首页 > 最新文献

Jsme International Journal Series A-solid Mechanics and Material Engineering最新文献

英文 中文
Improving Joint Properties of Friction Welded Joint of High Tensile Steel 提高高强度钢摩擦焊接接头接头性能
M. Kimura, M. Kusaka, K. Seo, A. Fuji
This report describes the improvements in the joint properties of friction welded joint of 780MPa class high tensile steel. Welded joint made by a continuous drive friction welding machine, the conventional method, had not obtained 100% joint efficiency despite applying forge pressure. This was due to the softening of the welded interface zone for heat input during braking times. Therefore, we developed a continuous drive friction welding machine with an electromagnetic clutch to prevent heat input during braking time. We proposed the process as “The Low Heat Input Friction Welding Method (the LHI method).” In this case, the joint had the same tensile strength as the base metal at friction time when the friction torque reached the initial peak torque. That is, the welded joint obtained 100% joint efficiency by using only the friction stage up to the initial peak torque without the forge (upsetting) stage, despite the existence of a slightly softened region adjacent to the welded interface. Furthermore, the softened region was hardly generated when this joint was made by applying forge pressure at the initial peak torque. In conclusion, a welded joint of high tensile steel made by only the friction stage of the LHI method had excellent joint properties. The LHI method has a lot of advantages for joining such materials as super fine grain steel with which conventional fusion welding processes have difficulty.
本文介绍了780MPa级高强钢摩擦焊接接头接头性能的改善。传统的连续驱动摩擦焊机焊接接头在施加锻造压力的情况下,焊接效率仍不能达到100%。这是由于焊接界面区软化的热量输入在制动时间。因此,我们开发了一种带电磁离合器的连续驱动摩擦焊机,以防止制动时的热量输入。我们提出的工艺为“低热输入摩擦焊接法(LHI方法)”。在这种情况下,当摩擦力矩达到初始峰值力矩时,接头的抗拉强度与母材相同。也就是说,尽管焊接界面附近存在一个略微软化的区域,但仅使用摩擦阶段(直至初始峰值扭矩)而不使用锻造(镦粗)阶段,焊接接头获得了100%的接头效率。在初始峰值扭矩下施加锻造压力时,该接头几乎不会产生软化区。综上所述,仅通过LHI方法的摩擦阶段制成的高强度钢焊接接头具有优异的接头性能。对于超细晶粒钢等传统熔焊工艺难以连接的材料,LHI方法具有许多优点。
{"title":"Improving Joint Properties of Friction Welded Joint of High Tensile Steel","authors":"M. Kimura, M. Kusaka, K. Seo, A. Fuji","doi":"10.1299/JSMEA.48.399","DOIUrl":"https://doi.org/10.1299/JSMEA.48.399","url":null,"abstract":"This report describes the improvements in the joint properties of friction welded joint of 780MPa class high tensile steel. Welded joint made by a continuous drive friction welding machine, the conventional method, had not obtained 100% joint efficiency despite applying forge pressure. This was due to the softening of the welded interface zone for heat input during braking times. Therefore, we developed a continuous drive friction welding machine with an electromagnetic clutch to prevent heat input during braking time. We proposed the process as “The Low Heat Input Friction Welding Method (the LHI method).” In this case, the joint had the same tensile strength as the base metal at friction time when the friction torque reached the initial peak torque. That is, the welded joint obtained 100% joint efficiency by using only the friction stage up to the initial peak torque without the forge (upsetting) stage, despite the existence of a slightly softened region adjacent to the welded interface. Furthermore, the softened region was hardly generated when this joint was made by applying forge pressure at the initial peak torque. In conclusion, a welded joint of high tensile steel made by only the friction stage of the LHI method had excellent joint properties. The LHI method has a lot of advantages for joining such materials as super fine grain steel with which conventional fusion welding processes have difficulty.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2005-10-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"129163812","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 19
Tensile Straightening of Superfine Wire and Residual Stress Measurement Using Focused Ion Beam 超细丝拉伸矫直及聚焦离子束残余应力测量
Tsutomu Yamashita, Kazunari Yoshida
The general method of reducing curving or bending for midsize wires or sheets is straightening using rollers and / or levelers. For superfine wires, similarly, high straightness is needed. However, it is very di ffi cult to deal with superfine wires due to their fineness and low tensile strength. In our study, warm tensile straightening processes for superfine gold wire, which is widely used as bonding material between leads and IC chips in semiconductors, were examined. Furthermore, finite element analyses of drawing and tensile straightening of superfine wires were carried out. The correlation between straightness and axial residual stress, which was calculated using the curve width when half of the wire was removed by sputtering with a focused ion beam (FIB), was studied. As a result of our studies, the improvement of straightness by tensile straightening of superfine gold wire was demonstrated, and the relationship between axial residual stress and straightness of wires was clarified.
