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2013 International Conference on Manipulation, Manufacturing and Measurement on the Nanoscale最新文献

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Coating method of micro pattern based on microscopic injection system 基于显微注射系统的微花纹涂层方法
Ailong Zhang, Zhao Xin, Wu Ming, Xizeng Feng
It's of significance to study coating method of micro pattern, which plays an important role in the research of biological growth in cell scale. To avoid high cost for micro fabrication in traditional coating method and at the same time to improve flexibility, a novel coating approach based on microscopic injection system is proposed in the paper. In contrary to traditional micro injection, controlling pressure is just used to keep the balance of solution in injection pipette while interfacial force at tip between solution and substrate is used to drive out solution for coating. According to the proposed method, micro stripe and micro dot pattern coating are achieved in our experiment, which verifies the effectiveness of the method. Meanwhile, neural stem cells(NSCs) growth and distribution controlling results verifies the practical application value of the coating method.
研究微图案的包膜方法对研究细胞尺度下的生物生长具有重要意义。为了避免传统涂层方法微加工成本高,同时提高柔性,提出了一种基于显微注射系统的新型涂层方法。与传统的微注射不同的是,控制压力只是为了保持注射吸管中溶液的平衡,而利用溶液与基材之间尖端的界面力来驱出溶液进行涂层。根据所提出的方法,在实验中实现了微条纹和微网点图案涂层,验证了该方法的有效性。同时,神经干细胞(NSCs)的生长和分布控制结果验证了该涂层方法的实际应用价值。
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引用次数: 1
Growth of porous InP: Transition from three to two dimensional structures 多孔InP的生长:从三维结构到二维结构的转变
Z. Weng, An'gang Yuan, Weixun Mi, Wendan Zhang, Cuiting Wu, Zuobin Wang
We present the transition state of porous InP from three to two dimensions, which is explored during electrochemical etching at constant current density in NaCl solutions on n-InP(100) wafers. The `node' of the three dimensional structure revealed by scanning electron microscopy are consistent with the oscillatory periods, and that the smooth curve is corresponding to the uniformly vertical pores along with the <;001> direction. In addition, the onset and end of the oscillations shift ahead of times with increasing current densities. Furthermore, the transition of porous InP was discussed based on the surface curvature, the diffusion-control, and the reactive heat.
本文研究了多孔InP在NaCl溶液中恒流密度的电化学刻蚀过程中从三维到二维的过渡状态。扫描电镜显示的三维结构“节点”与振荡周期一致,光滑曲线对应的是沿方向均匀垂直的孔隙。此外,随着电流密度的增加,振荡的开始和结束时间提前。在此基础上,从表面曲率、扩散控制和反应热三个方面讨论了多孔InP的相变过程。
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引用次数: 3
Characterization of nanolaminate thickness using multi-parametric surface plasmon resonance 利用多参数表面等离子体共振表征纳米层合材料厚度
J. Kuncova-Kallio, A. Jokinen, J. Sadowski, Niko Granqvist
Nanolaminates play a significant role in the precision optical components, and protective barrier coatings. We present a new non-destructive method for characterization of nanolaminates in terms of thickness and refractive index based on Multi-Parametric Surface Plasmon Resonance (MP-SPR). In this paper, we briefly compare novel MP-SPR technology and traditional ellipsometry approach and then show MP-SPR on three examples that would be difficult-to-measure with ellipsometry. In the first case, MP-SPR is used to measure thickness of Langmuir-Blodgett multilayer film of Cr-Au-SACd, where each SACd layer can be measured individually without averaging. In the second case, vacuum deposited Cr-Au-TaC (tetragonal amorphous carbon) is measured. In the third case, alternating nanolayers of Al2O3-Pt deposited by Atomic Layer Deposition are measured. This shows that Multi-Parametric Surface Plasmon Resonance (MP-SPR) overcomes drawbacks of traditional optical methods and enables measurements of metal (light absorbing) nanolaminates and of ultrathin nanolayers.
