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Effect of Bonding Temperature on the Interfacial Microstructure and Mechanical Properties of W/Steel Joints Diffusion-Bonded with a CoFeNi Interlayer 结合温度对钴铁镍中间层扩散结合的 W/Steel 接头的界面微观结构和机械性能的影响
IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
JOM
Pub Date : 2024-09-23 DOI: 10.1007/s11837-024-06877-9
Chunyan Wang, Guoyun Tao, Shuibao Liang, Kuijing Song, Chengyong Wang, Yucheng Wu, Zhihong Zhong

Realizing the reliable bonding of tungsten (W) and reduced activation ferritic/martensitic (RAFM) steel is of significance for the fabrication of plasma-facing components in fusion reactors. Considering the significant differences in physical and chemical properties between the substrates of W and RAFM steel, the development of novel joining materials has attracted much attention in recent years. In the present work, a medium entropy alloy CoFeNi interlayer was selected to diffusion bond W and RAFM steel by utilizing an electric field-assisted joining technique. The effect of bonding temperature on the interface microstructure and mechanical properties of the joint was studied at room temperature. For the joints diffusion-bonded in the temperature range between 800°C and 1100°C for 15 min under 20 MPa, good metallurgical bonding without cracks and discontinuities were achieved at both the steel/CoFeNi and CoFeNi/W interfaces. Face-centered cubic (FCC) solid solutions were formed at the steel/CoFeNi interface, while both FCC and μ phases were identified at the CoFeNi/W interface. The W/CoFeNi/steel joint diffusion bonded at 900°C has the highest tensile strength of 313 MPa. Moreover, the comparison of the joint tensile strength between this work and previous researches has been discussed.

实现钨(W)和还原活化铁素体/马氏体(RAFM)钢的可靠结合对于制造聚变反应堆中的等离子体面组件具有重要意义。考虑到 W 和 RAFM 钢基材在物理和化学性质上的显著差异,新型连接材料的开发近年来备受关注。在本研究中,利用电场辅助接合技术,选择了中熵合金 CoFeNi 中间层来扩散接合 W 和 RAFM 钢。在室温下研究了接合温度对接合界面微观结构和机械性能的影响。在 20 兆帕的压力下,在 800°C 至 1100°C 的温度范围内扩散接合 15 分钟后,钢/CoFeNi 和 CoFeNi/W 界面都实现了良好的冶金接合,没有出现裂缝和不连续性。在钢/CoFeNi 界面形成了面心立方(FCC)固溶体,而在 CoFeNi/W 界面则发现了 FCC 和 μ 相。在 900°C 温度下扩散结合的 W/CoFeNi/W 钢接头的抗拉强度最高,达到 313 兆帕。此外,还讨论了本研究与之前研究的接头抗拉强度对比。
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引用次数: 0
Strength Behavior of Niobium-Based Refractory Systems 铌基耐火体系的强度行为
IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
JOM
Pub Date : 2024-09-23 DOI: 10.1007/s11837-024-06847-1
Krishna Joshi, Pankaj Kumar

A comprehensive assessment of the quasi-static strength behavior of niobium (Nb)-based refractory systems, including the conventional Nb alloys and refractory high-entropy alloys (RHEAs), in a broad temperature range has been performed in this review. The strength and ductility data of the Nb-based refractory systems in varying temperature ranges manufactured by various methods have been compiled and discussed to correlate the manufacturing, material characteristics, deformation, and strength behavior. The microstructure characteristics and the interstitial contaminations have been identified as the dominating factors in controlling strength behavior in the low-temperature range of the Nb alloys. In the intermediate temperature range, the dynamic strain recovery plays a significant role in dictating the strength behavior, while, in the high-temperature domain, the diffusion-assisted deformation process leads to significant strength reduction. Nb-based RHEAs have been found to have great potential for applications in extreme temperatures (> 1200°C). A wide range of strength and ductility is possible in Nb-based RHEAs. Solid-solution strengthening largely controls the variation in strength, ductility, and thermal stability of RHEAs.

