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A Comparative Morphological Study of the Genus Juniperus L. ( Cupressaceae) in North of Iraq 标题伊拉克北部桧属(柏科)的比较形态学研究
Pub Date : 2020-07-28 DOI: 10.33899/edusj.2020.127106.1073
Dr.Haees Sayel Al Jowary, A. A. Al-Sharefy
A new species Registration of juniper is Juniperus macrocarpa, permissions not previously registered in Flora of Iraq that were composed (Guest researchers and Ali alRawi,1966) so only two species of Juniperus oxycedrus and Juniperus polycarpos were registered at the time. The research included a classification of the species Juniperus which belong to the Cupressaceae family that grown a wild plants in north of Iraq, using the morphological characteristics of (3) species of veins mentioned in (7) sites distributed in provinces of (FNI,MAM and MSU )Nineveh, Dohuk and Sulaymaniyah.
在伊拉克植物志中未登记的新登记种为大柏(Juniperus macrocarpa)(客座研究员和Ali alRawi,1966),因此当时只登记了两个种:oxycedrus和polycarpos。本研究利用分布在伊拉克北部(FNI、MAM和MSU)尼尼微、杜胡克和苏莱曼尼亚省(7)个地点的(3)种叶脉的形态特征,对伊拉克北部生长的一种野生柏科植物Juniperus进行了分类。
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引用次数: 0
A Taxonomic Study of Macro-and Micro Morphological Features of Fruits and Seeds Cultivars of the Species Belonging to the Genus Morus L. (Moraceae) Cultivated in the North of Iraq 伊拉克北部栽培桑属(桑科)果实和种子品种宏观和微观形态特征的分类研究
Pub Date : 2020-07-28 DOI: 10.33899/edusj.2020.127107.1074
Raad Hammad Al-Badrany, Aamer Al-mathidy
The present research deals with the study of morphological characters of the fruits and seeds of the cultivars belonging to the species Morus alba L. Namely (ʽBeautiful Dayʼ, ʽBig Whiteʼ, ʽReaseʼ, ʽGreeceʼ, ʽPearlʼ, ʽBorder Sweetʼ, ʽPendulaʼ); Morus latifolia Poir (ʽKokuse Koreanʼ); Morus rubra L. (ʽAmarahʼ); Morus nigra L. (ʽShamiʼ); Morus macroura Miq (ʽKing Whiteʼ); ʽDwarfʼ and Morus hybrid (ʽTiceʼ, ʽWellingtonʼ) Which cultirated in North of Iraq. The study includes characters of the fruits (Shape, Color, Dimension, Size, Number of the fruitlet in the fruit) and the characters of the seeds (Shape, Color, Dimension, Number of the seeds in the fruit, and surface ornamentation). The results showed some changes in morphological characteristics of the fruits and seeds examined by light microscope (L.M), in addition to the surface ornamentation of the seeds examined by scanning electron microscope (SEM). They also showed five types of the surface ornamentation (Reticulate, Muricate, Foreate undulate, Polygonal, and Ruminate) for cultivars species studied, showed that importance value in the separation between the cultivars of the species studied belonging to the genus Morus L. Keyword: Morphological, Systematic, Fruits, Seeds, Genus Morus L. سنجلا عاونا فانصا روذبو رامثل ةقيقدلاو ةماعلا ةيرهظملا تافصلل ةيفينصت ةسارد Morus L. ( Moraceae قا رعلا لامش يف ةعورزملا ) 178 ةيفينصت ةسا رد لا تافصلل ةيرهظم ةقيقدلاو ةماعلا سنجلا عاونا فانصا روذبو رامثل Morus L. ( Moraceae قا رعلا لامش يف ةعورزملا ) 1 ينا ردبلا دومحم دمح دعر .د.م.أ يديضاعملا دومحم نسحم رماع قا رعلا / لصوملا ةعماج /ةفرصلا مولعلل ةيبرتلا ةيلك / ةايحلا مولع مسق dr.amer.1956@yahoo.com raadhamad42@gmail.com ملاتسلاا لوبقلا 31 / 05 / 2020 26 / 07 / 2020 DOI: 10.33899/edusj.2020.127107.1074 ةصلاخلا تافصلا ةسا رد يلاحلا ثحبلا لوانت ةيرهظملا ةقيقدلاو ةماعلا روذبو رامثل لأ فانص سنجلل عاونلأا Morus L. فانصلأاب تلثمت يتلاو ʽBeautiful Dayʼ و ʽBig Whiteʼ و ʽReaseʼ و ʽGreeceʼ و ʽPearlʼ و ʽBorder Sweetʼ و ʽPendulaʼ عونلل Morus alba L. فنصلاو ʽKokuso Koreanʼ عونلل Morus latifolia Poir و ʽAmarahʼ عونلل M. rubra L. و ʽShamiʼ عونلل Morus nigra L. نافنصلاو ʽKing Whiteʼ و ʽDwarfʼ عونلل Morus macroura Miq نافنصلاو ʽTiceʼ و ʽWellingtonʼ عونلل Morus hybrid قا رعلا لامش يف ةعورزملا . و ت ض تنم ةرمثلا يف تا ريمثلا ددعو اهمجحو اهداعباو اهنولو اهلكش ثيح نم رامثلا تافص ةسا ردلا تافصو ةدحاولا ا روذبل ةيحطسلا ةفرخزلا عونو ةدحاولا ةرمثلا يف روذبلا ددعو داعبلااو نوللاو لكشلا ثيح نم Seed Surface ornamentation جئاتنلا ترهظاو .اهل كلانه يف تا رياغت ضعب يتلا روذبلاو رامثلا تافص ( يئوضلا رهجملا مادختساب تصحف LM ) Light microscope نع لاضف ا نيب روذبلل يحطسلا ءاسكل ت فرخز يف فانصلأا اهت ةيحطسلا Surface ornamentation مادختسابو حساملا ينورتكللاا رهجملا Scanning Electron Microscope (SEM) تدجو ذإ يكبش حطس تاذ يهو عاونأ ةسمخب Reticulate معان يميلحو Muricate رقنم جومتمو Foreate undulate علضمو Polygonal بحسنمو Ruminate يف لزع يف ةيفينصت ةيمهأ اهل يتلاو ةسا ردلا ديق فانصلأا عونأ سنج ىلا ةدئاعلاو ةسوردملا عاونلأا نيب فانصلأا Morus L. . ةيحاتف
本研究研究了桑树(Morus alba L.)品种果实和种子的形态特征,即:(Beautiful Day ', Big White ', Rease ', greek ', Pearl ', Border Sweet ', Pendula ');桑(韩国);桑属植物;桑属植物;Morus macoura Miq (King White);矮子和桑的杂交品种(古泰斯,古威灵顿),栽培于伊拉克北部。研究包括果实的性状(形状、颜色、尺寸、大小、果实中小果粒的数量)和种子的性状(形状、颜色、尺寸、果实中种子的数量、表面纹饰)。结果表明,光镜下果实和种子的形态特征发生了一些变化,扫描电镜下种子的表面纹饰也发生了变化。结果表明,桑属栽培品种的表面纹饰有5种类型,即网状纹饰、褶皱纹饰、波状纹饰、多边形纹饰和反刍纹饰,对桑属栽培品种间的区分具有重要意义。形态学、系统、水果、种子、桑属属l .سنجلاعاونافانصاروذبورامثلةقيقدلاوةماعلاةيرهظملاتافصللةيفينصتةسارد桑属l .(桑科قارعلالامشيفةعورزملا)178年ةيفينصتةساردلاتافصللةيرهظمةقيقدلاوةماعلاسنجلاعاونافانصاروذبورامثل桑属l .(桑科قارعلالامشيفةعورزملا)1يناردبلادومحمدمحدعردم。。أيديضاعملادومحمنسحمرماعقارعلال/صوملاةعماج/ةفرصلامولعللةيبرتلاةيلك/ةايحلامولعمسقdr.amer.1956@yahoo.com raadhamad42@gmail.comملاتسلاالوبقلا31 / 05/2020 26 / DOI: 07/202010.33899 / edusj.2020.127107.1074ةصلاخلاتافصلاةسارديلاحلاثحبلالوانتةيرهظملاةقيقدلاوةماعلاروذبورامثللأفانصسنجللعاونلأا桑属l .فانصلأابتلثمتيتلاوʽ美丽的日子ʼوʽ白色ʼوʽ原因ʼوʽ希腊ʼوʽ珍珠ʼوʽ边境甜ʼوʽ翻车机ʼعونلل桑属alba l .فنصلاوʽKokuso韩国ʼعونلل桑属latifolia Poirوʽ派别ʼعونللm . rubra l .وʽShamiʼعونلل桑属黑质l .نافنصلاوʽ王白色ʼوʽ矮ʼعونلل桑属macroura筛选نافنصلاوʽ泰斯ʼوʽ惠灵顿ʼعونلل桑属混合قارعلالامش يف ةعورزملا。وتضتنمةرمثلايفتاريمثلاددعواهمجحواهداعباواهنولواهلكشثيحنمرامثلاتافصةساردلاتافصوةدحاولااروذبلةيحطسلاةفرخزلاعونوةدحاولاةرمثلايفروذبلاددعوداعبلااونوللاولكشلاثيحنم种子表面纹饰جئاتنلاترهظاو。اهلكلانهيفتارياغتضعبيتلاروذبلاورامثلاتافص(يئوضلارهجملامادختسابتصحفLM)光学显微镜نعلاضفانيبروذبلليحطسلاءاسكلتفرخزيففانصلأااهتةيحطسلا表面装饰مادختسابوحساملاينورتكللاارهجملا扫描电子显微镜(SEM)تدجوذإيكبشحطستاذيهوعاونأةسمخب网状معانيميلحوMuricateرقنمجومتموForeate波形علضمو多边形بحسنميو反刍فلزعيفةيفينصتةيمهأاهليتلاوةساردلاديقفانصلأاعونأسنجىلاةدئاعلاوةسوردملاعاونلأانيبفانصلأا桑属l。ةيحاتفملا تاملكلا:سنج،روذبلا،رامثلا،فينصتلا،ةيرهظملا桑属l .ةمدقملاتوتلاسنجنا桑属l .