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Analysing Gray Cast Iron Data using a New Shapiro-Wilks test for Normality under Indeterminacy 用新的Shapiro-Wilks不确定正态性检验分析灰铸铁数据
IF 1.4 4区 材料科学 Q2 Materials Science Pub Date : 2020-12-19 DOI: 10.1080/13640461.2020.1846959
M. Aslam
ABSTRACT Shapiro–Wilks test is popularly used for testing the normality of the data. Shapiro–Wilks test using the idea of neutrosophic statistics is discussed in this paper. The necessary equations are given under the indeterminacy environment. The testing procedure of the proposed test is given and explained with the help of chemical data. The performance of the proposed Shapiro–Wilks test is discussed with the Shapiro–Wilks test under the classical statistics. From the comparison, it is concluded that the proposed Shapiro–Wilks test is affective to apply when the data are obtained under uncertain environment.
摘要Shapiro–Wilks检验常用于检验数据的正态性。本文讨论了利用中性粒细胞统计学思想进行的Shapiro-Wilks检验。给出了不确定性环境下的必要方程。给出了该试验的试验程序,并结合化学数据进行了说明。将所提出的Shapiro-Wilks检验与经典统计学下的Shapiro-Vilks检验的性能进行了讨论。从比较中可以得出结论,当数据是在不确定的环境下获得时,所提出的Shapiro–Wilks检验是有效的。
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引用次数: 6
New insight of Ca element refining grain structure in commercial purity Mg based on the first-principle calculation 基于第一性原理计算对商品纯镁中Ca元素细化晶粒结构的新认识
IF 1.4 4区 材料科学 Q2 Materials Science Pub Date : 2020-12-16 DOI: 10.1080/13640461.2020.1861856
G. Peng, Y. Gu, G. Song, Y. Wang, Songyi Chen
ABSTRACT The first-principle calculation was used to understand new insight of Ca element refining grain structure in commercial purity Mg. Negative adsorption energy, strong ionic bond and negative shift of partial density of states verify that Ca element is readily adsorbed on the surface of MgO. Combined with analysis of interfacial bonding between Mg2Ca and α-Mg, new insight of Mg2Ca layer formed via Ca adsorption efficiently nucleating α-Mg was proposed. Adsorption of other alkaline earth elements (Be, Sr or Ba) and the crystallographic feature of Be, Mg17Sr2 and Mg17Ba2 along with the experimental results further consolidate new insight of Ca element refining grain structure in commercial purity Mg.
摘要利用第一性原理计算,对工业纯Mg中Ca元素细化晶粒结构的新见解进行了理解。负吸附能、强离子键和部分态密度的负移证实了Ca元素容易吸附在MgO表面。结合对Mg2Ca与α-Mg界面结合的分析,提出了通过Ca吸附形成Mg2Ca层使α-Mg有效成核的新见解。其他碱土元素(Be、Sr或Ba)的吸附以及Be、Mg17Sr2和Mg17Ba2的晶体学特征以及实验结果进一步巩固了Ca元素在商业纯Mg中细化晶粒结构的新见解。
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引用次数: 1
Role of Cerium on the creep properties of the Mg-Sn-Al based alloys 铈对Mg-Sn-Al基合金蠕变性能的影响
IF 1.4 4区 材料科学 Q2 Materials Science Pub Date : 2020-11-01 DOI: 10.1080/13640461.2020.1853929
Aslı Önür, Gülşah Germen Tutaş, Hüseyin Şevik
ABSTRACT In the present study, the effect of Ce alloying element with different quantities (1 and 2 wt.%) on the microstructure and mechanical properties of Mg-5Sn-2Al alloy was investigated. Phase analyses and microstructural studies were carried out using XRD and SEM. It was observed that base alloy was composed of the α-Mg and Mg2Sn intermetallic phase, and after Ce addition Ce5Sn4 intermetallic phase was formed. Also, an increase was detected on the microhardness of the base alloy with increasing Ce addition. The test results showed that Ce addition has no notable effect on the tensile properties at room temperature but has a positive effect at elevated temperatures. Furthermore, creep properties of the Mg-5Sn-2Al alloy were obviously improved by adding Ce. The values of stress exponents and activation energy indicated that the dominant creep mechanisms of the alloys were identified dislocation climb controlled creep..