本综述对铌(Nb)基耐火材料体系(包括传统铌合金和耐火高熵合金(RHEAs))在广泛温度范围内的准静态强度行为进行了全面评估。我们汇编并讨论了通过各种方法制造的铌基耐火材料体系在不同温度范围内的强度和延展性数据,以便将制造、材料特性、变形和强度行为联系起来。在铌合金的低温范围内,微观结构特征和间隙污染被认为是控制强度行为的主要因素。在中间温度范围内,动态应变恢复对强度行为起着重要作用,而在高温领域,扩散辅助变形过程会导致强度显著降低。人们发现,铌基 RHEAs 在极端温度(1200°C)下具有巨大的应用潜力。铌基 RHEAs 的强度和延展性范围很广。固溶强化在很大程度上控制着 RHEAs 强度、延展性和热稳定性的变化。
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引用次数: 0
A Review of Multiphysics Coupling Mechanical Behavior of Titanium-Coated Heterogeneous Wing for Re-entry Hypersonic Vehicle 重返大气层高超音速飞行器钛涂层异质翼多物理耦合力学行为综述
IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
JOM
Pub Date : 2024-09-18 DOI: 10.1007/s11837-024-06878-8
Fei Liu, Jiaqiang Li, Kunyu Chen, Yang Li, Mingyi Zhang, Chong Zhao, Chi Xiao, Yong Huan

The titanium-coated alloy heterogeneous structure has been widely used in the manufacture of re-entry hypersonic vehicle wings. However, due to the extreme and complex hypersonic service environment, the strength of the Ti alloy matrix is easily reduced under the synergistic action of complex loads such as aerodynamic heat, vibration, corrosion, and noise. This results in a mismatch of structural strength at the interface structure in the titanium-coated alloy, leading to destruction of the wing aerodynamic shape. At the same time, multiple load synergies can also lead to defects such as cracks and holes in the surface coating, damaging wing structural integrity. In addition, under the combined action of frequency- and time-domain loads, the wing structure will also experience creep deformation, leading to fatigue–creep interaction, exacerbating the accumulation of wing damage, and posing a serious threat to the service safety of the re-entry hypersonic vehicle. Therefore, this paper first reviews current research hotspots of re-entry hypersonic vehicle technology, and then analyzes the strengthening–toughening mechanism, high-temperature fatigue behavior, high-temperature creep behavior, and the damage prediction model of the titanium-coated alloy’s heterogeneous structure. Finally, it summarizes and prospects future research directions.

钛涂层合金异质结构已广泛应用于再入高超音速飞行器机翼的制造。然而,由于高超音速服役环境极端复杂,在气动热、振动、腐蚀和噪声等复杂载荷的协同作用下,钛合金基体的强度很容易降低。这将导致钛涂层合金界面结构强度失配,从而破坏机翼气动外形。同时,多重载荷的协同作用还会导致表面涂层出现裂纹和孔洞等缺陷,破坏机翼结构的完整性。此外,在频域和时域载荷的共同作用下,机翼结构还会发生蠕变变形,导致疲劳-蠕变相互作用,加剧机翼损伤的累积,对再入高超声速飞行器的服役安全构成严重威胁。因此,本文首先回顾了当前再入高超声速飞行器技术的研究热点,然后分析了钛涂层合金异质结构的强化-增韧机理、高温疲劳行为、高温蠕变行为和损伤预测模型。最后,对未来的研究方向进行了总结和展望。
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引用次数: 0
Phase Diagram of CaO-Al2O3-VOx Slag System Under Reducing Atmosphere 还原气氛下 CaO-Al2O3-VOx 熔渣体系的相图
IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
JOM
Pub Date : 2024-09-18 DOI: 10.1007/s11837-024-06866-y
Chengjun Liu, Xiaoxiang Xie, Jiyu Qiu, Wenjie Li, Guojie Huo

