This study aims to investigate the influences of temperature and critical additives (suspension aid and dispersant) on the rheological performances of oil well cement slurries. A high-temperature and high-pressure rheometer was used to evaluate the rheology of high-temperature cement slurries at eight different temperatures (30 °C, 60 °C, 90 °C, 120 °C, 150 °C, 180 °C, 210 °C and 220 °C) using multiple “ramp and hold” testing schemes. Test results reveal that almost all slurries exhibit thermal thinning and shear thinning behavior and that the shear thinning effect is enhanced at high temperatures. However, increases in slurry viscosity with increasing temperature at certain temperature ranges are also observed, typically at relatively low shear rates (<100 s−1), which can be attributed to both structural changes of polymer additives and cement hydration reactions. Apparent viscosity of cement slurries generally increases with increasing dosage of suspension aid and decrease with increasing dosage of dispersant. It is found that all the seven rheological models investigated in this study fit well with the experimental results at temperatures between 30 °C and 120 °C, but the fitting quality deteriorates at higher temperatures, especially for the two-parameter models (such as the Bingham-plastic and Power-law models). The three-parameter Hershel-Bulkley (H-B) model is observed to provide the best fitting quality to experimental data at all temperatures. The variations of all three H-B model parameters as functions of temperature can be divided into two stages (30 °C–120 °C and 150 °C–220 °C) due to increases in slurry viscosity at approximately 150 °C and each stage can be fitted reasonably well with a quadratic equation. The yield stress obtained by the H-B model typically show an increasing trend with increasing temperature and increasing dosage of suspension aid. The rheology test results of water solutions of pure suspension aid and dispersant exhibit apparent different behaviors compared to that of cement slurries, which can be attributed to the influences of cement hydration as well as its interactions with cement additives.
扫码关注我们
求助内容:
应助结果提醒方式:
