Low carbon ferromanganese was nitrided through gas-solid reaction. The nitriding process has been carried out on lab scale at temperature range 800°C–950°C at different nitrogen pressures. Temperature, time, and partial nitrogen pressure of nitriding process of fine low carbon ferromanganese were investigated. Nitrogen content, in weight percent, was more than 9%. MATLAB software was used to derive mathematical model to predict nitrogen content as a function of temperature and nitrogen pressure. According to derived model, nitrogen content can be calculated by the following equation: , where, T is nitriding temperature in K and P is nitrogen pressure in bar. The experimental results are in good agreement with the predicted results. The results showed that nitrogen content, at steady state, is mainly depending on temperature and pressure of nitriding process. MATLAB is a good tool to make precision mathematical model.
{"title":"Mathematical Model of Prediction of Nitrogen Pickup in Nitriding Process of Low Carbon Ferromanganese","authors":"S. Ghali","doi":"10.1155/2014/793508","DOIUrl":"https://doi.org/10.1155/2014/793508","url":null,"abstract":"Low carbon ferromanganese was nitrided through gas-solid reaction. The nitriding process has been carried out on lab scale at temperature range 800°C–950°C at different nitrogen pressures. Temperature, time, and partial nitrogen pressure of nitriding process of fine low carbon ferromanganese were investigated. Nitrogen content, in weight percent, was more than 9%. MATLAB software was used to derive mathematical model to predict nitrogen content as a function of temperature and nitrogen pressure. According to derived model, nitrogen content can be calculated by the following equation: , where, T is nitriding temperature in K and P is nitrogen pressure in bar. The experimental results are in good agreement with the predicted results. The results showed that nitrogen content, at steady state, is mainly depending on temperature and pressure of nitriding process. MATLAB is a good tool to make precision mathematical model.","PeriodicalId":16342,"journal":{"name":"Journal of Metallurgy","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2014-07-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84102562","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Al-11 wt.% Si-11 wt.% Fe (11.29 at.% Si-5.6 at.% Fe) melt was rapidly solidified into ribbons and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), and microhardness technique. The Rietveld X-ray diffraction analysis was applied successfully to analyze microstructure and phase precipitations. On the basis of the aluminum peak shifts measured in the XRD scans, a solid solubility extension value of 1 at.% Si in -Al was determined. SEM investigations confirmed presence of a spherical shape -phase particles in addition to needle and spherical shape -phase particles with contents of 1.1 wt.% and 10.1 wt.% as deduced by XRD analysis. During prolonged annealing process at 350°C/25 h, -phase disappeared, -phase content increased to 30 wt.%, and Si presence becomes more evident as deduced by XRD analysis. EDS analysis confirmed that these particles observed in the as-melt spun alloy are of lower Fe content comparing to those usually observed in the as-cast counter-part alloy. Besides, the length distribution of needle shape -particles has been shortened to be diverse from 1 to 5 μm. The as-melt spun ribbons exhibited enhancement of hardness to 277 HV and further increased during heat treatment (150°C/12 h) to 450 HV. This improvement of microstructure and hardness are the influence of microstructural refinement and modification obtained during the rapid solidification process.
