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Sensitivity and Specificity of Various Techniques for the Trace Elemental Analysis on Teeth: A Critical Review 各种牙齿微量元素分析技术的敏感性和特异性综述
Pub Date : 2018-08-11 DOI: 10.17063/bjfs7(4)y2018230
Monika Singh, J. Sehrawat, Vishal Sharma
Trace elements play an important and complex role in the human metabolism and, although present in only minute concentrations, can be either beneficial or detrimental to health. Qualitative and quantitative analyses of the trace elements from human teeth are performed using various methods. Atomic absorption spectroscopy (AAS) and Inductively coupled plasma atomic emission spectroscopy (or mass spectroscopy) (ICP-AES, MS) are the most popular methods for trace element analysis Previous studies have set the framework for developing methods aimed at elemental analysis from bones and teeth but there are areas in which the field still needs to progress. Research must be undertaken to expand the techniques to include more precision, non-destructiveness and accuracy and high detection limit, including additional human bones and teeth, non-human bones and teeth, non-skeletal materials, and to trace present and past life behaviours like migration pattern, nutrition status and occupational or environmental exposure, human provenance and reconstruction of migration pathways as well substance abuse in human skeletal remains and in living beings.
微量元素在人体代谢中起着重要而复杂的作用,虽然浓度极低,但对健康可能有益,也可能有害。对人类牙齿中的微量元素进行了多种方法的定性和定量分析。原子吸收光谱(AAS)和电感耦合等离子体原子发射光谱(或质谱)(ICP-AES, MS)是最流行的微量元素分析方法,以前的研究已经为开发针对骨骼和牙齿的元素分析方法建立了框架,但该领域仍有许多领域需要改进。必须进行研究以扩大技术,使其包括更精确、非破坏性和准确性以及更高的检测限度,包括更多的人类骨骼和牙齿、非人类骨骼和牙齿、非骨骼材料,并追踪现在和过去的生活行为,如迁移模式、营养状况和职业或环境暴露、人类来源和迁移途径的重建以及人类骨骼遗骸和生物的药物滥用情况。
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引用次数: 2
NBOMe Designer Drugs: GC-MS and LC-QTOF/MS Detection on Blotter Paper by Brazilian Federal Police (Rio Grande do Sul, Brazil) 巴西联邦警察对吸墨纸的GC-MS和LC-QTOF/MS检测(南里奥格兰德州)
Pub Date : 2018-06-24 DOI: 10.17063/BJFS7(3)Y2018193_2
C. A. Wayhs, M. Reis, K. Mariotti, W. Romão, B. Vaz, F. Barreto, R. S. Ortiz, R. Limberger
The NBOMes are classified as new psychoactive substances and have recently become popular as drugs of abuse, being associated with several intoxication cases and even deaths, leading to its ban in several countries. Until now, the most widely used analytical instrument among forensic laboratories in Brazil is GC-MS. In this study, this instrumentation was employed for routine analyzes of twenty blotter paper seizure by Brazilian Federal Police (BFP) in the southernmost state of the country. However, to acquire more information about these samples, LC-QTOF/MS was used as a supplementary analysis to determinate degradation products, metabolites and unknown compounds. The GC-MS analysis detected only 25B-NBOMe, while the LC-QTOF/MS analysis detected 25B-NBOMe, 2C-B and MDMA. The compounds found in these analyzes are quite different from that found 194 Brazilian Journal of Forensic Sciences, Medical Law and Bioethics 7(3):193-204 (2018) C. A. Y. Wayhs et al. in the national profile of seizures by BFP, suggesting that another rout or supplier act in this region. For research and drug intelligence purposes the use of more versatile, sensitive and specific analytical tool provides a greater number of information that could be employed as a valuable strategy in the drug trafficking combat.
