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A new polyazomethine-based pyrazole moiety and its reinforced nanocomposites @ ZnO for antimicrobial applications. 一种新型聚氮甲基吡唑分子及其增强纳米复合材料 @ ZnO 用于抗菌应用。
IF 1.6 4区 化学 Q3 POLYMER SCIENCE Pub Date : 2024-05-15 eCollection Date: 2024-01-01 DOI: 10.1080/15685551.2024.2352897
Aqilah A Hakami, Hajar S Alorfi, Thoraya A Farghaly, Mahmoud A Hussein

A new class of biologically active polyazomethine/pyrazole and their related nanocomposites, polyazomethine/pyrazole/zinc oxide nanoparticles, have been successfully synthesized through the polycondensation technique in the form of polyazomethine pyrazole (PAZm/Py4-6) and polyazomethine/pyrazole/zinc oxide nanoparticles (PAZm/Py/ZnOa-c). The polymeric nanocomposites were prepared with a 5% loading of zinc oxide nanofiller using the same preparation technique, in addition to the help of ultrasonic radiation. The characteristics of the new polymers, such as solubility, viscometry, and molecular weight, were examined. All the polymers were completely soluble in the following solvents: concentrated sulfuric acid, formic acid, dimethylformamide, dimethyl sulfoxide, and tetrahydrofuran. Furthermore, the weight loss of the polyazomethine pyrazole (4, 5, and 6) at 800 °C was 67%, 95%, and 86%, respectively, which indicates the thermal stability of these polymers. At 800 °C, the polyazomethine/pyrazole/zinc oxide nanoparticles (a, b, and c) lost 74%, 68%, and 75% of their weight, respectively. This shows that adding zinc oxide nanoparticles made these compounds more stable at high temperatures. The X-Ray diffraction pattern of the polyazomethine pyrazole (PAZm/Py4-6) shows a number of sharp peaks with varying intensities. The polymers that were studied had straight crystal structures. Furthermore, the measurements of polyazomethine/pyrazole/zinc oxide nanoparticles (PAZm/Py/ZnOa-c) indicate a good merging of zinc oxide nanoparticles into the matrix of polymers. The antimicrobial activity of polymers and polymer nanocomposites was tested against some selected bacteria and fungi. The synthesized polymer (c) shows the highest activity against the two types of gram-negative bacteria selected. Most tested compounds were found to be effective against gram-positive bacteria except polyazomethine pyrazole (PAZm/Py5) and polyazomethine pyrazole (PAZm/Py6), which do not exhibit any activity. The synthesized polymers and their related nanocomposites were tested for their ability to kill the chosen fungi. All of them were effective against Aspergillus flavus, but only polyazomethine pyrazole (PAZm/Py4) and polyazomethine/pyrazole/zinc oxide (PAZm/Py/ZnOc) were effective against Candida albicans.

