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Effect of smoking Arkela or Al-shesha on the antioxidant in human body 吸烟阿克拉或阿什沙对人体抗氧化剂的影响
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2020.165297
N. Younis
The research involved collected (50) sample from serum of Arkela smokers and (50) sample control for period from 15/10/2013 to 15/3/2014 and the age between(15-60)year for men only then determination of some antioxidant (Glutathione, Ceruloplasmin, Vitamin E and C, Malondialdehyde) in serum of Arkela smokers compared with non smokers, the results demonstrated a significant increase in the level of Ceruloplasmin and Malondialdehyde concentration and a significant decrease in the level of Glutathione and Vitamin E and C concentration in smokers compared with control. The results also demonstrated a non-significant change in the level of antioxidant concentration of Arkela smokers with age groups and Body Mass Index BMI. While the results demonstrated a significant decrease in the level of Glutathione and Vitamin E and C and a significant increase in the level of Ceruloplasmin and Malondialdehyde in serum blood smokers (more than two hours) in the day and (more than two years) compared with smokers in (less from hour)in the day and (1-11 months) respectively.
本研究收集了2013年10月15日至2014年3月15日期间,男性年龄在15-60岁之间的Arkela吸烟者(50份)血清和对照组(50份)血清中抗氧化剂(谷胱甘肽、铜蓝蛋白、维生素E和C、丙二醛)的含量,并与非吸烟者进行了比较。结果表明,与对照组相比,吸烟者的蓝蓝蛋白和丙二醛水平显著增加,谷胱甘肽水平和维生素E和C浓度显著降低。研究结果还表明,不同年龄组和体重指数(BMI)的Arkela吸烟者的抗氧化剂浓度水平没有显著变化。结果表明,与白天(少于1小时)和(1-11个月)的吸烟者相比,白天(超过2小时)和(超过2年)的血液吸烟者血清谷胱甘肽、维生素E和C水平显著降低,血清铜蓝蛋白和丙二醛水平显著升高。
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引用次数: 0
Indirect Spectrofluorometric Determination of Enoxaparin Sodium in Pharmaceutical Formulation (Injection) by Ion Association Complex Formation with Acriflavine Dye 与吖啶黄染料离子缔合法间接荧光光谱法测定制剂(注射剂)中依诺肝素钠的含量
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2019.125843.1001
mohamed thamer aghwan, Elham Sadullah Al-talibi
Abstract A simple, sensitive and selective spectrofluorometric method has been developed for the determination of enoxaparin sodium in bulk and dosage forms (injection). The method was based on the quantitative quenching effect of enoxaparin on the native fluorescence of acriflavine due to the formation of nonfluorescent supramolecular ion association complex between the studied drug and acriflavine dye in aqueous solution. The decrease of acriflavine fluorescence was observed at 506 nm after excitation at 402 nm. The relationship between quenching fluorescence intensity and concentration of enoxaparin sodium was linear in the range 0.05-20 μg/ml and with correlation coefficient 0.9990 and with LOD and LOQ 0.011 and 0.035 μg/ml respectively. The average recovery was 100.51% and RSD is less than 3.23%. The stoichiometry of enoxaparin to acriflavine was calculated a 1:4. The method was applied successfully to the determination of enoxaparin as injection formulation and the results were in a good agreement with certified value and standard addition procedure.
建立了一种简便、灵敏、选择性的荧光光谱法测定依诺肝素钠原料药和注射液剂型的含量。该方法基于依诺肝素在水溶液中与吖啶黄染料形成非荧光超分子离子缔合络合物,对吖啶黄天然荧光的定量猝灭作用。在402 nm激发后,在506 nm处观察到吖啶黄素荧光减弱。猝灭荧光强度与依诺肝素钠浓度在0.05 ~ 20 μg/ml范围内呈线性关系,相关系数为0.9990,定量限和定量限分别为0.011和0.035 μg/ml。平均回收率为100.51%,RSD < 3.23%。依诺肝素与吖啶黄的化学计量比为1:4。该方法成功地应用于依诺肝素注射液的测定,结果与认证值和标准添加程序吻合良好。
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引用次数: 0
Thermodynamic and Kinetic Study of Adsorption of Azo Dyes Derived for 4-amino Anti pyrene by Activated Carbon 活性炭吸附4-氨基抗芘偶氮染料的热力学和动力学研究
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2019.125920.1006
Salah Hekmat
A commercial activated carbon was used for the study of adsorption of two diazo dyes from aqueous solution employing batch method. These dyes were synthesized in our laboratory from the reaction of 4amino-antipyrene 4-AAP and β-Naphthol with p-amino phenol and p-amino benzaldehyde via diazonium ions. The effect of pH, temperature, and contact time on dye removal was investigated. The apparent thermodynamic parameters were estimated and the obtained results concluded that, the dyes adsorbed onto activated carbon are driven by entropy effect, exothermic and spontaneous processes. The kinetic study of adsorption of the considered dyes was conducted by applying four models the pseudo-first order, pseudosecond order ,Elovich and intra particules diffusion kinetic models. The results showed that, the second order equation fit better the experimental data. The intra particule diffusion model indicates that, there are more than mechanism controlling the adsorption process.
采用间歇式活性炭对两种重氮染料进行了吸附研究。这些染料是由4-氨基-安替芘4-AAP和β-萘酚与对氨基酚和对氨基苯甲醛经重氮离子反应合成的。考察了pH、温度和接触时间对染料去除率的影响。对表观热力学参数进行了估计,结果表明,染料吸附在活性炭上是由熵效应、放热和自发过程驱动的。采用拟一级、拟二级、Elovich和颗粒内扩散动力学模型对染料的吸附进行了动力学研究。结果表明,二阶方程与实验数据拟合较好。颗粒内扩散模型表明,控制吸附过程的机理不止一个。
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引用次数: 0
Effect of Allelopathic Potential of Corn, Sunflower , Field Capacity and Ascorbic Acid In Growth of Two Wheat cultivars 玉米、向日葵化感电位、田间容量和抗坏血酸对两个小麦品种生长的影响
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2020.126418.1034
mohamed saied fisal
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引用次数: 1
Assessment of Fungal Growth at Hemodialysis and Peritoneal Dialysis Unit in Hawler Teaching Hospital 霍勒教学医院血液透析及腹膜透析病房真菌生长情况评估
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2020.126676.1049
Vian Badraddin Al-Barzinji
Dialysis is used when the patient's kidneys can no longer perform their functions normally; it is a treatment that performs the functions of natural kidneys. Most patients begin dialysis when their kidneys have lost 85-90% of their ability to work naturally and they have to depend on dialysis for the rest of their lives, is called end –stage renal disease (ESRD). Infection in patients with end stage renal disease (ESRD) is usually treated with hemodialysis (HD) or peritoneal dialysis (PD). End stage renal disease a major cause of morbidity and mortality, in order to assess the fungal growth at hemodialysis and peritoneal dialysis unit a descriptive study was conducted at hemodialysis and peritoneal dialysis units in Hawler teaching hospital, from 15 of January to the end of May 2017;the study also includes the access sites and peritoneal catheter site. Factors that affected the access site among dialysis patient in the hospital. Sample of 63 patients, who were attending to the dialysis unit at time of the data collection, had been taken; in addition to that swab samples had been gathered from access site and peritoneal catheter site. The results of the study revealed that the fungal growth was positive at dialysis access sites, where the total percentage was 84.1% and that of peritoneal catheter site was 15.85%. In these unites, different types of filamentous fungi and yeasts had been successfully isolated.
当病人的肾脏不能再正常发挥其功能时,就需要进行透析;这是一种发挥天然肾脏功能的治疗方法。大多数患者开始透析时,他们的肾脏已经失去了85-90%的自然工作能力,他们不得不依靠透析度过余生,这被称为终末期肾病(ESRD)。终末期肾病(ESRD)患者的感染通常通过血液透析(HD)或腹膜透析(PD)治疗。终末期肾脏疾病是发病率和死亡率的主要原因,为了评估血液透析和腹膜透析单元的真菌生长情况,我们于2017年1月15日至5月底在霍勒教学医院的血液透析和腹膜透析单元进行了描述性研究,研究还包括通路部位和腹膜导管部位。影响医院透析患者通道位置的因素。收集数据时正在透析病房就诊的63例患者的样本;除此之外,还从接入处和腹膜导管处收集了拭子样本。研究结果显示,透析通路部位真菌生长阳性,总比例为84.1%,腹膜导管部位真菌生长阳性比例为15.85%。在这些单元中,已成功分离出不同类型的丝状真菌和酵母。
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引用次数: 1
Reasons of the transformed toward NOSQL Databases and its data models 向NOSQL数据库转换的原因及其数据模型
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2020.165303
Shaymaa Ahmed Razoqi
The relational database model is the main focus of the database for the previous time. It provides robust data storage and structure that supports transaction characteristics and data retrieval with structured query languageSQL. The emergence of web technologies and clustering technology in large servers called for the need to store unstructured data and move away from the pattern of tables and static fields and not topic to transaction conditions, especially in distributed systems. Instead, it used CAP theory. New data models are emergence including: Document Data model, Key-Value model, Column-Family model, and Graph model, And new programming languages that deal with these models. An asset inventory system is a model of systems that are not topic to a fixed structure. Each location in the organization has fairly different assets and assets in the same location have different specifications that are difficult to organize in the form of tables and columns. For this reason using of NOSQL CouchDB database system was adopted and the use of MAP-REDUCE technology to organize data display and Cloudant Query in Mango-view method to retrieve data from the inventory database.