ةيتوتلاةلئاعلاىلإيمتنييذلاو桑科ةبتر罗萨莱斯لكشبومنياجشار،ةرمعمتاريجشوتابننكسملايئانثوايداحأومنيبرتيفةفلتخمبرتلايفديجلكشبرهزيوسنجلاعاونافانصاروذبورامثلةقيقدلاوةماعلاةيرهظملاتافصللةيفينصتةسارد桑属l .(桑科قارعلالامشيفةعورزملا)179年تاذةيضماحلاpH值(6.2 7(ةرارحةجردبو)30)18°Cايثارودقعمدعيو،رياغتلاىلعةريبكةيلباقهلوةفلتخملاتائيبلايفعساوقاطنىلعراشتنلااو فيكتلاو [1،2]。وهصيخشتوةيتابنلاعيماجملافصولساسلااةدعاقلاتاتابنللةيرهظملاتافصلادعتروهظنممغرلاباتافصلاهذهتظفتحا،ةيفينصتلاتاساردلايفةعساواقافاتحتفيتلاةيملعلالئاسولاروطتوةثيدحلاتاساردلا،نوفنصملالبقنماهيلعفرعتلاواهزييمتةيناكملاكلذوةرادصلاهلزنمبونكميلاونوفنصملااهيلعدنتسييتلاينصتةساردةيأيفاهنعءانغتسلااعضودنعوةنيعلليلولااصيخشتلادنعلقحلايفاميسلاو،ةمدقتمةيفضعبلانعاهضعبةنيعمةيفينصتبتارملزعلحاتفم[3]。نّيبو[4]ةيفينصتةيمهأتاذهفشكتلحارموهومنةرتفللاختابنلاءازجأعيمجلةيفينصتلاةلدلأانألةديدجلافانصلاافيصوتلةيرهظملاتارشؤملانأولكعونةردقلااهليتلاتافصلانمةعومجمىلعدمتعت。ضعبلانعاهضعبفانصلاازييمتيفنأ[5]صخش34ذارامثللةيرهظملاتافصلاىلعدامتعلاابايكرتيفيمانلاتوتلانمافنصظحلاةرمثلاصئاصخيفةميقريياعموةريبكتافلاتخادوجواهمادختسانكميصيخشتيفسنجلةعباتلاعاونلأاتوتلا。امكمدختسا[6]فينصتوصيخشتيفرامثللةيرهظملاتافصلاةيثارولابيكارتلا基因型توتللضيبلااalba l。امأ[7]ىلعادامتعاةيلامشلااكيرمايفةيمانلافانصلاليفينصتحاتفمعضودقف。رامثلاوقارولااتافص[تصخشنيحيف8ةيرهظملاتافصلامادختس
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引用次数: 0
Preparation of Some Benzothiazole Polymers and Study Their Electrical Conductivity Properties 苯并噻唑类聚合物的制备及其导电性能研究
Pub Date : 2020-07-26 DOI: 10.33899/edusj.2020.126945.1066
A. Khattab, Haitham Ahmed Ayoob, Laith Mohammed Altaan
As the conjugated polymers are doped with some electron donor or acceptor dopants, their electrical conductivity increased thoroughly to about 10 Ω.cm. The doping of the polymers may give an n or p semiconductor characteristic according to the types of the dopants that are used. Within the frame of this work, four types of conjugated polymers with benzothiazole as a major moiety in their backbone have been prepared. The prepared monomers and polymers have been characterized by FTIR spectroscopy. Elemental analysis of the polymers (CHN) demonstrates their chemical structure while the DSC thermal analysis illustrates its Tg. The polymers were doped with two types of dopants, iodine and sodium iodide. The electrical conductivity of the doped polymers was measured with three probe cell. The results show increasing in the electrical conductivity with dopant concentration to some levels. The activation energy of the electrical conductivity process was also studied by measuring the electrical conductivity in different temperature. According to the magnitude of the activation energy, we can conclude that the chain flexibility is the dominate factor that influenced on electrical conductivity. Hall Effect and hot probe measurements reveal that the polymer can be considered as n or p type according to the type of the doping. It was concluded that the doping with iodine produced an n-type while the doping with sodium iodide produced the ptype.
在共轭聚合物中掺入电子供体或电子受体掺杂剂后,其电导率提高到10左右Ω.cm。根据所使用的掺杂剂的类型,所述聚合物的掺杂可以具有n或p半导体特性。在本研究的框架内,制备了四种以苯并噻唑为主要基团的共轭聚合物。用FTIR光谱对所制备的单体和聚合物进行了表征。元素分析显示了聚合物的化学结构,DSC热分析显示了其Tg。聚合物中掺杂了两种类型的掺杂剂:碘和碘化钠。用三探针电池测量了掺杂聚合物的电导率。结果表明,随着掺杂浓度的增加,电导率有所提高。通过测量不同温度下的电导率,研究了导电过程的活化能。根据活化能的大小,我们可以得出,链的柔韧性是影响电导率的主要因素。霍尔效应和热探针测量表明,根据掺杂的类型,聚合物可以被认为是n型或p型。结果表明,碘掺杂产生n型,碘化钠掺杂产生p型。
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引用次数: 1
Investigating the Numerical solution of the BoltzmannTransport Equation in silicon in Momentum Space Using Computational Systems of Different Dimensions 用不同维数的计算系统研究动量空间中硅的玻尔兹曼输运方程的数值解
Pub Date : 2020-07-26 DOI: 10.33899/edusj.2020.126828.1057
M. Hussien, M. Mahmood
The Boltzmann transport equation is the basic equation for solving the transport of charge carrier (electrons, holes) problems in semiconductor devices. The distribution function has been obtained from the solution of this equation. The distribution function is important in calculating semiconductor properties, which can be used to calculate the average electron energy, the charge carrier concentration, and other properties. In this work the semi-classical Boltzmann transport equation in silicon was solved using analytical / numerical methods in steady state case in momentum space. The analytical solution is requires expressing the distribution function using Legendre polynomials expansion the first two terms of the expansion, by taking into account the effect of both acoustic elastic scattering and nonelastic scattering in addition to the effect of nonparabolic energy band structure. In order to obtain the numerical solution of Boltzmann transport equation the finite difference method is used. The differential equation is transformed to linear difference equation which can represented by matrices. Numerical systems with different dimensions are designed to calculate the distribution function with the least possible time to maintain the accuracy of the solution for different applied electric field which represent the low and high field regions at temperatures T= (77, 300) K. The obtained results showed good agreement with published data that used other calculation methods such as the Monte Carlo simulation method for all the system used in this work. Keyword: Boltzmann equation in Silicon, numerical solution for Boltzmann transport equation, Legendre polynomial expansion method نوكيلسلا يف لاقتنلال نامزتلوب ةلداعمل يددعلا لحلا ءاصقتسا يف تاموظنم مادختساب مخزلا ءاضف ةيباسح .ةفلتخم داعبأب 109 نوكيلسلا يف لاقتنلال نامزتلوب ةلداعمل يددعلا لحلا ءاصقتسا يف تاموظنم مادختساب مخزلا ءاضف ةيباسح .ةفلتخم داعبأب دومحم دجام دومحم نيسح حلاص دمحم زاتمم ءايزيفلا مسق ةفرصلا مولعلل ةيبرتلا ةيلك − لصوملا ةعماج momtaz_hussien@uomosul.edu.iq mahmood.majed.mahmood@gmail.com ملاتسلاا لوبقلا 24 / 03 / 2020 22 / 07 / 2020 DOI: 10.33899/edusj.2020.126828.1057 صخلملا لئاسم لحل ةمدختسملا ةيساسلاا ةلداعملا نامزتلوبل لاقتنلاا ةلداعم دعت نورتكللاا( ةنحشلا لماح لاقتنا ، )ةوجفلا يف طئابن أ ةلداعملا هذه لح للاخ نم عيزوتلا ةلاد ىلع لوصحلا نكميو تلاصوملا هابش ، باسح يف ةمهم عيزوتلا ةلاد دعت اهمدختسا نكمي يتلا ،تلاصوملا هابشأ صئاصخ طسوتم باسح يف ةقاط نورتكللإا لا نم اهريغو ةنحشلا لماح زيكرتو خ صاو . ةيليلحت ةقيرط مادختساب نوكيلسلا يف نامزتلوبل ةيكيسلاكلا هبش لاقتنلاا ةلداعم لح مت ثحبلا اذه يف / ةلاح يف ةيددع را رقتسلاا مخزلا ءاضف يف . عيزوتلا ةلاد نع ريبعتلا يليلحتلا لحلا بلطتي لا دودح تاددعتم مادختساب ب كلذو ردنج أ لولاا نيدحلا ذخ ا نم لك ريثأت رابتعلاا رظنب ذخلاا عم ردنجلا تاددعتم تادادتما نم يناثلاو لا ةنرملا ريغ ةراطتسلاا و ةنرملا ةيعمسلا ةراطتس إ ةفاض ىلا قورفلا ةقيرط مدختسن نامزتلوب ةلداعمل يددعلا لحلا ىلع لوصحللو .ئفاكملا ريغ ةقاطلا ةمزح بيكرت ريثأت ةددحملا ذا تافوفصملاب اهليث
玻尔兹曼输运方程是解决半导体器件中载流子(电子、空穴)输运问题的基本方程。由该方程的解得到了分布函数。分布函数在计算半导体性质时很重要,它可以用来计算平均电子能量、载流子浓度和其他性质。本文采用解析/数值方法在动量空间中求解了稳态情况下硅中的半经典玻尔兹曼输运方程。解析解需要同时考虑声弹性散射和非弹性散射的影响以及非抛物能带结构的影响,用勒让德多项式展开前两项来表示分布函数。为了得到玻尔兹曼输运方程的数值解,采用了有限差分法。将微分方程转化为可以用矩阵表示的线性差分方程。设计了不同尺寸的数值系统,在尽可能短的时间内计算分布函数,以保持在温度T= (77,300) k时不同外加电场(代表低场区和高场区)解的准确性。所得到的结果与使用其他计算方法(如蒙特卡罗模拟方法)对本工作中使用的所有系统的数据具有良好的一致性。关键字:硅中的玻尔兹曼方程,玻尔兹曼输运方程的数值解,勒让德多项式展开法نوكيلسلايفلاقتنلالنامزتلوبةلداعمليددعلالحلاءاصقتسايفتاموظنممادختسابمخزلاءاضفةيباسح。ةفلتخمداعبأنب109وكيلسلايفلاقتنلالنامزتلوبةلداعمليددعلالحلاءاصقتسايفتاموظنممادختسابمخزلاءاضفةيباسح。ةفلتخمداعبأبدومحمدجامدومحمنيسححلاصدمحمزاتممءايزيفلامسقةفرصلامولعللةيبرتلاةيلك−لصوملاةعماجmomtaz_hussien@uomosul.edu.iq mahmood.majed.mahmood@gmail.comملاتسلاالوبقلا24 / 03/2020 22 / DOI: 07/202010.33899 / edusj.2020.126828.1057صخلملالئاسملحلةمدختسملاةيساسلااةلداعملانامزتلوبللاقتنلااةلداعمدعتنورتكللاا(ةنحشلالماحلاقتنا،)ةوجفلايفطئابنأةلداعملاهذهلحللاخنمعيزوتلاةلادىلعلوصحلانكميوتلاصوملاهابش،باسحيفةمهمعيزوتلاةلاددعتاهمدختسانكمييتلا،تلاصوملاهابشأصئاصخطسوتمباسحيفةقاطنورتكللإالانماهريغوةنحشلالماحزيكرتوخصاو。ةيليلحتةقيرطمادختسابنوكيلسلايفنامزتلوبلةيكيسلاكلاهبشلاقتنلااةلداعملحمتثحبلااذهيف/ةلاحيفةيددعرارقتسلاامخزلاءاضفيف。عيزوتلاةلادنعريبعتلايليلحتلالحلابلطتيلادودحتاددعتممادختساببكلذوردنجألولاانيدحلاذخانملكريثأترابتعلاارظنبذخلااعمردنجلاتاددعتمتادادتمانميناثلاولاةنرملاريغةراطتسلااوةنرملاةيعمسلاةراطتسإةفاضىلاقورفلاةقيرطمدختسننامزتلوبةلداعمليددعلالحلاىلعلوصحللو。ئفاكملاريغةقاطلاةمزحبيكرتريثأتةددحملاذاتافوفصملاباهليثمتنكمييتلاةيطخلاقورفلاةلداعمىلإةيلضافتلاةلداعملاليوحتمتيتاموظنمةدعميمصتمت。لكلعيزوتلاةلادباسحلةفلتخمداعبأبةيددعةيئابرهكتلااجملوةقدلاثيحنمتاموظنملاهذهنيبةنراقملاتمتو،ةموظنمةفلتخمةطلسمةيلاعلاتلااجملاةقطنمىلاةئطاولاتلااجملاةقطنمنمدتمتةرارحلايتجرددنعوT =(77、300)K،قفاوتاهيلعلوصحلامتيتلاجئاتنلاترهظأواديجدختسايتلاةروشنملاجئاتنلاعميتنومةاكاحمةقيرطلثمىرخاقرطت。ثمحبلايفةمدختسملاتاموظنملامظعملوولراكنامزتلوبةلداعم:ةلادلاتاملكلانوكيلسلايف،نامزتلوبللاقتنلااةلداعمليددعلالحلا،لادودحتاددعتمةقيرطردنج。نوكيلسلايفلاقتنلالنامزتلوبةلداعمليددعلالحلاءاصقتسايفتاموظنممادختسابمخزلاءاضفةيباسح。ةفلتخمداعبأب110ةمدقملارهظتةساردةيمهاعيزوتلاةلادميمصتيفاهتاقيبطتوتلاصوملاهابشاطئابن،لاجملاريثأتروتسزنارتلثمةينورتكللاااذمدقتةيلامتحاعيزوتلاةلادانلمخزلاءاضفيفنيعمةجومهجتمنم)تضاوجفلاوتانورتكللاا(ةنحشلالماحداجياالأنورتكلي[1]نامزتلوبللاقتنلااةلداعملحقئارطتعونتةيليلحتقئارطىلاذاايسااعيزوتعيزوتلاةلادلناضارتفامتعيزوتواايليوسكاما[3,[2]。ذاةيليلحتلاةقيرطلاتاذىدمنمضةددحمةيئايزيفجذامنىلعةرصتقمنوكتاهنالااةديججئاتندودحمةقاطلل[1]كلذكولااهمادختسانكميتلاصوملاهابشاضعبللثمديانسرامويلاكلا砷化镓لاواهمادختساحصيتلاصوملاهابشاعيمجلةيلاعلاتلااجملادنع[4]هجوتلامت。كلذلةجيتنباسحونامزتلوبللاقتنلااةلداعملحلةيددعقئارطمادختسلانيثحابلالبقنمولراكيتنومةاكاحمةقيرطلثمعيزوتلاةلاديتلادمتعتىلععيزوتلاةلادباسحلقرغتسملاتقولا(5、6、7)。ةقيرطميدقتمتةيليلحتةيددعتقولاليلقتلجانمونمضتييليلحتلابناجلاطلاهذهيفةقيرةلادكعيزوتلاةلادليثمتلاءزجمضتيتلاردنجرظانتمارخأوريغرظانتمدعبةفوفصمىلاةيضايرلاتلاداعملاليوحتلقورفلاتلاداعممادختسامتيفيددعلابناجلااماضيوعتلانعةقاطلانمددحمىدموةفلتخمميق[8]。
{"title":"Investigating the Numerical solution of the BoltzmannTransport Equation in silicon in Momentum Space Using Computational Systems of Different Dimensions","authors":"M. Hussien, M. Mahmood","doi":"10.33899/edusj.2020.126828.1057","DOIUrl":"https://doi.org/10.33899/edusj.2020.126828.1057","url":null,"abstract":"The Boltzmann transport equation is the basic equation for solving the transport of charge carrier (electrons, holes) problems in semiconductor devices. The distribution function has been obtained from the solution of this equation. The distribution function is important in calculating semiconductor properties, which can be used to calculate the average electron energy, the charge carrier concentration, and other properties. In this work the semi-classical Boltzmann transport equation in silicon was solved using analytical / numerical methods in steady state case in momentum space. The analytical solution is requires expressing the distribution function using Legendre polynomials expansion the first two terms of the expansion, by taking into account the effect of both acoustic elastic scattering and nonelastic scattering in addition to the effect of nonparabolic energy band structure. In order to obtain the numerical solution of Boltzmann transport equation the finite difference method is used. The differential equation is transformed to linear difference equation which can represented by matrices. Numerical systems with different dimensions are designed to calculate the distribution function with the least possible time to maintain the accuracy of the solution for different applied electric field which represent the low and high field regions at temperatures T= (77, 300) K. The obtained results showed good agreement with published data that used other calculation methods such as the Monte Carlo simulation method for all the system used in this work. Keyword: Boltzmann equation in Silicon, numerical solution for Boltzmann transport equation, Legendre polynomial expansion method نوكيلسلا يف لاقتنلال نامزتلوب ةلداعمل يددعلا لحلا ءاصقتسا يف تاموظنم مادختساب مخزلا ءاضف ةيباسح .ةفلتخم داعبأب 109 نوكيلسلا يف لاقتنلال نامزتلوب ةلداعمل يددعلا لحلا ءاصقتسا يف تاموظنم مادختساب مخزلا ءاضف ةيباسح .ةفلتخم داعبأب دومحم دجام دومحم نيسح حلاص دمحم زاتمم ءايزيفلا مسق ةفرصلا مولعلل ةيبرتلا ةيلك − لصوملا ةعماج momtaz_hussien@uomosul.edu.iq mahmood.majed.mahmood@gmail.com ملاتسلاا لوبقلا 24 / 03 / 2020 22 / 07 / 2020 DOI: 10.33899/edusj.2020.126828.1057 صخلملا لئاسم لحل ةمدختسملا ةيساسلاا ةلداعملا نامزتلوبل لاقتنلاا ةلداعم دعت نورتكللاا( ةنحشلا لماح لاقتنا ، )ةوجفلا يف طئابن أ ةلداعملا هذه لح للاخ نم عيزوتلا ةلاد ىلع لوصحلا نكميو تلاصوملا هابش ، باسح يف ةمهم عيزوتلا ةلاد دعت اهمدختسا نكمي يتلا ،تلاصوملا هابشأ صئاصخ طسوتم باسح يف ةقاط نورتكللإا لا نم اهريغو ةنحشلا لماح زيكرتو خ صاو . ةيليلحت ةقيرط مادختساب نوكيلسلا يف نامزتلوبل ةيكيسلاكلا هبش لاقتنلاا ةلداعم لح مت ثحبلا اذه يف / ةلاح يف ةيددع را رقتسلاا مخزلا ءاضف يف . عيزوتلا ةلاد نع ريبعتلا يليلحتلا لحلا بلطتي لا دودح تاددعتم مادختساب ب كلذو ردنج أ لولاا نيدحلا ذخ ا نم لك ريثأت رابتعلاا رظنب ذخلاا عم ردنجلا تاددعتم تادادتما نم يناثلاو لا ةنرملا ريغ ةراطتسلاا و ةنرملا ةيعمسلا ةراطتس إ ةفاض ىلا قورفلا ةقيرط مدختسن نامزتلوب ةلداعمل يددعلا لحلا ىلع لوصحللو .ئفاكملا ريغ ةقاطلا ةمزح بيكرت ريثأت ةددحملا ذا تافوفصملاب اهليث","PeriodicalId":15610,"journal":{"name":"Journal of Education Science","volume":"8 1","pages":"108-123"},"PeriodicalIF":0.0,"publicationDate":"2020-07-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"79649326","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Comparative Morphological Study of Pollen Grains and Seeds of Cultivars from the Species Pyrus malus L. and Pyrus communis L. Cultivated in Northern of Iraq 伊拉克北部栽培梨和梨品种花粉粒和种子的比较形态学研究
Pub Date : 2020-06-13 DOI: 10.33899/EDUSJ.2020.127063.1069
M. Shehab, Amer Al-Maathidy
The present research includes a comparative morphological characters of pollen grains and seeds of (8) cultivars belonging the species Pyrus malus L. namely ("EarlyGold", "GrannySmith", "Royal Cala", "Red Delicious", "Golden Delicious", "Honey Crisp", "Mcintosh", Cox") and (6) Cultivars belonge to the species Pyrus communis L. namely ("Coneference", Decana", "Bonica", "Alkhatuni","Alothmani", "William) which cultivated in northern of Iraq. Were examined by light and scanning electron microscope (SEM). The result of pollen grains showed that pattern tricolporate and the shape in polar view triangular or spherical -triangular or tetrangular but in equatorial view spherical or ovate and surface configuration was striate in all cultivars of the species. The morphological characters of seeds (Shape, Color, Dimension of width and Length, Number of seeds in fruit), in addition to indumentum were found to be diagnostic value for separation cultivars from the two species. In addition to its surface configuration, it was Striate in "EarlyGold", "RoyalCala", "Honey Crisp", "Mcintosh" and "Cox" and Striate papillae in GrannySmith, while the "Coneference", "Decana" and "Bonica, Alkhatuni, and Alothmani had a surface configuration pitted, and Irregular Reticular in Red Delicious and Reticulate papillae in cultivar William, while Golden Deliciou was unique as having an alveolate surface, The quantitative and qualitative morphological characters of pollen grains and seeds were found to be diagnostic value for separation cultivars from the species. Keyword: Pyrus L., Pollen grains, seeds. ةسا رد ةيرهظم حافتلا فانصا روذبو حاقل بوبحل ةنراقم Pyrus malus L. ىرثمكلاو Pyrus communis L. امش يف ةعورزملا ل قا رعلا باهش دمحم رمع ىنم 1 * ، يديضاعملا دومحم نسحم رماع 2 1 و 2 مولع مسق قا رعلا ،لصوملا ،لصوملا ةعماج ،ةفرصلا مولعلل ةيبرتلا ةيلك ،ةايحلا Journal of Education and Science (ISSN 1812-125X), Vol: 29, No: 4, 2020 (90-107) 91 ةصلاخلا : ة ر ملا ا مممصلل ة ةافم ةيةيرمممصت ةمممتا ةس رلاحلا لح لا لممممضت حافللا بوبحل Pollen grains ةوذبلاو Seeds مممممممممممممممممل 8 ) حامممممم تلا لم اممممممرمممممممممممممصأ Pyrus$malus$L. " ره EarlyGold "و " GrannySmith " "و RoyalCala "و " Red$Delicious " "و Golden$Deliciou "و " HoneyCrisp "و " Mcintosh " "و Cox " و 6 ر م لا لم امرمممممممممممممصأ ) Pyrus communis L. رهو " Coneference "و " Decana "و " Bonica "و " Alkhatuni "و " Alothmani "و " William " امم ممممممممممممما رف ةممعوةزملا ،قا رعلا رتلا ر وممممضلا ر ملا ما رتممممتاد تممممصحف Light microscope ممممتاملا ر ورت للاا ر ملاو Scanning electron microscope (SEM) بوف لاو ساقلاا ةيديد خا ر لم ا اد حافللا بوبح ةمممممممممتا ةس ج ات ر ظاو Tricolporate رب فلا ر رملا رف ا لمممممممممماو Polar view ةم ل م Trangular ةم ورك وأ – م ةم ل Spherical-triangular وا ام اوزلا ةمييامبة Tetrangular ةميريعم ىلإ رفو ر اوتمممممممتلاا ر رملا Equatorial view ة ورك Spherical ة ومممممممضيب وا Ovate ة رم ةيح مممممممسلا ا تفرقخو Striate عيمج رف ليعورلا ارممصأ اهس عو ا ولو ا لممماو اهساعدا ليح لم ةوذبلل ة ر ملا ا ممصلا ت
本研究对伊拉克北部种植的梨属(Pyrus malus L.) 8个品种(“EarlyGold”、“GrannySmith”、“Royal Cala”、“Red Delicious”、“Golden Delicious”、“Honey Crisp”、“Mcintosh”、Cox”)和6个品种(“conefence”、Decana、“Bonica”、“Alkhatuni”、“Alothmani”、“William”)的花粉粒和种子的形态特征进行了比较。光镜和扫描电镜(SEM)检查。结果表明,所有品种的花粉粒形态均为三聚体,极观为三角形或球形,极观为三角形或四边形,赤道观为球形或卵形,表面形态为条纹。种子的形态特征(形状、颜色、宽度和长度尺寸、果实中种子的数量)和被毛对两种植物的分离具有诊断价值。除了表面结构外,“EarlyGold”、“RoyalCala”、“Honey Crisp”、“Mcintosh”和“Cox”的表面结构为条纹状,“GrannySmith”的表面结构为条纹状乳头,“conefence”、“Decana”和“Bonica”、Alkhatuni和Alothmani的表面结构为凹坑状,“Red Delicious”和“William”的表面结构为网状乳头,“Golden Delicious”的表面结构为不规则网状,而“Golden Delicious”的表面结构为凹槽状。花粉粒和种子的定量和定性形态特征对品种的分离具有诊断价值。关键词:梨,花粉粒,种子ةساردةيرهظمحافتلافانصاروذبوحاقلبوبحلةنراقمPyrus马吕斯l .ىرثمكلاوPyrus普通的l .امشيفةعورزملالقارعلاباهشدمحمرمعىن1 *،ميديضاعملادومحمنسحمرماع2 1ومولعمسققارعلا،لصوملا،لصوملاةعماج،ةفرصلامولعللةيبرتلاةيلك،ةايحلا教育和科学杂志》(ISSN 1812 - 125 x),卷:29日不:4,2020年(90 - 107)91年ةصلاخلا:ةرملاامممصللةةافمةيةيرمممصتةمممتاةسرلاحلالحلالممممضتحافللابوبحل花粉粒ةوذبلاو种子ممممممممممممممممم8)حلاممممممتلالماممممممرمممممممممممممصأPyrus马吕斯美元L。”“رهEarlyGoldو“GrannySmithوRoyalCala”و“红色美元美味”“و黄金美元美味”و“密脆”و“麦金托什”“و考克斯”و6رملالمامرمممممممممممممصأ)Pyrus普通的l .رهو“Coneferenceو“Decana”و“Bonicaو“Alkhatuni”و“Alothmaniو“威廉”امممممممممممممممارفةممعوةزملا،قارعلارتلاروممممضلارملامارتممممتادتممممصحمف光显微镜مممتاملارورتللاارملاو扫描电子显微镜(SEM)بوفلاوساقلااةيديدخارلماادحافللابوبحةمممممممممتاةسجاترظاوTricolporateربفلاررملارفالمممممممممماو极地视图ةملمTrangularةموركوأ——مةمل球面三角وااماوزلاةمييامبةTetrangularةميريعمىلإرفوراوتمممممممتلااررملا赤道视图ةورك球形ةومممممممضيبوا卵形ةرمةيحمممممممسلااتفرقخو纹状عيمجرفليعورلاارممصأاهسعواولوالممماواهساعداليحلمةوذبللةرملااممصلاتممتةسو،ةحاولاةرملارفليباهسعحوارتذإ،2 4رمصرفةذب)“Alothmani”(阿罗特玛尼)(8 - 12 لي رمصلا رف ذب)“金色美味”و“威廉”اتفرقخلعيمضف،ةرمتاكذاةيحمممممممسلا纹状رفارمممممممصلاا“EarlyGold”“وRoyalCala”و“蜜脆”و“麦金托什”و“考克斯”اميلحاذةرمو纹状乳头状突起رممصلارفGrannySmith”،ليحرفنأارممصلأا”Coneference“و”Decana”“وBonica“و”Alkhatuni“و”Alothmani”ةرفرمةمميحمممممممممممممسلااممتفرقختمماممك对决ومميمممممممممممممماامترمريغ网状不规则رصلارف“红色美味ة美元ريغصاميلحاذرماو网状乳头状突起رفرصلا威廉ليحرفرممممممممصلاسرا“黄金美元美味”ذهومدابرررمممممممممت蜂窝状的بوبحوةوذبللةييورلاوةيملاةرملااممممممممصلاو،。ةتوةملاليعورلاارصأزعولصفرفةيةيرصتةميقرظأحافللا:ةيحاتفملاتاملكلاسرجPurusحافللابوبح،。ةوذبلا،ةمدقملا介绍اتاراغتةركواتحيمةلوممسدخاتمتالأةيةيرممصتلااممتاةلارفرممتاممتلاالكرلاارللةرملااممصلاةممتاةسعتةةافماصلادرتلاةيتاتلااةماعلالمتو,اتارلافيرصتوصيرشتلقرلالتألمعتوةازتمةيمهأابسكأاممرقلاالاونورممممصملاايلعرتممممسلعاممممضعدةيةيرممممصتلابتارملازعلحاتمعممممورعوةريعللرلولااصيرممممشتلارعلفحلارفاميممممتلاوةيحرمممممشتلاامممممصلالعيمممممضفرقلااضعلايةيايم،ةولرلاولاةيداةولاامممممصلاسمعترتلاةترملاعتةرملاامممممصلاف[ةيئيبلاارييغتلامامأةيتوبدرترتلاكلتاميت1،2。]حامفللابوبحملعمع孢粉学اولااليبةمينيبلاوةمةوتلاامقيعلاعبةوممحترفةمملاةميجولويبلامولعلالمةيةيرمممممممممممممصترياعمكةلوبفمرفكلذلةيئيبلاورلاداهردأتمعىلإحافللابوبحةيمهاسوعتوةلترملاةيتارلالاوعلاوسارجلااولااليبزييمتلل[ةيقارلااتارلارفاو3。 本研究对伊拉克北部种植的梨属(Pyrus malus L.) 8个品种(“EarlyGold”、“GrannySmith”、“Royal Cala”、“Red Deli
{"title":"Comparative Morphological Study of Pollen Grains and Seeds of Cultivars from the Species Pyrus malus L. and Pyrus communis L. Cultivated in Northern of Iraq","authors":"M. Shehab, Amer Al-Maathidy","doi":"10.33899/EDUSJ.2020.127063.1069","DOIUrl":"https://doi.org/10.33899/EDUSJ.2020.127063.1069","url":null,"abstract":"The present research includes a comparative morphological characters of pollen grains and seeds of (8) cultivars belonging the species Pyrus malus L. namely (\"EarlyGold\", \"GrannySmith\", \"Royal Cala\", \"Red Delicious\", \"Golden Delicious\", \"Honey Crisp\", \"Mcintosh\", Cox\") and (6) Cultivars belonge to the species Pyrus communis L. namely (\"Coneference\", Decana\", \"Bonica\", \"Alkhatuni\",\"Alothmani\", \"William) which cultivated in northern of Iraq. Were examined by light and scanning electron microscope (SEM). The result of pollen grains showed that pattern tricolporate and the shape in polar view triangular or spherical -triangular or tetrangular but in equatorial view spherical or ovate and surface configuration was striate in all cultivars of the species. The morphological characters of seeds (Shape, Color, Dimension of width and Length, Number of seeds in fruit), in addition to indumentum were found to be diagnostic value for separation cultivars from the two species. In addition to its surface configuration, it was Striate in \"EarlyGold\", \"RoyalCala\", \"Honey Crisp\", \"Mcintosh\" and \"Cox\" and Striate papillae in GrannySmith, while the \"Coneference\", \"Decana\" and \"Bonica, Alkhatuni, and Alothmani had a surface configuration pitted, and Irregular Reticular in Red Delicious and Reticulate papillae in cultivar William, while Golden Deliciou was unique as having an alveolate surface, The quantitative and qualitative morphological characters of pollen grains and seeds were found to be diagnostic value for separation cultivars from the species. Keyword: Pyrus L., Pollen grains, seeds. ةسا رد ةيرهظم حافتلا فانصا روذبو حاقل بوبحل ةنراقم Pyrus malus L. ىرثمكلاو Pyrus communis L. امش يف ةعورزملا ل قا رعلا باهش دمحم رمع ىنم 1 * ، يديضاعملا دومحم نسحم رماع 2 1 و 2 مولع مسق قا رعلا ،لصوملا ،لصوملا ةعماج ،ةفرصلا مولعلل ةيبرتلا ةيلك ،ةايحلا Journal of Education and Science (ISSN 1812-125X), Vol: 29, No: 4, 2020 (90-107) 91 ةصلاخلا : ة ر ملا ا مممصلل ة ةافم ةيةيرمممصت ةمممتا ةس رلاحلا لح لا لممممضت حافللا بوبحل Pollen grains ةوذبلاو Seeds مممممممممممممممممل 8 ) حامممممم تلا لم اممممممرمممممممممممممصأ Pyrus$malus$L. \" ره EarlyGold \"و \" GrannySmith \" \"و RoyalCala \"و \" Red$Delicious \" \"و Golden$Deliciou \"و \" HoneyCrisp \"و \" Mcintosh \" \"و Cox \" و 6 ر م لا لم امرمممممممممممممصأ ) Pyrus communis L. رهو \" Coneference \"و \" Decana \"و \" Bonica \"و \" Alkhatuni \"و \" Alothmani \"و \" William \" امم ممممممممممممما رف ةممعوةزملا ،قا رعلا رتلا ر وممممضلا ر ملا ما رتممممتاد تممممصحف Light microscope ممممتاملا ر ورت للاا ر ملاو Scanning electron microscope (SEM) بوف لاو ساقلاا ةيديد خا ر لم ا اد حافللا بوبح ةمممممممممتا ةس ج ات ر ظاو Tricolporate رب فلا ر رملا رف ا لمممممممممماو Polar view ةم ل م Trangular ةم ورك وأ – م ةم ل Spherical-triangular وا ام اوزلا ةمييامبة Tetrangular ةميريعم ىلإ رفو ر اوتمممممممتلاا ر رملا Equatorial view ة ورك Spherical ة ومممممممضيب وا Ovate ة رم ةيح مممممممسلا ا تفرقخو Striate عيمج رف ليعورلا ارممصأ اهس عو ا ولو ا لممماو اهساعدا ليح لم ةوذبلل ة ر ملا ا ممصلا ت","PeriodicalId":15610,"journal":{"name":"Journal of Education Science","volume":"9 1","pages":"90-107"},"PeriodicalIF":0.0,"publicationDate":"2020-06-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"79663614","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Calculation Values of potential Stickiness (S*) and Apparent Activation Energy (AAE) from Adsorption of Some Aromatic Carboxylic Acids on the Surface of a New Adsorbent Substance 一种新型吸附剂表面吸附芳香族羧酸的潜在粘性(S*)和表观活化能(AAE)的计算值
Pub Date : 2020-06-13 DOI: 10.33899/EDUSJ.2020.126168.1021
Khaleel Ibrahim Alniemi
This study includes calculation of the potential stickiness (S) and apparent activation energy (AAE) by the adsorption process of some aromatic carboxylic acids using sand (clay) as a new adsorbent material. This clay was collected from dust storms coming to the city of Mosul. The obtained results showed that physical adsorption which is achieved by applying the modified Arrhenius equation through the values of (S *) and (AAE) which have low values and bear a negative charge is preferable. Adsorption process occurs in two-step mechanism. The effect of the concentration of the acidic solution, temperature and the substituted groups SO3, NO2, OH, NH2 on the aromatic ring) was studied to clarify the nature of the association between organic carboxylic acid anions and inorganic metal oxides to form a complex surface model. The study concluded that the values of (S *) for all acids were less than one and they were more than the value of zero. Also, the values of (AAE) gave an indication that the adsorption process is exothermic and spontaneous. The presence of water molecules and (H) ions in solution is very important to change the nature of the clay surface. Keyword: Potential stickiness, apparent activation energy, aromatic carboxylic acids, new adsorbent material. Introduction: Adsorption is an effective and important method to remove pollution. It is simple and low-cost [1][2]. The substituted benzoic acids (5SSA, ONBA, OABA) are used in chemical industry, these acids are considered harmful substances for humans [3] [4] [5]. As an adsorbent material, Clay, consists of poly metal oxides from a rocky source [6] and different inorganic materials [7]. Metal oxides on the clay surface contain negative polar charges [8] as active sites that attract positive ions by absorbing them through physical forces. This type of attraction is called physical adsorption, while the chemical absorption occurs when the surface contains unsaturated electrons. Knowledge of adsorption mechanism is important for designing physical type of adsorption systems, through which absorbent material can be recovered and the process accomplished in an easy and Ind Calculation Values of potential Stickiness (S*) and Apparent Activation..... 78 inexpensive way. The (AAE) values represent the desired degree of the optimum temperature to achieve the complete adsorption process. Whether it occurs spontaneously or not and whether the adsorption process is endothermic or exothermic, the positive or negative values of (AAE) give a good description of the thermodynamic condition for the adsorption process. Materials and Methods : 1The chemicals were used without further purification and they were supplied by Fluka and BDH companies. 2The new clay was used as an adsorbent material. This clay was collected (using clean and dry plastic containers) from dust storms that hit the city of Mosul. The clay has been sifted (filtered out) using a sieve (75) micrometer and the surface area was (3434) cm
计算了砂(粘土)作为新型吸附剂吸附芳香族羧酸过程的潜在黏度(S)和表观活化能(AAE)。这些粘土是从摩苏尔市的沙尘暴中收集来的。结果表明,采用修正的Arrhenius方程,通过低值带负电荷的(S *)和(AAE)进行物理吸附效果较好。吸附过程采用两步法。研究了酸性溶液浓度、温度和取代基(SO3、NO2、OH、NH2)对芳环的影响,阐明了有机羧酸阴离子与无机金属氧化物缔合形成复杂表面模型的性质。研究得出结论,所有酸的(S *)值都小于1,大于0。(AAE)值表明吸附过程是自发的、放热的。水分子和(H)离子在溶液中的存在对改变粘土表面的性质是非常重要的。关键词:潜在粘性,表观活化能,芳香羧酸,新型吸附材料。导读:吸附是一种有效而重要的去除污染的方法。这是简单和低成本[1]b[2]。取代苯甲酸(5SSA, ONBA, OABA)用于化学工业,这些酸被认为是对人体有害的物质[3]b[4][5]。粘土是一种吸附剂,由来自岩石源[6]的多金属氧化物和不同的无机材料[7]组成。粘土表面的金属氧化物含有负极电荷[8],作为通过物理力吸收正离子的活性位点。这种类型的吸引称为物理吸附,而化学吸收发生在表面含有不饱和电子时。了解吸附机理对于设计物理类型的吸附系统是很重要的,通过这种系统可以回收吸收材料,并在一个简单的过程中完成吸附过程便宜的方法。(AAE)值代表实现完全吸附过程所需的最佳温度的程度。无论是否自发发生,无论吸附过程是吸热还是放热,(AAE)的正值或负值都能很好地描述吸附过程的热力学条件。材料和方法:1 .化学物质未经进一步纯化,由Fluka和BDH公司提供。该新型粘土被用作吸附剂材料。这些粘土是从袭击摩苏尔市的沙尘暴中收集来的(使用干净干燥的塑料容器)。粘土用(75)微米筛过(滤出),表面积为(3434)cm/gm。它是在摩苏尔技术研究所使用“平面装置”测量的。在Badush水泥厂使用x射线外观型(pan - analytical 7602 EA, Almelo)测量粘土成分(见表1)。表1。粘土组成8.5 pH 37.36% CaO 19.71% SiO2 5.91% AL2O3 3.47% MgO 1.89% Fe2O3 0.48% SO3溶液制备:以5%无水乙醇和95%蒸馏水为混合溶剂,制备了3种不同浓度的酸(5SSA, ONBA, OABA)溶液。以(酚酞)为指示剂,用(邻苯二甲酸氢钾)滴定制得(0.1),(0.01)M氢氧化钠的标准溶液。采用间歇法研究吸附过程。采用5A程控水浴,配有振动器,速度为100循环/分钟。6在所有浓度的吸附过程中使用等量的吸附剂。7 .最佳吸附条件为:a .粘土用量=0.06 gm。b .酸浓度=5 × 10 mol / l。c .最佳pH =每种酸的自然pH。d .每种酸与吸附率的接触时间见表2。表(2)25℃时粘土表面酸的接触时间和吸附百分比。潜在粘性(S*)和表观活化计算值.....79 %吸附接触时间(min)酸76 40 5SSA 92 30 ONBA 74 40 OABA在(20-60)℃的温度范围内对吸附过程进行研究,得到吸附后溶液中残留酸的浓度(S)。g在不同温度(20-60)℃下,计算不同浓度下吸附材料表面覆盖的离子量。 此外,它从放热过程转变为吸热过程
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引用次数: 1
Spectrophotometric Determination of Thiamine hydrochloride Via Oxidative Coupling Reaction Using 4-Aminoantipyrine 4-氨基安替比林氧化偶联分光光度法测定盐酸硫胺素
Pub Date : 2020-06-12 DOI: 10.33899/EDUSJ.2020.126895.1062
R. Al-Luhaiby, Mohammed S. Al-Enizzi
A sensitive spectrophotometric method has been developed for the determination of thiamine hydrochloride by oxidative coupling reaction of thiamine with the reagent 4-aminoantipyrine (4-AAP) in the presence of copper sulphate as oxidizing agent in alkaine medium forming a reddish brown colour. The product show maximum absorption at 335 nm. The molar absorptivitiy is 26410.59 l/mol.cm for concentrations obeyed Beer’s law in the range 0.2-18 μg.ml. The recovery was 100.93 % with relative standard deviation < 2.0 % for thiamine hydrochloride.Thiamine and reagent 4-AAP product was formed in the ratio of 1:1. The stability constant of the product was 3.39×10 l.mol for thiamine hydrochloride indicating the good stability of this product. The optimum conditions for full colour development are described and the proposed method was applied successfully for determination of thiamine in the pharmaceutical preparation (Neurorubine). The common excipients used as additives in pharmaceutical do not interfere in the proposed method.
以硫酸铜为氧化剂,在碱介质中,硫胺素与4-氨基安替比林(4-AAP)氧化偶联反应,形成红棕色,建立了测定盐酸硫胺素的灵敏分光光度法。该产品在335 nm处有最大吸收。摩尔吸光度为26410.59 l/mol。在0.2 ~ 18 μg.ml范围内,浓度符合比尔定律。盐酸硫胺素的回收率为100.93%,相对标准偏差< 2.0%。硫胺素与试剂4-AAP产物按1:1的比例生成。盐酸硫胺素的稳定常数为3.39×10 l.mol,表明该产品具有良好的稳定性。描述了全色显色的最佳条件,并成功地应用于药物制剂(neurorrubine)中硫胺素的测定。在制药中作为添加剂使用的常见赋形剂不干扰所提出的方法。
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引用次数: 0
A Friendly Environment Approach for determination of paracetamol 环境友好法测定对乙酰氨基酚
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2019.125964.1011
H. Mahmood
This paper involves a determination of paracetamol using less environment harmful reagent; the hydroxy analog of the pharmaceutical naproxen replaces the chemical reagent in which it is used as a coupling agent for the diazotized p-aminophenol (the hydrolysis product of paracetamol).The paper offers a determination of an analgesic paracetamol in the presence of high content of another analgesic . Paracetamol azo-dye formed shows the higher absorption peak at 500 nm. Absorbanceconcentration relation is liner over the range from 10 to 650 μg/20ml, (i.e. 0.5-32.5 ppm) with a good sensitivity (molar absorptivity 1.2x10 l.mol.cm) ; good precision (RSD better than ±0.275%) and high accuracy (relative error less than + 0.77%), Sandell's sensitivity index is 0.0124μg.cm, the calculated limit of detection (LOD) is 0.0030 μg/ml and the evaluated limit of quantitation (LOQ) is 0.0101 μg/ml. The application of the method exhibits a successful results for determination of paracetamol in dosage forms and it's already applied for the determination of paracetamol in presence of naproxen .
