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Obsidian hydration dating by infrared transmission spectroscopy 利用红外透射光谱测定黑曜石水化年代
IF 1.6 3区 地球科学 Q1 Arts and Humanities Pub Date : 2024-05-15 DOI: 10.1111/arcm.12982
Fernando Franchetti, Gustavo Neme, Adolfo Gil, M. Laura Salgan, Alexander K. Rogers, James Davenport, Raven Garvey, Olga Trofimova, Thegn N. Ladefoged, Christopher M. Stevenson
The obsidian dating method converts the quantity of diffused molecular water within a near‐surface hydration layer to elapsed time using an experimentally derived diffusion coefficient predicted from the structural water content of the glass. Infrared spectroscopic transmission measurements on transparent archaeological samples record vibrational responses of water bands in the near‐infrared region, permitting determination of structural water content (OH), and the amount of diffused ambient water (H2O). In this application, the H2O water band at 5200 cm−1 is measured directly. The accuracy of the approach is assessed by an evaluation of the precision of each contributing variable. The new protocol is evaluated using obsidian artifacts from radiocarbon‐dated deposits at Salamanca Cave in Argentina.
黑曜石年代测定法利用从玻璃的结构水含量预测的实验得出的扩散系数,将近表面水合层内扩散的分子水量转换为经过的时间。对透明考古样品进行的红外光谱透射测量记录了近红外区域水带的振动响应,从而可以确定结构水含量(OH)和扩散的环境水(H2O)量。在本应用中,直接测量了 5200 cm-1 处的 H2O 水带。通过评估各变量的精确度来评估该方法的准确性。使用阿根廷萨拉曼卡洞穴放射性碳年代沉积物中的黑曜石文物对新方案进行了评估。
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引用次数: 0
Taking shape: A new geometric morphometric approach to quantifying dental fluctuating asymmetry and its application to the evaluation of developmental stress 成形:量化牙齿波动不对称的新几何形态计量学方法及其在发育压力评估中的应用
IF 1.6 3区 地球科学 Q1 Arts and Humanities Pub Date : 2024-05-15 DOI: 10.1111/arcm.12973
Ben Wigley, Eleanor Stillman, Elizabeth Craig‐Atkins
Although evaluating developmental stress is challenging, it is critical to understanding phenotypic adaptation and differentials in morbidity and mortality related to spatiotemporal variation in environmental and cultural factors. This paper presents a new, reproducible, and reliable geometric morphometric (GM) protocol through which stress‐induced deviations to symmetry, known as fluctuating asymmetry (FA), can be robustly quantified. A case study, in which maternally mediated early‐life stress in human skeletal remains is explored through first permanent molar (M1) FA, illustrates the method's effectiveness and wide‐ranging potential to revolutionise the investigation of themes such as stress intensity, developmental processes, and buffering mechanisms in past populations.
尽管评估发育压力具有挑战性,但它对于了解表型适应以及与环境和文化因素时空变化相关的发病率和死亡率差异至关重要。本文介绍了一种新的、可重复的、可靠的几何形态计量(GM)方案,通过该方案,可对压力引起的对称性偏差(即波动不对称(FA))进行稳健的量化。一项案例研究通过第一恒磨牙(M1)FA探讨了人类骨骼遗骸中由母体介导的早期生活压力,说明了该方法的有效性和广泛潜力,可以彻底改变对过去人群的压力强度、发育过程和缓冲机制等主题的研究。
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引用次数: 0
Geochemical signature identifying features and archaeological structures in eastern Amazonian Terra Preta sites 确定亚马逊东部 Terra Preta 遗址特征和考古结构的地球化学特征
IF 1.6 3区 地球科学 Q1 Arts and Humanities Pub Date : 2024-05-14 DOI: 10.1111/arcm.12977
Majd Nidal Aboul Hosn, Bruno Apolo Miranda Figueira, Paulo Sérgio Taube Junior, José Francisco Berredo Reis da Silva, B. Archanjo, Kashif Gul, Sumeet Malik, M. L. da Costa
The present work describes the chemistry and mineralogy of soils such as Terra Preta Arqueológica (TPA) or Terra Preta de Índio (TPI) from the Bitoca I and II sites, located in the Salobo Region (Carajás Mineral Province, Pará‐Brazil). The results revealed chemical and mineralogical characteristics that are similar to other TPAs found throughout the Amazon region, such as relatively high levels of Ca (average of 3600 ppm), P (average of 850 ppm), Mn (average of 730 ppm), Zn (average of 55 ppm), and Cu (average of 63 ppm). In soils related to the characteristics of occupation by huts and campfires, the mineralogical composition is represented by quartz, kaolinite, calcite, muscovite, anatase, hematite, goethite, and gibbsite. Amorphous phases have also been identified mainly as calcium phosphates and organic matter (humic and fulvic acids). The analysis of the features/structures described here helped in the identification/verification of areas destined for different activities within the sites.