纳米层合材料在精密光学元件和防护屏障涂层中发挥着重要作用。提出了一种基于多参数表面等离子体共振(MP-SPR)表征纳米层合材料厚度和折射率的无损方法。本文简要比较了新方法和传统的椭偏方法,并举例说明了椭偏方法难以测量的三个例子。在第一种情况下,MP-SPR用于测量Cr-Au-SACd的Langmuir-Blodgett多层膜的厚度,其中每个SACd层可以单独测量而无需平均。在第二种情况下,真空沉积的Cr-Au-TaC(四方非晶碳)被测量。在第三种情况下,测量了原子层沉积法沉积Al2O3-Pt的交替纳米层。这表明,多参数表面等离子体共振(MP-SPR)克服了传统光学方法的缺点,能够测量金属(吸光)纳米层和超薄纳米层。
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引用次数: 1
A novel micro-nano measurement method for line width using confocal microscopy with super-resolution image restoration 一种利用超分辨率图像恢复共聚焦显微技术测量线宽的微纳新方法
Dali Liu, Lirong Qiu, Weiqian Zhao
A novel micro-Nano measurement method using confocal microscopy with super-resolution image restoration is proposed to achieve the measurement of all of the lateral dimensions of the line width step sample including the dimension that is smaller than the diffraction limit. In this method, first, the step is over-sampling scanned to obtain the intensity image data at focal plane; and then using the respective restoration to obtain super-resolution restoration images of the flat region and the bevel region; finally, the ideal profile is estimated from the restoration images and used to locate the edges of the structures to measure. Maximum likelihood estimation algorithm based on Markov filed is adopted for the image restoration. Experimental results of the measurement for the lateral dimensions of TGZ02 100nm height standard show that this method can accurately measure the period and all of the lateral dimensions of the step. The method reaches an average measurement value of 0.162μm for the bevel edge, and it is 0.015μm smaller than that measured by AFM.
提出了一种利用超分辨率图像恢复的共聚焦显微技术实现线宽阶跃样品所有横向尺寸的测量,包括小于衍射极限的尺寸。该方法首先进行过采样扫描,获得焦平面处的强度图像数据;然后利用各自的复原得到平面区域和斜角区域的超分辨率复原图像;最后,从恢复图像中估计出理想轮廓,并用于定位待测量结构的边缘。图像复原采用基于马尔可夫场的极大似然估计算法。TGZ02 100nm高度标准横向尺寸测量的实验结果表明,该方法能够准确测量周期和台阶的所有横向尺寸。该方法对斜角的平均测量值为0.162μm,比原子力显微镜测量值小0.015μm。
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引用次数: 1
Fabrication of a single CuO nanowire-based gas sensor working at room temperature 室温下单CuO纳米线气体传感器的制备
Chaolei Huang, Xiaojun Tian, Jie Liu, Wenxue Wang, Z. Dong, Lianqing Liu
CuO is an important p-type metal oxide semiconductor material and it has been used in many fields for its excellent physical and chemical properties, such as field effect transistors, photovoltaic cells, field emission nanodevices, and chemical and gas sensors. In this paper, CuO nanowires are synthesized by thermal oxidation of copper foil and suitable DEP parameters are chosen to assemble a single CuO nanowire on microelectrodes to fabricate a single CuO nanowire-based device. Experiments in this paper show that the single CuO nanowire-based device can work as field effect transistor and gas sensor. The single CuO nanowire device has a significant respond to the atmosphere with alcohol at room temperature, so it has potential to work as an alcohol gas sensor at room temperature. The single CuO nanowire device also has quick and significant respond to the humidity at room temperature and a novel liner relationship between conductivity and the relative humidity from 30% to 100%.
CuO是一种重要的p型金属氧化物半导体材料,由于其优异的物理和化学性能,在场效应晶体管、光伏电池、场发射纳米器件、化学和气体传感器等领域得到了广泛的应用。本文通过对铜箔进行热氧化合成CuO纳米线,并选择合适的DEP参数,在微电极上组装单根CuO纳米线,制备基于CuO纳米线的器件。本文的实验表明,单CuO纳米线器件可以作为场效应晶体管和气体传感器。单CuO纳米线器件在室温下对含有酒精的大气有明显的响应,因此具有在室温下作为酒精气体传感器的潜力。单CuO纳米线器件对室温下的湿度也有快速而显著的响应,并且电导率与相对湿度之间具有新颖的线性关系,从30%到100%。
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引用次数: 2
Drive mode control for MEMS gyroscopes with electrostatically tunable structure 具有静电可调结构的MEMS陀螺仪的驱动模式控制
Hui-Jie Zhu, Zhong-he Jin, Shi-chang Hu, Wei Ma, Yidong Liu
Variable-area capacitor with tuning capability is used to control the drive mode of MEMS gyroscopes for constant-frequency oscillation. The proposed control approach tunes the drive axis natural frequency to a preselected frequency and regulates the amplitude of the drive axis vibration. The algorithm mainly implemented using a field-programmable-gate-array (FPGA) is tested on a MEMS gyroscope operating at atmospheric pressure which is of our own manufacture. First measurement results of the novel digital prototype show the amplitude variance of the detected signal of drive axis is 26ppm in an hour while the phase variance is 45ppm.