The phase diagram information of the CaO-Al2O3-VOx system is of significant importance for the direct alloying study of vanadium (V) during the smelting process of V-containing alloy steel, as well as for subsequent process optimization. This study has utilized the high-temperature phase equilibrium experimental method, combined with scanning electron microscope–energy dispersive spectrometer (SEM–EDS), electron probe micro-analysis (EPMA) and X-ray photoelectron spectroscopy (XPS) detection techniques, to research the phase equilibrium of the CaO-Al2O3-VOx system under argon (Ar) atmosphere at 1400°C. This study reveals that the phase diagram of CaO-Al2O3-VOx system, under the specified conditions, comprises 4 three-phase regions, 7 two-phase regions, and a liquid phase region. This study has plotted the CaO-Al2O3-V2O5-VO2 three-dimensional phase diagram and represented the phase equilibrium in CaO-Al2O3-V2O5, CaO-Al2O3-VO2, CaO-Al2O3-VO2.335, and Ca-Al-V systems. At the same time, the reliability of each projected phase diagram was quantitatively assessed.

CaO-Al2O3-VOx 体系的相图信息对于含钒合金钢冶炼过程中钒(V)的直接合金化研究以及后续工艺优化具有重要意义。本研究利用高温相平衡实验方法,结合扫描电子显微镜-能量色散光谱仪(SEM-EDS)、电子探针显微分析(EPMA)和 X 射线光电子能谱(XPS)检测技术,对 1400°C 氩气(Ar)气氛下 CaO-Al2O3-VOx 体系的相平衡进行了研究。研究发现,在特定条件下,CaO-Al2O3-VOx 体系的相图包括 4 个三相区、7 个两相区和 1 个液相区。本研究绘制了 CaO-Al2O3-V2O5-VO2 三维相图,并表示了 CaO-Al2O3-V2O5、CaO-Al2O3-VO2、CaO-Al2O3-VO2.335 和 CaAl-V 体系的相平衡。同时,还对每个投影相图的可靠性进行了定量评估。
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引用次数: 0
TMS Member News TMS 会员新闻
IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
JOM
Pub Date : 2024-09-11 DOI: 10.1007/s11837-024-06858-y
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引用次数: 0
Your 2025 TMS Membership: What’s New for the Year Ahead? 您的 2025 TMS 会员资格:来年有什么新变化?
IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
JOM
Pub Date : 2024-09-11 DOI: 10.1007/s11837-024-06861-3
Srini Chada
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引用次数: 0
In Situ, Parallel Monitoring of Relative Temperature, Material Emission, and Laser Reflection in Powder-Blown Directed Energy Deposition 对粉末喷射定向能量沉积过程中的相对温度、材料发射和激光反射进行原位并行监测
IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
JOM
Pub Date : 2024-09-10 DOI: 10.1007/s11837-024-06837-3
Samantha Webster, Jihoon Jeong, Rujing Zha, Shuheng Liao, Alberto Castro, Lars Jacquemetton, Darren Beckett, Kornel Ehmann, Jian Cao

In situ monitoring is critical for developing new control methods, advanced materials and toolpath planning strategies in laser beam directed energy deposition (DED-LB). Coaxial melt pool monitoring has typically been performed with cameras [e.g., infrared, two-color pyrometer, charge-coupled device, or complementary metal-oxide semiconductor], which have focused on melt pool morphology and temperature distribution. While these techniques capture critical deposition information, they do not capture other important phenomena such as the unique coupling between the laser and melt pool, which limits the design and generality of open-loop and closed-loop process control. We establish in situ, parallel signals by monitoring multiple process phenomena at the same time through different wavelength bands and thermal correlation. Increased laser coupling was observed using in situ, parallel monitoring, where lower reflectivity/higher absorption of the laser light within a vapor depression led to an increase in thermal emission in the visible region. Ultimately, a relationship between each change in process parameter and the relative absorption of the laser was established. In situ monitoring of the laser coupling phenomena not only provides insight into material processing conditions but will also enable more complex control in DED-LB processes.

在激光束定向能量沉积 (DED-LB) 过程中,原位监测对于开发新的控制方法、先进材料和工具路径规划策略至关重要。同轴熔池监测通常使用相机[如红外线、双色高温计、电荷耦合器件或互补金属氧化物半导体]进行,重点关注熔池形态和温度分布。虽然这些技术能捕捉到关键的沉积信息,但却无法捕捉到其他重要现象,如激光与熔池之间的独特耦合,这就限制了开环和闭环过程控制的设计和通用性。我们通过不同波长带和热相关性同时监测多种过程现象,从而建立原位并行信号。利用原位并行监测,我们观察到激光耦合的增加,在蒸汽凹陷处激光的反射率降低/吸收率增加,导致可见光区域的热辐射增加。最终,确定了工艺参数的每次变化与激光相对吸收之间的关系。对激光耦合现象的现场监测不仅可以深入了解材料的加工条件,还能在 DED-LB 过程中实现更复杂的控制。
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引用次数: 0
Effect of Heat Treatment on Mechanical Properties of 17-4 PH Stainless Steel Gyroid Lattice Structures Manufactured by Selective Laser Melting and a Study on Weight Reduction Methods 热处理对通过选择性激光熔化制造的 17-4 PH 不锈钢陀螺格构机械性能的影响以及减重方法研究
IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
JOM
Pub Date : 2024-09-09 DOI: 10.1007/s11837-024-06821-x
Sreekanth Asapu, Ravi Kumar Y

Weight reduction is critical in various engineering applications, as it directly impacts performance, efficiency, and overall cost-effectiveness. Topology optimization (TO) and lattice structures are effective methods for weight reduction, and such intricate designs are typically produced by additive manufacturing (AM). This research article presents an experimental investigation on the mechanical properties of uniform and gradient gyroid lattice structures manufactured through selective laser melting (SLM) using 17-4 precipitated hardening (PH) stainless steel (SS) material. The study focuses on analysing the effects of three different heat treatment processes on the compressive mechanical behaviour of the lattice structures using stress–strain graphs. Uniform lattices demonstrate superior mechanical properties by ensuring consistent structure stiffness and strength. Heat treatments decreased the grain size, resulting in increased yield strength for uniform and gradient structures compared to as-built samples. From the results, as-built samples showed higher plateau stress and energy absorption due to lower martensite content, leading to increased stress in the plateau region. Furthermore, different weight reduction methods such as TO, lattices, and the combination of TO and lattice can be studied and explained using an anchor bracket by utilising uniform and gradient-type sandwich lattice.

在各种工程应用中,减重至关重要,因为它直接影响到性能、效率和整体成本效益。拓扑优化(TO)和晶格结构是减轻重量的有效方法,而这种复杂的设计通常是通过增材制造(AM)生产出来的。本研究文章介绍了对使用 17-4 沉淀硬化(PH)不锈钢(SS)材料,通过选择性激光熔融(SLM)制造的均匀和梯度陀螺晶格结构的机械性能进行的实验研究。研究重点是利用应力应变图分析三种不同热处理工艺对晶格结构压缩机械性能的影响。均匀的晶格可确保结构刚度和强度的一致性,从而表现出优异的机械性能。与原样相比,热处理可减小晶粒尺寸,从而提高均匀结构和梯度结构的屈服强度。从结果来看,由于马氏体含量较低,导致高原区应力增加,坯料样品显示出较高的高原应力和能量吸收。此外,还可以利用均匀和梯度型夹层晶格,使用锚支架研究和解释不同的减重方法,如 TO、晶格以及 TO 和晶格的组合。
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引用次数: 0
The 2023 TMS Annual Financial Report 2023 TMS 年度财务报告
IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
JOM
Pub Date : 2024-09-09 DOI: 10.1007/s11837-024-06862-2
Brad Boyce, James J. Robinson
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引用次数: 0
TMS Meeting Headlines TMS 会议头条
IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
JOM
Pub Date : 2024-09-09 DOI: 10.1007/s11837-024-06865-z
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引用次数: 0
期刊
JOM
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