{"title":"Microstructure and Microhardness Evolutions of High Fe Containing Near-Eutectic Al-Si Rapidly Solidified Alloy","authors":"E. M. Ahmed, M. Ebrahim","doi":"10.1155/2014/587265","DOIUrl":"https://doi.org/10.1155/2014/587265","url":null,"abstract":"Al-11 wt.% Si-11 wt.% Fe (11.29 at.% Si-5.6 at.% Fe) melt was rapidly solidified into ribbons and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), and microhardness technique. The Rietveld X-ray diffraction analysis was applied successfully to analyze microstructure and phase precipitations. On the basis of the aluminum peak shifts measured in the XRD scans, a solid solubility extension value of 1 at.% Si in <path id=\"x1D6FC\" d=\"M545 106q-67 -118 -134 -118q-24 0 -40 37.5t-30 129.5h-2q-47 -72 -103 -119.5t-108 -47.5q-47 0 -76 45.5t-29 119.5q0 113 85 204t174 91q47 0 70 -33.5t43 -119.5h3q32 47 80 140l55 13l10 -9q-47 -80 -138 -201q17 -99 27.5 -136t22.5 -37q23 0 69 61zM333 204\u0000q-14 98 -31 149.5t-50 51.5q-49 0 -94 -70t-45 -164q0 -55 15.5 -86t40.5 -31q70 0 164 150z\"> -Al was determined. SEM investigations confirmed presence of a spherical shape -phase particles in addition to needle and spherical shape <path id=\"x1D6FD\" d=\"M558 587q0 -32 -14 -61t-40 -53.5t-48.5 -41t-54.5 -36.5q144 -51 144 -174q0 -55 -43.5 -108t-104.5 -87q-77 -42 -131 -42q-31 0 -54 20t-31 47l11 18q48 -29 108 -29q79 0 119.5 43t40.5 109t-44.5 107.5t-119.5 50.5l22 47q34 1 65 21q96 61 96 157q0 42 -24 67.5\u0000t-62 25.5q-24 0 -43.5 -9t-35 -29.5t-27 -44t-22.5 -63t-19.5 -75.5t-18.5 -91q-57 -294 -68 -380q-26 -190 -35 -200q-26 -31 -97 -37l-4 26q19 9 48 170l77 413q23 121 52.5 187.5t83.5 114.5q70 62 148 62q51 0 88.5 -34t37.5 -91z\"> -phase particles with contents of 1.1 wt.% and 10.1 wt.% as deduced by XRD analysis. During prolonged annealing process at 350°C/25 h, -phase disappeared, -phase content increased to 30 wt.%, and Si presence becomes more evident as deduced by XRD analysis. EDS analysis confirmed that these particles observed in the as-melt spun alloy are of lower Fe content comparing to those usually observed in the as-cast counter-part alloy. Besides, the length distribution of needle shape -particles has been shortened to be diverse from 1 to 5 μm. The as-melt spun ribbons exhibited enhancement of hardness to 277 HV and further increased during heat treatment (150°C/12 h) to 450 HV. This improvement of microstructure and hardness are the influence of microstructural refinement and modification obtained during the rapid solidification process.","PeriodicalId":16342,"journal":{"name":"Journal of Metallurgy","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2014-05-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85294817","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Corrosion inhibitive performance of some thiophene derivatives during the acidic corrosion of carbon steel surface in 1 M HCl was investigated by chemical technique (weight loss) and electrochemical techniques (potentiodynamic polarization, electrochemical frequency modulation, and electrochemical impedance spectroscopy). The effect of temperature on the corrosion rate was investigated by the weight loss method, and some thermodynamic parameters for corrosion and adsorption processes were determined and discussed. The results show that the inhibition efficiency increased with the increase in inhibitor concentration and temperature. The adsorption of thiophene derivatives on the carbon steel surface obeys Langmuir adsorption isotherm. The obtained results indicated that the investigated compounds are chemically adsorbed on the steel surface. Potentiodynamic polarization studies showed that these compounds are mixed-type inhibitors and the results obtained from the techniques are in good agreement.
采用化学技术(失重法)和电化学技术(动电位极化法、电化学调频法和电化学阻抗谱法)研究了噻吩衍生物在碳钢表面1 M HCl酸性腐蚀中的缓蚀性能。采用失重法研究了温度对腐蚀速率的影响，并对腐蚀和吸附过程的热力学参数进行了确定和讨论。结果表明，缓蚀剂的缓蚀效率随缓蚀剂浓度和温度的增加而增加。噻吩衍生物在碳钢表面的吸附遵循Langmuir吸附等温线。结果表明，所研究的化合物在钢表面有化学吸附。动电位极化研究表明，这些化合物为混合型抑制剂，所得结果吻合较好。