本研究描述了位于萨洛博地区(巴西帕拉州卡拉哈斯矿产省)比托卡 I 号和 II 号矿址中的 "Terra Preta Arqueológica (TPA) "或 "Terra Preta de Índio (TPI) "等土壤的化学和矿物学特征。研究结果表明,这些土壤的化学和矿物学特征与整个亚马逊地区发现的其他 TPA 相似,如钙(平均含量为 3600 ppm)、磷(平均含量为 850 ppm)、锰(平均含量为 730 ppm)、锌(平均含量为 55 ppm)和铜(平均含量为 63 ppm)含量相对较高。在与小屋和篝火占用特征有关的土壤中,矿物成分主要有石英、高岭石、方解石、麝香石、锐钛矿、赤铁矿、鹅铁矿和辉绿岩。此外,还发现了无定形相,主要是磷酸钙和有机物(腐殖酸和富勒酸)。对此处描述的特征/结构的分析有助于确定/核实遗址内用于不同活动的区域。
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引用次数: 0
Human ancient DNA analysis in Latin America: Current state and challenges 拉丁美洲的古人类 DNA 分析:现状与挑战
IF 1.6 3区 地球科学 Q1 Arts and Humanities Pub Date : 2024-05-14 DOI: 10.1111/arcm.12979
Constanza de la Fuente Castro, Gonzalo Figueiro
Ancient DNA analysis has greatly contributed to understanding the population history of several species. In the last 20 years, the field has undergone an important transformation: particularly in our species, thousands of ancient genomes have been analyzed worldwide, providing evidence of population movements and interactions through time. However, several researchers have raised concerns about the way the field is developing and how collaborations are being established. In this work, we describe and evaluate the situation in Latin America, considering both what we have learned about population history through paleogenetics and how it has developed in the region.
古 DNA 分析为了解一些物种的种群历史做出了巨大贡献。在过去的 20 年里,这一领域发生了重大转变:特别是在我们这个物种中,全世界已有数千个古基因组得到分析,为不同时期的种群迁移和相互作用提供了证据。然而,一些研究人员对该领域的发展方式和合作方式提出了担忧。在这项工作中,我们描述并评估了拉丁美洲的情况,同时考虑了我们通过古遗传学对种群历史的了解以及古遗传学在该地区的发展情况。
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引用次数: 0
Petrographic and geochemical analyses of pottery from Wadi Tanuf, Oman: Approaching pottery production in south‐eastern Arabia during the second and first millennia BCE 对阿曼 Wadi Tanuf 出土陶器的岩相学和地球化学分析:公元前二千年至公元前一千年阿拉伯东南部陶器生产的近况
IF 1.6 3区 地球科学 Q1 Arts and Humanities Pub Date : 2024-05-08 DOI: 10.1111/arcm.12974
Takehiro Miki, Taichi Kuronuma, Brandi L. MacDonald, Michael D. Glascock, Yasuhisa Kondo
This study describes the petrographic and geochemical characteristics of pottery collected from Mugharat al‐Kahf and WTN02 in Wadi Tanuf, north‐central Oman, to clarify interregional similarities and differences in pottery production techniques and examine the existence of interregional trade in pottery with respect to changes in mobile communities. Potsherds from these sites were characterised using thin‐section petrography and instrumental neutron activation analysis. Results revealed that several clay fabrics and tempers were used during the Wadi Suq period (2000–1600 BCE). A region‐wide similarity exists in pottery‐making techniques in terms of the tempering of specific minerals (Oman ophiolite) used in the Early Iron Age (1300–300 BCE). Geochemical results indicate differences in clay sources between the Wadi Suq period and the Early Iron Age in Wadi Tanuf and the unlikelihood of the interregional trade of domestic pottery.
本研究描述了从阿曼中北部塔努夫谷的 Mugharat al-Kahf 和 WTN02 采集的陶器的岩石学和地球化学特征,以澄清陶器制作技术的地区间异同,并研究陶器的地区间贸易是否与移动群落的变化有关。利用薄片岩石学和仪器中子活化分析对这些遗址出土的陶器进行了特征描述。结果显示,在瓦迪苏克时期(公元前 2000-1600 年),人们使用了多种粘土结构和温度。就早期铁器时代(公元前 1300-300 年)使用的特定矿物(阿曼蛇绿岩)的调质而言,整个地区的制陶技术存在相似性。地球化学研究结果表明,瓦迪苏克时期与瓦迪塔努夫早期铁器时代的粘土来源不同,不可能存在地区间的家庭陶器贸易。
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引用次数: 0
Microbotanical analysis in artifacts of the CABUZA phase (900–1200 ce), Azapa Valley, northern Chile: Vessels and rites of “eating and drinking with the dead” in post‐Tiwanaku times 智利北部阿扎帕山谷卡布扎阶段(公元前 900-1200 年)文物中的微生物分析:后提瓦纳库时代的容器和 "与死者同吃同喝 "仪式
IF 1.6 3区 地球科学 Q1 Arts and Humanities Pub Date : 2024-05-08 DOI: 10.1111/arcm.12972
Juan Pablo Ogalde, Fiorella Valeria Villanueva, Luis Ramón Huaman Mesía, Natalia Carolina Aravena Sanchez
We report observations of wear traces and microbotanical analysis of 29 ceramics, one pot of Cucurbita sp., and one wooden spoon—all artifacts of the AZ‐6 and AZ‐71 cemeteries of the Cabuza cultural phase (900–1200 ce), Azapa Valley, northern Chile—. The results show some unused artifacts (11) besides 21 samples that were positive for starches of Zea mays, Cucurbita sp., Manihot esculenta, Ipomoea batatas, or Phaseolus sp., in addition to vegetable remains (13 cases). This evidence is interpreted as an expression of funerary rites in post‐state times, which could be an inheritance of the Andean Tiwanaku State (ca. 500–1000 ce).
我们报告了对智利北部阿萨帕山谷卡布萨文化阶段(公元前 900-1200 年)AZ-6 和 AZ-71 墓地出土的 29 件陶瓷器、一个葫芦罐和一个木勺的磨损痕迹观察和微生物分析结果。研究结果表明,除了 21 个样本对玉米、葫芦属、马尼荷属、红苕属或相思豆属淀粉呈阳性反应外,还有一些未使用过的人工制品(11 件),此外还有蔬菜残留物(13 件)。这一证据被解释为后国家时代丧葬仪式的一种表现形式,可能是对安第斯提瓦纳库国家(约公元前 500-1000 年)的继承。
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引用次数: 0
A medium‐throughput approach for improved taxonomic identification of lipids preserved in ancient pottery 改进古陶器中保存的脂质分类鉴定的中等通量方法
IF 1.6 3区 地球科学 Q1 Arts and Humanities Pub Date : 2024-05-07 DOI: 10.1111/arcm.12976
Léa Drieu, Jasmine Lundy, Rachel K. Smith, Ed Bergström, Helen Talbot, Milena Primavera, Girolamo Fiorentino, Oliver E. Craig, Jane Thomas‐Oates
Organic residue analysis (ORA) is a valuable tool for the study of ancient diets, but conventional methods remain limited in terms of taxonomic identification or to resolve mixtures. Here, we propose a method to further explore a class of compounds—triacylglycerols (TAGs)—using high‐resolution mass spectrometry to overcome these limitations in an attempt to better characterise culinary practices. Over 70 medieval Sicilian pots and a wide range of authentic fresh products were studied by matrix‐assisted laser desorption/ionisation–mass spectrometry (MALDI‐MS and MALDI‐MS/MS). MALDI‐MS analysis can distinguish fresh foodstuffs but provides little additional information regarding the contents of archaeological pottery compared to conventional ORA methods. In contrast, product ion analyses were able to deconvolute a range of animal carcass fat mixtures. In addition, detailed analysis of the composition of saturated T44 and unsaturated T50–T54 TAGs was able to provide greater taxonomic resolution regarding dairy products and plant oils.
有机残留物分析(ORA)是研究古代饮食的重要工具,但传统方法在分类鉴定或解决混合物方面仍然存在局限性。在此,我们提出了一种利用高分辨率质谱进一步探索三酰甘油(TAGs)这类化合物的方法,以克服这些局限性,尝试更好地描述烹饪方法。研究人员利用基质辅助激光解吸/电离质谱(MALDI-MS 和 MALDI-MS/MS)对 70 多种中世纪西西里锅和各种地道的新鲜产品进行了研究。与传统的 ORA 方法相比,MALDI-MS 分析可以区分新鲜食品,但对考古陶器的内容提供的额外信息很少。与此相反,产物离子分析能够解构一系列动物尸体脂肪混合物。此外,对饱和 T44 和不饱和 T50-T54 TAGs 成分的详细分析能够提供有关乳制品和植物油的更高分类分辨率。
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引用次数: 0
XRF Analysis of Village and Urban Basalt Architecture in the Hippos Territorium during the Roman Period 对罗马时期希波斯领地村庄和城市玄武岩建筑的 XRF 分析
IF 1.5 3区 地球科学 N/A ARCHAEOLOGY Pub Date : 2024-04-29 DOI: 10.1111/arcm.12975
Mechael Osband, Michael Eisenberg, Jeffery R. Ferguson

This case study examines the use of X-ray fluorescence (XRF) as an effective method for defining distinct chemical compositions of local basalt stone from different sources in the Roman period, even when their quarries have not been identified. It also deals with the archaeological question if public and monumental structures from a village and urban site shared the same stone sources and stonemason's workshops. Ninety-six samples from the Hippos Territorium, mainly from the polis of Hippos and the village of Majduliyya, were analyzed. XRF was found to be an effective method for defining distinct chemical compositions of local basalt materials from different sources. The distinct composition of the basalt stones between the two sites provided valuable insights into socio-economic relationships, shedding light on the nature of city–village dynamics in the region. Additionally, it aids in discerning whether diverse basalt sources were utilized in both private and public constructions, as well as installations within a single site. Methodological questions and the application of this method in the archaeological research of basalt-based architecture are also addressed.

本案例研究将 X 射线荧光 (XRF) 作为一种有效方法,用于确定罗马时期不同来源的当地玄武岩石材的不同化学成分,即使这些石材的采石场尚未确定。该研究还涉及一个考古问题,即一个村庄和城市遗址的公共建筑和纪念性建筑是否共享相同的石料来源和石匠作坊。对来自希波斯领地的 96 块样本进行了分析,这些样本主要来自希波斯市镇和 Majduliyya 村。研究发现,XRF 是确定当地不同来源玄武岩材料不同化学成分的有效方法。两个遗址之间不同的玄武岩石头成分为了解社会经济关系提供了宝贵的信息,揭示了该地区城市-村庄动态的本质。此外,它还有助于辨别私人和公共建筑以及单一遗址内的装置是否使用了不同的玄武岩资源。此外,还探讨了方法问题以及该方法在玄武岩建筑考古研究中的应用。
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引用次数: 0
The emperor's new glass: The introduction of Carolingian wood ash glass in North Sea trade 皇帝的新玻璃北海贸易中卡洛林木灰玻璃的引入
IF 1.6 3区 地球科学 Q1 Arts and Humanities Pub Date : 2024-04-11 DOI: 10.1111/arcm.12968
Gry H. Barfod, Lene L. Feveile, Søren M. Sindbæk

Micro-X-ray fluorescence (XRF) screening of 244 glass sherds from Ribe, Denmark, identified 23 wood ash glasses. The closely dated finds pinpoint the arrival of the earliest wood ash glass produced in Western Europe in this important North Sea trading hub. This glass type was absent among glass from 700 to 790 CE but feature strongly from 790 to 810 CE. Electron microprobe analysis (EMPA) and laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) analysis of 24 glasses show the presence of four types. We show the strengths of classifying wood ash glass based on the glass-producing sands and conclude that the earliest production took place on a considerable scale and had a major impact on glass circulation in Northern Europe in the ninth century.

