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Microhardness modeling of hydroxyapatite ceramics using random forest methods 用随机森林方法模拟羟基磷灰石陶瓷的显微硬度
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-12-17 DOI: 10.1007/s11182-025-03639-1
A. E. Rezvanova, A. N. Ponomarev, B. S. Kudryashov, M. I. Kochergin, V. Yu. Pogudin

The paper presents models for a prediction of the Vickers microhardness in the indentation load range of 100 to 500 gf. Machine learning methods (random decision forest and adaptive boosting) are used to develop these models for ceramic materials based on hydroxyapatite with the addition of reinforcing multi-walled carbon nanotubes in the amount of 0.1 and 0.5 wt.%. The input data for the model development include the sample type, test load and indenter diameter. A comparative analysis of training quality metrics such as the mean absolute, root mean square, and mean absolute percentage errors and the determination coefficient help to identify the method providing the lowest prediction error. The results of the regression analysis show that the adaptive boosting model with the high (0.918) determination coefficient and low (10.135) mean absolute error demonstrate the highest training accuracy. The proposed predictive models allow to determine the best machine learning method for predicting the Vickers microhardness of ceramic materials based on hydroxyapatite with regard the obtained nonlinear dependencies.

本文提出了在100 ~ 500gf压痕载荷范围内维氏显微硬度的预测模型。利用机器学习方法(随机决策森林和自适应增强)开发了基于羟基磷灰石的陶瓷材料的模型,并添加了0.1和0.5 wt.%的增强多壁碳纳米管。模型开发的输入数据包括样品类型、试验载荷和压头直径。训练质量指标的比较分析,如平均绝对、均方根、平均绝对百分比误差和确定系数,有助于确定提供最低预测误差的方法。回归分析结果表明,自适应增强模型具有较高的决定系数(0.918)和较低的平均绝对误差(10.135),训练精度最高。提出的预测模型可以根据所获得的非线性依赖关系确定预测羟基磷灰石陶瓷材料维氏显微硬度的最佳机器学习方法。
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引用次数: 0
Nanocomposite-filled slot enhancing radiation of a triple band antenna 纳米复合材料填充缝隙增强三波段天线辐射
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-12-17 DOI: 10.1007/s11182-025-03650-6
A. S. Vasu, N. R. Lakshmi, T. K. Sreeja

A nanocomposite-filled slot antenna is designed to improve the radiation of a triple band radiator which consists of two rigid radiating elements united to the central strip of a coplanar waveguide (CPW) antenna. The longer strip resonates at the lower resonance frequency and the shorter strip—at the middle resonance frequency. The upper band of the triple band radiator is formed by the L slot on the left CPW ground. The gain and bandwidth of the proposed radiator are improved by a nanocomposite-filled slot. A better cross polarization of the radiator is achieved by decreasing the coupling of rigid radiating elements by spacing them properly. The compact structure is attained by uniting the radiating strips to the 5.00 mm wide signal-generating strip. The proposed radiator bandwidth is within 3.08–3.80 GHz for the lower band, 4.57–5.56 GHz for the middle band and 5.95–7.51 GHz for the upper band, which covers WLAN, WiMAX, 5G and Wi-Fi with an enhanced gain. The proposed radiator is suitable for practical wireless applications due its good radiation characteristics.

为了提高三波段共面波导(CPW)天线的辐射性能,设计了一种纳米复合材料填充缝隙天线。较长的条带在较低的共振频率共振,较短的条带在中共振频率共振。三波段散热器的上波段由左侧CPW接地上的L槽组成。利用纳米复合材料填充槽提高了辐射器的增益和带宽。通过适当间距减小刚性辐射元件的耦合,可以获得较好的交叉极化效果。紧凑的结构是通过将辐射条连接到5.00 毫米宽的信号产生条而实现的。提议的辐射器带宽下频段为3.08-3.80 GHz,中频段为4.57-5.56 GHz,上频段为5.95-7.51 GHz,覆盖了增益增强的WLAN、WiMAX、5G和Wi-Fi。该辐射器具有良好的辐射特性,适合实际无线应用。
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引用次数: 0
Synthesis of mesoporous TiO2 photocatalytically active under visible light or UV radiation 在可见光或紫外线辐射下合成具有光催化活性的介孔TiO2
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-12-17 DOI: 10.1007/s11182-025-03621-x
E. A. Ovodok, M. I. Ivanovskaya, S. K. Poznyak, D. A. Kotsikau, S. V. Zlotski, V. V. Uglov, A. E. Seleznev, A. A. Vereschaka

