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Synthesis, characterization, Biological Activity, and corrosion inhibition study of two dyes from 4-aminophenol 两种4-氨基酚染料的合成、表征、生物活性及缓蚀性能研究
Pub Date : 2023-09-30 DOI: 10.31185/wjps.215
Sura Hamid, None Aseel F. Abdullah, None Mohammed M. Mohammed, None Fatma A. Khazaal
In the study, the reaction used to create the azo dyes (B and N)of 4-aminophenol with β-naphthol and 3-nitrophenol. These compounds were characterized by technology analysis as FT-IR and 1H-NMR and physical properties were assessed. The synthesis compounds of biological activity were studied against two types of bacterial positive-grams (Staphylococcus aureus) and negative-grams (E.coli) and given good results. The azo compounds were studied as corrosion inhibitors in the dissolution of carbon steel 45 in (0. 1M) HCl solution. the inhibitors of dyes were inspected using the polarization of technique. The compounds (B and N) show inhibition high efficiency.
本研究采用β-萘酚和3-硝基酚制备4-氨基苯酚偶氮染料B和N。通过FT-IR、1H-NMR等技术分析对化合物进行了表征,并对化合物的物理性质进行了评价。对合成的化合物对阳性克氏菌(金黄色葡萄球菌)和阴性克氏菌(大肠杆菌)的生物活性进行了研究,并取得了良好的效果。研究了偶氮化合物作为缓蚀剂在碳钢45 in(0。1M) HCl溶液。利用极化技术对染料的抑制剂进行了检测。化合物B和N的抑菌效果较好。
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引用次数: 0
Evaluated the Effect of Titanium Dioxide Nanoparticles on the Activity of Creatinine and Urea Levels in Dialysis Patients 评估二氧化钛纳米颗粒对透析患者肌酐和尿素水平活性的影响
Pub Date : 2023-09-30 DOI: 10.31185/wjps.184
Nasser Alqurashy
Abstract Nanotechnology is an emerging field that has got a phenomenal interest in the last few decades. Medical application is considered one of the most important ambitions in this field. The objective was to evaluate the biological effects of (TiO2-NPs) on urea and creatinine activity among kidney patients. The titanium dioxide (TiO2) nanoparticles were created using the photocell technique, and for characterization used XRD and TEM. The research population consisted of 60 individuals, both male and female, with renal disease and older than 40 years old who were on dialysis without taking any drugs. Two groups were created out of them (30 control group and 30 dialysis patients group). The two groups' serum was collected using a straightforward sampling approach. Creatinine and urea levels were measured for the control group, and for the dialysis group before the addition of TiO2-NPs; and also after the addition of TiO2-NPs. Furthermore, creatinine and urea concentrations were determined using a spectrophotometric method. The XRD investigations showed that titanium dioxide nanoparticles are crystalline and the size ranged from 11-29 nm, according to photographs taken using TEM. The present investigation showed that (TiO2-NPs) significantly lowered the levels of creatinine and urea in individuals with renal disease. Our findings demonstrated, for the first time, that TiO2 nanoparticles considerably declined the levels of creatinine and urea among dialysis patients. Future research should be done to confirm this affects TiO2-NPs.
