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Processing and Functional Evaluation of Titanium Thin Films for Biomimetic Micro Actuator 仿生微驱动器用钛薄膜的制备及功能评价
T. Sakai, Sodai Hoshiai, E. Nakamachi
Titanium (Ti) thin films were created on glass and Pb(Zr, Ti)O3 (PZT) substrates using magnetic RF sputtering apparatus. Nano-indentation tests were carried out to study the influence of the Ti thin layer on piezoelectric properties. The piezoelectric properties of the PZT plate and a Ti sputtered one were also measured by laser Doppler vibrometer. Furthermore, some characteristics, such as crystalline structure, depth profiles, and surface roughness of the films were observed by means of an atomic force microscope (AFM). Main conclusions obtained in this study are summarized as follows: (1) From detailed observation and analytical results of AFM, the surface roughness, Ra, tends to increase as Ti film thickness increases. (2) Some of the mechanical properties, such as reduced modulus Er and hardness H obtained from nano-indentation tests, are significantly related to film thickness. (3) The validity of piezoelectric finite element analysis (ANASYS program) for deformation of a piezoelectric material was investigated. As a result, piezoelectric response properties are present in as-received PZT specimens and Ti-sputtered PZT specimens. Experimental and FE analytical results indicate that the piezoelectric coefficient is significantly influenced by Ti layer.
采用射频磁溅射装置在玻璃和Pb(Zr, Ti)O3 (PZT)衬底上制备了钛(Ti)薄膜。采用纳米压痕试验研究了Ti薄层对压电性能的影响。用激光多普勒振动仪测量了PZT板和Ti溅射板的压电性能。此外,利用原子力显微镜(AFM)观察了薄膜的晶体结构、深度分布和表面粗糙度等特征。本研究的主要结论总结如下:(1)从AFM的详细观察和分析结果来看,表面粗糙度Ra随Ti膜厚度的增加而增加。(2)纳米压痕试验获得的一些力学性能,如降低模量Er和硬度H,与薄膜厚度显著相关。(3)研究了压电有限元分析(ansys程序)对压电材料变形的有效性。结果表明,接收态PZT试样和ti溅射态PZT试样均具有压电响应特性。实验和有限元分析结果表明,Ti层对压电系数有显著影响。
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引用次数: 1
Reproduction of FRP Blade Failure for Wind Power Generators by Lightning and its Mechanism 风力发电机玻璃钢叶片遭雷击破坏的再现及其机理
H. Sakamoto, M. Hanai
In Japan, lightning damage to FRP blades for wind power generators is increasing, together with the increase in wind power generator installation in recent years. Lightning damage is a big issue in Japan since lightning in Japan seems to be severer than in Europe and the US. In Kochi, Shikoku, Japan, six 600-750kW grade generators have been installed, and some of them have been damaged by lightning several times. In order to solve this issue, the Kochi University of Technology received a research request of lightning protection, sponsored by the Kochi prefecture in 2002. After surveying the literature and questioning related organizations such as NREL (National Renewable Energy Laboratories) and Toray USA, experiments to reproduce lightning damage to FRP specimens were planned. The specimens prepared for this research are 1/2 size models and a 2/4 part of the full size blade. In the previous experiment, flat plate specimens of 450mm width × 2.5m length × 4mm thickness were used, and the experiments produced the damage by lightning. However, the damages were not exactly the same as the ones in the actual field. Therefore, this experiment aims to reproduce the blade failure in the actual field and to clarify the failure mechanism, using the 1/2 size blade model and full size blade specimens. The experiments were conducted mainly in the Toshiba Hamakawasaki High Voltage High Power Testing Laboratory as was made in the previous experiments. This Testing Laboratory is one of the biggest test laboratory for experiments involving high electric voltage and large current. The results showed the reproduction of the failed blades in fields, and clarified the failure mechanism.