Mesoporous nanosized titania with a high specific surface area is synthesized by titanium carbide oxidation with nitric acid followed by a heat treatment of the product. The effect of heating temperature on the structural characteristics of TiO2 and its activity in the photodecomposition reaction of the dye (rhodamine B) is studied. It is shown that compared with the well-known photocatalyst, Degussa P25, the photocatalytic activity of the samples heat-treated at 200°C and 400 °C is improved, when exposed to visible and UV radiation, respectively. The high photoactivity of the TiO2 sample (200°C) under exposure to visible light is due to a high specific surface area, the presence of COx and NOx groups on the surface, and the structure of the anatase phase with a trace of rutile phase. Under exposure to the UV radiation, the TiO2 sample (400°C) is characterized by high photoactivity attributed to a high specific surface area and oxygen structure defects (O).

采用碳化钛与硝酸氧化并对产物进行热处理的方法合成了具有高比表面积的介孔纳米二氧化钛。研究了加热温度对TiO2结构特性及其在染料(罗丹明B)光分解反应中的活性的影响。结果表明,与众所周知的光催化剂Degussa P25相比,分别在200°C和400 °C下热处理的样品在可见光和紫外辐射下的光催化活性有所提高。TiO2样品(200℃)在可见光下具有较高的光活性,这是由于其具有较高的比表面积,表面存在COx和NOx基团,且其锐钛矿相结构中含有微量金红石相。在紫外线照射下,TiO2样品(400°C)由于具有高比表面积和氧结构缺陷(O−)而具有高光活性。
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引用次数: 0
Structure formation and tribological properties of bronze-Fe composite materials produced by electron beam additive manufacturing 电子束增材制造青铜-铁复合材料的结构形成及摩擦学性能
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-12-17 DOI: 10.1007/s11182-025-03641-7
V. M. Semenchuk, A. O. Panfilov, A. V. Filippov, K. S. Osipovich, D. A. Gurianov, A. V. Chumaevskii, S. Yu. Tarasov, E. A. Kolubaev

The paper investigates the microstructure and properties of composite materials based on aluminum-manganese bronze and stainless steel. It is demonstrated that the microstructure has an effect on the tribological behavior of aluminum-manganese bronze–steel composites under dry friction and boundary lubrication conditions. The tribology testing results indicate a catastrophic wear of composites. The increased steel content in the bronze matrix leads to a dramatic growth in the wear intensity during the dry friction due to the enhanced adhesive interaction between the counter body and the sample. Tribology testing at the boundary lubrication shows an acceptable tribological performance and a moderate wear rate for the composite materials.

研究了铝锰青铜与不锈钢复合材料的组织和性能。结果表明,在干摩擦和边界润滑条件下,微观组织对铝锰青铜钢复合材料的摩擦学性能有影响。摩擦学试验结果表明,复合材料存在突变磨损。铜基体中钢含量的增加导致干摩擦过程中磨损强度的急剧增长,这是由于基体与试样之间的粘接相互作用增强所致。边界润滑处的摩擦学试验表明,复合材料具有良好的摩擦学性能和适度的磨损率。
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引用次数: 0
TEM study of deformation bands created by mechanical cycling of a superelastic Ti-50.9 at.% Ni alloy 超弹性Ti-50.9 at机械循环变形带的透射电镜研究。% Ni合金
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-12-15 DOI: 10.1007/s11182-025-03623-9
S. L. Girsova, T. M. Poletika, S. M. Bitter

The effect of cyclic tensile deformation in the loading/unloading mode in the superelastic loop region on the deformation structure of a nanocrystalline aging superelastic Ti-50.9 at.% Ni alloy is studied. It is shown that the initial stage (from 0 to 5–10 cycles) corresponds to the accumulation of dislocations with the formation of a three-dimensional network with the nodes pinned by Ti3Ni4 particles, which inhibits the dislocation activity. After 10 loading cycles, there develop additional accommodative deformation mechanisms in the strengthened dislocation structure. It is found out that the relaxation of high internal stresses results in the formation of the reorientation mesobands, which ensure effective stress relaxation due to a local lattice reorientation.