{"title":"Some Thiophene Derivatives as Corrosion Inhibitors for Carbon Steel in Hydrochloric Acid","authors":"A. Fouda, A. Attia, A. Negm","doi":"10.1155/2014/472040","DOIUrl":"https://doi.org/10.1155/2014/472040","url":null,"abstract":"Corrosion inhibitive performance of some thiophene derivatives during the acidic corrosion of carbon steel surface in 1 M HCl was investigated by chemical technique (weight loss) and electrochemical techniques (potentiodynamic polarization, electrochemical frequency modulation, and electrochemical impedance spectroscopy). The effect of temperature on the corrosion rate was investigated by the weight loss method, and some thermodynamic parameters for corrosion and adsorption processes were determined and discussed. The results show that the inhibition efficiency increased with the increase in inhibitor concentration and temperature. The adsorption of thiophene derivatives on the carbon steel surface obeys Langmuir adsorption isotherm. The obtained results indicated that the investigated compounds are chemically adsorbed on the steel surface. Potentiodynamic polarization studies showed that these compounds are mixed-type inhibitors and the results obtained from the techniques are in good agreement.","PeriodicalId":16342,"journal":{"name":"Journal of Metallurgy","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2014-05-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"90044323","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
The influence of heat treatment on microstructure and mechanical properties of high chromium white cast iron alloyed with titanium was investigated. The austenitizing temperatures of 980°C and 1150°C for 1 hour each followed by tempering at 260°C for 2 hours have been performed and the effect of these treatments on wear resistance/impact toughness combination is reported. The microstructure of irons austenitized at 1150°C showed a fine precipitate of secondary carbides (M6C23) in a matrix of eutectic austenite and eutectic carbides (M7C3). At 980°C, the structure consisted of spheroidal martensite matrix, small amounts of fine secondary carbides, and eutectic carbides. Titanium carbides (TiC) particles with cuboidal morphology were uniformly distributed in both matrices. Irons austenitized at 980°C showed relatively higher tensile strength compared to those austenitized at 1150°C, while the latter showed higher impact toughness. For both cases, optimum tensile strength was reported for the irons alloyed with 1.31% Ti, whereas maximum impact toughness was obtained for the irons without Ti-addition. Higher wear resistance was obtained for the samples austenitized at 980°C compared to the irons treated at 1150°C. For both treatments, optimum wear resistance was obtained with 1.3% Ti.
{"title":"Heat Treatment in High Chromium White Cast Iron Ti Alloy","authors":"K. Ibrahim, M. Ibrahim","doi":"10.1155/2014/856408","DOIUrl":"https://doi.org/10.1155/2014/856408","url":null,"abstract":"The influence of heat treatment on microstructure and mechanical properties of high chromium white cast iron alloyed with titanium was investigated. The austenitizing temperatures of 980°C and 1150°C for 1 hour each followed by tempering at 260°C for 2 hours have been performed and the effect of these treatments on wear resistance/impact toughness combination is reported. The microstructure of irons austenitized at 1150°C showed a fine precipitate of secondary carbides (M6C23) in a matrix of eutectic austenite and eutectic carbides (M7C3). At 980°C, the structure consisted of spheroidal martensite matrix, small amounts of fine secondary carbides, and eutectic carbides. Titanium carbides (TiC) particles with cuboidal morphology were uniformly distributed in both matrices. Irons austenitized at 980°C showed relatively higher tensile strength compared to those austenitized at 1150°C, while the latter showed higher impact toughness. For both cases, optimum tensile strength was reported for the irons alloyed with 1.31% Ti, whereas maximum impact toughness was obtained for the irons without Ti-addition. Higher wear resistance was obtained for the samples austenitized at 980°C compared to the irons treated at 1150°C. For both treatments, optimum wear resistance was obtained with 1.3% Ti.","PeriodicalId":16342,"journal":{"name":"Journal of Metallurgy","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2014-04-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83512107","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
The tests of uniaxial tensile by 10, 20, and 30% at strain rates of 0.1, 1, 60, 120, and 300 mm/min in rolling direction and transverse direction of recrystallized cold-rolled low-carbon steel sheets were carried out. The effect of rate and degree of deformation on the texture, structure, and mechanical properties were studied. The texture transformations and the growth of the anisotropy of mechanical properties with increasing strain rate up to 120 mm/min are explained by the effect of crystallographic intragranular slip and twinning of deformation mechanism. The further increase of deformation rate leads to texture scattering and decreasing of properties anisotropy, which are bound to the difficulty of intragranular sliding and activation of grain boundary sliding.