摘要研究了不同添加量(1和2wt%)的Ce合金元素对Mg-5Sn-2Al合金组织和力学性能的影响。用XRD和SEM进行了相分析和微观结构研究,发现基体合金由α-Mg和Mg2Sn金属间相组成,添加Ce后形成Ce5Sn4金属间相。此外,随着Ce添加量的增加,基体合金的显微硬度也有所增加。试验结果表明,Ce的添加对室温拉伸性能没有显著影响,但对高温拉伸性能有积极影响。Ce的加入明显改善了Mg-5Sn-2Al合金的蠕变性能。应力指数和活化能值表明,合金的主要蠕变机制为位错爬控蠕变。。
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引用次数: 1
Mechanism of bonding of Fe/Al bimetal during heat treatment of compound cast parts 复合铸件热处理过程中Fe/Al双金属结合机理
IF 1.4 4区 材料科学 Q2 Materials Science Pub Date : 2020-11-01 DOI: 10.1080/13640461.2020.1853392
H. Honarjoo, R. Raiszadeh
ABSTRACT The formation of bonding between Al and Fe after the initial compound casting and during a heat treatment regime is investigated. No significant bonding was observed between the two metals after the initial casting. This observation was attributed to the presence of oxide films on the liquid Al and solid Fe alloys. The heat treatment of the cast part at 973 K (700°C) for at least 15 min is shown to cause the two alloys to bond to each other seamlessly. The cracks that formed on the Al oxide layer (due to the pouring stresses or the remelting of the alloy) is suggested to provide the necessary paths for the contact between the Al melt and the trapped atmosphere between the Al and Fe alloys, and the contact between the Al melt and the Fe surface. A detailed mechanism for the bonding is presented in this paper.
摘要:本文研究了Al和Fe在初始复合铸造后和热处理过程中形成的键合。初次铸造后,两种金属之间没有明显的结合。这一观察结果归因于液态铝和固态铁合金上存在氧化膜。在973 K(700°C)下对铸件进行至少15分钟的热处理可以使两种合金无缝地结合在一起。在Al氧化层上形成的裂纹(由于浇注应力或合金的重熔)为Al熔体与Al和Fe合金之间的俘获气氛以及Al熔体与Fe表面的接触提供了必要的途径。本文详细介绍了这种结合的机理。
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引用次数: 3
Development of ultra-high strength carbide-free bainitic cast steels 超高强度无碳化物贝氏体钢的研制
IF 1.4 4区 材料科学 Q2 Materials Science Pub Date : 2020-11-01 DOI: 10.1080/13640461.2020.1843778
N. Tenaglia, A. Basso, J. Massone, R. Boeri
ABSTRACT High-silicon cast steels and proper heat treatment cycles were designed in order to obtain carbide-free bainitic microstructures. The design process allowed to obtain the desired microstructures after heat treatment cycles compatible with industrial practices and using low amounts of inexpensive alloying elements. The different chemical compositions and austempering temperatures tested resulted in ultra-high-strength steels showing remarkably total elongations. The obtained tensile properties satisfy the minimum requirements specified for AHSS in ASTM A1088 standard, and also the requirements for high-strength cast steels stated in ASTM A148. Moreover, many microstructures developed in this work reach the tensile performance of the very expensive maraging steels.
为了获得无碳化物贝氏体组织,设计了高硅铸钢和适当的热处理循环。该设计过程允许在热处理循环后获得所需的微观结构,该热处理循环与工业实践兼容,并使用少量廉价的合金元素。测试的不同化学成分和等温淬火温度导致超高强度钢显示出显著的总伸长率。获得的拉伸性能满足ASTM A1088标准中规定的AHSS的最低要求,以及ASTM A148中规定的高强度铸钢的要求。此外,在这项工作中开发的许多微观结构达到了非常昂贵的马氏体时效钢的拉伸性能。
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引用次数: 1
Phase transition and microstructure investigation of perferritic isothermed ductile iron (IDI) 过铁素体等温球墨铸铁(IDI)的相变及显微组织研究
IF 1.4 4区 材料科学 Q2 Materials Science Pub Date : 2020-10-21 DOI: 10.1080/13640461.2020.1833477
M. Landesberger, R. Koos, Maximilian Erber, Matteo Pernumian, S. Masaggia, M. Hoelzel, W. Volk
ABSTRACT Optical analysis, dilatometry as well as neutron diffraction are utilised to investigate the phase transition within ductile iron both in-situ and after the heat treatment process for perferritic isothermed ductile iron (IDI). A suitable annealing temperature is chosen by calculating a phase diagram for the investigated alloy. The phase transition which happens slightly above upper intercritical temperature is followed by neutron diffraction, while dilatometry elucidates the IDI microstructure evolution for cooling rates from 40 to 0.125 K/s. The dilatometry results are visualised in a CCT diagram and further investigated with metallography. An additionally used colour etching method is basis for discussing the formation of the pearlitic/ferritic network. The presence of 2 vol.-% of ferrite was sufficient to achieve the typical IDI microstructure. Finally, the cementite phase volume fractions and crystal structure are evaluated. . The lattice constants of ferrite and cementite were independent of the formed microstructure.
