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The Influence of TiB2 Particles on the Artificial Aging Behavior of TiB2/Al–5Cu Composite TiB2 颗粒对 TiB2/Al-5Cu 复合材料人工老化行为的影响
IF 2.6 3区 材料科学 Q2 Materials Science Pub Date : 2024-05-11 DOI: 10.1007/s40962-024-01316-6
Yiwang Jia, Xiaojuan Shang, YunChe, Zhengcai Liu, Qibin Liu, Renguo Zhang, Sanquan Men, Xiang Li, Yongxiang Li

This study investigated the artificial aging process of TiB2/Al–5Cu composite, with a focus on the influence of TiB2 particles on the precipitation behavior of the composite. Additionally, a comparative analysis of the microhardness and tensile properties between the TiB2/Al–5Cu composite and the Al–5Cu alloy was conducted. X-ray Diffraction (XRD) analysis reveals that the TiB2/Al–5Cu composite consists of TiB2 and Al2Cu phases. The Scanning Electron Microscopy (SEM) imagery demonstrates a predominantly cellular crystal composition in the composite. Notably, as the aging time progresses, there’s an initial increase followed by a subsequent decrease in the gray grain boundaries of the composite. Transmission Electron Microscopy (TEM) images uncover the presence of needle-like θ phase, TiB2, and dislocations within the TiB2/Al–5Cu composite. The incorporation of TiB2 particles has emerged as a pivotal factor in significantly curtailing the artificial aging duration. With the peak hardness aging time determined at a mere 8 h, the TiB2/Al–5Cu composite showcases substantially higher hardness levels compared to the Al–5Cu base alloy. Remarkably, the optimum aging time for achieving the best mechanical properties in the composites is reduced from 20 to 8 h. Directly comparing the TiB2/Al–5Cu composite to the Al–5Cu alloy under peak aging conditions, notable enhancements in both yield strength (22%) and tensile strength (41%) are observed. Additionally, a slight increase in elongation is observed in the TiB2/Al–5Cu composite.

本研究调查了 TiB2/Al-5Cu 复合材料的人工老化过程,重点研究了 TiB2 颗粒对复合材料析出行为的影响。此外,还对 TiB2/Al-5Cu 复合材料和 Al-5Cu 合金的显微硬度和拉伸性能进行了对比分析。X 射线衍射 (XRD) 分析表明,TiB2/Al-5Cu 复合材料由 TiB2 和 Al2Cu 两相组成。扫描电子显微镜(SEM)图像显示,复合材料中主要是蜂窝状晶体成分。值得注意的是,随着老化时间的推移,复合材料的灰色晶界开始增加,随后逐渐减少。透射电子显微镜(TEM)图像显示,TiB2/Al-5Cu 复合材料中存在针状 θ 相、TiB2 和位错。TiB2 颗粒的加入是显著缩短人工老化时间的关键因素。与 Al-5Cu 基合金相比,TiB2/Al-5Cu 复合材料的峰值硬度老化时间仅为 8 小时,因此硬度水平大大提高。在峰值老化条件下,将 TiB2/Al-5Cu 复合材料与 Al-5Cu 合金进行直接比较,可观察到屈服强度(22%)和拉伸强度(41%)均有显著提高。此外,还观察到 TiB2/Al-5Cu 复合材料的伸长率略有增加。
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引用次数: 0
Simulation and Experimental Investigation of a Combined Control Method for Stray Grain During Single Crystal Blade Solidification 单晶叶片凝固过程中杂散晶粒组合控制方法的模拟与实验研究
IF 2.6 3区 材料科学 Q2 Materials Science Pub Date : 2024-05-11 DOI: 10.1007/s40962-024-01357-x
Haoyu Zhao, Kun Bu, Binqiang Wang, Sheng Mou, Pengguo Duan

It is of great significance to effectively prevent the stray grain defect at the edge plate of nickel-based superalloy single crystal blades. In this study, the evolution of the mushy zone and the growth of grain adjacent to the edge plate was first simulated by the temperature field and cellular automaton-finite element (CAFÉ) model, combined with a single crystal blade solidification experiment; it was proved that modifying the withdrawal rate alone was insufficient to prevent the stray grain formation. Then, the formation reason of the heat barrier zone and the irregular distribution pattern of the mold shell thickness were revealed by quantifying the present mold shell thickness near the edge plate through an industrial conical beam computed tomography. Based on these results, a combined control method for stray grain was proposed, which involves the use of precise measures such as non-uniform mold design, exact addition of process bars, and variable withdrawal rate. Simulation analysis demonstrated that this method can substantially reduce the undercooling range and average undercooling at the edge plate by 45.5% and 31.6%, respectively, and then eliminate the isolated undercooling zone. The macrostructure and microstructure of the blade cast by this method verified the effectiveness in inhibiting stray grain, and it will be a promising approach to manufacturing single crystal blades.

有效防止镍基超合金单晶叶片边缘板的杂散晶粒缺陷具有重要意义。本研究首先通过温度场和单元自动机-有限元(CAFÉ)模型,结合单晶叶片凝固实验,模拟了叶片刃板附近的粘滞区和晶粒生长的演变过程;实验证明,仅通过改变退模速率不足以防止杂散晶粒的形成。然后,通过工业锥形束计算机断层扫描对边缘板附近的现有模壳厚度进行量化,揭示了热障区的形成原因和模壳厚度的不规则分布模式。在此基础上,提出了游离晶粒的组合控制方法,包括使用非均匀模具设计、精确添加工艺棒和可变退模率等精确措施。仿真分析表明,该方法可将边缘板的欠冷范围和平均欠冷量分别大幅降低 45.5% 和 31.6%,进而消除孤立的欠冷区。用这种方法铸造的叶片的宏观结构和微观结构验证了抑制杂散晶粒的有效性,它将是制造单晶叶片的一种有前途的方法。
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引用次数: 0
Three-Dimensional Micromechanical Modelling of Deformation Behaviour of Rheocast A356 Alloy 流变铸造 A356 合金变形行为的三维微观力学建模
IF 2.6 3区 材料科学 Q2 Materials Science Pub Date : 2024-05-10 DOI: 10.1007/s40962-024-01342-4
Durgesh Kumar Pandey, Prosenjit Das

In this study, a micromechanical approach is used to investigate the deformation behaviour of rheocast Al–7Si–0.3Mg alloy. The alloy is rheocast using a cooling slope (at 45° and 60° angles) after melt treatment with a grain refiner addition (0.15% by weight Al–5Ti–1B master alloy). The comparison is made with the conventionally cast sample of the same alloy. Microscale instability of the rheocast alloy occurring at the onset of deformation, due to the strain incompatibility between the primary and eutectic phases, causes stress and strain localization as well as a triaxial state of stress, which subsequently governs void initiation and growth in the said alloy. A commercial finite element (FE) code ABAQUS is used to simulate microscale deformation behaviour of the three-dimensional representative volume elements (RVE) of approximated and as well as actual microstructure of the said alloy under uniaxial tensile loading. Although, globally uniaxial tensile loading is applied over the RVEs, however, stress triaxiality causes local variation of stress state, as evident from biaxial tensile stress state observed at grain boundaries of the above-mentioned RVEs, whereas uniaxial tensile stress is observed at the central location of these RVEs. Simulation results reveal that the macroscale deformation behaviour of the said alloy is determined by its microscopic features such as shape, size, distribution (spread of primary Al grains within the volume element) and volume fraction of primary Al grains. Moreover, distribution as well as volume fraction of eutectic Si also plays deciding role in deformation behaviour of the alloy. The FE model predictions of improved deformation behaviour/stress distribution evidenced in the rheocast + grain refined alloy is validated via phase level mechanical properties of the alloy, estimated from nanoindentation.

