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Failure of Inconel 600 Thin-Walled Tubes Due to Nitriding 氮化导致的铬镍铁合金600薄壁管失效
Pub Date : 1900-01-01 DOI: 10.31399/asm.fach.power.c9001676
M. Griffiths, J. Slade, A. McDonald
The self-powered flux detectors used in some nuclear reactors are Pt or V-cored co-axial cables with MgO as an insulator and Inconel 600 as the outer sheath material. The detectors are designed to operate in a He atmosphere; to maximize the conduction of heat (generated from the interaction with gamma radiation) and to prevent corrosion. A number of failures have occurred over the years because of a loss of the He cover gas in the assembly. This has resulted in either acid attack on the Inconel 600 sheath in a wet environment or gaseous corrosion in a dry environment. In the latter case, nitriding and embrittlement occurred at temperatures as low as 300 to 400 deg C (determined from an examination of the oxidation of the Zircaloy-2 carrier rod on which the detectors were mounted). Recent results are described and discussed in terms of the oxidation and nitriding kinetics of Zircaloy-2 and Inconel 600, respectively.
一些核反应堆中使用的自供电磁通探测器是铂芯或v芯同轴电缆,以氧化镁为绝缘体,英科乃尔600为外护套材料。这些探测器被设计成在氦大气中工作;最大限度地传导热量(与伽马辐射相互作用产生)并防止腐蚀。多年来,由于组件中He盖气体的损失,发生了许多故障。这将导致在潮湿环境中对Inconel 600护套的酸腐蚀或在干燥环境中对Inconel 600护套的气体腐蚀。在后一种情况下,氮化和脆化发生在低至300至400℃的温度下(通过检查安装探测器的锆合金2载体棒的氧化情况确定)。本文分别从锆合金-2和铬镍铁合金- 600的氧化和氮化动力学的角度对最近的研究结果进行了描述和讨论。
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引用次数: 0
Evaluation of the Vent Header Crack at Edwin I. Hatch Unit #2 Nuclear Power Station 埃德温·哈奇2号机组泄气口裂缝评价
Pub Date : 1900-01-01 DOI: 10.31399/asm.fach.power.c9001146
C. Czajkowski
A metallurgical failure analysis was performed on pieces of the cracked vent header pipe from the Edwin I. Hatch Unit 2 Nuclear power plant. The analysis consisted of optical microscopy, chemical analysis, mechanical Charpy impact testing, and fractography. It was found that the material of the vent header met the mechanical and chemical properties of ASTM A516 Grade 70 carbon-manganese steel material and microstructures were consistent with this material. Fracture faces of the cracked pipe were predominantly brittle in appearance with no evidence of fatigue contribution. The NDTT (Nil ductility Transition Temperature) for this material was approximately -51 deg C (-60 deg F). The fact that the material's NDTT was significantly out of the normal operating range of the pipe suggested an impingement of low temperature nitrogen (caused by a faulty torus inerting system) induced a thermal shock in the pipe which, when cooled below its NDTT, cracked in a brittle manner.
对埃德温·哈奇核电站2号机组通风管断裂件进行了冶金失效分析。分析包括光学显微镜、化学分析、机械夏比冲击试验和断口学。结果表明,该排气总管材料符合ASTM A516 70级碳锰钢材料的力学和化学性能,显微组织与该材料一致。裂纹管的断口表面以脆性为主,无疲劳作用。该材料的NDTT(零延性转变温度)约为-51摄氏度(-60华氏度)。事实上,材料的NDTT明显超出了管道的正常工作范围,这表明低温氮气的撞击(由有缺陷的环面惯性系统引起)在管道中引起了热冲击,当冷却到NDTT以下时,管道以脆性方式破裂。
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引用次数: 0
Field Metallography Aids NDT of Evaluation of Indications in Turbine Main Column Horizontal Plate Welds at Power Plant 现场金相分析有助于电厂汽轮机主柱水平钢板焊缝的无损检测评价
Pub Date : 1900-01-01 DOI: 10.31399/asm.fach.power.c9001661
D. Diaz, S. Benson
An evaluation of indications in the main turbine building column horizontal plate welds was conducted by the joint efforts of field metallography and nondestructive examinations. The turbine building main column horizontal plate welds were selected at random and were inspected to find discontinuities, metallurgical evaluation of the discontinuities, analysis of any failure modes, and determination of the best repair techniques. The welds were made with prequalified joints in accordance with AWS D1.1-77 and required only visual inspection. More sensitive inspection methods were applied to the welds in order to better define the indications found with the visual inspections. Cracks were found in 17 field welds and in two test plate welds. The causes of the cracking are related to the weld design and installation procedure. Three field welds were rejected because of the depth of the cracks. The NDT inspections, evaluations, method of field metallography, analysis and conclusions are discussed with recommendations for corrective actions in the following report.