摘要# x0D;纳米技术是一个新兴的领域,在过去的几十年里得到了惊人的兴趣。医学应用被认为是该领域最重要的目标之一。目的是评估(TiO2-NPs)对肾脏患者尿素和肌酐活性的生物学效应。利用光电池技术制备了二氧化钛纳米颗粒,并用XRD和TEM对其进行了表征。研究人群包括60名男性和女性,患有肾脏疾病,年龄在40岁以上,在不服用任何药物的情况下进行透析。将其分为两组(对照组和透析患者组各30人)。两组的血清采用直接抽样方法采集。对照组和透析组在加入TiO2-NPs前测定肌酐和尿素水平;在加入TiO2-NPs后也是如此。此外,用分光光度法测定肌酐和尿素浓度。XRD研究表明,二氧化钛纳米颗粒呈结晶状,尺寸在11 ~ 29 nm之间。目前的研究表明,(TiO2-NPs)可显著降低肾脏疾病患者的肌酐和尿素水平。我们的研究结果首次证明,TiO2纳米颗粒显著降低了透析患者的肌酐和尿素水平。未来的研究应该证实这对TiO2-NPs的影响。
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 Nanotechnology is an emerging field that has got a phenomenal interest in the last few decades. Medical application is considered one of the most important ambitions in this field. The objective was to evaluate the biological effects of (TiO2-NPs) on urea and creatinine activity among kidney patients. The titanium dioxide (TiO2) nanoparticles were created using the photocell technique, and for characterization used XRD and TEM. The research population consisted of 60 individuals, both male and female, with renal disease and older than 40 years old who were on dialysis without taking any drugs. Two groups were created out of them (30 control group and 30 dialysis patients group). The two groups' serum was collected using a straightforward sampling approach. Creatinine and urea levels were measured for the control group, and for the dialysis group before the addition of TiO2-NPs; and also after the addition of TiO2-NPs. Furthermore, creatinine and urea concentrations were determined using a spectrophotometric method. The XRD investigations showed that titanium dioxide nanoparticles are crystalline and the size ranged from 11-29 nm, according to photographs taken using TEM. The present investigation showed that (TiO2-NPs) significantly lowered the levels of creatinine and urea in individuals with renal disease. Our findings demonstrated, for the first time, that TiO2 nanoparticles considerably declined the levels of creatinine and urea among dialysis patients. Future research should be done to confirm this affects TiO2-NPs.","PeriodicalId":167115,"journal":{"name":"Wasit Journal of Pure sciences","volume":"55 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-09-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136342354","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Stabilization of Multi Fractional order Differential Equation with Delay time and Feedback Control 具有时滞和反馈控制的多分数阶微分方程的镇定
Pub Date : 2023-09-30 DOI: 10.31185/wjps.210
Badiea S, None Raheam A. Al-Saphoy, None Sameer Q. Hassan
In this paper, a new study is dealt and presented the nonlinear control system consists of nonlinear differential equations of fractional orders with a mixture of ordinary derivatives of the first and second order that are unstable before feedback gain, we will study this nonlinear control system after feedback gain and prove the local asymptotically stable of the system by using a set of conditions that illustrated the stability of these systems, the work was reinforced with application examples that were programmed to reach illustrations that show the stability of the systems offered with high efficiency and accuracy.
本文研究了一类在反馈增益前是不稳定的一阶和二阶常导数混合的分数阶非线性微分方程的非线性控制系统,我们将研究反馈增益后的非线性控制系统,并利用一组说明系统稳定性的条件证明系统的局部渐近稳定。通过应用实例对工作进行了加强,这些应用实例显示了系统的稳定性,并具有高效率和准确性。
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引用次数: 0
Preparation, Characterization and Adsorption Properties of Chitosan-Iron Nanocomposite 壳聚糖-铁纳米复合材料的制备、表征及吸附性能研究
Pub Date : 2023-09-30 DOI: 10.31185/wjps.209
Juman Naser
Magnetic iron oxide nanoparticles (Fe3O4NPs) were prepared using the co-precipitation technique successfully. The prepared nanoparticles were used to modify chitosan (CHT) to use the produced nanocomposite (CHT/ Fe3O4NPs) as an adsorbent surface for removing methyl green dye from its aqueous solution .Infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), X-ray dispersion spectroscopy (EDS), X-ray diffraction spectroscopy (XRD) and thermal gravimetric analysis (TGA) were used to characterize (Fe3O4NPs) and (CHT/ Fe3O4NPs). The system of adsorption was described by Langmuir, Freundlich and Temken models. The adsorbed dye capacity increases with increasing temperature which indicates to the endothermic nature of adsorption.
