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Electrical Response of Al Based Zr-Doped Stacked Tri-Layer HfO2 Deposited at Various Substrate Temperature 不同基底温度下沉积的铝基掺锆堆叠三层 HfO2 的电响应
IF 0.6 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1007/s11182-024-03198-x
R. Sultana, K. Islam, S. Chakraborty

This study examines how the substrate temperature affects the electrical characteristics of the Zr-doped HfO2/Al/Zr-doped HfO2 (HZO/Al/HZO) tri-layer stack. Tri-layer stack is deposited by a simultaneous use of RF magnetron sputtering for HfO2 and DC magnetron sputtering for Zr and Al targets. During deposition, the substrate temperature is varied from 25 to 300°C. The observed hysteresis loop is prominent for the stack deposited at room temperature, while it becomes minute at higher temperatures. Interface trap density and oxide charge density of the tri-layer stack are minimum at 300°C and maximum at room temperatures. Frequency dispersion is detected in the stack deposited at room temperature, but it disappears in stacks deposited at 300°C. In addition, compared to other tri-layer stacks, the stack deposited at 300°C shows good conductivity. Therefore, compared to other samples, the tri-layer stack deposited at 300°C has improved electrical characteristics. It is shown that the substrate temperature has a significant impact on the electrical properties of the stack.

本研究探讨了衬底温度如何影响掺锆 HfO2/Al/掺锆 HfO2(HZO/Al/HZO)三层叠层的电气特性。三层叠层通过同时使用射频磁控溅射和直流磁控溅射来沉积 HfO2 和 Zr 和 Al 靶件。在沉积过程中,基片温度在 25 至 300°C 之间变化。观察到的滞后环在室温下沉积的堆栈中很明显,而在较高温度下则变得很微小。三层堆栈的界面陷阱密度和氧化物电荷密度在 300°C 时最小,而在室温时最大。在室温下沉积的堆栈中检测到频率分散,但在 300°C 下沉积的堆栈中频率分散消失了。此外,与其他三层堆栈相比,在 300°C 下沉积的堆栈具有良好的导电性。因此,与其他样品相比,在 300°C 下沉积的三层叠层具有更好的电气特性。这表明,基底温度对叠层的电气特性有重大影响。
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引用次数: 0
Thermodynamic Modeling of the C90–N2 System C90-N2 系统的热力学建模
IF 0.6 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1007/s11182-024-03205-1
N. M. Barbin, L. V. Yakupova, D. I. Terent’ev, V. T. Kuanyshev, A. I. Burumbaev, D. I. Burumbaev

Using the method of computer thermodynamic modeling, the stability of higher fullerene C90 heated in a nitrogen atmosphere at a pressure of 0.1 MPa is studied. The simulation is performed using the TERRA software package in the temperature range from 273 K to 3373 K. The equilibrium composition of compounds in the C90–N2 system is obtained and the physico-chemical processes causing the formation of these compounds are described. The equilibrium constants of the processes forming the equilibrium composition of compounds are calculated for different temperature ranges using the least squares method.

利用计算机热力学建模方法,研究了在压力为 0.1 兆帕的氮气环境中加热高等富勒烯 C90 的稳定性。利用 TERRA 软件包在 273 K 至 3373 K 的温度范围内进行了模拟。得出了 C90-N2 体系中化合物的平衡组成,并描述了导致这些化合物形成的物理化学过程。使用最小二乘法计算了不同温度范围内形成化合物平衡组成的过程的平衡常数。
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引用次数: 0
Structure and Properties of Surfacing Made of High-Entropy High-Speed Steel 高熵高速钢堆焊面的结构与性能
IF 0.6 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1007/s11182-024-03196-z
A. B. Yuriev, Yu. F. Ivanov, V. E. Gromov, A. I. Potekaev, Yu. A. Abzaev, A. A. Klopotov, S. S. Minenko, A. S. Chapaikin, A. P. Semin

Using the methods of advanced material physics, the structural-phase state of a layer of high-entropy high-speed non-equiatomic molybdenum tool steel formed by electric arc surfacing in a nitrogen atmosphere is studied. The thermodynamical and mechanical (elastic moduli) properties of the surfaced layer are examined in a temperature interval of 300–1400°C, and a phase-composition diagram is presented. It is observed that a temperature increase is accompanied by an α→γ polymorphic transformation, followed by a decrease in the content of carbide phases and elastic moduli.