采用对环境危害较小的试剂测定对乙酰氨基酚;药物萘普生的羟基类似物取代了作为重氮化对氨基酚(扑热息痛的水解产物)偶联剂的化学试剂。本文提供了一种在另一种镇痛药的高含量存在下对乙酰氨基酚的测定方法。对乙酰氨基酚偶氮染料在500 nm处有较高的吸收峰。在10 ~ 650 μg/20ml(即0.5 ~ 32.5 ppm)范围内,吸光度与浓度呈线性关系,具有良好的灵敏度(摩尔吸光度为1.2 × 10 l.mol.cm);精密度好(RSD优于±0.275%),准确度高(相对误差小于+ 0.77%),Sandell的灵敏度指数为0.0124μg。计算检出限(LOD)为0.0030 μg/ml,定量评价限(LOQ)为0.0101 μg/ml。应用该方法可成功测定各剂型对乙酰氨基酚的含量,并已应用于萘普生存在下对乙酰氨基酚的含量测定。
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引用次数: 3
Rheological modifications of the asphalt-polymer system using microwave technology 用微波技术对沥青-聚合物体系进行流变改性
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2020.165302
Rand Raad Matti, K. Owaid
This research aimed to prepare different types of asphaltic materials having a good rheological properties compared with the non-modified asphaltic materials. Different polymers and microwaves were used to prepare the modified asphalt in different ways. The first method is based on the modification of asphalt with reclaim tire rubber using anhydrous aluminum chloride catalyst at 360 watt at different times, The second method depends on the same principle of the first method with the introduction of sulfur as an additive and the third method is based on the same principle of the first method but the change of polymer added to the polyamethyl methacrylate and with the introduction of sulfur as an additive. The latter method is the same principle of the first method but the change of polymer added to mixtures of (1:1)(polymer_polymer)(recycled tire rubber polyamethyl methacrylate)with the introduction of sulfur as an additive. The above methods we obtained asphaltic materials which can be used in paving and mastic depending on the measured (ductility, penetration , softening point). Key world: Rheological Modification, Microwave, Polymers , Asphalt. Journal of Education and Science (ISSN 1812-125X), Vol: 29, No: 2, 2020 (26-44) 27 تلفسا( ماظنل ةيجولويرلا تاريوحتلا – فيووركياملا ةينقت مادختساب )رميلوب يتم دعر دنر , ديوع دمحا دلاخ ءايميكلا مسق , ةفرصلا مولعلل ةيبرتلا ةيلك , ةعماج لصوملا قا رعلا ,لصوملا , ملا ةصلاخ ةيتلفسلإا داوملا نم ةفلتخم عاونأ ريضحت ىلإ ةسا ردلا هذه فدهت , يتلا عاونلأا صخلأابو ديج ةيجولوير صاوخ كلتمت ة ةيتلفسلإا داوملا عم ةنراقملاب .ةروحملا ريغ و مدِختُسا ةفلتخم تا رميلوب تَ ةينقتو ركياملا و ضحتل فيو ري كلذو روحمُلا تلفسلإا ةفلتخم بيلاسأب دمتعي , بولسلاا لولأا ىلع تا راطلإا طاطم عم تلفسلإا ريوحت مادختساب داعمُلا موينمللأا ديرولك زافح يئاملالا ( ةقاط دنع 360 ) طاو ةفلتخم نامزأبو , ىلع دمتعيف يناثلا بولسلأا امأ سفن أدبم بولسلاا لأا لو لاخدإ عم يفاضإ ةدامك تيربكلا ة دمتعي نيح يف , لاثلا بولسلاا ث أدبم سفن ىلع لأا إ فاضملا رميلوبلا ريغتب نكلو لولأا بولس ىل ليثم يلوبلا تلايركاثيم , إ عم لاخد تيربكلا ةيفاضإ ةدامك , أ ام لأا لأا بولس ريخ لأا أدبم سفن وهف لأا بولس لو نكل ريغتب إ فاضملا رميلوبلا ىل م داعملا تا راطلإا طاطم( نم جئا ز – يلوب ليثم )تلايركاثيم ةبسنب 1 : 1 رميلوب( _ )رميلوب إ عم لاخد تيربكلا ةيفاضإ ةدامك , و بيلاسلأا نم لوصحلا مت أ جذامن ىلع هلاع إ ةيجولوير تافصاوم تاذ ةيتلفس , ملإاب اهمادختسا ناك و طيلبتلا لاجم يف تعا ةبوطرلل ةعنام داومك اهمادختسا نكمي ىرخأ ا رجا مت يتلا تاسايقلا ىلع اًدام ؤ ه ةيذافنلاو ةلاطتسلاا( ا .)ةنويللا ةجردو ةيحاتفملا تاملكلا : تا ريوحتلا لويرلا تا رميلوبلا ,فيووركياملا ,ةيجو لإا , .تلفس ةمدقملا تلفسلإا وه نع ةرابع ةينوبراكورديه ةدام وأ دوسأ نول تاذ قماغ ينب ذ ي رياطت ةيلباق ةليلق ًايبسن [1] , بلص اذ هنوكب زاتميو بلص هبش وأ زل و ةج ةيلاع , ةرا رحلل ةعواطملا داوملا نم ربتعيو أ يأ , هن اسلا ةلاحلا ىلإ لوحتي يف ةلئ ةعفترملا ةرا رحلا تاجرد إ دوعيو ةضفخنملا ةرا رحلا تاجرد يف ةيعيبطلا ةبلصلا هتلاح ىل . ةماع ةروصب نوكتي تلفسلإا نم تابكرم نوبراكورديه ةي ةيموراو ةينيثفنو ةينيفا راب تاذ قت ةيلاع ةيئيزج نا زوا نم اه
本研究旨在制备与未改性沥青材料相比具有良好流变性能的不同类型沥青材料。利用不同的聚合物和微波以不同的方式制备改性沥青。第一种方法是利用无水氯化铝催化剂在不同时间以360瓦的功率对再生轮胎橡胶进行沥青改性;第二种方法是基于与第一种方法相同的原理,但引入硫作为添加剂;第三种方法是基于与第一种方法相同的原理,但引入硫作为添加剂改变了添加到聚甲基丙烯酸甲酯中的聚合物。后一种方法的原理与第一种方法相同,但将聚合物添加到(1:1)(聚合物-聚合物)(再生轮胎橡胶聚甲基丙烯酸甲酯)的混合物中,并引入硫作为添加剂,改变了聚合物的结构。根据所测的(延性、渗透性、软化点),用上述方法得到了可用于铺装的沥青材料和胶泥。关键词:流变改性,微波,聚合物,沥青。《教育与科学杂志》(ISSN 1812-125X),第29卷,编号:2020(26-44) 27تلفسا(ماظنلةيجولويرلاتاريوحتلا——فيووركياملاةينقتمادختساب)رميلوبيتمدعردنر,ديوعدمحادلاخءايميكلامسق,ةفرصلامولعللةيبرتلاةيلك,ةعماجلصوملاقارعلا,لصوملا,ملاةصلاخةيتلفسلإاداوملانمةفلتخمعاونأريضحتىلإةساردلاهذهفدهت,يتلاعاونلأاصخلأابوديجةيجولويرصاوخكلتمتةةيتلفسلإاداوملاعمةنراقملاب。ةروحملاريغومدِختُساةفلتخمتارميلوبتَةينقتوركياملاوضحتلفيوريكلذوروحمُلاتلفسلإاةفلتخمبيلاسأبدمتعي,بولسلاالولأاىلعتاراطلإاطاطمعمتلفسلإاريوحتمادختسابداعمُلاموينمللأاديرولكزافحيئاملالا(ةقاطدنع360)طاوةفلتخمنامزأبو,ىلعدمتعيفيناثلابولسلأاامأسفنأدبمبولسلاالأالولاخدإعميفاضإةدامكتيربكلاةدمتعينيحيف,لاثلابولسلااثأدبمسفنىلعلأاإفاضملارميلوبلاريغتبنكلولولأابولسىلليثميلوبلاتلايركاثيم,إعملاخدتيربكلاةيفاضإةدامك,أاملأالأابولسريخلأاأدبمسفنوهفلأابولسلونكلريغتبإفاضملارميلوبلاىلمداعملاتاراطلإاطاطم(نمجئاز——يلوبليثم)تلايركاثيمةبسنب1:1رميلوب(_)رميلوبإعملاخدتيربكلاةيفاضإةدامك,وبيلاسلأانملوصحلامتأجذامنىلعهلاعإةيجولويرتافصاومتاذةيتلفس,ملإاباهمادختساناكوطيلبتلالاجميفتعاةبوطرللةعنامداومكاهمادختسانكميىرخأارجامتيتلاتاسايقلاىلعاًدامؤهةيذافنلاوةلاطتسلاا(ا)ةنويللاةجردوةيحاتفملاتاملكلا:تاريوحتلالويرلاتارميلوبلا,فيووركياملا,ةيجولإا,。تلفسةمدقملاتلفسلإاوهنعةرابعةينوبراكورديهةداموأدوسأنولتاذقماغينبذيرياطتةيلباقةليلقًايبسن[1],بلصاذهنوكبزاتميوبلصهبشوأزلوةجةيلاع,ةرارحللةعواطملاداوملانمربتعيوأيأ,هناسلاةلاحلاىلإلوحتييفةلئةعفترملاةرارحلاتاجردإدوعيوةضفخنملاةرارحلاتاجرديفةيعيبطلاةبلصلاهتلاحىل。ةماعةروصبنوكتيتلفسلإانمتابكرمنوبراكورديهةيةيموراوةينيثفنوةينيفارابتاذقتةيلاعةيئيزجنازوانماهميقبرت(3000 - 200)لوم/مغ،لمتشيوريغوأةيقلحتابكرمىلعكلذكنلاىلعيوتحتةيقلحي،نيجسكولأاوتيربكلاونيجورتِهئاوتحانعلًاضفتايمكىلعنمةليلقلكينلاوديدحلاومويدانفلاتارذ。رثأتتتلفسلإاتافصةيئايزيفلاةجوزللاوةينابوذلا،نايلغلاةجردلثم[2]。خلا教育和科学杂志》(ISSN 1812 - 125 x),卷:29日不:2,2020(26-44)28باريثكنلاوتيربكلاتابكرمينيجسكولأاونيجورتوملارصانعلادعةينذإ,اةسناجتملاريغتارذلالمعتلخادتلاىلعةيبطقلتائيزجلانيب。وإنةعونتموةريثكتامادختساتلفسلإلأوءانبلاوةعانصلايفةسدنهلالامع[3]نمهبعتمتياملاًرظنلومخايميكةجوزلويئ,نيتيلاعةناتموةوقو,اقمولأاوضماوحلانمديدعللةريبكةموتايولقلاوحلام,ءاملاببوذيلاهنوكلاًضياو,إنيسحتمتتتلفسلإلةيجولويرلاصاوخلانةفلتخمقرطب,هيفمدختسملاضرغللاًعبتةددعتمبيلاسأبوإنإفكلذلةفاضتارميلوبلالإاصاوخنيسحتيفةديجةقيرطربتعتتلفسذإ,هتيعونولأاتافاضملاتارميلوبلالثمتيفلاامعتسارثكريوحتلا[4]ولإاصاوخلريوحتلاةيلمعنإةيجولويرلاتلفسيجولويرلاصاوخةةيرميلوبلاداوملاب,ةريثكدئاوفىلعلمعتيهفةدايزةبلاصكسامتولإاتلفسنسحتكلذبوهتمواقملوةرارحلاتاجرديزتوةدسكلألجيزملاةمواقمنمدلافورظللولكآتةيرارقتسانمديزتو,)قيتعتلا(ةيوجلاجيزملاوهتوقونسحينمكسامتلاوقصلاتلاصاوخ[5]أفصرلافيلاكتلازتخاووناكملااردقطيلبتلا[6],حرتقانملوأنإكلهتسملاطاطملاةفاضإةركف)(废橡胶وهتلفسلإلةروحمةدامكملاعلا(麦当劳,1966)ذإ,متتاطمةفاضإاتلكونيتقيرطبةفلاتلاتاراطلإاطيكشتنمضتتامهةريغصداعبأبطاطملالزواجتتلا2.5毫米