在日本,随着近年来风力发电机安装量的增加,风力发电机玻璃钢叶片的雷击损坏正在增加。雷电灾害在日本是一个大问题,因为日本的雷电似乎比欧洲和美国更严重。在日本四国高知市,已经安装了6台600-750kW级发电机,其中一些发电机被雷击多次损坏。为了解决这个问题,高知工业大学在2002年收到了由高知县赞助的防雷研究请求。在调查了文献并询问了相关组织,如NREL(国家可再生能源实验室)和Toray USA,计划了重现FRP试件雷击损伤的实验。为本研究准备的标本是1/2尺寸模型和2/4全尺寸叶片的一部分。在之前的实验中,采用的是450mm宽× 2.5m长× 4mm厚的平板试件,实验中产生的是雷击损伤。然而,这些损害与实际现场的损害并不完全相同。因此,本实验旨在利用1/2尺寸叶片模型和全尺寸叶片试件,在实际现场再现叶片的破坏过程,阐明其破坏机理。实验主要是在东芝滨川高压大功率测试实验室进行的,和之前的实验一样。本实验室是国内最大的高电压大电流实验实验室之一。研究结果显示了失效叶片在野外的再现,并阐明了失效机理。
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引用次数: 12
Stress and Strain Behaviors of Mg Alloy AZ31 in Plane Strain Compression AZ31镁合金平面应变压缩应力应变行为
Ikuo Yarita, T. Naoi, T. Hashizume
Most of magnesium alloy products are manufactured by die casting or thixo-molding processes. However, there is extremely little use of the products by metal forming due to high resisting plastic deformation in normal temperature and their expensive cost. In this study, to make clear the plastic deformability, stress and strain behaviors of Mg alloy AZ31 hot rolled sheet in plane strain compression in the temperature from 20 ◦ C to 250 ◦ C have been discussed. Tension test and plane strain compression test have been performed to obtain the equivalent stress and equivalent plastic strain relations. The plane strain compression tests with some lubricants have been performed, and the e ff ect of friction between die and deforming material on plastic deformation behaviors has been investigated by the elastic-plastic finite element analysis. Optical microstructures of deformed materials are also observed.
大多数镁合金产品是通过压铸或触敏成型工艺制造的。然而,由于其在常温下具有较高的抗塑性变形能力和昂贵的成本,金属成形的应用很少。为明确镁合金AZ31热轧薄板在20 ~ 250℃平面应变压缩条件下的塑性变形性能和应力应变行为。进行了拉伸试验和平面应变压缩试验,得到了等效应力和等效塑性应变关系。采用弹塑性有限元分析方法,研究了模具与变形材料之间的摩擦对塑性变形行为的影响。变形材料的光学显微结构也被观察到。
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引用次数: 3
Cleaning Effect of Interlayer Metal on the Joining Surface during Braze Pressure Welding 钎焊压力焊中连接面夹层金属的清洗效果
Yohei Inagaki, A. Suzumura, T. Ikeshoji, T. Yamazaki
Braze Pressure Welding (BPW) with high frequency induction heating is a newly developed pressure welding technique using interlayer metals for welding the general steel pipes for pipe arrangement in buildings. BPW enables to make joints by solid-state welding in air with relatively small deformation. In this method, the interlayer metal is expected to play the primary role in making high performance joints. It removes contaminations from the joining surface of the base metal and forms fillets at the gaps around the joint. It had been revealed by some experiments and/or numerical analyses in previous research that the BPW joint had higher tensile strength than the brazed joint, and that the fillet can improve the joint strength. In this study, in order to investigate the cleaning effect of interlayer metal more closely, a low carbon steel plate specimen was brazed mainly by Ni-based brazing filler using a tungsten spacer. The microscopy and EPMA analysis on the joints made by various brazing temperatures and durations confirmed that the oxide films on the joining surfaces were removed and discharged from the joining region by the interlayer metal.