研究了超弹性环区加载/卸载模式下的循环拉伸变形对时效超弹性Ti-50.9 at纳米晶变形结构的影响。研究了% Ni合金。结果表明:在初始阶段(0 ~ 5 ~ 10个循环),位错逐渐积累,形成三维网络,节点被Ti3Ni4颗粒钉住,位错活性受到抑制。经过10次加载循环后,强化的位错结构中出现了额外的调节变形机制。研究发现,高内应力的松弛导致重定向介带的形成,从而保证了局部晶格重定向引起的有效应力松弛。
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引用次数: 0
Influence of varying thermal cycle of post weld heat treatment on tensile characteristics of friction stir welded joints 焊后热处理不同热循环对搅拌摩擦焊接头拉伸特性的影响
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-12-15 DOI: 10.1007/s11182-025-03632-8
Atif Shazad, Muhammad Uzair, Maaz Akhtar, Abdul Shakoor

The paper investigates the artificial aging effect on the tensile behaviour of friction stir welding of the aluminum 2219-T87 material, focusing on the impact of different thermal cycles and soaking times. It is shown that artificial aging enhances the ultimate tensile strength (UTS) and yield strength (YS). Aging at 165 °C for 12 h increases the YS by 14.2% due to precipitation hardening. However, aging at 175 °C for 12 h reduces both the UTS and YS due to an excessive precipitation. Ductility decreases with the precipitation hardening, but aging at 165 °C for 12 h retains 9% elongation. In contrast, aging at 175 °C for the same period reduces elongation to 7.4%. Prolonged aging at 165 °C for 18 h further reduces the material ductility.

研究了人工时效对2219-T87铝合金搅拌摩擦焊拉伸性能的影响,重点研究了不同热循环次数和浸泡时间对搅拌摩擦焊拉伸性能的影响。结果表明,人工时效提高了材料的极限抗拉强度和屈服强度。165 °C时效12 h,由于析出硬化,YS提高了14.2%。然而,在175 °C下时效12 h,由于析出过多,UTS和YS都降低了。随着析出硬化,塑性降低,但在165 °C时效12 h,伸长率仍保持9%。相反,在175 °C时效相同时间,伸长率降至7.4%。在165 °C下延长时效18 h,进一步降低了材料的延展性。
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引用次数: 0
Thermal stability of V–W–Cr–Zr alloy after combined treatment V-W-Cr-Zr合金复合处理后的热稳定性
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-12-15 DOI: 10.1007/s11182-025-03636-4
I. A. Smirnov, D. A. Osipov, K. V. Grinyaev, I. A. Ditenberg

The effect of high-temperature annealing on the microstructure and microhardness of a V–Cr–Zr–W alloy subjected to a combined treatment, involving a modified thermomechanical treatment and a chemical-heat treatment by the method of internal oxidation, is investigated. It is shown that as a result of this combined treatment the alloy thermal stability increases by a few hundred degrees. It is expected that the high structural-phase inhomogeneity of this alloy after its combined treatment is a consequence of the inhomogeneity of highly defective states and the specific features of introducing oxygen in the internal-oxidation stage.

研究了高温退火对V-Cr-Zr-W合金显微组织和显微硬度的影响。结果表明,这种复合处理使合金的热稳定性提高了几百度。综合处理后合金的高组织相不均匀性是高缺陷态的不均匀性和内氧化阶段引入氧的特殊特征的结果。
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引用次数: 0
Dependence of efficiency of oxide ceramics radiation synthesis on time of high-energy electron-beam irradiation 高能电子束辐照时间对氧化陶瓷辐射合成效率的影响
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-12-15 DOI: 10.1007/s11182-025-03642-6
V. M. Lisitsyn, E. F. Polisadova, A. A. Karnaukhova, V. I. Oleshko, N. D. Tran, A. T. Tulegenova, M. G. Golkovski

A technology for producing porous oxide ceramics by irradiating the crucible with an electron beam with an electron energy of 1.4 MeV and a power density of 2.8–55 kW/cm2 is described. The effect of the rate of the powder charge irradiation on the efficiency of the radiation synthesis—conversion of a mixture of the precursor powders into a ceramic material—is studied. It is found out that increasing the speed of the crucible irradiation with the electron beam from 0.125 to 2.5 cm/s, given an equal absorbed radiation dose, leads to an increase in the efficiency from 70 to 98%. The role of electron beam energy losses in the powder volume as a result of irradiation is discussed.