摘要利用光学分析、膨胀计和中子衍射研究了全铁等温球墨铸铁(IDI)在原位和热处理后的相变。通过计算所研究合金的相图来选择合适的退火温度。相变发生在略高于上临界温度的温度之后是中子衍射,而膨胀计阐明了在40至0.125K/s的冷却速率下IDI微观结构的演变。膨胀测量结果在CCT图中可视化,并用金相学进行进一步研究。另外使用的彩色蚀刻方法是讨论珠光体/铁素体网络形成的基础。2体积%铁氧体的存在足以实现典型的IDI微观结构。最后,对渗碳体的相体积分数和晶体结构进行了评价。铁素体和渗碳体的晶格常数与所形成的微观结构无关。
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引用次数: 0
Effects of thermal exposure on the microstructure and mechanical properties of Al-12Si-4Cu-1Ni-1Mg-2Mn piston alloys 热暴露对Al-12Si-4Cu-1Ni-1Mg-2Mn活塞合金组织和力学性能的影响
IF 1.4 4区 材料科学 Q2 Materials Science Pub Date : 2020-10-21 DOI: 10.1080/13640461.2020.1838077
B. Lin, S. Xia, Yue Tang, Yuliang Zhao, Kun Liu, Huaqiang Xiao, Shaobo Li, Weiweng Zhang
ABSTRACT The effect of thermal exposure on the elevated-temperature mechanical properties of heat-treated Al-12Si-4Cu-1Ni-1 Mg-2Mn piston alloys was investigated using optical microscopy (OM), scanning electron microscope (SEM), transmission electron microscopy (TEM), and tensile tests at elevated temperatures. The results showed that coarsening of the strengthening precipitates following a prolonged exposure at 350°C had a deleterious effect on the elevated-temperature tensile properties. Further thermal exposure up to 50 h did not result in even a slight reduction in the strength. After exposure at 350°C, the value of elevated-temperature ultimate tensile strengths of Al-12Si-4Cu-1Ni-1 Mg-2Mn piston alloys were 92, 80, and 73 MPa for 0 h, 10 h, and 100 h of thermal exposure, respectively, which are superior to those of the commercial piston alloys. The high-performance, elevated-temperature mechanical properties of Al-12Si-4Cu-1Ni-1 Mg-2Mn piston alloys can be attributed to the high thermal stability Mn-rich intermetallics and Al3CuNi.
摘要采用光学显微镜(OM)、扫描电子显微镜(SEM)、透射电子显微镜(TEM)和高温拉伸试验研究了热暴露对热处理的Al-12Si-4Cu-1Ni-1Mg-2Mn活塞合金高温力学性能的影响。结果表明,在350°C下长时间暴露后,强化沉淀物的粗化对高温拉伸性能产生了有害影响。长达50小时的进一步热暴露甚至没有导致强度的轻微降低。在350°C下暴露后,Al-12Si-4Cu-1Ni-1Mg-2Mn活塞合金在热暴露0小时、10小时和100小时的高温极限拉伸强度分别为92、80和73MPa,这优于商业活塞合金。Al-12Si-4Cu-1Ni-1Mg-2Mn活塞合金的高性能、高温力学性能可归因于富含Mn的金属间化合物和Al3CuNi的高热稳定性。
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引用次数: 3
The origin of thermal expansion differences in various size fractions of silica sand 不同粒径硅砂热膨胀差异的成因
IF 1.4 4区 材料科学 Q2 Materials Science Pub Date : 2020-10-20 DOI: 10.1080/13640461.2020.1838078
Judit Svidró, A. Diószegi, József Tamás Svidró
ABSTRACT In this study, thermophysical properties of a commonly used silica sand were investigated and their relation to its granulometric and chemical composition was studied. Thermal expansion and differential scanning calorimetry tests were performed on individual fractions of the silica sand together with X-ray fluorescence measurements to determine their constituents. It was found that the various size fractions of silica sand exhibit different levels of thermal expansion based on the differences in SiO2 content. The expansion behaviour of two additional silica samples and a recycled olivine sand was also investigated in relation to its grain size to justify the findings.