高频感应加热钎焊压力焊是一种新兴的利用层间金属焊接建筑管道布置用普通钢管的压力焊技术。BPW可以在空气中以相对较小的变形进行固态焊接。在这种方法中,层间金属有望在制造高性能接头中发挥主要作用。它可以去除母材连接表面的污染物,并在连接周围的间隙处形成圆角。以往的一些实验和数值分析表明,钎焊接头具有比钎焊接头更高的抗拉强度,而圆角可以提高接头的抗拉强度。为了更深入地研究层间金属的清洗效果,本研究主要采用镍基钎料和钨垫片钎焊低碳钢试样。对不同钎焊温度和时间下的接头进行了显微分析和EPMA分析,证实了连接表面的氧化膜被层间金属从连接区域移除并排出。
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引用次数: 2
Bias in the Weibull Strength Estimation of a SiC Fiber for the Small Gauge Length Case 小规长情况下SiC纤维威布尔强度估计中的偏差
T. Morimoto, S. Nakagawa, S. Ogihara
It is known that the single-modal Weibull model describes well the size effect of brittle fiber tensile strength. However, some ceramic fibers have been reported that single-modal Weibull model provided biased estimation on the gauge length dependence. A hypothesis on the bias is that the density of critical defects is very small, thus, fracture probability of small gauge length samples distributes in discrete manner, which makes the Weibull parameters dependent on the gauge length. Tyranno ZMI Si-Zr-C-O fiber has been selected as an example fiber. The tensile tests have been done on several gauge lengths. The derived Weibull parameters have shown a dependence on the gauge length. Fracture surfaces were observed with SEM. Then we classified the fracture surfaces into the characteristic fracture patterns. Percentage of each fracture pattern was found dependent on the gauge length, too. This may be an important factor of the Weibull parameter dependence on the gauge length.
单模态威布尔模型很好地描述了脆性纤维抗拉强度的尺寸效应。然而,一些陶瓷纤维的单模态Weibull模型对规长依赖性的估计存在偏差。关于偏差的一个假设是,临界缺陷的密度非常小,因此小规长样品的断裂概率呈离散分布,这使得威布尔参数依赖于规长。以Tyranno ZMI Si-Zr-C-O光纤为例。拉伸试验已在几种规格长度上完成。推导出的威布尔参数与规范长度有关。用扫描电镜观察断口形貌。然后将断裂面划分为特征断裂模式。每种裂缝类型的百分比也与测量长度有关。这可能是威布尔参数依赖于量规长度的一个重要因素。
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引用次数: 14
Solubility and Dissolution Rate of Ni Base Alloy to Molten Ag-Cu-Pd Brazing Filler 镍基合金在熔银铜钯钎料中的溶解度和溶解速率
T. Ikeshoji, Y. Watanabe, A. Suzumura, T. Yamazaki
During the brazing process of the rocket engine’s nozzle skirt assembly made from Fe-Ni based super alloy pipes with Pd based brazing filler, the erosion corrosion pits were sometimes engraved on those pipes’ surface. The corrosion is considered to be assisted by the dynamic flow of the molten brazing filler. In order to estimate the amount of erosion corrosion and to prevent it, the solubility and the dissolution rate of Ni to the molten Ag-Cu-Pd brazing filler are measured experimentally. The Ni crucible poured with the Ag-Cu-Pd brazing filler was heated up to 1320K and quenched after the various keeping time. The microstructure of the solidified brazing filler part’s cross sections was observed, and the amount of the dissolved Ni was estimated using the image processing technique. The solubility was about 5.53mass%and the initial dissolution rate was 6.28 × 10-3mass%/s. Using these data, more elaborate dynamic flow simulation will be able to conduct.
在用Pd基钎料钎焊铁镍基高温合金管对火箭发动机喷嘴裙架总成进行钎焊过程中,有时会在管表面刻下侵蚀腐蚀坑。腐蚀被认为是由熔融钎焊填料的动态流动辅助的。为了估计侵蚀腐蚀的程度和防止侵蚀腐蚀,实验测量了Ni在钎料熔液中的溶解度和溶解速率。将加入Ag-Cu-Pd钎料的Ni坩埚加热至1320K,经过不同保温时间后进行淬火。利用图像处理技术对钎焊填料凝固后截面的显微组织进行了观察,并估算了Ni的溶解量。溶解度约为5.53mass%,初始溶出速率为6.28 × 10-3mass%/s。利用这些数据,将能够进行更精细的动态流动模拟。
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引用次数: 3
Improvement of Interfacial Adhesion in Bamboo Polymer Composite Enhanced with Micro-Fibrillated Cellulose 微纤化纤维素增强竹高分子复合材料界面附着力的研究
K. Okubo, T. Fujii, N. Yamashita
Current study presents one of effective techniques to improve mechanical properties of PLA (Poly-Lactic Acid)-based bamboo fiber composite. Commercially available Micro-Fibrillated Cellulose (MFC) obtained from wood pulp was applied as an enhancer to the composite. The bamboo fibers were extracted by steam explosion method and they were also rubbed in water to remove xylem (soft-wall cells). The liquid-based MFC, PLA and the bamboo fiber were mixed in water for several minutes and they were filtrated under vacuum pressure. To fabricate the composite, remained sheets were then hot pressed after dry. Three-point bending strength and Mode I fracture toughness of the composite were significantly improved, even when 10% of the MFC was added into the PLA/BF composite in weight. If small amount of MFC added into the bamboo fiber composite, tangled MFC fibers prevented the growth of micro crack along the interface between bamboo fiber and matrix.
