":null,"pages":null},"PeriodicalIF":3.3,"publicationDate":"2021-07-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39190496","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The Effect of Deproteinizing Agents on Bond Strength of Resin-based Materials to Enamel: A Systematic Review and Meta-Analysis of In Vitro Studies. 脱蛋白剂对Resin-based材料与牙釉质结合强度的影响:体外研究的系统回顾和荟萃分析。
IF 3.3 3区 医学 Q1 Dentistry Pub Date : 2021-07-23 DOI: 10.3290/j.jad.b1649893
Miguel Ángel Fernández-Barrera, Adriana Fernandes da Silva, América Patricia Pontigo-Loyola, J Eliezer Zamarripa-Calderón, Evandro Piva, Carlos Enrique Cuevas-Suárez

Purpose: To systematically review the literature to evaluate whether the bond strength of resin-based materials to enamel is affected by deproteinizing agents.

Materials and methods: This systematic review and meta-analysis was conducted according to the PRISMA statement. PubMed, ISI Web of Science, Cochrane Library, SciELO, Scopus, LILACS, IBECS, and BVS databases were screened up to December 2020. Eligibility criteria included in vitro studies that reported the effect of a deproteinizing agent applied before or after acid etching on the immediate or long-term bond strength of resin-based materials to enamel. The meta-analysis was carried out using Review Manager (version 5.3.5). A global comparison was performed with the standardized mean difference based on random-effect models at a significance level of α = 0.05.

Results: A total of 23 studies were included in the meta-analysis. In all the studies, only the immediate bond strength was evaluated. The bond strength of the materials was improved by the application of NaOCl or papain prior to enamel etching with phosphoric acid (p ≤ 0.006). None of the deproteinizing agents had a significant effect when applied after etching with phosphoric acid (p ≥ 0.27).

Conclusions: Based on in vitro studies, deproteinization with sodium hypochlorite or papain-based agents increases the immediate bond strength of resin-based materials to enamel only when used prior to phosphoric-acid etching.

目的:系统回顾文献,评价脱蛋白剂是否影响树脂基材料与牙釉质的结合强度。材料和方法:本系统综述和荟萃分析按照PRISMA声明进行。PubMed、ISI Web of Science、Cochrane Library、SciELO、Scopus、LILACS、IBECS和BVS数据库的筛选截止到2020年12月。资格标准包括体外研究,这些研究报告了在酸蚀之前或之后应用脱蛋白剂对树脂基材料与牙釉质的即时或长期结合强度的影响。meta分析使用Review Manager(5.3.5版本)进行。采用基于随机效应模型的标准化均差进行全局比较,显著性水平为α = 0.05。结果:meta分析共纳入23项研究。在所有的研究中,只评估了直接粘结强度。磷酸刻蚀前应用NaOCl或木瓜蛋白酶可提高材料的结合强度(p≤0.006)。磷酸蚀刻后应用脱蛋白剂均无显著效果(p≥0.27)。结论:根据体外研究,只有在磷酸蚀刻之前使用次氯酸钠或木瓜蛋白酶脱蛋白才能增加树脂基材料与牙釉质的直接结合强度。
{"title":"The Effect of Deproteinizing Agents on Bond Strength of Resin-based Materials to Enamel: A Systematic Review and Meta-Analysis of In Vitro Studies.","authors":"Miguel Ángel Fernández-Barrera,&nbsp;Adriana Fernandes da Silva,&nbsp;América Patricia Pontigo-Loyola,&nbsp;J Eliezer Zamarripa-Calderón,&nbsp;Evandro Piva,&nbsp;Carlos Enrique Cuevas-Suárez","doi":"10.3290/j.jad.b1649893","DOIUrl":"https://doi.org/10.3290/j.jad.b1649893","url":null,"abstract":"<p><strong>Purpose: </strong>To systematically review the literature to evaluate whether the bond strength of resin-based materials to enamel is affected by deproteinizing agents.</p><p><strong>Materials and methods: </strong>This systematic review and meta-analysis was conducted according to the PRISMA statement. PubMed, ISI Web of Science, Cochrane Library, SciELO, Scopus, LILACS, IBECS, and BVS databases were screened up to December 2020. Eligibility criteria included in vitro studies that reported the effect of a deproteinizing agent applied before or after acid etching on the immediate or long-term bond strength of resin-based materials to enamel. The meta-analysis was carried out using Review Manager (version 5.3.5). A global comparison was performed with the standardized mean difference based on random-effect models at a significance level of α = 0.05.</p><p><strong>Results: </strong>A total of 23 studies were included in the meta-analysis. In all the studies, only the immediate bond strength was evaluated. The bond strength of the materials was improved by the application of NaOCl or papain prior to enamel etching with phosphoric acid (p ≤ 0.006). None of the deproteinizing agents had a significant effect when applied after etching with phosphoric acid (p ≥ 0.27).</p><p><strong>Conclusions: </strong>Based on in vitro studies, deproteinization with sodium hypochlorite or papain-based agents increases the immediate bond strength of resin-based materials to enamel only when used prior to phosphoric-acid etching.</p>","PeriodicalId":55604,"journal":{"name":"Journal of Adhesive Dentistry","volume":null,"pages":null},"PeriodicalIF":3.3,"publicationDate":"2021-07-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39190049","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
Effect of EDTA Concentrations as Irrigation Solution on Bonding of Fiber Posts into Root Canals with Universal Adhesives. EDTA灌洗液对纤维桩into根管与通用粘接剂粘接的影响。
IF 3.3 3区 医学 Q1 Dentistry Pub Date : 2021-07-23 DOI: 10.3290/j.jad.b1650173
Yançanã Luizy Gruber, Thaís Emanuelle Bakaus, Alessandra Reis, Osnara Maria Mongruel Gomes, João Carlos Gomes, Giovana Mongruel Gomes