本研究采用微机械方法研究流变铸造 Al-7Si-0.3Mg 合金的变形行为。合金是在添加晶粒细化剂(0.15%(重量)Al-5Ti-1B 母合金)的熔体处理后,利用冷却斜坡(45° 和 60°角)进行流变铸造的。与相同合金的传统铸造样品进行了比较。由于原生相和共晶相之间的应变不相容性,流变铸造合金在变形开始时会出现微观不稳定性,导致应力和应变局部化以及三轴应力状态,进而影响上述合金中空洞的产生和增长。我们使用商业有限元(FE)代码 ABAQUS 来模拟上述合金在单轴拉伸载荷下近似和实际微观结构的三维代表体积元素(RVE)的微尺度变形行为。虽然在 RVE 上施加的是全局单轴拉伸载荷,但应力的三轴性会导致应力状态的局部变化,在上述 RVE 的晶界处观察到的双轴拉伸应力状态就是证明,而在这些 RVE 的中心位置观察到的是单轴拉伸应力。模拟结果表明,上述合金的宏观变形行为取决于其微观特征,如形状、尺寸、分布(原生铝晶粒在体积元素中的分布)和原生铝晶粒的体积分数。此外,共晶硅的分布和体积分数也对合金的变形行为起着决定性作用。流变铸造+晶粒细化合金的变形行为/应力分布得到了改善,其有限元模型预测结果通过合金的相级机械性能(由纳米压痕估算得出)得到了验证。
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引用次数: 0
Solidification Processing of Reduced Graphene Oxide Dispersed Aluminum Composites by Squeeze Casting 用挤压铸造法凝固处理还原氧化石墨烯分散铝复合材料
IF 2.6 3区 材料科学 Q2 Materials Science Pub Date : 2024-05-10 DOI: 10.1007/s40962-024-01348-y
A. G. Arsha, Omid Ghaderi, T. P. D. Rajan, P. K. Rohatgi

The present paper is on the processing of Al (A356)- reduced Graphene Oxide (rGO) composites by the squeeze casting technique to obtain improved mechanical and thermal properties. Reduced graphene oxide, a two-dimensional carbon allotrope with very high mechanical properties and thermal conductivity is used as a reinforcement in A356 aluminum alloy. Graphite was initially converted to rGO using the Hummers Method. 0.3 to 0.75 wt% weight percentages of rGO were incorporated into the aluminum alloy using a combination of stir mixing in semisolid state followed by squeeze casting, a hybrid method was employed to produce rGO reinforced A356 alloy matrix composite after applying mechanical stirring for uniform dispersion. Squeeze pressure was crucial for increasing the cooling rate to get finer microstructure, and eliminating the porosity. Reduced Graphene oxide uniformly within the Al 356 alloy matrix by applying both mechanical stirring for dispersion and squeeze pressure for rapid solidification and pore free casting. The squeeze cast Al 356-0.5%rGO composites after T6 heat treatment had an increase in tensile strength from 260 MPa for A356 alloy to 346 MPa, an increase in hardness 106 BHN to 130 BHN, and a reduction in coefficient of thermal expansion (CTE) from 21.7 × 10−6/°C to 10.8 × 10−6/°C at RT-50 °C. These results suggest potential applications of these composites in high performance industrial, automotive, and aerospace sectors.

本文介绍了通过挤压铸造技术加工铝(A356)-还原氧化石墨烯(rGO)复合材料,以获得更好的机械性能和热性能。还原氧化石墨烯是一种二维碳同素异形体,具有极高的机械性能和热导率,被用作 A356 铝合金的增强材料。最初采用 Hummers 法将石墨转化为 rGO。在铝合金中加入 0.3 至 0.75 wt% 重量百分比的 rGO,在半固态下进行搅拌混合,然后进行挤压铸造,在应用机械搅拌均匀分散后,采用混合方法生产出 rGO 增强 A356 合金基复合材料。挤压压力对提高冷却速度以获得更精细的微观结构和消除孔隙至关重要。通过机械搅拌使氧化石墨烯均匀地分散在 Al 356 合金基体中,并施加挤压力使其快速凝固和无孔隙浇铸。经过 T6 热处理后,挤压铸造的 Al 356-0.5%rGO 复合材料的抗拉强度从 A356 合金的 260 兆帕提高到 346 兆帕,硬度从 106 BHN 提高到 130 BHN,在 RT-50 °C 时的热膨胀系数 (CTE) 从 21.7 × 10-6/°C 降低到 10.8 × 10-6/°C。这些结果表明,这些复合材料有望应用于高性能工业、汽车和航空航天领域。
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引用次数: 0
Comparison of Microstructure and Non-metallic Inclusions in Top-Filled and Bottom-Filled Gray Iron Castings 顶部填充和底部填充灰铁铸件中显微结构和非金属夹杂物的比较
IF 2.6 3区 材料科学 Q2 Materials Science Pub Date : 2024-05-10 DOI: 10.1007/s40962-024-01356-y
Evan Carter, Jingjing Qing, Mingzhi Xu