摘要本研究对一种常用硅砂的热物理性质进行了研究,并研究了其与粒度和化学成分的关系。对硅砂的各个部分进行热膨胀和差示扫描量热测试,并进行X射线荧光测量,以确定其成分。研究发现,基于SiO2含量的差异,不同粒度的硅砂表现出不同的热膨胀水平。还研究了两个额外的二氧化硅样品和一个回收的橄榄石砂的膨胀行为与其粒度的关系,以证明这一发现的合理性。
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引用次数: 6
Extrema of micro-hardness in fully pearlitic compacted graphite cast iron 完全珠光体压实石墨铸铁的显微硬度极值
IF 1.4 4区 材料科学 Q2 Materials Science Pub Date : 2020-09-02 DOI: 10.1080/13640461.2020.1832308
J. Lacaze, C. Moussa, Y. Thébault, W. Guesser
ABSTRACT For improving the mechanical strength of cast irons, a fully pearlitic matrix is sought by alloying with tin, copper and manganese. This applies in particular to the compacted graphite irons considered here. While average macro- and micro-hardness values were similar for the four fully pearlitic alloys under study, it was found that high copper and low tin content showed some very high maximum micro-hardness values, significantly higher than the corresponding mean. Such values may be seen as hard points in the material that would certainly impair machinability. Discussion of the reasons for these extreme values opens directions for further studies.
为了提高铸铁的机械强度,通过与锡、铜和锰合金化来寻求完全珠光体基体。这尤其适用于这里考虑的压实石墨铁。虽然四种完全珠光体合金的宏观和微观硬度平均值相似,但高铜含量和低锡含量合金的最大显微硬度值非常高,显著高于相应的平均值。这些值可能被视为材料中的硬点,这肯定会损害可加工性。对这些极值原因的讨论为进一步研究开辟了方向。
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引用次数: 3
Effect of the cooling rate on the tensile strength of pearlitic lamellar graphite cast iron 冷却速率对珠光体层状石墨铸铁抗拉强度的影响
IF 1.4 4区 材料科学 Q2 Materials Science Pub Date : 2020-09-02 DOI: 10.1080/13640461.2020.1822573
F. O. Lima, L. F. Bauri, H. B. Pereira, C. Azevedo
ABSTRACT The effects of cooling rate and carbon equivalent on the tensile strength of pearlitic lamellar graphite cast irons were investigated. The cooling rate was varied from 6°C/s to 35°C/s for values of the carbon equivalent equal to 4.17% and 3.83%. The increase in the cooling rate promoted the refining of the eutectic cell size, primary dendrite modulus, interdendritic hydraulic diameter and pearlite interlamellar spacing. The increase in the cooling rate also refined their graphite flakes, changing the morphology from B to E type. The reduction in the carbon equivalent increased the proportion of primary dendrites from 25% to 40%. The maximum tensile strength increased from 274 to 524 MPa with the increase in the cooling rate and the reduction in the carbon equivalent. These results were used to test two tensile strength predictive models based on modified versions of the Griffith and Hall-Petch equations.
研究了冷却速度和碳当量对珠光体片层石墨铸铁抗拉强度的影响。当碳当量分别为4.17%和3.83%时,冷却速率在6°C/s至35°C/s之间变化。冷却速率的增加促进了共晶细胞尺寸、初生枝晶模量、枝晶间水力直径和珠光体层间距的细化。冷却速率的增加也细化了它们的石墨薄片,使其形态从B型变为E型。碳当量的减少使一次枝晶的比例从25%增加到40%。随着冷却速率的增加和碳当量的减少,最大抗拉强度从274 MPa增加到524 MPa。这些结果用于测试两个基于Griffith和Hall-Petch方程修正版本的抗拉强度预测模型。
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引用次数: 3
期刊
International Journal of Cast Metals Research
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