采用具有调谐能力的变面积电容控制MEMS陀螺仪的驱动方式,实现恒频振荡。该控制方法将驱动轴固有频率调谐到预定频率,并调节驱动轴的振动幅值。该算法主要采用现场可编程门阵列(FPGA)实现,并在自制的常压MEMS陀螺仪上进行了测试。首先,新型数字样机的测量结果表明,驱动轴的检测信号在1小时内的幅值变化为26ppm,相位变化为45ppm。
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引用次数: 6
Exploring charge inversion in electrolyte mixtures of trivalent and monovalent ions 探索三价和一价离子混合电解质中的电荷反转
Li Xiang, Gutian Zhao, Di Zhang, Yunfei Chen
At room temperature ion-ion correlations and counterions volume effect play a crucial role in the description of the electrical double layer of colloidal particles. In fact, in many instances, the inclusion of the short range correlations between ions in the study of the ionic distribution and the consideration of the ion's size lead to quite different results with respect to the classical treatment (where ions are assumed to be points). In particular, these discrepancies become more noticeable for highly charged particles in the presence of moderate or highly multivalent counterion concentrations. Moreover, it can be shown that the existence of an electrolyte mixture consisting of multi- and monovalent counterions may cause that system to become overcharged, a feature that cannot be predicted from a classical point of view based on the Boltzmann distribution function. In order to explore the charge inversion in electrolyte mixtures of trivalent and monovalent ions, the interaction of mica surfaces in two different concentrations of LaCl3 before and after adding NaCl is investigated through the surface force apparatus(SFA) and these experimental results can demonstrate that the charge inversion is indeed enhanced by a monovalent salt.
在室温下,离子-离子相关和反离子体积效应在描述双电层胶体粒子中起着至关重要的作用。事实上,在许多情况下,在离子分布的研究中包括离子之间的短程相关性,并考虑离子的大小,导致与经典处理(假设离子是点)完全不同的结果。特别是,在存在中等或高度多价反离子浓度的高电荷粒子中,这些差异变得更加明显。此外,可以证明,由多价和单价反离子组成的电解质混合物的存在可能导致该系统变得过充电,这是基于玻尔兹曼分布函数的经典观点无法预测的特征。为了探索三价离子和一价离子混合电解质中的电荷反转,通过表面力仪(SFA)研究了两种不同浓度LaCl3中加入NaCl前后云母表面的相互作用,实验结果表明,一价盐确实增强了电荷反转。
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引用次数: 0
A novel positioning stage with resolution enhancement functionality for nano manipulation 一种具有纳米操作分辨率增强功能的新型定位平台
Chongrui Du, Weihai Chen, Xiantao Sun, Yunjie Wu, Jianbin Zhang, Wenjie Chen
With the rapid development of nano science and precision engineering, a positioning system with high resolution is indispensable to meet the requirement of precise positioning. This paper presents the design and modeling of a flexure-based positioning stage with the functionality of resolution enhancement. To achieve high enhancement ratio, two sets of displacement reduction mechanisms are incorporated and configured serially in a monolithic symmetrical design. Following the assumption that the flexure hinge can be equivalent to an ideal revolute joint with a torsional spring, theoretical models are established to analyze the resolution enhancement ratio and dynamic performance of the positioning stage. Moreover, finite element analysis (FEA) is conducted to study the performances of the mechanism and verify the theoretical models. The results show that the proposed mechanism can achieve a resolution enhancement ratio of 18.75 to improve the positioning performance, and the first order natural frequency of the mechanism is 535.5Hz, which guarantees the bandwidth of the positioning operation.