利用先进的材料物理学方法,研究了在氮气环境中通过电弧堆焊形成的高熵高速非等原子钼工具钢层的结构相态。在 300-1400°C 的温度区间内考察了堆焊层的热力学和机械(弹性模量)特性,并给出了相组成图。研究发现,温度升高伴随着 α→γ 多晶体转变,随后碳化物相含量和弹性模量下降。
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引用次数: 0
Corrosion Resistance of TiNi-Based Biocompatible Composite Materials After Electron Beam Treatment 电子束处理后 TiNi-Based 生物兼容复合材料的抗腐蚀性
IF 0.6 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1007/s11182-024-03197-y
E. A. Bolshevich, S. G. Anikeev, N. V. Artyukhova, A. V. Shabalina, S. A. Pakholkina

Porous-monolithic TiNi-based materials are fabricated by sintering TiNi powder on monolithic TiNi plates, followed by their surface modification with a low-energy high-current electron beam. Their corrosion resistance is examined in a biological medium by the method of voltamperometry using linear scanning, and their structural features are studied by the methods of optical profilometry, scanning electron microscopy and X-ray microanalysis. A comparison of the corrosion rates of the porous-monolithic samples is performed, and it is found out that the new composites possess better corrosion resistance compared to that of TiNi plates due to a homogeneous phase composition of the surface. A treatment of the TiNi-based powder alloy with LEHCEB is thought to be effective in optimizing the properties of materials used in implantology.

通过在整体钛镍板上烧结钛镍粉,然后用低能量大电流电子束对其进行表面改性,制备出了多孔整体钛镍基材料。利用线性扫描伏安法检测了它们在生物介质中的耐腐蚀性,并利用光学轮廓仪、扫描电子显微镜和 X 射线显微分析法研究了它们的结构特征。对多孔整体样品的腐蚀速率进行了比较,结果发现,与钛镍板相比,新型复合材料具有更好的耐腐蚀性,这是因为其表面的相组成是均匀的。用 LEHCEB 对钛镍基粉末合金进行处理被认为能有效优化植入学所用材料的性能。
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引用次数: 0
Spectroscopic Analysis and TL Glow Curve Studies of Eu3+-Doped Er2SiO5 Phosphor 掺杂 Eu3+ 的 Er2SiO5 磷光体的光谱分析和 TL 辉光曲线研究
IF 0.6 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1007/s11182-024-03206-0
Ram Krishna Deshmukh, N. Kumar Swamy, Vikas Dubey, A. V. Chandrasekhar, G. Naveen Kumar, M. C. Rao

Synthesis and characterization of Eu3+-doped Er2SiO5 phosphor are reported. The samples are prepared using the modified conventional solid-state synthesis technique with variable concentrations of doping ions and their structural studies are carried out by X–ray diffraction (XRD). The information on the morphology of the samples prepared with optimized doping ion concentrations is obtained by scanning electron microscopy (SEM). A photoluminescence (PL) analysis of the phosphor samples is also done for the fixed doping ion concentrations. The identified PL emission bands are attributed to the intra 4f transitions of a Eu3+ ion, such as 5D07F1 at 590 nm, 5D07F0 at 602 and 5D07F2 at 613 nm. The corresponding transitions of the doping ions and the concentration quenching effect are studied in detail. The 1931 Commission Internationale de l’éclairage (CIE) (x, y) chromaticity coordinates show the spectral distribution calculated from the PL emission spectrum. A thermoluminescence (TL) glow curve analysis is performed for variable doping ion concentrations, and the corresponding trap parameters are calculated using the Computerized Glow Curve Deconvolution (CGCD) technique. Our study shows that as-prepared phosphor may be useful for display devices.

