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Investigation of the Quality of Flywheel SG Iron Sand Casting Using the Optimized Riser Dimensions: Numerical Simulation and Experimental Validation 使用优化的立管尺寸调查飞轮 SG 铁砂铸造的质量:数值模拟与实验验证
IF 2.6 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-09 DOI: 10.1007/s40962-024-01407-4
Rajat Upadhyaya, Kamlesh Kumar Singh, Sujeet Kumar Gautam, Rajeev Kumar, Himanshu Khandelwal, J. D. Sharma

The primary objective of this investigation is to employ computational simulation analysis of casting to determine effective riser dimensions and eliminate shrinkage porosity in actual spheroidal graphite (SG) iron flywheel casting. A simulation software, Pro-CAST, is used to simulate the solidification process under varying process conditions (i.e., without a riser and with an effective dimension riser). The simulation results are then confirmed by a subsequent experiment using green sand casting. Additionally, a thorough investigation is conducted to determine the correlation between the shrinkage behavior and its morphological characteristics of the cast components. The simulation results infer that the un-optimized dimension of the riser causes the shrinkage porosity and void formation largely in the thicker section, due to the lower eutectic solidification time. However, when the dimension of the riser is optimized, this effect is mitigated simply by ensuring the eutectic solidification time is higher than the eutectic solidification of the thicker section; thus, the mold is completely filled with no shrinkage porosity or void formation. It is evident that there is a good agreement between simulation and experiment when comparing the resulting appearance of components in simulations and experiments.

这项研究的主要目的是利用铸造计算模拟分析来确定有效的冒口尺寸,并消除实际球状石墨(SG)铁飞轮铸件中的缩孔。模拟软件 Pro-CAST 用于模拟不同工艺条件下的凝固过程(即不使用冒口和使用有效尺寸冒口)。模拟结果通过随后的绿砂铸造实验得到证实。此外,还进行了深入调查,以确定收缩行为与铸造部件形态特征之间的相关性。模拟结果推断,由于共晶凝固时间较短,未优化的冒口尺寸会在较厚的部分造成收缩气孔和空隙的形成。然而,当优化了隔水管的尺寸后,只需确保共晶凝固时间高于较厚部分的共晶凝固时间,就可以减轻这种影响;因此,模具可以完全填充,不会产生收缩气孔或空洞。通过比较模拟和实验得出的组件外观,可以明显看出模拟和实验之间存在良好的一致性。
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引用次数: 0
A Study of the Influence and Mechanism of Alumina Ceramic Powder on the High-Temperature Strength of NaCl–Na2CO3 Cores in Die-Casting Production 氧化铝陶瓷粉对压铸生产中 NaCl-Na2CO3 铁芯高温强度的影响及机理研究
IF 2.6 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-08 DOI: 10.1007/s40962-024-01400-x
Yang Li, Lai Song, Guangyu Chen, Weihua Liu, Jingkai Zhang, Changyu Sun, Xue Zou, Minghui Bai

Water-soluble salt core materials have high bending strength at room temperature. During high-pressure casting, water-soluble salt cores must withstand high temperatures and impact loads. To obtain a composite water-soluble salt core suitable for high-pressure casting components, sodium chloride and sodium carbonate are used as base salt materials. Ceramic particles of alumina are used as reinforcement materials in the preparation of a water-soluble composite salt core with excellent high-temperature strength via gravity casting. The microstructures of the salt core and fracture surface are observed and characterized. The use of alumina to enhance the sensitivity of the binary salt cores results in a low thermal crack sensitivity coefficient. The alumina particles dispersed in the matrix prevent crack propagation. Simulation results show that sodium aluminate has strong interfacial bonding abilities with other components in the salt core, affecting its high-temperature strength. Further results confirm that sodium aluminate formation enhances the high-temperature strength of salt cores.