采用共沉淀法成功制备了磁性氧化铁纳米颗粒(Fe3O4NPs)。利用所制备的纳米颗粒对壳聚糖(CHT)进行修饰,制备的纳米复合材料(CHT/ Fe3O4NPs)作为吸附剂表面,用于去除水溶液中的甲基绿染料,并用红外光谱(FT-IR)、扫描电子显微镜(SEM)、x射线色散光谱(EDS)、x射线衍射光谱(XRD)和热重分析(TGA)对(Fe3O4NPs)和(CHT/ Fe3O4NPs)进行表征。吸附体系用Langmuir、Freundlich和Temken模型描述。染料吸附容量随温度的升高而增大,表明吸附的吸热性质。
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引用次数: 0
Applying Adomian Decomposition Method for solving the Covid-19 epidemic with Vaccine Adomian分解法在新型冠状病毒疫苗防控中的应用
Pub Date : 2023-09-30 DOI: 10.31185/wjps.202
Somaya Saad Faisal
Abstract— A pandemic Covid-19 is an epidemic that spreads over a big region, Crosse international borders, and often affects a lot of people. Only a few pandemics result in severe illness in a subset of people or in an entire community. The virus has mainly affects the elderly population. The virus, that causes Covid-19, has mainly been transmitted through droplet generate once an infected persons exhales, sneezes and coughs. These symptoms are too heavy; to hang in air, and quickly, fall on surface or floor. The COVID-19 pandemic model including the Vaccination Campaign is of natural phenomenon which can be represented as a system of differential equations for the first order; the mathematical models include a system of several second order nonlinear equations. We applied the Adomian decomposition methods to the mathematical models of Covid-19. The main advantage of this method is that it can be directly applied to all kinds of linear and nonlinear differential equations, homogeneous or nonhomogeneous, with constant or variable coefficients. The derivatives of all compartments of the coronavirus model are continuous at t ≥ 0. The solutions of the model are non-negativity. It indicates that the, infection, will be gradually the epidemic and disappear will, stop. If, R_0>1, the average of each affected individually. More than one person has infected, and the incidence of infection is in wrinkles. That means the epidemic, will not be end, while maintain the existence of the disease, the R_0=1 means that each infected patient results in an average infections.
摘要:新冠肺炎疫情是一场大范围、跨国界、影响人群的流行病。只有少数几次大流行导致一小部分人或整个社区出现严重疾病。该病毒主要影响老年人。导致Covid-19的病毒主要通过感染者呼气、打喷嚏和咳嗽时产生的飞沫传播。这些症状太严重了;悬在空中,然后迅速地落到地面或地板上。包括疫苗接种运动在内的COVID-19大流行模型是一种自然现象,可以表示为一阶微分方程系统;数学模型包括一个由多个二阶非线性方程组成的系统。我们将Adomian分解方法应用于新冠肺炎的数学模型。该方法的主要优点是可以直接应用于各种线性和非线性微分方程,无论是齐次的还是非齐次的,常系数的还是变系数的。冠状病毒模型各室室的导数在t≥0时连续。模型的解是非负性的。它表明,感染,将逐渐流行和消失,将停止。如果,R_0>1,表示每个受影响个体的平均值。不止一人感染,感染的发生率在皱纹。这意味着疫情不会结束,同时保持疾病的存在,R_0=1意味着每个感染患者导致的平均感染。
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引用次数: 0
The effect of phytoestrogen (lignan) on the levels of some hormo-nal parameters in white female rats induced osteoporosis 植物雌激素(木脂素)对骨质疏松大鼠一些激素参数的影响
Pub Date : 2023-09-30 DOI: 10.31185/wjps.180
Zainab Zaidan Al-Jubor, None Aseel Najah Sabour
The current study aimed to evaluate the effectiveness of the phytoestrogen (lignan) in some hormonal parameters of white female rats induced osteoporosis with Prednisolone. The present study included two main experiments, In the first experiment 50 adult white female rats were divided into two groups, The first group G1 was considered a control group and the second group, G2 was induced into osteoporosis by Prednisolone at a dose of 40 mg/kg of body weight For two months. The second main experiment divided the remaining animals (from the first group of the first experiment into three subgroups) and the remaining animals (from the second group of the first experiment into two subgroups): negative control group C was dosed with distilled water, group T1 was considered a positive control that was continued with Prednisolone at a dose of 40 mg/kg of body weight, group T2, was induced osteoporosis and administered the phytoestrogens(lignan) at a dose of 20 mg/kg, the healthy T3 group was administered the phytoestrogens(lignan) at a dose of 20 mg/kg, and the T4 group was administered the phytoestrogens(lignan) at a dose of 20 mg/kg. And Prednisolone at a dose of 40 mg/kg simultaneously for 30 days. After the end of the second experiment, the weights of the animals were recorded and then anesthetized with chloroform withdrawal blood samples from the heart directly for hormonal tests that represent estrogen, FSH, LH. The results showed a significant decrease (P<0.05) in each of the average estrogen, FSH, LH level in the T1 group (positive control) when comparing to the negative group. while the cause of the phytoestrogen(lignan) improved The hormonal parameters and showed a significant increase (P<0.05) in estrogen, FSH, LH level in T2,T3,T4groups when comparing to T1 (positive control). We conclude from the current study the effective and positive role shown by phytoestrogens(lignan) in improving and enhancing the hormonal parameters and reducing the negative effects of induced osteoporosis in white female rats.