报告了掺杂 Eu3+ 的 Er2SiO5 荧光粉的合成和表征。样品的制备采用了掺杂离子浓度可变的改良传统固态合成技术,并通过 X 射线衍射 (XRD) 进行了结构研究。通过扫描电子显微镜(SEM)获得了优化掺杂离子浓度制备的样品的形态信息。此外,还对固定掺杂离子浓度的荧光粉样品进行了光致发光(PL)分析。确定的 PL 发射带归因于 Eu3+ 离子的 4f 内跃迁,如 590 纳米波长处的 5D0→7F1、602 纳米波长处的 5D0→7F0 和 613 纳米波长处的 5D0→7F2。详细研究了掺杂离子的相应转变和浓度淬灭效应。1931 年国际照明委员会(CIE)(x, y)色度坐标显示了根据 PL 发射光谱计算出的光谱分布。针对不同的掺杂离子浓度进行了热发光(TL)辉光曲线分析,并利用计算机辉光曲线解卷积(CGCD)技术计算了相应的阱参数。我们的研究表明,制备的荧光粉可用于显示器件。
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引用次数: 0
Structure and Properties of Antiferromagnetic Dirac Semi-Metal EuZnSb2 反铁磁性狄拉克半金属 EuZnSb2 的结构与性质
IF 0.6 4区 物理与天体物理 Q3 Physics and Astronomy Pub Date : 2024-06-03 DOI: 10.1007/s11182-024-03189-y
Xiang Shi, Huxin Yin, Xucai Kan, Xiansong Liu, Yuyan Han

A EuZnSb2 antiferromagnetic (AFM) semi metal with a P4/nmm space group (No. 129) is synthesized using the Sb-flux method. The magnetic properties, specific heat, and resistivity of the EuZnSb2 single crystals are analyzed. The magnetic and specific heat properties indicate an antiferromagnetic order of Eu2+ with TN ~ 20 K. The magnetic field is observed to suppress the AFM transition of Eu2+ and the magnetic susceptibility vs. temperature curves exhibit differences when the magnetic field is applied along the ab-plane and c-axis of EuZnSb2 single crystal, reflecting a weak in-plane anisotropy of Eu2+. When the temperature is below 20 K, a spin‒flop transition of the AFM order appears at approximately 1.6 T. The electronic transport measurements indicate that a EuZnSb2 single crystal exhibits metallic properties and an extremely unsaturated positive MR effect. A twofold period of anisotropic magnetoresistance is observed, indicating that the resistivity characteristics correlate with the magnetic field intensity and the angle between the magnetic field direction and the crystallographic axis direction. These studies contribute to enriching the magnetic, specific thermal, and electrical transport properties of EuZnSb2. These results also provide valuable information for further research on other AFM materials.

利用 Sb-flux 方法合成了空间群为 P4/nmm(129 号)的 EuZnSb2 反铁磁(AFM)半金属。分析了 EuZnSb2 单晶体的磁性能、比热和电阻率。当磁场沿 EuZnSb2 单晶的 ab 平面和 c 轴施加时,磁感应强度与温度的关系曲线表现出差异,这反映了 Eu2+ 在面内的微弱各向异性。电子传输测量结果表明,EuZnSb2 单晶具有金属特性和极不饱和的正磁共振效应。观察到两倍周期的各向异性磁阻,表明电阻率特性与磁场强度以及磁场方向和晶体轴方向之间的角度相关。这些研究有助于丰富 EuZnSb2 的磁性、比热和电传输特性。这些结果也为进一步研究其他原子力显微镜材料提供了宝贵的信息。
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引用次数: 0
Enhanced Thermal Performance of Alkali-Treated Bamboo, Coir, and Date Palm Fiber Composites for Solar Distillation Applications 提高经碱液处理的竹子、椰子纤维和椰枣纤维复合材料在太阳能蒸馏应用中的热性能
IF 0.6 4区 物理与天体物理 Q3 Physics and Astronomy Pub Date : 2024-06-03 DOI: 10.1007/s11182-024-03191-4
P. Yadav, O. Prakash

This study investigates the thermal conductivity and moisture absorption characteristics of bamboo, coir, and date palm fiber composites, specifically examining their suitability for use in solar distillation applications. Four composite samples comprising alkali-treated bamboo and coir fiber (sample 1), untreated bamboo and coir fiber (sample 2), treated coir and date palm fiber (sample 3), and untreated coir and date palm fiber (sample 4) have been experimentally analyzed. Samples 1 and 3 showed 17.6 and 16.6% lower thermal conductivities and 45.8 and 44.2% lower moisture absorptions than untreated samples 2 and 4. Alkali-treated fibers had decreased lignin and hemicellulose and more cellulose, supporting the observed benefits after chemical analysis. Post-alkali scanning electron microscopy showed improved fiber surface morphology, highlighting cellulose energy-saving significance. The results indicate that these composites, due to their improved thermal insulation characteristics, provide a sustainable choice for integration into solar distillation systems.