目前研究提出了一种改善聚乳酸基竹纤维复合材料力学性能的有效方法。从木浆中提取的市售微纤化纤维素(MFC)被用作复合材料的增强剂。采用蒸汽爆破法提取竹纤维,并在水中摩擦去除木质部(软壁细胞)。将液体基MFC、PLA和竹纤维在水中混合几分钟,在真空压力下进行过滤。为了制造复合材料,剩下的薄片在干燥后被热压。即使在PLA/BF复合材料中添加10%的MFC,复合材料的三点抗弯强度和I型断裂韧性也有显著提高。如果在竹纤维复合材料中加入少量的MFC,缠绕的MFC纤维会阻止竹纤维与基体界面上微裂纹的生长。
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引用次数: 121
3-Dimensional Analysis of Deformation of Disk Wheels and Transverse Force of Wheel Bolts 盘式车轮变形及车轮螺栓横向力的三维分析
T. Kagiwada, H. Harada
Loosening of the wheel nuts, which fix the disk wheels of automobiles to the wheel hub, may be the cause of accidents where the wheel falls off while the automobile is running. When the transverse force of wheel bolts exceeds a certain proportion of the bolt shaft force, the wheel nut begins to loosen. Further, the force on the bolt shaft may also be influenced by the loads acting to the wheel through the moment caused by the offset of the wheel. This study determined the 3-dimensional deformation of the disk wheels and the transverse forces on the wheel bolt by 3-dimensional numerical analysis. The results established that the transverse force was influenced by the bolt shaft force caused by the bolt fastening and was superposed on that due to the load, and that it fluctuated greatly during the revolution of the wheel. This phenomenon may be a large factor in the loosening of wheel nuts.
将汽车盘式车轮固定在轮毂上的车轮螺母松动,可能是汽车行驶中车轮脱落事故的原因。当车轮螺栓的横向力超过螺栓轴力的一定比例时,车轮螺母开始松动。此外,螺栓轴上的力也可能受到通过车轮偏置引起的力矩作用于车轮的载荷的影响。通过三维数值分析,确定了盘形轮的三维变形和轮螺栓的横向受力。结果表明:横向力受螺栓紧固产生的螺栓轴力的影响,并叠加在载荷作用下的横向力上,且横向力在车轮旋转过程中波动较大。这种现象可能是车轮螺母松动的一个很大的因素。
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引用次数: 0
Transient Creep Behavior of a Plain Woven SiC Fiber/SiC Matrix Composite 平纹编织SiC纤维/SiC基复合材料的瞬态蠕变行为
Takayuki Bessho, T. Ogasawara, T. Aoki, T. Ishikawa, Y. Ochi
The present work investigates the transient creep behavior of a plain woven Tyranno™ Lox-M (Si-Ti-C-O) fiber/SiC matrix composite at 1473K in air. Tensile creep tests were carried out under a constant load between 80 and 160MPa. A creep strain rate is generally represented by e∝ σn with a constant stress exponent, however the stress exponent decreased with time for this composite material. Monotonic tensile tests were also conducted for loading rates of 0.03, 0.3, and 3kN/min in order to investigate the effect of creep strain on tensile stress/strain behavior. Based on the empirical transient creep equation and creep-hardening model, stress/strain curves under monotonic tensile loading were predicted. A good correlation was obtained between the predicted and measured composite stress/strain curves using strain-hardening model.