本研究旨在评价植物雌激素(木脂素)对强的松龙诱导的白种雌性大鼠骨质疏松的一些激素参数的影响。本研究主要包括两个实验,第一个实验将50只成年雌性白种大鼠分为两组,第一组G1作为对照组,第二组G2以40 mg/kg体重的剂量泼尼松龙诱导骨质疏松2个月。第二次主实验将剩余动物(从第一次实验的第一组分为三个亚组)和剩余动物(从第一次实验的第二组分为两个亚组):-前控制C组和蒸馏水,T1组被认为是一个积极的控制与强的松的剂量持续40毫克/公斤的体重,T2,是植物雌激素诱导骨质疏松和管理(木酚素)的剂量20毫克/公斤,健康T3组管理植物雌激素(木酚素)的剂量20毫克/公斤,和T4组管理植物雌激素(木酚素)的剂量20毫克/公斤。同时给予强的松龙40mg /kg剂量,持续30天。在第二次实验结束后,记录动物的体重,然后用氯仿麻醉直接从心脏提取血液样本进行激素测试,代表雌激素,FSH, LH。结果显示,与阴性组相比,T1组(阳性对照)的平均雌激素、FSH、LH水平均显著降低(P<0.05)。而植物雌激素(木脂素)的原因改善了激素参数,T2、T3、t4组的雌激素、FSH、LH水平较T1组(阳性对照)显著升高(P<0.05)。本研究表明植物雌激素(木脂素)在改善和提高雌性白鼠的激素参数,减少骨质疏松的负面影响方面具有积极作用。
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引用次数: 0
Data Collected and Analysis of COVID-19 Infection Status: Case Study of Iraqi Hospital Patients in Diwaniyah and Najaf Governorates COVID-19感染状况数据收集与分析:以伊拉克迪瓦尼耶省和纳杰夫省医院患者为例
Pub Date : 2023-09-30 DOI: 10.31185/wjps.173
Haitham Abdulaaima, Ali Hasan Taresh
In recent years, the coronavirus (COVID-19) spread in a dangerous and rapidly. It first appeared in the Chinese city of Wuhan in early December 2019, causing many cases of infection and death because of the rapid spread of the virus throughout the world. The conversion of patient information from paper to electronic helps the medical staff and researchers analyze and retrieve information faster. In this paper, we gathered data about patients infected with COVID-19 who were registered in the Iraqi hospitals of two governorates (Diwaniyah and Najaf) from 2020 to 2023. In addition, we used machine learning algorithms that protect the infection of the data entered for the patient. The highest accuracy (average in both datasets od Diwaniyah and Najaf) ) are achieved by both the algorithms Nave Bayes (90%) and Decision tree (90%) , while the K nearest neighbor (89%), Random forest() and artificial neural network (84).