一般的方法减少弯曲或弯曲为中等大小的电线或板是矫直使用辊和/或矫直机。对于超细线材,同样需要高直线度。然而,由于超细丝的细度和低抗拉强度,处理超细丝非常困难。在我们的研究中,研究了在半导体中广泛用作引线和IC芯片之间的粘合材料的超细金线的热拉伸矫直工艺。在此基础上,对超细丝的拉拔和拉伸矫直进行了有限元分析。利用聚焦离子束溅射去除一半金属丝时的曲线宽度计算了金属丝直线度与轴向残余应力之间的关系。研究结果表明,拉伸矫直可以提高超细金丝的直线度,并阐明了轴向残余应力与金属丝直线度的关系。
{"title":"Tensile Straightening of Superfine Wire and Residual Stress Measurement Using Focused Ion Beam","authors":"Tsutomu Yamashita, Kazunari Yoshida","doi":"10.1299/JSMEA.48.322","DOIUrl":"https://doi.org/10.1299/JSMEA.48.322","url":null,"abstract":"The general method of reducing curving or bending for midsize wires or sheets is straightening using rollers and / or levelers. For superfine wires, similarly, high straightness is needed. However, it is very di ffi cult to deal with superfine wires due to their fineness and low tensile strength. In our study, warm tensile straightening processes for superfine gold wire, which is widely used as bonding material between leads and IC chips in semiconductors, were examined. Furthermore, finite element analyses of drawing and tensile straightening of superfine wires were carried out. The correlation between straightness and axial residual stress, which was calculated using the curve width when half of the wire was removed by sputtering with a focused ion beam (FIB), was studied. As a result of our studies, the improvement of straightness by tensile straightening of superfine gold wire was demonstrated, and the relationship between axial residual stress and straightness of wires was clarified.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"17 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2005-10-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"130326069","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
Consolidation at Low Heat in Mechanically Alloyed Ti-Al Powders 机械合金钛铝粉末的低温固结
T. Okabe, T. Kanameda
Mechanical alloying (MA) of Ti-48mol%Al powder mixtures was performed for relatively short milling times (10.8-86.4ks) by planetary ball mill. The MA powders were hot-pressed at relatively low temperatures (673-873K) and pressures (200-600MPa). The influence of hot press temperature and pressure on consolidation (densification, reactive synthesis, etc.) in the MA powders was investigated. In this experiment, some non-reactive Ti powders remained in the consolidated materials, but the optimum hot press conditions for consolidation by reactive sintering were determined by the MA conditions (milling duration, etc.). Subsequently, the hot-pressed specimens were tested for hot-working by compressive creep testing at 1273K and initial pressure of 50MPa. The hot workability was excellent for superplasticity-like deformation. The densification and alloying did not alter the ultra-fine grain size, and the highest density and greatest change in density by hot-working was obtained by the powders milled for longest time.