nhomes被归类为新的精神活性物质,最近作为滥用药物流行起来,与几起中毒案件甚至死亡有关,导致若干国家禁止使用nhomes。到目前为止,巴西法医实验室中使用最广泛的分析仪器是GC-MS。在这项研究中,该仪器被用于巴西联邦警察(BFP)在该国最南部州查获的20张吸墨纸的常规分析。然而,为了获得更多关于这些样品的信息,我们使用LC-QTOF/MS作为补充分析来确定降解产物、代谢物和未知化合物。GC-MS分析仅检测到25B-NBOMe, LC-QTOF/MS分析检测到25B-NBOMe、2C-B和MDMA。在这些分析中发现的化合物与在巴西法医学、医学法律和生物伦理学杂志7(3):193-204(2018)中发现的化合物完全不同。C. A. Y. Wayhs等人在BFP缉获的全国概况中发现的化合物表明,该地区有另一个组织或供应商在行动。在研究和毒品情报方面,使用更通用、更敏感和更具体的分析工具可提供更多的信息,这些信息可作为打击毒品贩运的宝贵战略加以利用。
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引用次数: 2
Identificação Papiloscópica em Cadáveres Carbonizados – Considerações Médico Legais e a Importância da Integração Pericial 烧焦尸体的papiloscopic鉴定-法律医学考虑和专家整合的重要性
Pub Date : 2018-06-24 DOI: 10.17063/BJFS7(3)Y2018205_2
A. Silva, Fernando Carvalho dos Santos, Marcelo Mari de Castro, P. Bordoni, L. Bordoni
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引用次数: 4
Decipherment Of Disappeared Ink: A Case Study 解密消失的墨水:一个案例研究
Pub Date : 2018-05-31 DOI: 10.17063/BJFS7(3)Y2018156
Deshpande Hemantini, Mulani Khudbudin
The disappeared or invisible inks are fluids used to for secret writing. These types of inks are revealed by heat, chemical reaction and UV light. Disappearing inks are acid base indicators showing different colours at different pH. Writing with this type of ink disappears after about 65 h. These inks could be used for forging the documents such as agreements, cheques, property documents and other important documents. Many destructive and nondestructive methods are available for forensic decipherment of these disappeared writing. In present communication, a simple nondestructive method is applied for decipherment of disappeared signatures on share transfer agreement and other related documents.
消失或看不见的墨水是用于秘密书写的液体。这些类型的油墨是揭示了热、化学反应和紫外线。消失墨水是一种酸碱指示剂,在不同的ph值下显示不同的颜色。用这种墨水书写约65小时后就会消失。这种墨水可用于伪造文件,如协议、支票、财产文件和其他重要文件。许多破坏性和非破坏性的方法可用于法医破译这些消失的文字。在目前的通信中,对股权转让协议和其他相关文件上的消失签名,采用一种简单的无损方法进行解密。
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引用次数: 2
Interpretação do Padrão das Manchas de Sangue em um Caso de Homicídio em Local Inidôneo 过失杀人案件中血迹模式的解释
Pub Date : 2018-05-31 DOI: 10.17063/bjfs7(3)y2018162
V. W. Botteon
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引用次数: 2
Investigação do Sexo e Idade através de Mensurações em Ossos Occipitais de Crânios Secos de Adultos 通过测量成人干颅骨枕骨来研究性别和年龄
Pub Date : 2018-03-28 DOI: 10.17063/bjfs8(4)y2019178
Brenno Victor dos Santos Nascimento, Marcus Vinícius da Silva, Gabriel Cunha Brito, Erasmo de Almeida Júnior
A Medicina Legal tem grande importância no processo de identificacao humana, principalmente quando os especialistas da area recebem para analise apenas a porcao cefalica do corpo. O objetivo deste estudo e verificar o dimorfismo sexual e a predicao da idade atraves de mensuracoes em ossos occipitais de crânios secos de adultos. Os autores estudaram uma amostra de 149 crânios secos, sendo 90 masculinos e 59 femininos, que pertenceram a individuos com idade acima de 20 anos, e com sexo e idade conhecidos com total seguranca. Foram realizadas as seguintes mensuracoes: distância entre os forames condilares (ifc); distância entre o forame condilar direito e o basio (fcd-b); distância entre o forame condilar esquerdo e o basio (fce-b), alem de uma area triangular formada por estas medidas lineares (atz). Todas as variaveis passaram por uma analise de variância a fim de se testar a existencia de efeito do sexo, alem de que sua normalidade residual foi avaliada pelos coeficientes de assimetria, de curtose e pelo teste de Shapiro-Wilk. De acordo com a analise estatistica, houve indice de acerto de 69,6% por regressao logistica. Foram tambem verificadas estatisticas basicas como a media e intervalo de confianca atraves do teste t e tambem utilizado o metodo da regressao linear multipla para a predicao da idade, constatando que o modelo apresentou resultados significantes em duas variaveis. (p=0,0105). Os resultados permitiram a elaboracao de metodologia estatistica para o diagnostico do sexo e idade em observacoes futuras.
法医学在人体识别过程中具有重要意义,特别是当该领域的专家只接受头部部分的分析时。本研究的目的是通过测量成年干颅骨枕骨来验证性别二态性和年龄预测。作者研究了149个干颅骨样本,其中男性90个,女性59个,年龄在20岁以上,性别和年龄完全确定。进行以下测量:髁突孔之间的距离(ifc);右髁孔与基底孔距离(fcd-b);左髁突孔与基底孔之间的距离(fce-b),以及由这些线性测量(atz)形成的三角形区域。对所有变量进行方差分析,以检验是否存在性别效应,并通过不对称系数、峰度和夏皮罗-威尔克检验评估其残差正态性。根据统计分析,物流回归的准确率为69.6%。通过t检验验证了基本统计数据的均值和置信区间,并对年龄预测采用多重线性回归方法,发现模型在两个变量上显示了显著的结果。(p = 0105)。结果允许在未来观察中发展诊断性别和年龄的统计方法。
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引用次数: 1
La hermenéutica-dialéctica como método de análisis cualitativo en enfermería 解释学-辩证法作为护理中的定性分析方法
Pub Date : 2018-03-17 DOI: 10.17063/BJFS7(2)Y2018123
V. F. R. Nava, C. A. A. Ventura, L. Casique, A. Castañón
The hermeneutic-dialectical analysis is a method that a nursing researcher uses consciously or unconsciously during the process of qualitative data analysis. This method begins as a proposal by Jurgen Habermas in his dialogue with Gadamer in order to show him that the universality of hermeneutics is in reason when the subject is capable of criticizing tradition and authority with an overview to transform reality. In isolation, the concept of hermeneutics has suffered a semantic metamorphosis in historical events; being an art or theory in explaining, translating or interpreting biblical, philosophical and legal texts, until it becomes a philosophical school characterized by the idea: “Truth is the fruit of interpretation. Alternatively, dialectic considers the art of conversation, dialogue, difference, opposition, discrepancy, controversy or argumentation. Dialectic is a branch of philosophy that confirms conflict between two judgments, generating these a final product named the resulting process. Because of this, when considering the advantages and disadvantages of both methods, Habermas remarks that his proposal of Hermeneutic-Dialectic analysis seeks the interpretation of hermeneutics with the critical application of dialectic, that within the qualitative data analysis in nursing, can be used to discover resemblances, inconsistencies, as well as being interpretative and critical in generating knowledge inside the nursing profession.
诠释-辩证分析是护理研究者在定性数据分析过程中自觉或不自觉使用的一种方法。这种方法始于尤尔根·哈贝马斯在与伽达默尔的对话中提出的一种建议,目的是向伽达默尔表明,当主体能够批判传统和权威时,解释学的普遍性就在理性中,并以一种概观来改造现实。孤立地说,解释学的概念在历史事件中遭受了语义的变形;成为解释、翻译或解释圣经、哲学和法律文本的一门艺术或理论,直到它成为一个哲学流派,其特点是:“真理是解释的成果。”另外,辩证法考虑的是谈话、对话、差异、反对、矛盾、争议或论证的艺术。辩证法是哲学的一个分支,它证实两种判断之间的冲突,产生最终的产物,称为结果过程。正因为如此,在考虑两种方法的优缺点时,哈贝马斯评论说,他提出的解释学-辩证法分析寻求解释学的解释,批判性地应用辩证法,在护理的定性数据分析中,可以用来发现相似之处,不一致之处,以及在护理专业内部产生知识的解释性和批判性。
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引用次数: 1
Abuso Sexual em Adultos: Casuística do Posto Médico-Legal de Ribeirão das Neves - Minas Gerais 成人性虐待:ribeirao das Neves - Minas Gerais医疗法律站的案例研究
Pub Date : 2018-03-17 DOI: 10.17063/bjfs7(2)y2018137
P. Bordoni, N. R. Gomes, R. Horta, L. Bordoni
Sexual violence is present throughout the world, affects both sexes and occurs in all cultures and social classes. Women are the main victims of sexual abuse (SA), considered a major public health problem. In cases of SA, the medical examiner has the role of searching for objective medical evidence, in addition to participating in the integrated network of victim care. The objective of this research was to analyze the forensic reports of SA in a specific geographic context, to better understand the characteristics of the victims and the forensic findings. The forensic reports of SA victims who were 18 years of age or older examined in Ribeirao das Neves Institute of Forensic Medicine between 2015 and 2016 were analyzed. All of them were female, totaling 11.6 % of the 242 forensic reports of SA completed in the period. The average age was 28 years, vaginal intercourse was the most common practice and in half the cases the abuse was committed by strangers. Most had no genital lesions and none had anal lesions. There were extragenital lesions in half of the cases. In most reports the recent occurrence of vaginal intercourse could not be demonstrated. These data add epidemiological information for better understanding the profile of the SA adult victim, and may contribute to the establishment of possible intervention and prevention measures.