水溶性盐芯材料在室温下具有很高的抗弯强度。在高压铸造过程中,水溶性盐芯必须承受高温和冲击载荷。为获得适用于高压铸造部件的复合水溶性盐芯,可使用氯化钠和碳酸钠作为基盐材料。在通过重力浇铸制备具有优异高温强度的水溶性复合盐芯时,使用了氧化铝陶瓷颗粒作为增强材料。对盐芯和断裂面的微观结构进行了观察和表征。使用氧化铝提高二元盐芯的灵敏度,可获得较低的热裂纹灵敏系数。分散在基体中的氧化铝颗粒可防止裂纹扩展。模拟结果表明,铝酸钠与盐芯中的其他成分具有很强的界面结合能力,从而影响了盐芯的高温强度。进一步的结果证实,铝酸钠的形成可提高盐芯的高温强度。
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引用次数: 0
Effects of Sc–Er Rare Earth on Solidification Microstructure and Mechanical Properties of A360 Alloy 稀土钪对 A360 合金凝固微观结构和机械性能的影响
IF 2.6 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-08 DOI: 10.1007/s40962-024-01397-3
Shuaijie Yuan, Jianfei Peng, Wanlin Wang, Yan Zhan, Jie Zeng, Peiyuan Gan, Junyu Ji

Hypoeutectic Al-Si alloy (A360) is widely used to high-pressure die casting components used in the aerospace, automobile and building industries. An experimental investigation has been conducted concerning the effect of different rare earth Sc and Er additions on the solidification process of A360 alloy. The results indicate that a precipitation phase Al(Sc, Er)2Si2 is formed with the addition of Sc and Er elements. Moreover, the eutectic Si phase evolves from a coarse block-like and irregular polygonal into a granular morphology, and its average size value is decreased from 25.48 μm to 9.46 μm when the content of Sc–Er increases from 0 wt% to 0.6 wt%. In addition, the alloy exhibits an outstanding combination of mechanical and wear resistance properties at a Sc–Er addition of 0.6 wt%. Compared with the unmodified alloy, its ultimate tensile strength has increased from 82.7 MPa to 148.4 MPa and average friction coefficient has decreased from 0.689 to 0.504.

Graphical Abstract

低共晶铝硅合金(A360)被广泛用于航空航天、汽车和建筑行业的高压压铸部件。实验研究了不同稀土 Sc 和 Er 添加量对 A360 合金凝固过程的影响。结果表明,添加 Sc 和 Er 元素后会形成沉淀相 Al(Sc,Er)2Si2。此外,当 Sc-Er 的含量从 0 wt% 增加到 0.6 wt% 时,共晶 Si 相从粗糙的块状和不规则的多边形演变成粒状形态,其平均粒度值从 25.48 μm 减小到 9.46 μm。此外,Sc-Er 的添加量为 0.6 wt%时,合金的机械性能和耐磨性能表现出了出色的结合。与未改性合金相比,其极限抗拉强度从 82.7 兆帕增加到 148.4 兆帕,平均摩擦系数从 0.689 降至 0.504。
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引用次数: 0
Numerical Analysis of the Influence of Demolding Temperature on Final Distortion in Gravity Die Casting Process 重力压铸工艺中脱模温度对最终变形影响的数值分析
IF 2.6 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-06 DOI: 10.1007/s40962-024-01398-2
S. Gor, N. Wolff, B. Pustal, A. Bührig-Polaczek

Distortion can be a prominent issue in the production of metal casting components, especially when using metal dies. Existing research underscores the pivotal role of the temperature at which the solidified component is extracted from the mold in contribution to the ultimate distortion of the component. This numerical investigation seeks a comprehensive understanding of the factors governing deformation by employing simulations that emulate experimental conditions. The study utilizes coupled thermomechanical simulations, executed through the commercial software “Abaqus,” across varying demolding temperatures. The temporal evolution of distortion is examined, with a focus on influential factors such as elastic and thermal strain. A quantitative and qualitative comparison is drawn between simulation outcomes and experimental results. The difference between experimental and simulation results was observed to increase linearly with higher demolding temperatures. The potential for leveraging the qualitative similarity between experimental and simulation results as a foundation for the development of distortion control strategies is deliberated.