采用行星球磨机对Ti-48mol%Al粉末混合物进行机械合金化(MA),研磨时间较短(10.8 ~ 86.4ks)。在相对较低的温度(673-873K)和压力(200-600MPa)下热压MA粉末。研究了热压温度和压力对MA粉末固结(致密化、反应合成等)的影响。在本实验中,固结材料中保留了一些非活性Ti粉,但反应烧结固结的最佳热压条件由MA条件(磨矿时间等)决定。随后,热压试样在1273K、50MPa初始压力下进行热加工压缩蠕变试验。对于类超塑性变形,热加工性能优异。致密化和合金化没有改变粉末的超细晶粒尺寸,而热加工粉末的密度最高,密度变化最大的是被磨时间最长的粉末。
{"title":"Consolidation at Low Heat in Mechanically Alloyed Ti-Al Powders","authors":"T. Okabe, T. Kanameda","doi":"10.1299/JSMEA.48.364","DOIUrl":"https://doi.org/10.1299/JSMEA.48.364","url":null,"abstract":"Mechanical alloying (MA) of Ti-48mol%Al powder mixtures was performed for relatively short milling times (10.8-86.4ks) by planetary ball mill. The MA powders were hot-pressed at relatively low temperatures (673-873K) and pressures (200-600MPa). The influence of hot press temperature and pressure on consolidation (densification, reactive synthesis, etc.) in the MA powders was investigated. In this experiment, some non-reactive Ti powders remained in the consolidated materials, but the optimum hot press conditions for consolidation by reactive sintering were determined by the MA conditions (milling duration, etc.). Subsequently, the hot-pressed specimens were tested for hot-working by compressive creep testing at 1273K and initial pressure of 50MPa. The hot workability was excellent for superplasticity-like deformation. The densification and alloying did not alter the ultra-fine grain size, and the highest density and greatest change in density by hot-working was obtained by the powders milled for longest time.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"6 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2005-10-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"126141512","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Micro-Impact Damage Caused by Mercury Bubble Collapse 汞泡破裂引起的微冲击损伤
M. Futakawa, T. Naoe, H. Kogawa, H. Date, Y. Ikeda
High-power spallation targets for neutron sources are being developed in the world. Mercury target will be installed at the material science and life facility in J-PARC, which will promote innovative science. The mercury target will be subjected to the pressure wave caused by proton bombarding in the mercury. The pressure wave propagation induces the cavitation in mercury that imposes localized impact damage on the target vessel. The impact erosion is a critical issue to decide the lifetime of target. An electromagnetic impact testing machine, MIMTM, was developed to reproduce the localized impact erosion damage and evaluate the damage formation. Additionally, droplet impact analyses were carried out to investigate the correlation between isolate pit profile and micro-jet velocity. We confirmed that the value of depth/radius was applicable to estimate micro-jet velocity, and the velocity at 560W in MIMTM equivalent to 1MW proton beam injection was ∼ 102m/s approximately.