介绍了用电子能量为1.4 MeV、功率密度为2.8 ~ 55 kW/cm2的电子束辐照坩埚制备多孔氧化物陶瓷的技术。研究了粉末电荷辐照速率对前驱体粉末混合物转化为陶瓷材料的辐射合成效率的影响。结果表明,在相同的辐射吸收剂量下,将电子束辐照坩埚的速度从0.125 cm/s提高到2.5 cm/s,可使辐照效率从70%提高到98%。讨论了辐照引起的电子束能量损失在粉末体积中的作用。
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引用次数: 0
Effect of different impact velocities on mechano-luminescence of natural calcite for mechanical sensors 不同冲击速度对天然方解石机械发光的影响
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-12-15 DOI: 10.1007/s11182-025-03591-0
Wei Peng, Faithfulstar K Bani, Janita Saji, Rocky Maximillian Pohlong Lamare, Guoqing Hu, Vikas Dubey

This paper studies the mechanoluminescence (ML) behavior of natural calcite under varying impact velocities to assess its potential use in passive mechanical sensing. Calcite samples obtained from Byrnihat, Meghalaya (26°03′03.8″N 91°52′11.0″E), were analyzed using X‑ray diffraction, field emission scanning electron microscopy, energy-dispersive X‑ray spectroscopy, and Fourier-transform infrared spectroscopy. The analysis confirms the formation of the nanocrystalline hexagonal phase with minor impurities that affect its luminescent properties. When subjected to the mechanical impact, the calcite consistently produces a sharp ML peak around 17 ms, regardless of the impact speed. The emitted light intensity shows a linear dependence on the impact velocity, suggesting a reliable correlation between the mechanical input and optical response. The emission decay follows a first-order exponential pattern, supporting its usefulness for identifying short-duration force events. A plot of time against the logarithm of intensity displays a clear negative slope, supporting this kinetic model. These research findings highlight the potential of natural calcite as a reliable and environmentally friendly material for mechanical sensor applications.

本文研究了天然方解石在不同冲击速度下的机械发光(ML)行为,以评估其在被动机械传感中的潜在应用。方解石样品采自梅加拉亚邦Byrnihat(26°03′03.8″N 91°52′11.0″E),采用X射线衍射、场发射扫描电子显微镜、能量色散X射线光谱和傅里叶变换红外光谱分析。分析证实了纳米晶六方相的形成,杂质较少,影响其发光性能。当受到机械冲击时,无论冲击速度如何,方解石始终在17 ms左右产生尖锐的ML峰值。发射光强度与冲击速度呈线性关系,表明机械输入和光响应之间存在可靠的相关性。发射衰减遵循一阶指数模式,支持其对识别短持续时间力事件的有用性。时间与强度对数的关系图显示出明显的负斜率,支持这种动力学模型。这些研究结果突出了天然方解石作为机械传感器应用的可靠和环保材料的潜力。
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引用次数: 0
Luminescence properties of Y3Al5–xGaxO12:Ce ceramics with various contents of Al, Ga, and Ce 不同Al、Ga、Ce含量Y3Al5-xGaxO12:Ce陶瓷的发光性能
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-12-15 DOI: 10.1007/s11182-025-03647-1
B. P. Gritsenko, A. A. Karnaukhova

The Y3Al5–xGaxO12:Ce ceramic samples are synthesized by the radiation method. The influence of precursors on the radiation synthesis process is studied. The influence of the Al/Ga ratio on the spectral and kinetic properties of luminescence of Y3Al5–xGaxO12:Ce ceramics manufactured by radiation synthesis is investigated. The luminescence spectra of the samples are measured using the optical spectrometry technique with a time resolution of 7 ns. It is shown that gallium shifts the spectrum to the high-energy region due to the appearance of a new emission band at 2.49 eV and decreases the luminescence intensity in the low-energy region of the spectrum and the contribution from the relatively slow processes to the luminescence decay.

采用辐射法制备了Y3Al5-xGaxO12:Ce陶瓷样品。研究了前驱体对辐射合成过程的影响。研究了Al/Ga比对辐射合成Y3Al5-xGaxO12:Ce陶瓷光谱和发光动力学性能的影响。利用时间分辨率为7 ns的光学光谱技术测量了样品的发光光谱。结果表明,在2.49 eV处,镓出现了一个新的发射带,使光谱向高能区偏移,降低了光谱低能区的发光强度和相对缓慢的发光过程对发光衰减的贡献。
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引用次数: 0
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Russian Physics Journal
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