近年来,冠状病毒(COVID-19)以危险和迅速的方式传播。它于2019年12月初首次出现在中国武汉市,由于该病毒在全球的迅速传播,造成了许多感染和死亡病例。患者信息从纸质到电子的转换有助于医务人员和研究人员更快地分析和检索信息。在本文中,我们收集了2020年至2023年在伊拉克两个省(迪瓦尼耶和纳杰夫)医院登记的COVID-19感染患者的数据。此外,我们使用机器学习算法来保护患者输入的数据不受感染。最高的准确率(Diwaniyah和Najaf两个数据集的平均值)是由两种算法(90%)和决策树(90%)实现的,而K近邻(89%),随机森林()和人工神经网络(84)。
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引用次数: 0
Kinetic Study for Janus Green Dye Adsorption from Aqueous Solutions Using Iraqi Bauxite Clay and its Composite 伊拉克铝土矿粘土及其复合材料对黄绿色染料的吸附动力学研究
Pub Date : 2023-03-26 DOI: 10.31185/wjps.116
Abbas Jumaa Sahal, A. Mohammed Abbas
Clays are considered important natural materials in the field of water purification, including bauxite clay (BAU) and its prepared and activated composite (BAU/CMC-AC) with carboxymethyl cellulose polymer. The ad-sorbent surfaces are characterized by FTIR and XRD techniques. The adsorp-tion of green janus (JG) from an aqueous solution with bauxite and its compo-site were studied under the influence of different conditions of the weight and size of adsorbed surface particles, contact time and temperature. The results were found to be: contact time (90, 45) min for maximum quantity adsorbed of (JG) dye on bauxite and its composite respectively. The experimental data were tested on pseudo 1st- and 2nd-order kinetic models. It was shown to apply more with the pseudo-2nd order kinetic model for both adsorbents. It also showed that the highest removal percentage were (78%, 88.5 %) for the bauxite surface and its composite (BAU, BAU/CMC-AC) at the preferred temperature
粘土是水净化领域中重要的天然材料,包括铝土矿粘土(BAU)及其与羧甲基纤维素聚合物制备的活化复合材料(BAU/CMC-AC)。采用FTIR和XRD技术对吸附表面进行了表征。研究了铝土矿及其复合材料在吸附表面颗粒的重量、大小、接触时间和温度等不同条件下对水溶液中绿毒的吸附性能。结果表明:(JG)染料在铝土矿及其复合材料上的最大吸附时间分别为(90,45)min。在拟一级和二级动力学模型上对实验数据进行了验证。结果表明,准二级动力学模型对两种吸附剂都更适用。在优选温度下,铝土矿表面及其复合材料(BAU、BAU/CMC-AC)的去除率分别为78%、88.5%
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引用次数: 0
Continuum Model on (HYTXW) of Fungal Growth 真菌生长的连续统模型(HYTXW
Pub Date : 2023-03-26 DOI: 10.31185/wjps.104
Nabaa Naeem Ghareeb, A. Shuaa
In general the growth of fungi needs to be resolved until its goal becomes a correction and thus, we minimize cost, effort, time and money. There-fore, we arrived at a mathematical solution using some techniques. In this paper, we studied its growth behavior and the effect of each branch on the fungus, then we combined a number of branches represented as mathematical model as partial differential equations (PDEs), approximate numerical solutions, and some math-ematical steps, such as non-dimensionalisation, finding stability or steady state and representing it on phase plane, we found approximate results for these types using MATLAB’s codes such as Pplane8 and Pdepe [1,7].
一般来说,真菌的生长需要解决,直到它的目标成为一个纠正,因此,我们最大限度地减少成本,精力,时间和金钱。因此,我们使用一些技术得出了一个数学解决方案。在本文中,我们研究了它的生长行为和每个分支对真菌的影响,然后我们结合了一些分支的数学模型,如偏微分方程(PDEs),近似数值解,以及一些数学步骤,如无量纲化,寻找稳定或稳态并在相平面上表示,我们使用MATLAB的代码如Pplane8和Pdepe[1,7]找到了这些类型的近似结果。
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引用次数: 0
γpg**- Closed Set in Topological Spaces γpg**-拓扑空间中的闭集
Pub Date : 2023-03-26 DOI: 10.31185/wjps.86
Ahmed Hussein Wajan Alrikabiu, Ali Khalaf Hussain
Abstract In this paper we investigate the definitions of g-closed sets, gp-closed sets, pg-closed sets, gsp-closed sets, g -closed sets, g-closed sets. we  introduced a new class of set called γpg**-closed sets which is settled properly in between the class of semi-closed and the class of g**-closed sets .  
摘要研究了g-闭集、gp-闭集、pg-闭集、gp-闭集、g-闭集、g-闭集的定义。在半闭集和g**闭集之间,引入了一类新的集γpg**-闭集。
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引用次数: 0
期刊
Wasit Journal of Pure sciences
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