Purpose: To evaluate the effect of different concentrations of ethylene-diamine-tetra acetic acid (EDTA) on bond strength (BS) and nanoleakage (NL) of fiber posts bonded into root canals.

Materials and methods: Seventy-two single roots were endodontically treated and divided into six groups (n = 12), according to the combination of the following factors: surface treatment (no irrigation [control], 17% EDTA, or 24% EDTA), and composite cement applied with an adhesive used in a self-etch mode (Single Bond Universal/RelyX Ultimate [SB], 3M Oral Care; Ambar Universal/Allcem [AM], FGM). After fiber post cementation, six 1-mm-thick disks were obtained for each root. Push-out bond strength (BS) was evaluated using 8 specimens per group, and the other 4 specimens were used to examine nanoleakage (NL). Data from BS and NL of each adhesive were evaluated by two-way ANOVA (surface treatment vs root region) and Tukey's test (α = 0.05).

Results: The application of 17% and 24% EDTA did not influence the bond strengths of either adhesive. In general, the application of 17% and 24% EDTA increased NL values for both adhesives.

Conclusion: Pre-treatment with different concentrations of EDTA was not able to improve the adhesion of fiber posts into root canals with universal adhesives..

目的:评价不同浓度的乙二胺四乙酸(EDTA)对纤维桩粘结into根canals的粘结强度(BS)和纳米渗漏(NL)的影响。材料和方法:对72根单根进行根管治疗,根据以下因素的组合分为6组(n = 12):表面处理(无冲洗[对照],17% EDTA,或24% EDTA),复合胶合剂应用于自蚀刻模式的粘合剂(single Bond Universal/RelyX Ultimate [SB], 3M Oral Care;Ambar Universal/Allcem [AM] [, FGM]]。纤维桩胶结后,每个根获得6个1 mm厚的盘。每组取8个试件进行推出粘结强度(BS)评估,其余4个试件进行纳米渗漏(NL)检测。采用双因素方差分析(表面处理vs根区)和Tukey检验(α = 0.05)对各胶粘剂的BS和NL数据进行评估。结果:应用17%和24% EDTA对两种胶粘剂的粘接强度of均无影响。总的来说,17%和24%的EDTA的应用增加了两种胶粘剂的NL值。结论:不同浓度的EDTA预处理均不能改善纤维桩into root canals与通用adhesives.的粘连性。
{"title":"Effect of EDTA Concentrations as Irrigation Solution on Bonding of Fiber Posts into Root Canals with Universal Adhesives.","authors":"Yançanã Luizy Gruber,&nbsp;Thaís Emanuelle Bakaus,&nbsp;Alessandra Reis,&nbsp;Osnara Maria Mongruel Gomes,&nbsp;João Carlos Gomes,&nbsp;Giovana Mongruel Gomes","doi":"10.3290/j.jad.b1650173","DOIUrl":"https://doi.org/10.3290/j.jad.b1650173","url":null,"abstract":"<p><strong>Purpose: </strong>To evaluate the effect of different concentrations of ethylene-diamine-tetra acetic acid (EDTA) on bond strength (BS) and nanoleakage (NL) of fiber posts bonded into root canals.</p><p><strong>Materials and methods: </strong>Seventy-two single roots were endodontically treated and divided into six groups (n = 12), according to the combination of the following factors: surface treatment (no irrigation [control], 17% EDTA, or 24% EDTA), and composite cement applied with an adhesive used in a self-etch mode (Single Bond Universal/RelyX Ultimate [SB], 3M Oral Care; Ambar Universal/Allcem [AM], FGM). After fiber post cementation, six 1-mm-thick disks were obtained for each root. Push-out bond strength (BS) was evaluated using 8 specimens per group, and the other 4 specimens were used to examine nanoleakage (NL). Data from BS and NL of each adhesive were evaluated by two-way ANOVA (surface treatment vs root region) and Tukey's test (α = 0.05).</p><p><strong>Results: </strong>The application of 17% and 24% EDTA did not influence the bond strengths of either adhesive. In general, the application of 17% and 24% EDTA increased NL values for both adhesives.</p><p><strong>Conclusion: </strong>Pre-treatment with different concentrations of EDTA was not able to improve the adhesion of fiber posts into root canals with universal adhesives..</p>","PeriodicalId":55604,"journal":{"name":"Journal of Adhesive Dentistry","volume":null,"pages":null},"PeriodicalIF":3.3,"publicationDate":"2021-07-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39190494","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
期刊
Journal of Adhesive Dentistry
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1