变形是金属铸造部件生产中的一个突出问题,尤其是在使用金属模具时。现有研究强调,凝固部件从模具中取出时的温度对部件的最终变形起着关键作用。这项数值研究通过模拟实验条件,力求全面了解影响变形的因素。研究利用商业软件 "Abaqus "对不同的脱模温度进行热力学耦合模拟。对变形的时间演变进行了研究,重点是弹性应变和热应变等影响因素。对模拟结果和实验结果进行了定量和定性比较。实验结果和模拟结果之间的差异随着脱模温度的升高而呈线性增长。讨论了利用实验和模拟结果之间的定性相似性作为开发变形控制策略基础的可能性。
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引用次数: 0
Thermal Profile and Microstructure Analysis of Al-Si with the Magnesium Addition under Different Cooling Conditions 不同冷却条件下加镁铝硅的热曲线和微观结构分析
IF 2.6 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-06 DOI: 10.1007/s40962-024-01388-4
M. F. Mohamad Tajudin, A. H. Ahmad, J. Alias, N. A. Abd Razak, S. Naher

Thermal analysis is an effective approach for studying the characteristics of materials under different temperature situations. The study implemented cooling curve analysis (CCA), complemented by computational methods for precisely evaluating the temperature variation of the molten alloy by employing two thermocouples. An aluminium alloy with 1 wt.% Mg addition was melted in graphite crucible and subjected to various cooling conditions, which included normal, slow, fast, and fastest cooling rate conditions. Normal cooling condition (A) was achieved when the crucible was allowed to cool down to room temperature. Meanwhile, the slow cooling condition (B) was achieved when the crucible was allowed to cool within the Kaowool insulator chamber. In addition, the fast (C) and fastest (D) cooling conditions were attained when the forced airflow was directed at the crucible at minimum and maximum speed, respectively. The temperature data were collected via K-type thermocouples connected to a Ni 9129 data acquisition system and DasyLab software. Cooling curves, cooling curves with baselines, dendritic coherency points, and solid fractions were then recorded using OriginPro 2019b software. The liquidus, eutectic, and solidus temperatures were determined. The microstructure of the alloy sample was characterised by optical microscopy (OM), scanning electron microscopy (SEM), combined with energy-dispersive X-ray spectroscopy (EDX), and X-ray diffraction (XRD) analysis. The results show that the high cooling rates produced smaller and more globular grain structures. The highest cooling rate condition produced smaller and globular microstructure formation at 944 µm2 and a circularity of 0.61, respectively. Meanwhile, the slow cooling condition produced the largest grain size at 1668 µm2 and a circularity of 0.46. The results show that higher cooling rates result in a smaller and more spherical grain structure than other cooling conditions. This underlines the significant influence of the cooling rate on the development of the microstructure during the solidification process. This comprehensive thermal analysis study has shed light on the significant influence of Mg addition and different cooling conditions on the Al-Si alloy's thermal properties and microstructure formation. The results contribute to understanding alloy solidification and may have practical implications for materials engineering and manufacturing.

热分析是研究不同温度条件下材料特性的有效方法。本研究采用了冷却曲线分析法(CCA),并辅以计算方法,通过使用两个热电偶精确评估熔融合金的温度变化。在石墨坩埚中熔化了添加 1 wt.% Mg 的铝合金,并将其置于各种冷却条件下,包括正常、慢速、快速和最快冷却速率条件。正常冷却条件(A)是让坩埚冷却到室温。同时,在慢速冷却条件(B)下,让坩埚在考伍尔绝缘体室内冷却。此外,当强制气流分别以最小和最大速度冲向坩埚时,可达到快速(C)和最快(D)冷却条件。温度数据通过连接到 Ni 9129 数据采集系统和 DasyLab 软件的 K 型热电偶采集。然后使用 OriginPro 2019b 软件记录冷却曲线、带基线的冷却曲线、树枝状相干点和固体分数。确定了液相温度、共晶温度和固相温度。通过光学显微镜(OM)、扫描电子显微镜(SEM),结合能量色散 X 射线光谱(EDX)和 X 射线衍射(XRD)分析,对合金样品的微观结构进行了表征。结果表明,高冷却速率产生的晶粒结构更小、更球状。最高冷却速率条件下形成的微观结构更小,呈球状,面积为 944 µm2,圆度为 0.61。同时,慢速冷却条件下产生的晶粒尺寸最大,为 1668 µm2,圆度为 0.46。结果表明,与其他冷却条件相比,较高的冷却速率会产生更小和更球形的晶粒结构。这凸显了冷却速率对凝固过程中微观结构发展的重要影响。这项全面的热分析研究揭示了添加镁和不同冷却条件对铝硅合金热性能和微观结构形成的重要影响。研究结果有助于理解合金凝固,并可能对材料工程和制造产生实际影响。
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引用次数: 0
Mechanical, Microstructural and Wear Studies of a Ceramic Hybrid Reinforced ZE41 Magnesium Metal Matrix Composite Through Stir Casting Route 通过搅拌铸造工艺对陶瓷混合增强 ZE41 镁金属基复合材料进行力学、微结构和磨损研究
IF 2.6 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-04 DOI: 10.1007/s40962-024-01392-8
N. Anand, Senthil Kumaran Selvaraj