采用现场金相检验和无损检测相结合的方法,对汽轮机主厂房立柱水平钢板焊缝的缺陷进行了评定。随机选取水轮机厂房主柱水平板焊缝,对焊缝进行不连续点检查、不连续点的冶金评价、失效模式分析和最佳修复工艺确定。焊缝采用符合AWS D1.1-77的预审接头,只需要目视检查。为了更好地确定目视检查发现的迹象,对焊缝采用了更灵敏的检查方法。在17个现场焊缝和两个试验板焊缝中发现了裂纹。开裂的原因与焊接设计和安装工艺有关。由于裂纹的深度,三个现场焊缝被拒绝。在下面的报告中讨论了无损检测、评估、现场金相方法、分析和结论,并提出了纠正措施建议。
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引用次数: 0
Analysis of Mercury Diffusion Pumps 汞扩散泵的分析
Pub Date : 1900-01-01 DOI: 10.31399/ASM.FACH.POWER.C9001679
K. Dunn
Several mercury diffusion pump stages in the Tritium Purification process at the Savannah River Site (SRS) have been removed from service for scheduled preventive maintenance. These stages have been examined to determine if failure has occurred. Evidence of fatigue around the flange portion of the pump has been seen. In addition, erosion and cavitation inside the throat of the venturi tube and corrosion on the other surface of the venturi tube has been observed. Several measures are being examined in an attempt to improve the performance of these pumps. These measures, as well as the noted observations, are described. Six stages [two machined (MP) and four electron beam (EB) welded] from the mercury diffusion pumps operating in the Tritium Purification process at SRS have been analyzed to determine their condition after nine months of usage. Several cracks were found around the necked region of the two MP stages. The EB welded stages, however, seemed to perform better in service; only two of four stages showed cracking. The cracking is caused by fatigue that has been enhanced by high stresses and tritium in the flange area. The EB welded stage appears to be a step in the right direction. Since the EB weld is a shrink fit, the surface is in compression, thereby eliminating crack propagation. In addition, shot peening has been employed to produce a compressive material surface since fatigue usually originates at the surface. Pitting was observed down the throat of the venturi. This pitting was caused by cavitation and erosion along the length of the venturi tube. Corrosion and pitting was seen on the exterior walls of the diffuser tubes. Stress-corrosion cracks were observed emanating from these corrosion pits. The corrosion likely occurred from the chloride ions present in the process cooling water. Shot peening is now being used in an attempt to place the outside of the diffuser tube in compression to eliminate the stress-corrosion cracking.
萨凡纳河站点(SRS)氚净化过程中的几个汞扩散泵级已从服务中移除,以进行定期预防性维护。对这些阶段进行了检查,以确定是否发生了故障。泵的法兰部分周围出现了疲劳迹象。此外,还观察到文丘里管喉部内部的侵蚀和空化现象,以及文丘里管另一侧表面的腐蚀现象。为了改进这些泵的性能,正在研究几种措施。文中描述了这些措施以及注意到的观察结果。对SRS氚净化过程中运行的汞扩散泵的六个阶段[两个机械加工(MP)和四个电子束焊接(EB)]进行了分析,以确定其使用9个月后的状况。在两个MP阶段的颈部周围发现了一些裂纹。然而,EB焊接级在使用中似乎表现更好;四个阶段中只有两个阶段出现裂缝。裂纹是由法兰区域的高应力和氚加剧的疲劳引起的。EB焊接阶段似乎是朝着正确方向迈出的一步。由于EB焊接是收缩配合,表面处于压缩状态,从而消除了裂纹扩展。此外,由于疲劳通常起源于表面,因此采用喷丸强化来产生压缩材料表面。在文丘里管的喉部观察到点蚀。这种点蚀是由沿文丘里管长度的空化和侵蚀引起的。扩散管的外壁出现腐蚀和点蚀。在这些腐蚀坑中发现了应力腐蚀裂纹。腐蚀可能是由工艺冷却水中的氯离子引起的。喷丸强化现在正被用于试图将扩散管的外部置于压缩中,以消除应力腐蚀开裂。
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引用次数: 0
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ASM Failure Analysis Case Histories: Power Generating Equipment
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