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Preparation of Ti/CFRTP joint strengthened by carbon fiber cloth 碳纤维布增强Ti/CFRTP接头的制备
Pub Date : 2016-01-01 DOI: 10.2978/JSAS.11001
Hitoki Hasegawa, Shigehito Inui, Kazuma Shiraishi, Sho Ishii, A. Kasai, Y. Matsumura, Y. Nishi
A Ti/CF/CFRTP joint method was suggested for the carbon fiber reinforced thermoplastic ABS polymer (CFRTP), and titanium (Ti) with extremely large friction force induced by broad interface of carbon fiber cloth. The tensile stress-strain curves of Ti/CF/CFRTP joint prepared by lamination method by ABS plates and CF-cloth sheets were obtained. The maximum tensile strength and its strain in Ti/CF/CFRTP joint were extremely higher than those of Ti/ABS joints prepared by wrap-casting and gluing. Developing the joint improved the safety level of tensile strength.
提出了一种Ti/CF/CFRTP连接碳纤维增强热塑性ABS聚合物(CFRTP)和钛(Ti)的方法,该方法由于碳纤维布的宽界面而产生极大的摩擦力。得到了ABS板与CF布复合制备Ti/CF/CFRTP接头的拉伸应力-应变曲线。Ti/CF/CFRTP接头的最大抗拉强度和应变均显著高于包铸和胶合制备的Ti/ABS接头。开发接头提高了抗拉强度的安全水平。
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引用次数: 1
Experimental and theoretical investigations of structural and thermoelectric properties of gallium doped ZnO thin films 掺镓ZnO薄膜结构与热电性能的实验与理论研究
Pub Date : 2016-01-01 DOI: 10.2978/JSAS.11007
S. Morikawa, Tsukasa Kobayashi, M. Takashiri
We performed experimental and theoretical investigations of structural and thermoelectric properties of Ga-doped ZnO thin films. We prepared the thin films by a RF magnetron sputtering with various argon gas pressures, followed by thermal annealing at 500°C for 60 min in vacuum condition. We evaluated surface morphology and crystallographic properties as the structural properties of the ZnO thin films. To estimate the thermoelectric properties, we performed Hall measurement and the measurements of electrical conductivity, Seebeck coefficient and power factor. For theoretical analysis, we estimated an energy band structure of ZnO by first-principle calculation (ABINIT) based on density function theory with local density approximation, followed by the calculation of transport properties by BoltzTraP code. As a result, we found that the thin films at 2.0 Pa obtained the highest power factor of 0.73 μW/(cm・K2). Even though the transport properties were exhibited certain differences between the experimental results and the theoretical results, we observed the approximate trend of the transport propeties of ZnO.
我们对掺杂ga的ZnO薄膜的结构和热电性能进行了实验和理论研究。在不同的氩气压力下,采用射频磁控溅射法制备薄膜,然后在500℃真空条件下退火60 min。我们评价了ZnO薄膜的表面形貌和晶体学性质作为其结构性质。为了估计热电性能,我们进行了霍尔测量和电导率、塞贝克系数和功率因数的测量。在理论分析方面,我们利用基于密度函数理论的第一性原理计算(ABINIT)估计了ZnO的能带结构,并采用BoltzTraP编码计算了ZnO的输运性质。结果发现,在2.0 Pa下,薄膜的功率因数最高,为0.73 μW/(cm·K2)。虽然实验结果和理论结果之间存在一定的差异,但我们观察到ZnO的输运性质的近似趋势。
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引用次数: 0
In-situ evaluation methodology of functional layer for fusion blanket systems 熔敷层系统功能层的原位评价方法
Pub Date : 2016-01-01 DOI: 10.2978/JSAS.11008
N. Suzuki, Ryousuke Sasaki, R. Toyoda, Y. Matsumura
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引用次数: 1
Development of organic-inorganic hybrid perovskite solar cells 有机-无机杂化钙钛矿太阳能电池的研究进展
Pub Date : 2016-01-01 DOI: 10.2978/JSAS.13001
C. Yamamoto, Katsunori Maeda, T. Kaneko, M. Isomura, Joel Yamakawa, Y. Kunugi
We have investigated effectiveness of electroluminescence (EL) measurement as an estimation method for organic-inorganic perovskite solar cells. EL images of CH 3 NH 3 PbI 3 -based solar cells under a constant voltage of 1 V were obtained. We evaluated a relationship between the current density-voltage (J-V) characteristics of the solar cells and these EL images. It was found that EL intensity from our solar cell has a distribution with respect to the position. Because EL intensity indicates correlation with the power conversion efficiency (PCE) of the solar cell, the distribution of EL intensity results from inhomogeneity of properties of material in the cell. These findings mean that an EL measurement is effective for estimation of perovskite solar cells. Moreover, we confirmed effects of applying a voltage during the EL measurement for the solar cell characteristics. By measuring EL for 15 min, decrease of EL intensity with time and decrease of PCE were observed. During the EL measurement with a constant voltage, the applied current density increased continuously. These findings suggest that the resistance of perovskite layer in the solar cell decreases by applying a voltage.