In this investigation, ZE41 magnesium alloys reinforced with 2% weight of SiC and B4C were manufactured through stir casting route under an inert environment. The microstructure of the unreinforced alloy, exhibits α Mg grains with uniformly distributed β Mg7Zn3 intermetallic phases at the grain boundaries. The addition of ceramic reinforcements decreased the average grain size and also formulated thin β Mg7Zn3 phases compared to the denser ones observed in the pure base matrix. The results of this work demonstrated that the tensile strength of the composites improved due to particle strengthening, grain refinement and presence of dislocations at the intermetallic regions and the best results were obtained for the hybrid ZE41 matrix (ZE41 + 2% SiC + 2% B4C). The tensile strengthening mechanisms of the composites are discussed and the expected theoretical values of yield strengths are calculated for comparison. Additionally, the specimens' elastic moduli were evaluated experimentally and theoretically (using the Tsai Halpin model), with the results showing good agreement, particularly for the hybrid composite. The morphologies of the fractured specimens were also analysed and it has been observed that the hybrid composite exhibited a ductile mode of fracture due to the presence of uniform dimples. The impact strength and hardness values of all the composites was also found experimentally and the best results were obtained for SiC and B4C composites which played a vital role in the selection of reinforcement particles for developing the hybrid composites. The wear analysis of the composites and their surface morphologies displayed considerable increase in friction coefficient and specific wear rate for hybrid composites at low and high loads.

Graphical Abstract

本研究在惰性环境下,通过搅拌铸造工艺制造了添加 2% SiC 和 B4C 的 ZE41 镁合金。未增强合金的微观结构表现为 α Mg 晶粒,晶界上均匀分布着 β Mg7Zn3 金属间相。添加陶瓷增强材料后,平均晶粒尺寸减小,β Mg7Zn3 相也变得稀疏,而纯基体中的β Mg7Zn3 相则更加致密。这项工作的结果表明,由于颗粒强化、晶粒细化和金属间区域位错的存在,复合材料的拉伸强度得到了提高,而混合 ZE41 基体(ZE41 + 2% SiC + 2% B4C)的结果最好。讨论了复合材料的拉伸强化机制,并计算了屈服强度的预期理论值,以进行比较。此外,还对试样的弹性模量进行了实验和理论评估(使用蔡-哈尔平模型),结果显示两者吻合良好,尤其是混合复合材料。此外,还对断裂试样的形态进行了分析,发现混合复合材料由于存在均匀的凹痕而呈现出韧性断裂模式。实验还发现了所有复合材料的冲击强度和硬度值,其中 SiC 和 B4C 复合材料的结果最好,这对选择开发混合复合材料的增强粒子起到了至关重要的作用。对复合材料及其表面形态进行的磨损分析表明,混合复合材料在低负荷和高负荷下的摩擦系数和特定磨损率都有显著增加。
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引用次数: 0
Revealing the Role of Minor Zn and Zr Element Addition in Hot Tearing Susceptibility of Mg–Gd–Y Alloy 揭示添加少量 Zn 和 Zr 元素在 Mg-Gd-Y 合金热撕裂敏感性中的作用
IF 2.6 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-04 DOI: 10.1007/s40962-024-01344-2
Bingcheng Li, Jing Zhang, Quan Dong, Fawang Ye