本研究调查了竹纤维、棕纤维和枣椰纤维复合材料的导热性和吸湿性,特别是研究了它们在太阳能蒸馏应用中的适用性。实验分析了四种复合材料样品,包括碱处理过的竹纤维和椰壳纤维(样品 1)、未处理过的竹纤维和椰壳纤维(样品 2)、处理过的椰壳纤维和枣椰纤维(样品 3)以及未处理过的椰壳纤维和枣椰纤维(样品 4)。与未经处理的样本 2 和样本 4 相比,样本 1 和样本 3 的导热率分别降低了 17.6% 和 16.6%,吸湿率分别降低了 45.8% 和 44.2%。碱处理后的纤维木质素和半纤维素减少,纤维素增加,支持了化学分析后观察到的优点。碱处理后的扫描电子显微镜显示纤维表面形态有所改善,凸显了纤维素的节能意义。研究结果表明,这些复合材料具有更好的隔热性能,是集成到太阳能蒸馏系统中的可持续选择。
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引用次数: 0
Calculation of Q-Cascade Parameters for Highly-enriched Silicon Isotopes 计算高浓度硅同位素的 Q 级联参数
IF 0.6 4区 物理与天体物理 Q3 Physics and Astronomy Pub Date : 2024-06-03 DOI: 10.1007/s11182-024-03187-0
A. A. Orlov, M. V. Petrov, A. V. Ovezova

The paper presents calculations of the two-stage separation of silicon isotopes in Q-cascade models. Feed flow profiles are obtained for Q-cascades, and the concentration distribution by stages is determined for silicon isotopes. It is shown that three highly-enriched (>99%) products can be obtained at a 35 g/s feed flow, namely: 32.31 g/s 28Si, 1.61 g/s 29Si, and 1.08 g/s 30Si.

本文介绍了 Q 级联模型中硅同位素两级分离的计算。获得了 Q 级联的进料流量曲线,并确定了硅同位素的各阶段浓度分布。结果表明,在进料流量为 35 克/秒的情况下,可以获得三种高富集(99%)的产品,即32.31 克/秒 28Si、1.61 克/秒 29Si 和 1.08 克/秒 30Si。
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引用次数: 0
Nanocomposite Structure Formation Under Laser Emission 激光发射下的纳米复合结构形成
IF 0.6 4区 物理与天体物理 Q3 Physics and Astronomy Pub Date : 2024-06-01 DOI: 10.1007/s11182-024-03177-2
A. P. Kuzmenko, A. Yu. Stavtsev, G. F. Kopytov, M. I. Gozman

The paper deals with the high-speed formation of nanocomposite structures on a polycarbonate matrix with a metal film affected by pulsed laser radiation at a wavelength of 1064 nm. Studied is the micro- and nanosized ordering depending on the laser power. Based on confocal laser scanning microscopy and using the area similarity method, structural groups and fractal dimensions are determined, and 2D-to-3D structure transition is studied herein.

本文论述了在波长为 1064 纳米的脉冲激光辐射作用下,在带有金属膜的聚碳酸酯基体上高速形成纳米复合结构的问题。研究对象是取决于激光功率的微米级和纳米级排序。基于共焦激光扫描显微镜和面积相似性方法,确定了结构群和分形尺寸,并研究了二维到三维结构的转变。
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引用次数: 0
Optical Radiation Interaction with Solids 光学辐射与固体的相互作用
IF 0.6 4区 物理与天体物理 Q3 Physics and Astronomy Pub Date : 2024-05-28 DOI: 10.1007/s11182-024-03169-2
B. P. Gritsenko, V. P. Krivobokov

The paper deals with the optical radiation interaction with solids. It is shown that none of the existing ideas about the light reflection gives explanations to the known phenomena arising from the interaction between optical radiation and a solid. It is suggested that the optical radiation reflection is a collective process associated with the self-organization of electrons with a photon. This suggestion explains a number of physical phenomena that have not been explained before, for example, the Goos–Hänchen and Imbert–Fedorov beam shifts, which are natural processes in such representation of reflection.

本文论述了光辐射与固体的相互作用。研究表明,现有的关于光反射的观点都无法解释光辐射与固体相互作用产生的已知现象。文章认为,光辐射反射是一个与电子与光子自组织相关的集体过程。这一观点解释了许多以前未曾解释过的物理现象,例如 Goos-Hänchen 和 Imbert-Fedorov 光束偏移,它们都是这种反射表象中的自然过程。
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引用次数: 0
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Russian Physics Journal
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