通过缩聚技术,成功合成了具有生物活性的新型聚氮甲胺/吡唑及其相关纳米复合材料--聚氮甲胺/吡唑/氧化锌纳米颗粒,即聚氮甲胺吡唑(PAZm/Py4-6)和聚氮甲胺/吡唑/氧化锌纳米颗粒(PAZm/Py/ZnOa-c)。使用相同的制备技术,并在超声波辐射的帮助下,制备了含有 5% 氧化锌纳米填料的聚合物纳米复合材料。对新聚合物的溶解度、粘度和分子量等特性进行了检测。所有聚合物都能完全溶于以下溶剂:浓硫酸、甲酸、二甲基甲酰胺、二甲亚砜和四氢呋喃。此外,聚氮甲基吡唑(4、5 和 6)在 800 ℃ 时的失重率分别为 67%、95% 和 86%,这表明了这些聚合物的热稳定性。800 °C 时,聚氮甲基吡唑/氧化锌纳米颗粒(a、b 和 c)的重量损失分别为 74%、68% 和 75%。这表明添加纳米氧化锌使这些化合物在高温下更加稳定。聚氮甲基吡唑(PAZm/Py4-6)的 X 射线衍射图样显示出一些强度不同的尖锐峰。所研究的聚合物具有平直的晶体结构。此外,聚氮甲基吡唑/氧化锌纳米颗粒(PAZm/Py/ZnOa-c)的测量结果表明,氧化锌纳米颗粒与聚合物基质的结合良好。测试了聚合物和聚合物纳米复合材料对一些特定细菌和真菌的抗菌活性。合成的聚合物 (c) 对所选的两种革兰氏阴性菌的活性最高。除了聚氮甲基吡唑(PAZm/Py5)和聚氮甲基吡唑(PAZm/Py6)没有表现出任何活性外,大多数测试化合物都对革兰氏阳性细菌有效。对合成的聚合物及其相关纳米复合材料杀死所选真菌的能力进行了测试。所有聚合物都对黄曲霉菌有效,但只有聚氮甲基吡唑(PAZm/Py4)和聚氮甲基/吡唑/氧化锌(PAZm/Py/ZnOc)对白色念珠菌有效。
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引用次数: 0
Effect of methyl methacrylate concentrations on surface and thermal analysis of composite polymer polymethylmethacrylates with mesogen reactive RM82 甲基丙烯酸甲酯浓度对带有中间反应物 RM82 的复合聚合物聚甲基丙烯酸酯的表面和热分析的影响
IF 1.6 4区 化学 Q3 POLYMER SCIENCE Pub Date : 2024-04-04 DOI: 10.1080/15685551.2024.2336657
Afrizal, Yusmaniar, Bryan Valentino, Asep Riswoko, Karin Khairunnisa Gumilar
This research report of the synthesis of composite polymers from liquid crystal mesogen reactive (RM82) monomers with Methyl methacrylate (MMA). The purpose of this research is analysis the effect ...
本研究报告介绍了液晶中间反应物(RM82)单体与甲基丙烯酸甲酯(MMA)合成复合聚合物的情况。本研究的目的是分析液晶介质反应(RM82)单体与甲基丙烯酸甲酯(MMA)合成复合聚合物的效果。
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引用次数: 0
Preparation and performance study of waterproof and breathable layer of alginate/aramid-based fabrics and flame-retardant multilayer combination. 藻酸盐/芳纶基织物防水透气层和阻燃多层组合的制备与性能研究。
IF 1.6 4区 化学 Q3 POLYMER SCIENCE Pub Date : 2024-02-19 eCollection Date: 2024-01-01 DOI: 10.1080/15685551.2024.2301804
Xiaoxiao Chen, Min Li, Miao Yu, Yutian Li

Alginate fibers have excellent flame-retardant properties and make up for other material defects by blending. To investigate the influence of the blending ratio of alginate fibers on the flame-retardant properties of waterproof and breathable layers for firefighting suits, this paper utilizes the needle-punching and hot-pressing nonwoven reinforcement processes to prepare waterproof and breathable layers based on alginate/aramid base cloths and conducts a series of performance tests on them. The results show that the char residue content of alginate blended base cloth is significantly improved relative to pure aramid, and the addition of alginate fibers to the base cloth of the waterproof and breathable layer improves its flame retardancy and thermal stability. The overall performance of the alginate/aramid blended base fabric waterproof and breathable layer was better than that of the aramid-based waterproof and breathable layer. Moreover, in the flame-retardant multilayer fabric system for firefighting apparel, the multilayer fabric system containing the alginate/aramid-based waterproof and breathable layer showed higher thermal protection performance. Therefore, the alginate/aramid-based waterproof and breathable layer can enhance the overall flame-retardant performance of firefighting clothing to a certain extent.

海藻酸纤维具有优异的阻燃性能,可通过混纺弥补其他材料的缺陷。为了研究海藻酸纤维的混纺比例对消防服防水透气层阻燃性能的影响,本文利用针刺和热压无纺布加固工艺制备了基于海藻酸/芳纶基布的防水透气层,并对其进行了一系列性能测试。结果表明,与纯芳纶相比,海藻酸盐混纺基布的炭残渣含量明显提高,防水透气层基布中添加海藻酸盐纤维后,其阻燃性和热稳定性均得到改善。海藻酸盐/芳纶混纺基布防水透气层的整体性能优于芳纶基防水透气层。此外,在用于消防服的阻燃多层织物系统中,含有藻酸盐/芳纶基防水透气层的多层织物系统显示出更高的热防护性能。因此,藻酸盐/芳纶基防水透气层可在一定程度上提高消防服的整体阻燃性能。
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引用次数: 0
Construction of a corresponding empirical model to bridge thermal properties and synthesis of thermoresponsive poloxamines. 构建相应的经验模型,以桥接热特性和热致性多羟胺的合成。
IF 1.6 4区 化学 Q3 POLYMER SCIENCE Pub Date : 2024-02-07 eCollection Date: 2024-01-01 DOI: 10.1080/15685551.2024.2313268
Zichun Yan, D Andrew Brown, Trey Alpi, Jiro Nagatomi, O Thompson Mefford

The thermoresponsive properties of poloxamine (tetra-branch PEO-PPO block copolymer) hydrogels are related to several variables. Of particular interest to this study were the molecular weight of the polymer, the molar ratio between PEO and PPO blocks, and the concentration of the aqueous solution. Accurately controlling the thermoresponsive behaviors of the polymer is critical to the application of such materials; therefore, the structure-property relationship of tetra-branch PEO-PPO block copolymer was studied by synthesis via anionic ring-opening polymerization (AROP). The structure-property relationships were studied by measuring the thermoresponsive behavior via differential scanning calorimetry (DSC) and developing an empirical model which statistically fit the collected data. This empirical model was then used for designing poloxamines that have critical micellization temperatures (CMT) between room temperature and physiological temperature. The model was validated with three polymers that targeted a CMT of 308 K (35°C). The empirical model showed great success in guiding the synthesis of poloxamines showing a temperature difference of less than 3 K between the predicted and the observed CMTs. This study showed a great potential of using an empirical model to set synthesis parameters to control the properties of the polymer products.

聚氧乙烯-聚氧丙烯嵌段共聚物)水凝胶的热致伸缩性能与多个变量有关。本研究特别关注聚合物的分子量、PEO 和 PPO 嵌段之间的摩尔比以及水溶液的浓度。精确控制聚合物的热致伸缩行为对此类材料的应用至关重要;因此,通过阴离子开环聚合(AROP)合成法研究了四支 PEO-PPO 嵌段共聚物的结构-性能关系。通过差示扫描量热仪(DSC)测量热致伸缩行为来研究结构-性能关系,并建立了一个经验模型,该模型在统计学上与收集到的数据相匹配。这一经验模型随后被用于设计临界胶束化温度 (CMT) 介于室温和生理温度之间的多羟胺。该模型通过三种聚合物进行了验证,它们的临界胶化温度为 308 K(35°C)。该经验模型在指导多羟胺的合成方面取得了巨大成功,其预测的 CMT 与观察到的 CMT 之间的温差小于 3 K。这项研究表明,使用经验模型来设定合成参数以控制聚合物产品的特性具有很大的潜力。
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引用次数: 0
Synthesis and performance evaluation of temperature and salt-resistant organic/inorganic composite copolymers 耐温耐盐有机/无机复合共聚物的合成与性能评估
IF 1.6 4区 化学 Q3 POLYMER SCIENCE Pub Date : 2023-12-28 DOI: 10.1080/15685551.2023.2296136
Yunbao Zhang, Jiamei Quan, Chengzhou Wang, Wentao Li, Ruofei Du, Hongchao Dong
Ordinary polymers have poor adaptability in high-temperature and high-salt reservoir environments due to their properties. Organic/inorganic composite copolymer microspheres have the advantages of ...
普通聚合物由于其特性,在高温、高盐储层环境中的适应性较差。有机/无机复合共聚物微球具有以下优点:...
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引用次数: 0
Prof. Dr. Yusuf Yagci (1952–2023) 优素福-亚格奇博士教授(1952-2023)
IF 1.6 4区 化学 Q3 POLYMER SCIENCE Pub Date : 2023-12-06 DOI: 10.1080/15685551.2023.2289333
Munmaya Mishra
Published in Designed Monomers and Polymers (Vol. 26, No. 1, 2023)
发表于《设计单体与聚合物》(第 26 卷,第 1 期,2023 年)
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引用次数: 0
3D bioprinted scaffolds of polysaccharide hydrogels in osteochondral and cartilage tissue engineering 骨软骨和软骨组织工程中的多糖水凝胶三维生物打印支架
IF 1.6 4区 化学 Q3 POLYMER SCIENCE Pub Date : 2023-12-01 DOI: 10.1080/15685551.2023.2284482
Jianghong Huang, Zhiwang Huang, Jianyi Xiong, Jiang Xia, Youquan Wang, Lei Yang, Yujie Liang
The construction of bioactive scaffolds with a suitable microenvironment for tissue regeneration provides a great promise for improving clinical treatment of osteochondral and full-thickness articu...
构建具有适宜组织再生微环境的生物活性支架为改善骨软骨和全厚关节的临床治疗带来了巨大希望。
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引用次数: 0
Emulsion copolymerization of vinyl chloride with poly (ethylene glycol) methyl ether methacrylate 氯乙烯与聚乙二醇甲基丙烯酸甲醚的乳液共聚
IF 1.6 4区 化学 Q3 POLYMER SCIENCE Pub Date : 2023-11-27 DOI: 10.1080/15685551.2023.2285087
Ye Jia, Lijun Fan, Changtong Song, Dong Chen, Xianhong Zhang, Yuhong Ma, Wantai Yang
In this work, we reported a novel emulsion copolymerization of vinyl chloride monomer (VCM) with amphipathic monomer poly (ethylene glycol) methyl ether methacrylate (PEGMA) by using sodium dodecyl...
本文报道了一种新型乳液共聚氯乙烯单体(VCM)与两亲性单体聚乙二醇甲基丙烯酸甲醚(PEGMA)的十二烷基钠。
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引用次数: 0
Experimental investigation of the mechanical properties of graphene oxide-silica nanoparticles reinforced rigid polyurethane foam 氧化石墨烯-二氧化硅纳米颗粒增强硬质聚氨酯泡沫材料力学性能的实验研究
IF 1.6 4区 化学 Q3 POLYMER SCIENCE Pub Date : 2023-11-18 DOI: 10.1080/15685551.2023.2281866
Dong Liu, Hailong Fu, Hongbin Zhang, Longqing Zou, Yuxuan Huang
This study aims to investigate the influence of rigid polyurethane foam (RPUF) as a filling material on the energy absorption performance of thin-walled tubes through experiments. Hybrid graphene o...
本研究旨在通过实验研究硬质聚氨酯泡沫塑料(RPUF)作为填充材料对薄壁管吸能性能的影响。混合石墨烯…
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引用次数: 0
Facile synthesis of functionalized polysiloxanes with nonconventional fluorescence by oxa-Michael addition reaction 用oxa-Michael加成反应快速合成具有非常规荧光的功能化聚硅氧烷
IF 1.6 4区 化学 Q3 POLYMER SCIENCE Pub Date : 2023-11-17 DOI: 10.1080/15685551.2023.2278230
Shiyao Jia, Shengyu Feng, Dengxu Wang
Developing a novel methodology for the synthesis of functionalized polysiloxanes is highly desirable because of their extensive applications in engineering, textile, construction, electronics, and ...
由于功能化聚硅氧烷在工程、纺织、建筑、电子等领域的广泛应用,开发一种新的合成方法是非常必要的。
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引用次数: 0
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Designed Monomers and Polymers
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