A bottom-filled rigging system was designed to produce gray iron castings, which was compared with a top-filled design in the present study. Filling and solidification of gray iron produced with the bottom-filled mold were compared with that for the top-filled mold. At similar cooling rate and solidification condition, the count of Type A graphite flakes was greater in the bottom-filled casting, while its graphite flakes were also finer in size. In addition, the statistical analysis of non-metallic inclusions using a scanning electron microscope equipped with auto feature analysis software also showed differences in inclusion composition, size, and population density between two castings. The results indicated that the filling turbulence promoted interactions between metal with air, which in turn influenced the formation of non-metallic inclusions. As a result, this impacted the nucleation of flake graphite in the gray iron.

为生产灰铁铸件,设计了一种底部填充的索具系统,并在本研究中将其与顶部填充的设计进行了比较。对使用底部填充模具和顶部填充模具生产的灰铁的填充和凝固情况进行了比较。在相似的冷却速度和凝固条件下,底部填充铸件的 A 型石墨片数量更多,石墨片的尺寸也更细。此外,使用配备自动特征分析软件的扫描电子显微镜对非金属夹杂物进行统计分析,也显示出两种铸件在夹杂物成分、尺寸和数量密度上的差异。结果表明,充填湍流促进了金属与空气之间的相互作用,进而影响了非金属夹杂物的形成。因此,这影响了灰铁中片状石墨的成核。
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引用次数: 0
3D Printed Smart Mold for Sand Casting: Monitoring Binder Curing 用于砂模铸造的 3D 打印智能模具:监控粘合剂固化
IF 2.6 3区 材料科学 Q2 Materials Science Pub Date : 2024-05-09 DOI: 10.1007/s40962-024-01314-8
Nathaniel Bryant, Josh O’Dell, Sairam Ravi, Jerry Thiel, Janely Villela, Juan Owen Villela, Eric MacDonald, Alan Alemán, Brandon Lamoncha, Brian Vuksanovich, Rich Lonardo

The design freedom of 3D printing allows for new mold designs—not possible with traditional approaches—such as helical sprues and spatially varying lattice castings. However, research on the curing time of printed molds, including the aging, requires more exploration. This study describes the experiments of 3D printed specimens in which embedded environmental sensors were fully encapsulated into sand blocks during an interruption of the binder jetting process. Subsequently, over a 28-day duration, humidity, volatile organic compound (VOC) generation, temperature and barometric pressure were captured for three environmental treatments. Mechanical testing of standard test specimens subjected to the same conditions was conducted. The sand structures held in high (uncontrolled) humidity and at reduced temperature were statistically weaker than a third treatment based on the hypothesis that high humidity and/or low temperatures impede curing.

三维打印的设计自由度允许采用传统方法无法实现的新型模具设计,例如螺旋浇口和空间变化的晶格铸件。然而,对打印模具固化时间(包括老化)的研究还需要更多探索。本研究介绍了三维打印试样的实验情况,其中嵌入的环境传感器在粘合剂喷射过程中断期间被完全封装到砂块中。随后,在 28 天的持续时间内,对三种环境处理方法的湿度、挥发性有机化合物 (VOC) 生成量、温度和气压进行了采集。在相同条件下对标准试样进行了机械测试。根据高湿度和/或低温会阻碍固化的假设,在高湿度(不受控制)和低温条件下的砂结构在统计学上比第三种处理方法更弱。
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引用次数: 0
GG20-GCI Brake Drum: The Effect of Mn/S on Machinability and Tensile Behavior GG20-GCI 制动鼓:Mn/S 对机械加工性能和拉伸行为的影响
IF 2.6 3区 材料科学 Q2 Materials Science Pub Date : 2024-05-09 DOI: 10.1007/s40962-024-01355-z
Hanie Ghanbari, Mostafa Ketabchi, Esmaeil Damavandi