关系数据库模型是上一篇文章中数据库的主要关注点。它提供了健壮的数据存储和结构,支持使用结构化查询语言esql进行事务特征和数据检索。大型服务器中web技术和集群技术的出现,要求存储非结构化数据,摆脱表和静态字段的模式,不受事务条件的影响,尤其是在分布式系统中。相反,它使用了CAP理论。新的数据模型出现了,包括文档数据模型、键值模型、列族模型和图模型,以及处理这些模型的新的编程语言。资产盘点系统是不受固定结构约束的系统模型。组织中的每个位置都有相当不同的资产,同一位置的资产具有不同的规范,难以以表格和列的形式进行组织。为此采用NOSQL CouchDB数据库系统,使用MAP-REDUCE技术组织数据显示,使用Mango-view方法中的Cloudant Query从库存数据库中检索数据。
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引用次数: 1
Some Theorems and Results on Solution of Kind of Volterra Integral Equations 一类Volterra积分方程解的若干定理和结果
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2020.165298
M. Khalil
We studied in this work a class of nonlinear Volterra integral equations with delay and present a sufficient condition for the bounded solution also we give an illustrative example which support the main result of this paper.
本文研究了一类具有时滞的非线性Volterra积分方程,给出了该方程有界解的充分条件,并给出了一个例子来支持本文的主要结果。
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引用次数: 0
Synthesis of New Oxazepine and Thaizolidine Compounds derived from Pyrimidine-2(2H)-one 由嘧啶-2(2H)- 1衍生的新恶氮平和噻唑烷化合物的合成
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2019.125908.1004
zainab hassan sulyman, Natiq G. Ahmed
In this paper the compounds (11-20) (methyl pyrimidine 2(1H)-one and others phenyl pyrimidine -2(1H)one) that had been already prepared from α, β unsaturated carbonyl compounds that are called chalcones, these compounds are usually prepared from the reaction of different aldehydes (4-methoxy benzaldehyde, 2-nitro benzaldehyde, 3-nitrobenzaldehyde, 4-N,N—dimethyle amino benzaldehyde, benzaldehyde, 4-nitrobenzaldehyde) with different ketones (acetone, acetophenone, 2-nitro acetophenone, 3nitro acetophenone) After preparing and purifying them a suitable mesurment for physical, chemical and spectroscopic properties had been made to get chalcones that reacted with urea under known chemical conditions to get the pyrimidinone compounds that we need. Pyrimidine compounds had been reacted with two aromatic amines (2,4dinitro aniline and 4amino acetophenone) using glacial acetic acid as catalyst in absolute ethanol giving a new compounds of schiff's bases (21-40). New thiazolidine 4-one (41-50) had been synthesized from the reacting of Schiff's bases (21-30) with thioglycolic acid in absolute ethanol. 1,3oxazepine derivatives. (51-60) had been prepared from reaction between Schiff's bases (31-40) and malic anhydrid in absolut ethanol. The structures of the Synthesized compounds had been estimated by IR, HNMR and some physical data.
本文研究了由α, β不饱和羰基化合物查尔酮合成的化合物(11-20)(甲基嘧啶2(1H)- 1和其他苯基嘧啶-2(1H) - 1),这些化合物通常是由不同的醛(4-甲氧基苯甲醛,2-硝基苯甲醛,3-硝基苯甲醛,4-N, n -二甲基氨基苯甲醛,苯甲醛,4-硝基苯甲醛)与不同的酮(丙酮,苯乙酮,2-硝基苯乙酮,2-硝基苯乙酮,2-硝基苯乙酮,2-硝基苯乙酮,2-硝基苯乙酮,2-硝基苯乙酮,在制备和纯化后,对查尔酮进行了物理、化学和光谱性质的测定,查尔酮在已知的化学条件下与尿素反应,得到我们需要的嘧啶类化合物。以冰醋酸为催化剂,在无水乙醇中,嘧啶类化合物与两种芳香胺(2,4二硝基苯胺和4氨基苯乙酮)反应,得到新的希夫碱化合物(21-40)。以希夫碱(21-30)与巯基乙酸为原料,在无水乙醇中合成了新的噻唑烷4- 1(41-50)。1、3 oxazepine衍生品。以希夫碱(31-40)和苹果酸酐为原料,在无水乙醇中制备了苹果酸酐(51-60)。通过红外光谱(IR)、核磁共振光谱(HNMR)和一些物理数据对所合成化合物的结构进行了表征。
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引用次数: 2
Studying the parameter gradient energy coefficient of Polyethylene glycol as a function of molecular weight with Freed Contribution 研究了聚乙二醇的参数梯度能系数随分子量的变化规律
Pub Date : 2020-06-01 DOI: 10.33899/EDUSJ.2020.165307
Malak Jaafar Ali, S. M. Nuri, S. M. Rajab
The gradient energy coefficient (  ) has a main function in extracting the polymers properties to help us to innovate and manufacture new polymers and different process like coating, wetting, foaming, adhesion operations. The Cahn-Hilliard (CH) theory [1], represents the free energy profile of polymer surfaces or interfaces. Considers the free energy profile of polymer surfaces or interfaces as inhomogeneous which has more than one phase. On the other hand, it has been used the Freed Bawendi contribution in conjunction with Cahn-Hilliard in treatment with architecture structure for polymers [2]. While Simha-Somcynsky (SS) theory describes the thermodynamic properties of both low and high molecular weights in terms of occupied site fraction (y) [3]. This study has been examined in the range of (313 -473) K temperatures and up to about (150) Mpa pressure. The quantitative success of our study is clearly appeared in the minimum and maximum deviations in the volume is 0.036 and 0.128
梯度能量系数()的主要功能是提取聚合物的性能,以帮助我们创新和制造新的聚合物和不同的工艺,如涂层,润湿,发泡,粘合操作。Cahn-Hilliard (CH)理论[1]表示聚合物表面或界面的自由能分布。认为聚合物表面或界面的自由能分布是不均匀的,具有多个相。另一方面,Freed Bawendi的贡献与Cahn-Hilliard一起用于聚合物的结构结构处理[2]。而Simha-Somcynsky (SS)理论则用占位分数(y)来描述低分子量和高分子量的热力学性质[3]。这项研究是在(313 -473)K的温度和高达(150)Mpa的压力范围内进行的。我们研究的定量成功明显表现在体积的最小和最大偏差分别为0.036和0.128
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引用次数: 0
Effect of Deposition Temperature on the Physical Performance of n-ZnO/p-Si Heterojunction 沉积温度对n-ZnO/p-Si异质结物理性能的影响
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2019.126043.1017
Y. Mohammed
Comparative study of the physical characteristics of n-ZnO/p-Si heterojunction diode has been done as a function of deposition temperature in the range of 300-600 °C. Transparent conducting (TC) Zinc Oxide (ZnO) thin films were deposited by atmospheric pressure chemical vapor deposition (APCVD) technique on the p-Si(100) and glass substrates. Also, the influences of different deposition temperature on the morphology and optical properties of ZnO films were studied. Both the average surface roughness (from 62.8 to 18.8 nm) and the root mean square (from 78.2 to 24 nm) of ZnO films were decreased with the increase in the deposition temperature. Optical transmittance measurement results exhibited good transparency within the visible wavelength range for the films prepared at a temperature above 400 C. The current-voltage (I-V) characteristics of the heterojunction diodes exhibited rectification behavior and depend on the deposition temperature. The electrical parameters of the n-ZnO/p-Si heterojunctions were also affected by the deposition temperature. The diodes prepared at a temperature above 400 C were possessed lower reverse saturation current and high rectification ratio compared to those fabricated at a relatively lower temperature such as 300 C or 400 °C. Such low a temperature grown n-ZnO/p-Si heterojunction diodes with lower reverse saturation current could be suitable for photo-detection applications.
对比研究了n-ZnO/p-Si异质结二极管的物理特性随沉积温度(300-600℃)的变化规律。采用常压化学气相沉积(APCVD)技术在p-Si(100)和玻璃衬底上沉积了透明导电氧化锌(ZnO)薄膜。研究了不同沉积温度对ZnO薄膜形貌和光学性能的影响。随着沉积温度的升高,ZnO薄膜的平均表面粗糙度从62.8 nm减小到18.8 nm,均方根从78.2 nm减小到24 nm。在400℃以上温度下制备的薄膜在可见光波长范围内具有良好的透光性。异质结二极管的电流-电压(I-V)特性表现出整流行为,并与沉积温度有关。n-ZnO/p-Si异质结的电学参数也受沉积温度的影响。与在相对较低的温度下如300或400°C制备的二极管相比,在高于400°C温度下制备的二极管具有较低的反向饱和电流和较高的整流比。这种低温生长的n-ZnO/p-Si异质结二极管具有较低的反向饱和电流,适合于光探测应用。
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引用次数: 2
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Journal of Education Science
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