{"title":"Rheological modifications of the asphalt-polymer system using microwave technology","authors":"Rand Raad Matti, K. Owaid","doi":"10.33899/edusj.2020.165302","DOIUrl":"https://doi.org/10.33899/edusj.2020.165302","url":null,"abstract":"This research aimed to prepare different types of asphaltic materials having a good rheological properties compared with the non-modified asphaltic materials. Different polymers and microwaves were used to prepare the modified asphalt in different ways. The first method is based on the modification of asphalt with reclaim tire rubber using anhydrous aluminum chloride catalyst at 360 watt at different times, The second method depends on the same principle of the first method with the introduction of sulfur as an additive and the third method is based on the same principle of the first method but the change of polymer added to the polyamethyl methacrylate and with the introduction of sulfur as an additive. The latter method is the same principle of the first method but the change of polymer added to mixtures of (1:1)(polymer_polymer)(recycled tire rubber polyamethyl methacrylate)with the introduction of sulfur as an additive. The above methods we obtained asphaltic materials which can be used in paving and mastic depending on the measured (ductility, penetration , softening point). Key world: Rheological Modification, Microwave, Polymers , Asphalt. Journal of Education and Science (ISSN 1812-125X), Vol: 29, No: 2, 2020 (26-44) 27 تلفسا( ماظنل ةيجولويرلا تاريوحتلا – فيووركياملا ةينقت مادختساب )رميلوب يتم دعر دنر , ديوع دمحا دلاخ ءايميكلا مسق , ةفرصلا مولعلل ةيبرتلا ةيلك , ةعماج لصوملا قا رعلا ,لصوملا , ملا ةصلاخ ةيتلفسلإا داوملا نم ةفلتخم عاونأ ريضحت ىلإ ةسا ردلا هذه فدهت , يتلا عاونلأا صخلأابو ديج ةيجولوير صاوخ كلتمت ة ةيتلفسلإا داوملا عم ةنراقملاب .ةروحملا ريغ و مدِختُسا ةفلتخم تا رميلوب تَ ةينقتو ركياملا و ضحتل فيو ري كلذو روحمُلا تلفسلإا ةفلتخم بيلاسأب دمتعي , بولسلاا لولأا ىلع تا راطلإا طاطم عم تلفسلإا ريوحت مادختساب داعمُلا موينمللأا ديرولك زافح يئاملالا ( ةقاط دنع 360 ) طاو ةفلتخم نامزأبو , ىلع دمتعيف يناثلا بولسلأا امأ سفن أدبم بولسلاا لأا لو لاخدإ عم يفاضإ ةدامك تيربكلا ة دمتعي نيح يف , لاثلا بولسلاا ث أدبم سفن ىلع لأا إ فاضملا رميلوبلا ريغتب نكلو لولأا بولس ىل ليثم يلوبلا تلايركاثيم , إ عم لاخد تيربكلا ةيفاضإ ةدامك , أ ام لأا لأا بولس ريخ لأا أدبم سفن وهف لأا بولس لو نكل ريغتب إ فاضملا رميلوبلا ىل م داعملا تا راطلإا طاطم( نم جئا ز – يلوب ليثم )تلايركاثيم ةبسنب 1 : 1 رميلوب( _ )رميلوب إ عم لاخد تيربكلا ةيفاضإ ةدامك , و بيلاسلأا نم لوصحلا مت أ جذامن ىلع هلاع إ ةيجولوير تافصاوم تاذ ةيتلفس , ملإاب اهمادختسا ناك و طيلبتلا لاجم يف تعا ةبوطرلل ةعنام داومك اهمادختسا نكمي ىرخأ ا رجا مت يتلا تاسايقلا ىلع اًدام ؤ ه ةيذافنلاو ةلاطتسلاا( ا .)ةنويللا ةجردو ةيحاتفملا تاملكلا : تا ريوحتلا لويرلا تا رميلوبلا ,فيووركياملا ,ةيجو لإا , .تلفس ةمدقملا تلفسلإا وه نع ةرابع ةينوبراكورديه ةدام وأ دوسأ نول تاذ قماغ ينب ذ ي رياطت ةيلباق ةليلق ًايبسن [1] , بلص اذ هنوكب زاتميو بلص هبش وأ زل و ةج ةيلاع , ةرا رحلل ةعواطملا داوملا نم ربتعيو أ يأ , هن اسلا ةلاحلا ىلإ لوحتي يف ةلئ ةعفترملا ةرا رحلا تاجرد إ دوعيو ةضفخنملا ةرا رحلا تاجرد يف ةيعيبطلا ةبلصلا هتلاح ىل . ةماع ةروصب نوكتي تلفسلإا نم تابكرم نوبراكورديه ةي ةيموراو ةينيثفنو ةينيفا راب تاذ قت ةيلاع ةيئيزج نا زوا نم اه","PeriodicalId":15610,"journal":{"name":"Journal of Education Science","volume":"50 2 1","pages":"26-44"},"PeriodicalIF":0.0,"publicationDate":"2020-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81088244","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Using of Acetylacetone-formaldehyde Reagent in Spectrophotometric Determination of Aniline in Various Water Samples 用乙酰丙酮-甲醛试剂分光光度法测定各种水样中苯胺
Pub Date : 2020-06-01 DOI: 10.33899/edusj.2020.126192.1022
N. Othman, S. Zakaria, M. Abdulla
A simple and accurate spectrophotometric method for the estimation of aniline in various water samples was done. The method was based on the condensation reaction of acetyl acetoneformaldehyde (AC-FA) reagent with aniline. to produce a yellow colored product, with maximum absorption at 417 nm, which has good stability at room temperature and it is very soluble in water (the medium of reaction). Beer's law is applied in the concentration range of 2.5 to 50 μg. ml of aniline with a molar absorptivity 3.864×10 l.mol.cm and Sandell's sensitivity index 0.0241 μg.cm , a relative error of – 0.51 to +4.15 % and a relative standard deviation of ±0.78 to ±1.28% depending on the concentration level. The study also included the effect of organic compounds on the recovery of aniline in water samples. Aniline is the simple type of primary aromatic amines as it enters into many industrial fields and is considered as an important material. Aniline regarded as major pollutant of water, thus, its estimation was studied in different samples of water such as river, tap and Zamzam well waters.
建立了一种简便、准确的测定各种水样中苯胺的分光光度法。该方法以乙酰丙酮甲醛(AC-FA)试剂与苯胺的缩合反应为基础。产黄色产物,最大吸收波长为417 nm,室温稳定性好,极易溶于水(反应介质)。在2.5 ~ 50 μg的浓度范围内适用Beer定律。ml的苯胺,摩尔吸光度3.864×10 l.mol.cm,桑德尔灵敏度指数0.0241 μg。Cm,相对误差为- 0.51 ~ + 4.15%,相对标准偏差为±0.78 ~±1.28%,取决于浓度水平。该研究还包括有机化合物对水样中苯胺回收的影响。苯胺是一类简单的伯胺类芳香胺,被广泛应用于许多工业领域,是一种重要的原料。苯胺作为水体的主要污染物,对河流、自来水、赞赞井水等不同水样对苯胺的估算进行了研究。
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引用次数: 0
期刊
Journal of Education Science
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