This study aims to assess the influence of the Mn to S ratios on the machinability and tensile behavior of GG20-gray cast iron brake drums. The effect of various Mn and S contents on microstructural characteristics such as type, size, and aspect ratio of graphite particles, interlamellar spacing of pearlite, and the distribution factor, size, and volume fraction of MnS were investigated. The microstructural results showed that a decrease in the Mn/S ratio to 5.1 and a decrease in the Ti/S ratio to under 0.11 promote the lengthy A-type graphite formation. Meanwhile, with the %Mn × %S value of about 0.08, the best uniform distribution of MnS inclusions has been obtained (about 55% of MnS inclusions are near A-type graphite flakes in the P1 specimen with %Mn × %S about 0.08 and Mn/S value of 5.1). Good machining in terms of less wear of the cutting tool and easier fragmentation of the chip in the sample with Mn/S value of 1.5 (0.65% Mn and 0.128% Sulfur) due to having more MnS inclusions, as well as a larger grain size graphite and its high aspect ratio have been obtained. The minimum tensile strength has been calculated to be 193MPa in the specimen with Mn/S value of 3.5 (0.55% manganese and 0.156% sulfur) due to the effects of higher sulfur content on changing the morphology of graphite to a higher aspect ratio. Meanwhile, at the same content of Mn (almost 0.55 wt%), further reduction of sulfur results in promoting E and D types of graphite in the microstructure.

Graphic Abstract

本研究旨在评估 Mn 与 S 的比率对 GG20 灰口铸铁制动鼓的可加工性和拉伸性能的影响。研究了不同 Mn 和 S 含量对微观结构特征的影响,如石墨颗粒的类型、尺寸和长宽比,珠光体的层间间距,以及 MnS 的分布因子、尺寸和体积分数。微观结构结果表明,Mn/S 比降至 5.1 和 Ti/S 比降至 0.11 以下会促进 A 型石墨的形成。同时,当 Mn × S%值约为 0.08 时,MnS夹杂物的分布均匀度最佳(在 Mn × S%值约为 0.08 和 Mn/S 值为 5.1 的 P1 试样中,约 55% 的 MnS 夹杂物靠近 A 型石墨片)。在 Mn/S 值为 1.5(锰含量为 0.65%,硫含量为 0.128%)的试样中,由于含有更多的 MnS 杂质,以及石墨晶粒尺寸更大、长宽比更高,因此切削工具的磨损更小,切屑更容易破碎,从而获得了良好的加工效果。在 Mn/S 值为 3.5(锰含量为 0.55%,硫含量为 0.156%)的试样中,计算得出的最小抗拉强度为 193MPa。同时,在相同的锰含量(近 0.55 wt%)下,进一步降低硫含量可促进微观结构中 E 型和 D 型石墨的形成。
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引用次数: 0
Mechanical and Wear Behavior of Al-Si5Cu3/ZrB2 In-Situ Reinforced Metal Matrix Composite Al-Si5Cu3/ZrB2 原位增强金属基复合材料的力学和磨损行为
IF 2.6 3区 材料科学 Q2 Materials Science Pub Date : 2024-05-07 DOI: 10.1007/s40962-024-01349-x
J. Jenix Rino, A. S. Vivekananda, N. Thangapandian, Balasivanandha Prabu Shanmugavel

In this study, the in-situ ZrB2/Al-Si5Cu3 aluminum alloy composites were fabricated through the salt-melt reaction route with different weight fractions of ZrB2 reinforcements, i.e., 2.5%, 5%, and 7.5%. The composites were tested for their density, hardness, tensile strength, flexural strength, impact strength, and wear properties. The influence of reinforcement on the properties was studied concerning the wt.% of reinforcement. The increase in density of composites compared to the matrix material confirms the formation of the in-situ reinforcement phase. The microstructure showed a desirable distribution of reinforced particles over the matrix at all weight fractions of the reinforcements in the composites. The ZrB2 particles formed in the matrix have particle sizes in the range from 255 nm to 955 nm and the grain size has been reduced from 242 microns to 110 microns as the result of particle-induced solidification. The hardness of the composites containing ZrB2 reinforcements of 2.5, 5, and 7.5 wt.% showed improvement by 8%, 17.5%, and 34% respectively compared to the parent alloy. There is an improvement in the tensile strength and elongation for the wt.% of ZrB2 up to 5 wt.%, from 115 MPa to 183 MPa, after which, there was a drop in the tensile strength. The detailed analysis of tensile fractography shows that the agglomerated ZrB2 reinforced particles at higher weight fractions lead to a decrease in strength. The results of flexural strength also affirm the strength of 5 wt.% ZrB2/Al-Si5Cu3 increased from the matrix material’s flexural strength of 337 MPa to 672 MPa. The wear study shows that the composite with 7.5 wt.% ZrB2 possesses a higher wear resistance. However, the impact strength did not show any differences in the weight % of reinforcement.