对来自丹麦里贝的 244 块玻璃碎片进行了显微 X 射线荧光 (XRF) 筛选,确定了 23 块木灰玻璃碎片。这些年代严谨的发现确定了西欧最早的木灰玻璃是在这个重要的北海贸易中心出产的。这种玻璃在公元 700 年至 790 年期间并不常见,但在公元 790 年至 810 年期间却很有特色。对 24 种玻璃进行的电子微探针分析(EMPA)和激光烧蚀电感耦合等离子体质谱分析(LA-ICP-MS)显示出四种类型。我们展示了根据玻璃生产砂对木灰玻璃进行分类的优势,并得出结论:最早的生产规模相当大,对九世纪北欧的玻璃流通产生了重大影响。
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引用次数: 0
Firing technology and physicochemical basis for porcelain from the Xing kiln in the late sixth century 六世纪末邢窑瓷器的烧造技术和理化基础
IF 1.6 3区 地球科学 Q1 Arts and Humanities Pub Date : 2024-04-02 DOI: 10.1111/arcm.12969
Ruofei Zong, Xiaoke Lu, Weidong Li, Changsong Xu
The rise of porcelain industry in northern China and the subsequent emergence of white porcelain production during the Northern dynasties (386–581 CE) played a pivotal role in shaping the historical trajectory of Chinese ceramics. Xing kiln is one of China's earliest and most representative white porcelain kilns. Herein, we investigated 23 porcelain sherds from the Neiqiu Xing kiln site during the late Northern dynasties and the early Sui dynasty (550–600 CE) from the perspective of firing temperature, firing atmosphere, and microstructure using a dilatometer, X‐ray photoelectron spectroscopy, and scanning electron microscopy. The results show that the early Xing porcelains were fired at high firing temperatures exceeding 1200°C with a reducing flame, and the adjustment of temperature promotes the emergence of early white porcelain. Moreover, the higher firing temperature of early Xing porcelain leads to the dominance of a glassy phase within the glaze, and the high bonding strength of the glaze and body caused by the body–glaze interaction layer formed with dense anorthite crystals. Overall, these findings provide valuable insights into the firing technology in the Xing kiln and even in North China during the late sixth century.
北朝时期(公元 386-581 年),中国北方制瓷业的兴起以及随后出现的白瓷生产在塑造中国陶瓷历史轨迹方面发挥了举足轻重的作用。邢窑是中国最早、最具代表性的白瓷窑之一。在此,我们使用扩张仪、X射线光电子能谱和扫描电子显微镜,从烧成温度、烧成气氛和微观结构的角度,对内邱邢窑遗址出土的23件北朝晚期和隋朝早期(公元550-600年)的瓷器碎片进行了研究。结果表明,早期邢瓷是在超过 1200°C 的高温下用还原焰烧成的,温度的调节促进了早期白瓷的出现。此外,早期邢瓷的烧成温度较高,导致釉内玻璃相占优势,釉与胎体的结合强度较高,这是因为胎体与釉的相互作用层中形成了致密的阳起石晶体。总之,这些发现为了解六世纪晚期邢窑乃至华北地区的烧制技术提供了宝贵的信息。
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引用次数: 0
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Archaeometry
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