{"title":"Influence of the Rate and Degree of Deformation on the Texture, Structure and Mechanical Properties of Steel","authors":"V. Usov, N. Shkatulyak, A. Bryukhanov, D. Fasmann","doi":"10.1155/2014/397279","DOIUrl":"https://doi.org/10.1155/2014/397279","url":null,"abstract":"The tests of uniaxial tensile by 10, 20, and 30% at strain rates of 0.1, 1, 60, 120, and 300 mm/min in rolling direction and transverse direction of recrystallized cold-rolled low-carbon steel sheets were carried out. The effect of rate and degree of deformation on the texture, structure, and mechanical properties were studied. The texture transformations and the growth of the anisotropy of mechanical properties with increasing strain rate up to 120 mm/min are explained by the effect of crystallographic intragranular slip and twinning of deformation mechanism. The further increase of deformation rate leads to texture scattering and decreasing of properties anisotropy, which are bound to the difficulty of intragranular sliding and activation of grain boundary sliding.","PeriodicalId":16342,"journal":{"name":"Journal of Metallurgy","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2014-03-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91389073","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
D. Kevorkov, M. Medraj, M. Aljarrah, Jian Li, E. Essadiqi, P. Chartrand, C. Fuerst
The Al-Mg-Sr system is experimentally studied at 400°C using EPMA and XRD techniques. It was determined that the intermetallic phases in the Al-Mg-Sr system have a tendency to form extended substitutional solid solutions. Two ternary phases were found in this system. Solubility limits of binary and ternary phases were determined and the phase equilibria among phases were established. The isothermal section of the Al-Mg-Sr system at 400°C has been constructed using results of the phase analysis and experimental literature data.
{"title":"Experimental Study of the Al-Mg-Sr Phase Diagram at 400°C","authors":"D. Kevorkov, M. Medraj, M. Aljarrah, Jian Li, E. Essadiqi, P. Chartrand, C. Fuerst","doi":"10.1155/2014/690623","DOIUrl":"https://doi.org/10.1155/2014/690623","url":null,"abstract":"The Al-Mg-Sr system is experimentally studied at 400°C using EPMA and XRD techniques. It was determined that the intermetallic phases in the Al-Mg-Sr system have a tendency to form extended substitutional solid solutions. Two ternary phases were found in this system. Solubility limits of binary and ternary phases were determined and the phase equilibria among phases were established. The isothermal section of the Al-Mg-Sr system at 400°C has been constructed using results of the phase analysis and experimental literature data.","PeriodicalId":16342,"journal":{"name":"Journal of Metallurgy","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2014-03-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91506054","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
A review of various factors affecting wetting and spreading has been presented. Various methods for wettability studies and critical issues concerning contact angle measurement are discussed. Reactive wetting has been given a special attention in the paper and recent developments in this area are summarized and discussed. Although advanced understanding of nonreactive wetting is currently available in the literature, complete understanding of reactive wetting is still lacking due to the complexity of the phenomenon. To date, there is no single model that is generally applicable to all reactive wetting systems. Reaction between the liquid drop and substrate can take the form of dissolution, intermetallic formation, or combination of both processes. Factors affecting wettability have been summarized and discussed as well as the major available techniques to investigate wetting behaviour.
{"title":"Progress in Wettability Study of Reactive Systems","authors":"Bolarinwa Komolafe, M. Medraj","doi":"10.1155/2014/387046","DOIUrl":"https://doi.org/10.1155/2014/387046","url":null,"abstract":"A review of various factors affecting wetting and spreading has been presented. Various methods for wettability studies and critical issues concerning contact angle measurement are discussed. Reactive wetting has been given a special attention in the paper and recent developments in this area are summarized and discussed. Although advanced understanding of nonreactive wetting is currently available in the literature, complete understanding of reactive wetting is still lacking due to the complexity of the phenomenon. To date, there is no single model that is generally applicable to all reactive wetting systems. Reaction between the liquid drop and substrate can take the form of dissolution, intermetallic formation, or combination of both processes. Factors affecting wettability have been summarized and discussed as well as the major available techniques to investigate wetting behaviour.","PeriodicalId":16342,"journal":{"name":"Journal of Metallurgy","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2014-03-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87904978","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
NiTi shape memory alloys are promising implant materials due to their shape memory effect and super elasticity. In the current study, some Ni50Ti50 (mass %) SMAs samples were prepared by investment casting. These samples were then anodized and thermally treated to improve the surface properties. A fully saturated oxide layer was obtained. The structure and hardness properties of the anodized surfaces were then investigated. A hard porous layer with no free Ni atoms could be obtained which can be used as prebiomimetic surface for biological application.