The hot tearing susceptibility (HTS) of Mg–5Gd–6Y alloy with 1 wt% Zn and 0.5 wt% Zr additions is investigated based on the constrained rod casting experiments and thermodynamic calculation. It shows that a minor Zn addition aggravates the HTS which cannot even be compensated by the grain refining effect of a further Zr addition. Moreover, the alloys with minor Zn and Zr addition show earlier hot tearing initiation (before the volumetric contraction force reaching minimum value). According to the calculation of prevailing criteria, minor Zn and Zr additions affecting the HTS has little relationship with the changing of the Scheil solidification curves. The mass formation of the X-Mg12YZn phases in alloys with a minor Zn addition is the main cause of earlier hot tearing initiation and higher HTS. The phases with a higher elastic modulus result in poor liquid feeding among the α-Mg matrix and early dendrite bridging, causing more cavities, earlier strain accumulation at hot spots, and consequently earlier hot tearing initiation and higher HTS.

基于约束棒铸造实验和热力学计算,研究了添加 1 wt% Zn 和 0.5 wt% Zr 的 Mg-5Gd-6Y 合金的热撕裂敏感性(HTS)。结果表明,少量 Zn 的添加会加剧 HTS,而进一步添加 Zr 的晶粒细化效应甚至无法弥补这一点。此外,添加少量 Zn 和 Zr 的合金会更早出现热撕裂(在体积收缩力达到最小值之前)。根据现行标准计算,少量添加 Zn 和 Zr 对 HTS 的影响与 Scheil 凝固曲线的变化关系不大。在添加少量 Zn 的合金中,X-Mg12YZn 相的大量形成是热撕裂提前开始和 HTS 提高的主要原因。弹性模量较高的相会导致α-镁基体之间的液体喂入不良和早期树枝晶架桥,从而造成更多的空穴、更早的热点应变积累,进而导致更早的热撕裂和更高的 HTS。
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引用次数: 0
Performance and Microstructural Features of Sodium Silicate Shell Cured via Microfluidic Droplets of Citric Acid Solution 通过柠檬酸溶液微流滴固化硅酸钠外壳的性能和微结构特征
IF 2.6 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-03 DOI: 10.1007/s40962-024-01394-6
Yujie Yuan, Chang Liu, Zhijun Chen, Zhongxing Tian, Xiangdong Liu

The large solid waste discharge of investment casting shells is closely related to its unstable performance of shells and uncontrolled curing reaction. The unique advantage of microfluidic technology is that it can effectively control the chemical reaction process. In the present work, an environmentally friendly citric acid widely used in food as hardening agent was employed to cure a sodium silicate shells. Droplets of citric acid solution with a concentration of 1.5 × 10−3 mol/L were generated by microfluidic technology and spread on the surfaces of shell specimens driven by air flow to induce the shell hardening. The green-, fired-, residual-strength, high temperature self-weight deformation, and gas to permeability of the shell were investigated. The results showed that the peak strength reached 30.38 MPa for green shell and 10.61MPa for the fired shell, about 26.4% and 17.4% higher than the immersion method, respectively. The fracture morphology of the shell observed by SEM (Scanning Electron Microscopy) confirmed that the more uniform, and far less cracks and micropores formed on the sodium silicate film of shells hardened by microfluidic droplets than the dipping method. The analysis of FTIR (Fourier Transform Infrared Spectroscopy) reveals that the final products of sodium silicate gel cured by microfluidic droplets achieved a high degree of polymerization and generated a relatively dense Si–O–Si cellular structure. The phase composition and thermal stability of the shell were analyzed by XRD (X-ray Diffraction) and TG-DSC (Thermogravimetric Differential Scanning Calorimetry). The results demonstrate that the improvement in hardening performance of shells is due to reaction microfluidic technology that can precisely control the volume and rate of hardening agent droplets, which can improve the repeatability and stability of the reaction in a short time, as well as reduce the damage of the gel film during the hardening process, and improve the quality of the gel film. The resulting shell can achieve higher strength and stability.