性暴力在世界各地都存在,影响到两性,发生在所有文化和社会阶层。妇女是性虐待的主要受害者,性虐待被认为是一个重大的公共卫生问题。在意外伤害案件中,法医除了参与受害者护理的综合网络外,还有寻找客观医学证据的作用。本研究的目的是分析特定地理背景下SA的法医报告,以更好地了解受害者的特征和法医调查结果。分析了2015年至2016年在Ribeirao das Neves法医研究所检查的18岁及以上SA受害者的法医报告。在此期间完成的242份SA法医报告中,全部为女性,占11.6%。他们的平均年龄是28岁,阴道性交是最常见的行为,其中一半的虐待是由陌生人实施的。大多数患者没有生殖器病变,也没有肛门病变。一半的病例有外阴病变。在大多数报告中,不能证明最近发生的阴道性交。这些数据增加了流行病学信息,有助于更好地了解SA成人受害者的概况,并可能有助于建立可能的干预和预防措施。
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引用次数: 2
O Tratamento da Dependência Química e os Direitos Humanos 药物依赖治疗与人权
Pub Date : 2018-03-06 DOI: 10.17063/bjfs7(2)y2018113
D. Silva, Marciana Fernandes Moll, C. Ventura
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引用次数: 0
Mortalidade de Mulheres em Idade Fértil por Causas Externas: Análise de 2274 Necropsias do IML-BH 外因育龄妇女死亡率:2274例IML-BH尸检分析
Pub Date : 2017-12-17 DOI: 10.17063/BJFS7(1)Y201752
P. Bordoni, Alice de Sá Gontijo Silva, Ana Carolina Fernandes Monteiro, Luciana de Resende Neiva, Talita Alvarenga Petrini Carvalho, W. Marinho, L. Bordoni
Female mortality presents important peculiarities in relation to the male, especially when studying the deaths due to external causes (DDEC). These are the third most important cause of death among women in Brazil. Considering the importance of DDEC for the criminal forensic sciences as well as the deficiency of national information involving necroscopic studies with these causes of death in women of reproductive age group (RAG), this research aimed to evaluate its epidemiological profile at the Forensic Medicine Institute of Belo Horizonte (FMI-BH). A descriptive and retrospective study was carried out in which the RAG women autopsied in the FMI-BH were evaluated in the period from 2006 to 2012. The 2,274 RAG autopsy reports in the period corresponded to 5.39% of the total necropsies and to 24.8 % of female autopsies performed in FMI-BH. This sample accounted for 67.8% of the total number of women victims of violent death necropsied in the same period. The mean age was 29.4 years, the majority had brown skin and 79.6% were single, widowed or legally separated. The most frequent circumstance of death was homicide (42%) and suicide the second (33%). Alcohol was found in 25.1% of the cases. In the positive cases for the toxicological examination, cocaine and marijuana were the most found substances. Together, these data better define the epidemiological profile of deaths due to external causes in women of childbearing age, contributing in the elaboration of intervention and prevention strategies.
与男性相比,女性死亡率呈现出重要的特点,特别是在研究外因死亡(DDEC)时。这是巴西妇女死亡的第三大原因。考虑到DDEC对刑事法医科学的重要性,以及缺乏涉及对育龄妇女这些死因进行尸检研究的国家信息,本研究旨在评估贝洛奥里藏特法医研究所(FMI-BH)的流行病学概况。对2006年至2012年期间在FMI-BH尸检的RAG妇女进行了描述性和回顾性研究。在此期间,2,274例RAG尸检报告占总尸检报告的5.39%,占FMI-BH女性尸检报告的24.8%。这一样本占同期死于暴力死亡的女性受害者尸体总数的67.8%。平均年龄为29.4岁,大多数为棕色皮肤,79.6%为单身、丧偶或合法分居。最常见的死亡原因是他杀(42%)和自杀(33%)。在25.1%的病例中发现了酒精。在毒理学检查呈阳性的病例中,可卡因和大麻是发现最多的物质。总之,这些数据更好地界定了育龄妇女因外因死亡的流行病学概况,有助于制定干预和预防战略。
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引用次数: 0
期刊
Brazilian Journal of Forensic Sciences, Medical Law and Bioethics
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