{"title":"Characteristics of Anodized Layer in Investment Cast Ni50Ti50 Shape Memory Alloy","authors":"S. El-Hadad, K. Ibrahim, L. Wagner","doi":"10.1155/2014/346328","DOIUrl":"https://doi.org/10.1155/2014/346328","url":null,"abstract":"NiTi shape memory alloys are promising implant materials due to their shape memory effect and super elasticity. In the current study, some Ni50Ti50 (mass %) SMAs samples were prepared by investment casting. These samples were then anodized and thermally treated to improve the surface properties. A fully saturated oxide layer was obtained. The structure and hardness properties of the anodized surfaces were then investigated. A hard porous layer with no free Ni atoms could be obtained which can be used as prebiomimetic surface for biological application.","PeriodicalId":16342,"journal":{"name":"Journal of Metallurgy","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2014-02-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"73380355","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Ternary Ni-Zn-P alloy thin films were electrolessly deposited on a carbon steel substrate from sulphate alkaline baths. The effect of deposition bath composition and process duration on the physical-chemical and corrosion characteristics of the obtained thin films was investigated. The thin films were characterized by EDAX analysis techniques and scanning electronic microscopy. Corrosion tests were performed in 3.5% sodium chloride solution and the corrosion current values were determined to be 4–12 μA, comparative to 15 μA for the uncoated steel sample.
{"title":"Microstructural Characterization and Corrosion Behavior of Electroless Ni-Zn-P Thin Films","authors":"I. Constantin","doi":"10.1155/2014/827393","DOIUrl":"https://doi.org/10.1155/2014/827393","url":null,"abstract":"Ternary Ni-Zn-P alloy thin films were electrolessly deposited on a carbon steel substrate from sulphate alkaline baths. The effect of deposition bath composition and process duration on the physical-chemical and corrosion characteristics of the obtained thin films was investigated. The thin films were characterized by EDAX analysis techniques and scanning electronic microscopy. Corrosion tests were performed in 3.5% sodium chloride solution and the corrosion current values were determined to be 4–12 μA, comparative to 15 μA for the uncoated steel sample.","PeriodicalId":16342,"journal":{"name":"Journal of Metallurgy","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2014-01-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"82643899","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Phase changes in a commercial AA8011 alloy from different initial microstructure conditions were studied using thermoelectric power (), differential scanning calorimetry (DSC), and transmission electron microscopy (TEM) techniques with the purpose of obtaining evidence of the interaction between recovery-precipitation and recrystallization-precipitation processes occurring during nonisothermal heating at different rates. Thermoelectric power and its thermal derivative reflect this evidence by a displacement of the characteristic precipitation peaks, the recovery and recrystallization contributions remaining masked by the strong incidence of the iron precipitation on that property, while DSC measurements detect the emergence of new peaks not observed on thermograms of homogenized samples. An exhaustive study of these peaks permits direct differentiation between precipitation and recovery-recrystallization contributions. TEM confirms the interaction between both processes by means of local observations.
{"title":"Experimental Study of the Interaction between Recrystallization and Precipitation Processes of an AA8011 Commercial Alloy","authors":"N. Luiggi, M. Valera, J. P. Rodríguez, J. Prin","doi":"10.1155/2014/345945","DOIUrl":"https://doi.org/10.1155/2014/345945","url":null,"abstract":"Phase changes in a commercial AA8011 alloy from different initial microstructure conditions were studied using thermoelectric power (), differential scanning calorimetry (DSC), and transmission electron microscopy (TEM) techniques with the purpose of obtaining evidence of the interaction between recovery-precipitation and recrystallization-precipitation processes occurring during nonisothermal heating at different rates. Thermoelectric power and its thermal derivative reflect this evidence by a displacement of the characteristic precipitation peaks, the recovery and recrystallization contributions remaining masked by the strong incidence of the iron precipitation on that property, while DSC measurements detect the emergence of new peaks not observed on thermograms of homogenized samples. An exhaustive study of these peaks permits direct differentiation between precipitation and recovery-recrystallization contributions. TEM confirms the interaction between both processes by means of local observations.","PeriodicalId":16342,"journal":{"name":"Journal of Metallurgy","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2014-01-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"80084217","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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