我们研究了电致发光(EL)测量作为有机-无机钙钛矿太阳能电池评估方法的有效性。获得了ch3nh3pbi3基太阳能电池在恒定电压1v下的EL图像。我们评估了太阳能电池的电流密度-电压(J-V)特性与这些EL图像之间的关系。结果表明,太阳能电池的发光强度随位置的变化呈一定的分布。由于发光强度与太阳能电池的功率转换效率(PCE)有关,因此发光强度的分布是由于电池中材料性质的不均匀性造成的。这些发现意味着EL测量对于钙钛矿太阳能电池的估计是有效的。此外,我们还证实了在EL测量过程中施加电压对太阳能电池特性的影响。通过15 min的电致发光测量,观察到电致发光强度随时间的增加而降低,PCE降低。在恒电压下的电致发光测量过程中,外加电流密度不断增大。这些发现表明,施加电压可以降低太阳能电池中钙钛矿层的电阻。
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引用次数: 0
Measurement of the negative ions temperature in the hydrogen sheet plasma using an omegatron mass spectrometer contained a function of an ion energy analyzer 利用欧米茄电子质谱仪测量氢片等离子体中的负离子温度,该质谱仪具有离子能量分析仪的功能
Pub Date : 2016-01-01 DOI: 10.2978/JSAS.11009
Toshikio Takimoto, T. Iijima, Yuta Tanaka, A. Tonegawa, K. Kawamura, Kohnosuke Sato
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引用次数: 0
Visualization experiment of gas flow in dry gas seals 干气密封中气体流动的可视化实验
Pub Date : 2016-01-01 DOI: 10.2978/JSAS.11005
D. Suzuki, Shogo Kodama, M. Ochiai, Y. Sunami, H. Hashimoto
Dry gas seals are widely used for turbomachinery. Recently, they are being required to much further reduce gas leakage from many industries. It has known that sealing characteristics depend strongly on the geometry and dimensions of the grooves on the surfaces. Therefore, we conducted the optimization of groove geometry for improving the sealing characteristics. Moreover, the optimized dry gas seal was made and it was verified the effectiveness. In this study, it is intended that the effect of the groove geometry is verified. Therefore, the experimental apparatus to perform the leakage quantity measurement and visualization experiment was made. Moreover, it was conducted the leakage quantity measurement and visualization experiment of the air lubricating flow.
干气密封广泛应用于涡轮机械。最近,它们被要求进一步减少许多行业的气体泄漏。众所周知,密封特性在很大程度上取决于表面沟槽的几何形状和尺寸。因此,我们对槽的几何形状进行了优化,以提高密封特性。制作了优化后的干气密封,并对其有效性进行了验证。在本研究中,旨在验证沟槽几何形状的影响。为此,研制了用于泄漏量测量和可视化实验的实验装置。此外,还进行了空气润滑流动的泄漏量测量和可视化实验。
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引用次数: 1
Platinum catalyst formed on carbon nanotube by in-liquid plasma method for application to fuel cell 液体等离子体法制备碳纳米管上的铂催化剂,用于燃料电池
Pub Date : 2016-01-01 DOI: 10.2978/JSAS.11002
Yutaro Ueno, Y. Show
The in-liquid plasma was formed in the CNT dispersion by applying pulse high voltage between the platinum electrodes. The generated plasma spattered the surface of platinum electrodes and dispersed platinum particles in the CNT dispersion. The platinum with the weight of 21 mg was spattered by the applying pulse high voltage for 20 minutes. The spattered platinum particle was supported on the CNT surface. The platinum particles on the CNT were applied to the catalyst of the polymer electrolyte fuel cell. The open voltage of 0.91V and the maximum power of 1.47mW/cm were observed for the fuel cell.
通过在铂电极之间施加脉冲高压,在碳纳米管色散中形成了液体等离子体。产生的等离子体溅射在铂电极表面,并在碳纳米管分散体中分散铂颗粒。将重量为21 mg的铂通过施加脉冲高压溅射20分钟。溅射的铂粒子被支撑在碳纳米管表面。将碳纳米管上的铂颗粒应用于聚合物电解质燃料电池的催化剂中。该燃料电池的开启电压为0.91V,最大功率为1.47mW/cm。
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引用次数: 0
Adhesion by EB-irradiation between Laminated Sheets of Fluororesin and Polyurethan eb辐照下氟树脂与聚氨酯层合板的粘附性
Pub Date : 2016-01-01 DOI: 10.2978/JSAS.11003
Y. Miyazawa, Masato Uyama, Sho Ishii, Masae Kanda, Y. Nishi
Two layer Fluororesin/PU laminated sheets of fluororesin and polyurethane (PU) were prepared by a double-step treatment consisting of applying low dose ≦ 0.65 MGy homogeneous low energy electron beam irradiation (HLEBI) to the 2-layer assembly where the HLEBI penetrates through the fluororesin and PU layers, respectively, prior to hot-press under 5 MPa and 403 K. Although the adhesion of the Fluororesin/PU sheets cannot be observed without the double-step treatment, bonding forces were created as evidenced by the mean adhesive forces of peeling resistance ( o F p ). An increasing trend in o F p occurs by the double-step treatment applying HLEBI up to 0.43 MGy, improving the safety level without radiation damage. When HLEBI cuts the chemical bonds and generates dangling bonds with nonbonding electrons in fluororesin and PU, the created adhesion between the laminated sheets can be explained. Based on surface analysis of the Fluororesin/PU laminated sheets after the peeling tests, fluorine was detected on the PU peeled surface, indicating the strong chemical bonding generated by the double-step treatment.
采用低剂量≦0.65 MGy的均匀低能电子束辐照(HLEBI),分别穿透氟树脂层和PU层,在5 MPa和403 K下热压制备两层氟树脂/PU层复合材料。虽然没有双步处理,氟树脂/PU片材的粘附性无法观察到,但从平均剥离阻力粘附力(o F p)可以看出,结合力是产生的。在0.43 MGy的HLEBI双步处理下,o - F有增加的趋势,在无辐射损伤的情况下提高了安全水平。当HLEBI切断化学键并与氟树脂和PU中的非键电子产生悬空键时,可以解释层压片之间产生的附着力。通过对剥离试验后的氟树脂/PU层合板的表面分析,在剥离后的PU表面检测到氟,表明双步处理产生了较强的化学键合。
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引用次数: 0
Evaluation of ion bombardment in DC magnetron sputtering DC 离子轰击在直流磁控溅射中的应用
Pub Date : 2015-01-01 DOI: 10.2978/JSAS.27.1
R. Toyoda, S. Miyata, Y. Matsumura, T. Iijima, A. Tonegawa, M. Takeuchi
Momentum of ion bombardment in sputtering deposition process, which strongly depends on internal stress of thin film, has been evaluated regarding to a new parameter P i we previously proposed for fine-tuning of mechanical, optical, electrical and magnetic properties. In this study, we demonstrate to estimate the P i defined as ( i / a ) p , where i the ion flux, a the atom flux and p the ion’s momentum, by means of Langmuir probe and multi-grid analyzer in a function of negative bias voltage applied on substrates V sub . As a result, it was found that the P i was roughly proportional to V sub except on lower voltage than 30 V. This indicates that the P i should be measured plasma-diagnostically under incident ion energy as low as plasma potential.
在溅射沉积过程中,离子轰击动量强烈依赖于薄膜的内应力,我们已经根据我们之前提出的用于微调机械、光学、电学和磁学性能的新参数pi进行了评估。在本研究中,我们证明了利用Langmuir探针和多栅格分析仪,以施加在基片V sub上的负偏置电压为函数来估计pi,定义为(i / a) P,其中i为离子通量,a为原子通量,P为离子动量。结果发现,除了低于30 V的电压外,pi与V sub大致成正比。这表明,在入射离子能量低于等离子体电位的情况下,等离子体诊断应该测量pi。
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引用次数: 0
Calibration of infrared video-oculography by using bioadhesive phosphorescent particles for accurate measurement of vestibulo-ocular reflex in mice 利用生物黏附磷光粒子对小鼠前庭眼反射进行红外视频眼成像校正
Pub Date : 2015-01-01 DOI: 10.2978/JSAS.27.11
Akira Katoh, T. Hatanaka, Eri Takeuchi, M. Uchida, H. Natsume
Akira KATOH, Tomomi HATANAKA, Eri TAKEUCHI, Masaki UCHIDA and Hideshi NATSUME 1 Institute of Innovative Science and Technology, Tokai University, 4-1-1 Kitakaname, Hiratsuka, Kanagawa 259-1292, Japan TEL: x81-463-58-1211(EX.5627) FAX: x81-463-50-2478 e-mail: akiraka@tokai-u.jp 2 School of Medicine, Tokai University, 143 Shimokasuya, Isehara, Kanagawa 259-1193, Japan 3 Faculty of Pharmaceutical Sciences, Josai University, 1-1 Keyakidai, Sakado, Saitama 350-0295, Japan (Received 8 December, 2015 Accepted 16 December, 2015)
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引用次数: 4
期刊
Journal of Advanced Science
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