本文研究了Tyranno™Lox-M (Si-Ti-C-O)纤维/SiC基复合材料在1473K空气中的瞬态蠕变行为。拉伸蠕变试验在80 ~ 160MPa恒定载荷下进行。蠕变应变率一般用e∝σn表示,应力指数恒定,但该复合材料的应力指数随时间而减小。为研究蠕变应变对拉伸应力/应变行为的影响,在0.03、0.3和3kN/min加载速率下进行了单调拉伸试验。基于经验瞬态蠕变方程和蠕变硬化模型,预测了单调拉伸载荷下的应力应变曲线。采用应变硬化模型对复合材料的应力应变曲线进行了预测,得到了较好的相关性。
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引用次数: 4
Effect of Microstructure on Fatigue Strength of Bovine Compact Bones 显微组织对牛致密骨疲劳强度的影响
Jong Heon Kim, M. Niinomi, T. Akahori, Junji Takeda, H. Toda
Despite its clinical importance in developing artificial bone, limited information is available regarding the microstructure with respect to the fatigue characteristics of bones. In this study, the fatigue characteristics of the bovine humerus and femur were investigated with respect to microstructures. Fatigue tests were conducted on the bovine humerus and femur at a stress ratio of 0.1 and a frequency of 10Hz. The fatigue strength of the plexiform bone is slightly greater than that of the haversian bone. This is because the volume fraction of voids in the haversian bone, which is the site of stress concentration, is higher than that of voids in the plexiform bone. Several microcracks are observed on the fatigue fracture surface of the haversian bone. The microcracks are short and their propagation directions are random. However, the number of the microcracks in the plexiform bone is very small. The microcracks are relatively long and their propagation directions are parallel to the longitudinal direction of the lamellar bone. Therefore, the crack requires relatively more energy to propagate across the lamella in the plexiform bone.
尽管人工骨在临床上具有重要意义,但有关骨骼疲劳特征的微观结构的信息有限。在这项研究中,疲劳特性的牛肱骨和股骨进行了研究,关于微观结构。对牛肱骨和股骨进行疲劳试验,应力比为0.1,频率为10Hz。丛状骨的疲劳强度略大于哈弗氏骨。这是因为哈弗氏骨(应力集中的部位)中空洞的体积分数高于丛状骨中的空洞。在哈氏骨的疲劳断口上观察到几个微裂纹。微裂纹长度短,扩展方向随机。然而,丛状骨的微裂纹数量很少。微裂纹较长,其扩展方向平行于板层骨的纵向。因此,在丛状骨中,裂纹需要相对较多的能量才能在骨板间传播。
{"title":"Effect of Microstructure on Fatigue Strength of Bovine Compact Bones","authors":"Jong Heon Kim, M. Niinomi, T. Akahori, Junji Takeda, H. Toda","doi":"10.1299/JSMEA.48.472","DOIUrl":"https://doi.org/10.1299/JSMEA.48.472","url":null,"abstract":"Despite its clinical importance in developing artificial bone, limited information is available regarding the microstructure with respect to the fatigue characteristics of bones. In this study, the fatigue characteristics of the bovine humerus and femur were investigated with respect to microstructures. Fatigue tests were conducted on the bovine humerus and femur at a stress ratio of 0.1 and a frequency of 10Hz. The fatigue strength of the plexiform bone is slightly greater than that of the haversian bone. This is because the volume fraction of voids in the haversian bone, which is the site of stress concentration, is higher than that of voids in the plexiform bone. Several microcracks are observed on the fatigue fracture surface of the haversian bone. The microcracks are short and their propagation directions are random. However, the number of the microcracks in the plexiform bone is very small. The microcracks are relatively long and their propagation directions are parallel to the longitudinal direction of the lamellar bone. Therefore, the crack requires relatively more energy to propagate across the lamella in the plexiform bone.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"42 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2005-10-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"121154396","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 17
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Jsme International Journal Series A-solid Mechanics and Material Engineering
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