随着纳米科学和精密工程的飞速发展,高分辨率的定位系统是满足精确定位要求必不可少的。提出了一种具有分辨率增强功能的柔性定位平台的设计与建模方法。为了实现高增强比,采用单片对称设计,将两套减排量机构合并并串联配置。在将柔性铰链等效为带扭簧的理想旋转关节的前提下,建立了理论模型,分析了定位台的分辨率增强率和动态性能。并进行了有限元分析,研究了机构的性能,验证了理论模型。结果表明,该机构可实现18.75的分辨率增强比,提高定位性能;该机构的一阶固有频率为535.5Hz,保证了定位操作的带宽。
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引用次数: 0
Structure design optimization of micro/nano angular-table with S-shape compliant structure s型柔顺结构微纳角工作台结构设计优化
M. Helal, W. Rong, Lining Sun
Micro-electromechanical Systems is a rapidly growing field that will permeate our everyday lives in the coming decades. Recently, the evolution in microelectronics of combining mechanical and electrical functions has brought about an exciting new field micro/nano-electro-mechanical system. Compliant mechanisms can play an important role in the design of micro-devices for micro-electro-mechanical systems applications. Compliant mechanism is flexible structures that generate desired motion by undergoing elastic deformations. The concept of structural optimization has been more and more widely accepted in many engineering fields. The structural optimization can result in a much more reasonable and economical structure design. In this investigation, structure optimization is applied for designing two-dimensional micro/nano angular-table compliant mechanism. The interface between Malab and Ansys were shown to obtain the optimal shape of the compliant mechanism. Structure design optimization of the two-dimension micro/nano angular-table with S-shape compliant structure was shown and all results are illustrated.
微机电系统是一个快速发展的领域,将在未来几十年渗透到我们的日常生活中。近年来,随着微电子学的发展,机械和电气功能的结合带来了一个令人兴奋的新领域微/纳米机电系统。柔性机构在微机电系统的微器件设计中起着重要的作用。柔性机构是一种通过弹性变形产生所需运动的柔性结构。结构优化的概念已越来越广泛地应用于许多工程领域。结构优化可以使结构设计更加合理和经济。本研究将结构优化技术应用于二维微纳角工作台柔性机构的设计。利用Malab和Ansys进行界面分析,得到了柔性机构的最优形状。给出了具有s形柔顺结构的二维微纳角工作台的结构优化设计,并对结果进行了说明。
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引用次数: 0
Fabrication of light emitting diode with ZnO nanorods on polymer coated silicon substrate 聚合物包覆硅衬底上ZnO纳米棒发光二极管的制备
Sadia Sarahnaz, Om Prakash Gujela, N. Afzulpurkar
ZnO nanorods are grown on p-type silicon substrates coated with a light emitting polymer PFO. Powdered PFO is mixed in toluene and spun coated on the Si substrate and heated before growing ZnO nanorods on them. PMMA solution in toluene is then spun coated on the nanorods to work as an insulating layer and the tips were etched using oxygen plasma. With Au and Al metal being used as top and bottom contacts, we fabricate a hybrid light emitting diode structure. In this work, we report the electrical and optical performances of the fabricated light emitting diode with a hybrid structure of Au/ZnO nanorods/PFO/ p-Si/Al. This fabricated heterojunction LED with 1 dimensional ZnO nanostructures exhibited IV characteristics of diode and photoluminescence were observed in a broad yellow-green spectrum.
ZnO纳米棒生长在p型硅衬底上,衬底上涂有发光聚合物PFO。将粉末PFO混合在甲苯中,纺丝涂覆在Si衬底上,加热后在其上生长ZnO纳米棒。然后将含甲苯的PMMA溶液旋转涂在纳米棒上,作为绝缘层,并用氧等离子体蚀刻尖端。采用金和铝作为上下触点,制备了一种混合发光二极管结构。在这项工作中,我们报告了具有Au/ZnO纳米棒/PFO/ p-Si/Al混合结构的制造发光二极管的电学和光学性能。所制备的具有一维ZnO纳米结构的异质结LED具有二极管的IV特性,并且在宽广的黄绿色光谱中观察到光致发光。
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引用次数: 6
期刊
2013 International Conference on Manipulation, Manufacturing and Measurement on the Nanoscale
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