在本研究中,通过盐熔反应路线制造了原位 ZrB2/Al-Si5Cu3 铝合金复合材料,其中添加了不同重量分数的 ZrB2 增强材料,即 2.5%、5% 和 7.5%。对复合材料的密度、硬度、拉伸强度、弯曲强度、冲击强度和磨损性能进行了测试。研究了增强材料的重量百分比对性能的影响。与基体材料相比,复合材料密度的增加证实了原位增强相的形成。微观结构显示,在复合材料中所有重量百分比的增强材料中,增强颗粒在基体上都有理想的分布。在基体中形成的 ZrB2 颗粒的粒径范围在 255 纳米到 955 纳米之间,由于颗粒诱导凝固,晶粒大小从 242 微米减小到 110 微米。与母合金相比,含有 2.5、5 和 7.5 重量百分比 ZrB2 增强材料的复合材料的硬度分别提高了 8%、17.5% 和 34%。ZrB2 的重量百分比在 5 重量百分比以下时,拉伸强度和伸长率有所提高,从 115 兆帕提高到 183 兆帕,之后拉伸强度有所下降。拉伸断裂图的详细分析表明,重量分数越高,ZrB2 增强颗粒的团聚会导致强度下降。抗折强度结果也证实,5 重量百分比 ZrB2/Al-Si5Cu3 的抗折强度从基体材料的 337 兆帕增加到 672 兆帕。磨损研究表明,含 7.5 wt.% ZrB2 的复合材料具有更高的耐磨性。不过,冲击强度并未因增强材料的重量百分比而出现任何差异。
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引用次数: 0
Nano-Al2O3 Particle Incorporated in Al Matrix Composite by Vortex-Free High-Speed Stir Casting 通过无涡流高速搅拌铸造在铝基复合材料中加入纳米 Al2O3 粒子
IF 2.6 3区 材料科学 Q2 Materials Science Pub Date : 2024-05-07 DOI: 10.1007/s40962-024-01345-1
Yinan Lu, Yunhui Du, Weiyi Zhang, Hongzhen Tan, Nan Zhang, Yi Luo, Peng Zhang

Vortex-free high-speed stir casting (VFHSC) methodology can achieve uniform dispersion of particles in melt without air entrapment for fabricating particle reinforced composites, and it has been proved to be feasible for preparing micron-composites by this methodology. In this work, in order to study deeply on particles in nano-size magnitude in composites by this methodology, the preparation of 1.5 vol.% Nano-Al2O3p/Al–Cu–Mg–Si composite is also investigated. The proper stirring parameters for ideal particle dispersion are determined to prepare the materials. Porosity of the composite can be limited to 0.147 % under the VFHSC methodology. The composition and microstructure of ingots, including the incorporation of Al2O3 particles as well as the morphology of precipitated phases, are examined by OM, XRD, SEM, TEM, HRTEM and EDS. The nano-particles are incorporated ideally in the matrix with restricted aggregation and sedimentation, and the well-bounded Al2O3–Al interface possesses semi-coherent interface. Moreover, the VFHSC 1.5 vol.% Nano-Al2O3p/Al–Cu–Mg–Si composite exhibits obvious strengthening, limited ductility reduction, higher hardness as well as better wear resistance than those of matrix, validating the efficacy of the VFHSC methodology on fabricating 1.5 vol.% Nano-Al2O3p/Al–Cu–Mg–Si composite. The work proves that incorporating nano-particles in Al matrix by VFHSC methodology is feasible and efficient. The work presented in this paper proposes a viable approach for the fabrication of nanocomposites using the stir casting method, thereby offering valuable insights for further research on stir casting technology.