熔模铸造型壳固体废物排放量大,与其型壳性能不稳定、固化反应不可控密切相关。微流控技术的独特优势在于可以有效控制化学反应过程。在本研究中,采用了一种广泛应用于食品中的环保型柠檬酸作为固化剂来固化硅酸钠铸壳。利用微流体技术生成浓度为 1.5 × 10-3 mol/L 的柠檬酸溶液液滴,并在气流的驱动下将其扩散到外壳试样表面,从而诱导外壳硬化。研究了壳体的生坯强度、烧成强度、残余强度、高温自重变形和气体渗透性。结果表明,绿壳的峰值强度达到 30.38 兆帕,烧成壳的峰值强度达到 10.61 兆帕,分别比浸泡法提高了约 26.4% 和 17.4%。扫描电子显微镜(SEM)观察到的贝壳断裂形态证实,微流液滴法硬化的贝壳硅酸钠膜上形成的裂纹和微孔比浸渍法更均匀、更少。傅立叶变换红外光谱(FTIR)分析表明,微流液滴固化硅酸钠凝胶的最终产品实现了高度聚合,并生成了相对致密的 Si-O-Si 蜂窝结构。通过 XRD(X 射线衍射)和 TG-DSC(热重差示扫描量热法)分析了外壳的相组成和热稳定性。结果表明,贝壳硬化性能的提高得益于反应微流控技术,该技术可以精确控制淬火剂液滴的体积和速率,从而在短时间内提高反应的重复性和稳定性,并减少硬化过程中对凝胶膜的破坏,提高凝胶膜的质量。由此产生的外壳可以达到更高的强度和稳定性。
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引用次数: 0
Metalcasting Industry Research 金属铸造行业研究
IF 2.6 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-03 DOI: 10.1007/s40962-024-01393-7
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引用次数: 0
Shrinkage Investigation of Ductile Iron Castings 球墨铸铁铸件的收缩调查
IF 2.6 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-01 DOI: 10.1007/s40962-024-01360-2
Anhua Yu, Michael Whaley

It has been a challenging mission to assure that ductile iron castings meet customer internal soundness specifications with acceptable process capabilities to get approval in new automotive model launch processes. Shrinkage conditions were investigated in the new program launch stage. Several factors were investigated including carbon equivalent, carbon levels, silicon levels, molten iron preconditioners and other additives. This study investigated shrinkage size by taking digital photos and measuring each shrinkage indication size using software comparing to the size limits from the customer Internal Soundness Specification. Thermal analysis was utilized to evaluate iron conditions to correlate shrinkage tendency. Statistical tools were applied to determine whether the factors in this investigation truly affected casting shrinkage characteristics. High process capability (Ppk) values were achieved by adopting optimal process parameters and using proper additives, and the program was launched successfully. Additional studies were conducted to confirm that the ductile iron meets customer specification including mechanical properties, microstructure, impact property, and casting hardnessunder all conditions.

如何确保球墨铸铁铸件符合客户的内部健全性规范,并具备可接受的工艺能力,以获得新车型推出流程的批准,一直是一项具有挑战性的任务。在新项目启动阶段,对收缩条件进行了调查。调查的因素包括碳当量、碳含量、硅含量、铁水预处理剂和其他添加剂。这项研究通过拍摄数码照片和使用软件测量每种收缩迹象的尺寸,并与客户内部完好性规范的尺寸限制进行比较,从而对收缩尺寸进行调查。热分析用于评估铁水条件,以关联收缩趋势。应用统计工具来确定本次调查中的因素是否真正影响了铸件的收缩特性。通过采用最佳工艺参数和适当的添加剂,获得了较高的工艺能力 (Ppk) 值,并成功启动了该计划。还进行了其他研究,以确认球墨铸铁在所有条件下都符合客户的规格要求,包括机械性能、微观结构、冲击性能和铸造硬度。
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引用次数: 0
期刊
International Journal of Metalcasting
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