无涡流高速搅拌铸造(VFHSC)方法可实现颗粒在熔体中的均匀分散,不会夹带空气,用于制造颗粒增强复合材料,而且该方法已被证明可用于制备微米复合材料。在本研究中,为了深入研究该方法在复合材料中的纳米级颗粒,还研究了 1.5 vol.% 纳米 Al2O3p/Al-Cu-Mg-Si 复合材料的制备。在制备材料时,确定了理想颗粒分散的适当搅拌参数。在 VFHSC 方法下,复合材料的孔隙率可限制在 0.147%。通过 OM、XRD、SEM、TEM、HRTEM 和 EDS 检查了铸锭的成分和微观结构,包括 Al2O3 颗粒的加入以及沉淀相的形态。纳米颗粒在基体中的结合非常理想,聚集和沉积受到限制,Al2O3-Al 界面具有良好的半相干界面。此外,与基体相比,VFHSC 1.5 Vol.% 纳米 Al2O3p/Al-Cu-Mg-Si 复合材料表现出明显的增强性、有限的延展性降低、更高的硬度和更好的耐磨性,验证了 VFHSC 方法在制造 1.5 Vol.% 纳米 Al2O3p/Al-Cu-Mg-Si 复合材料上的有效性。这项工作证明,通过 VFHSC 方法在铝基体中加入纳米颗粒是可行且高效的。本文介绍的工作为利用搅拌铸造法制造纳米复合材料提出了一种可行的方法,从而为进一步研究搅拌铸造技术提供了宝贵的见解。
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引用次数: 0
SiC and MWCNT Blending Actions on Functional Performance of Hybrid AA2024 Alloy Nanocomposite Via Two Step Stir Cast Route 通过两步搅拌铸造工艺掺入 SiC 和 MWCNT 对混合 AA2024 合金纳米复合材料功能性能的影响
IF 2.6 3区 材料科学 Q2 Materials Science Pub Date : 2024-05-07 DOI: 10.1007/s40962-024-01351-3
M. Aruna, S. Kaliappan, D. V. V. S. B. Reddy Saragada, R. Venkatesh, V. Vijayan, Manzoore Elahi M. Soudagar, V. Mohanavel, Ismail Hossain, A. H. Seikh

The hybrid aluminium alloy matrix composites are adopted in high-strength-to-weight ratio applications with technical benefits, including high strength, good hardness, better stability, and improved thermal stability. This research is enhancing microstructural and mechanical functional behaviours of the hybrid aluminium alloy (AA2024) nanocomposites by the blending actions of nano silicon carbides (SiC) particles and multi-walled carbon nanotube (MWCNT) via a two-step stir cast route. The contribution effect of SiC and MWCNT blending actions on metallography, physical/mechanical qualities, and resistance to corrosion individualities of hybrid AA2024 nanocomposites are studied by the procedure of the American Society for Testing and Materials (ASTM) and compared to monolithic cast AA2024 alloy characteristics. The hybrid AA2024 nanocomposite blended with SiC and MWCNT (weight percentages of 5 and 8%) exposed the specific tailored benefits like homogenous scattered reinforcements resulting in a lower percentage value of porosity (≤ 1%), excellent ultimate tensile strength of 330 MPa with acceptable elongation range of 10%, enhanced indentation resistance capabilities of 128 HV, specific toughness of 15.2 J/mm2, and enhanced corrosion performance.

混合铝合金基复合材料具有高强度、高硬度、高稳定性和高热稳定性等技术优势,被广泛应用于高强度-重量比应用领域。本研究通过两步搅拌铸造工艺,在纳米碳化硅(SiC)颗粒和多壁碳纳米管(MWCNT)的混合作用下,增强混合铝合金(AA2024)纳米复合材料的微观结构和机械功能行为。根据美国材料与试验协会(ASTM)的程序,研究了碳化硅和多壁碳纳米管混合作用对混合 AA2024 纳米复合材料的金相、物理/机械质量和抗腐蚀特性的贡献效应,并与整体铸造的 AA2024 合金特性进行了比较。混合了 SiC 和 MWCNT(重量百分比分别为 5%和 8%)的混合 AA2024 纳米复合材料具有特定的定制优势,如均匀分散的增强体导致较低的孔隙率百分比值(≤ 1%)、330 兆帕的优异极限拉伸强度(可接受的伸长率范围为 10%)、128 HV 的更强抗压痕能力、15.2 J/mm2 的比韧性以及更强的耐腐蚀性能。
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International Journal of Metalcasting
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