高功率中子源散裂靶正在世界范围内不断发展。水银靶将安装在J-PARC的材料科学与生命设施,这将促进创新科学。汞靶会受到汞中质子轰击产生的压力波。压力波的传播引起汞的空化,对靶血管造成局部冲击损伤。冲击侵蚀是决定目标寿命的关键问题。研制了电磁冲击试验机MIMTM,用于再现局部冲击侵蚀损伤并评估损伤形成。此外,还进行了液滴冲击分析,研究了孤立坑廓形与微射流速度的关系。我们证实了深度/半径值适用于估算微射流速度,在560W的MIMTM中,相当于1MW质子束注入的速度约为~ 102m/s。
{"title":"Micro-Impact Damage Caused by Mercury Bubble Collapse","authors":"M. Futakawa, T. Naoe, H. Kogawa, H. Date, Y. Ikeda","doi":"10.1299/JSMEA.48.234","DOIUrl":"https://doi.org/10.1299/JSMEA.48.234","url":null,"abstract":"High-power spallation targets for neutron sources are being developed in the world. Mercury target will be installed at the material science and life facility in J-PARC, which will promote innovative science. The mercury target will be subjected to the pressure wave caused by proton bombarding in the mercury. The pressure wave propagation induces the cavitation in mercury that imposes localized impact damage on the target vessel. The impact erosion is a critical issue to decide the lifetime of target. An electromagnetic impact testing machine, MIMTM, was developed to reproduce the localized impact erosion damage and evaluate the damage formation. Additionally, droplet impact analyses were carried out to investigate the correlation between isolate pit profile and micro-jet velocity. We confirmed that the value of depth/radius was applicable to estimate micro-jet velocity, and the velocity at 560W in MIMTM equivalent to 1MW proton beam injection was ∼ 102m/s approximately.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2005-10-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"132328645","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 8
Application of DLC Coating to Ironing Die DLC涂层在熨烫模上的应用
K. Dohda, H. Kubota, Y. Tsuchiya
The possibilities of application of DLC-Si coating to the die in dry ironing process have been investigated by strip-ironing type tribometer. Alloy tool steel and high speed steel were used as substrate material for ironing dies. Two types of substrate surface texture were prepared by lapping and grinding. And two types of die edge angle were prepared. High tensile strength steel and brass were tested as workpieces. The surface appearance of die, friction coefficient during ironing and surface roughness of ironed workpiece were measured. The friction coefficient of DLC-Si coated die in the dry ironing process is relatively low. Galling does not occur on the die surface. In case of high tensile strength steel, the damage grows with the number of tests. The surface roughness of a brass workpiece does not increase with repeat ironing. The DLC-Si coating could be applied to the dry ironing process in this investigated condition.
用带式摩擦计研究了干式熨烫过程中DLC-Si涂层在模具上应用的可能性。采用合金工具钢和高速钢作为熨烫模具的基材。通过研磨和研磨制备了两种基体表面织构。并制备了两种类型的模具边缘角。对高抗拉强度钢和黄铜作为工件进行了试验。对模具表面形貌、熨烫过程中的摩擦系数和熨烫后工件的表面粗糙度进行了测量。DLC-Si涂层模具在干烫过程中的摩擦系数相对较低。模具表面不会发生磨损。对于高抗拉强度钢,损伤随试验次数的增加而增大。重复熨烫不会增加黄铜工件的表面粗糙度。在此条件下,DLC-Si涂层可用于干式熨烫工艺。
{"title":"Application of DLC Coating to Ironing Die","authors":"K. Dohda, H. Kubota, Y. Tsuchiya","doi":"10.1299/JSMEA.48.286","DOIUrl":"https://doi.org/10.1299/JSMEA.48.286","url":null,"abstract":"The possibilities of application of DLC-Si coating to the die in dry ironing process have been investigated by strip-ironing type tribometer. Alloy tool steel and high speed steel were used as substrate material for ironing dies. Two types of substrate surface texture were prepared by lapping and grinding. And two types of die edge angle were prepared. High tensile strength steel and brass were tested as workpieces. The surface appearance of die, friction coefficient during ironing and surface roughness of ironed workpiece were measured. The friction coefficient of DLC-Si coated die in the dry ironing process is relatively low. Galling does not occur on the die surface. In case of high tensile strength steel, the damage grows with the number of tests. The surface roughness of a brass workpiece does not increase with repeat ironing. The DLC-Si coating could be applied to the dry ironing process in this investigated condition.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"109 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2005-10-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"128437463","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 12
Development of Thread Rolled Anti-Loosening Bolts Based on the Double Thread Mechanism and a Performance Evaluation 基于双螺纹机构的螺纹滚压防松螺栓的研制及性能评价
T. Takemasu, H. Miyahara
It has already been proven that bolt fasteners based on the double thread mechanism have an excellent anti-loosening performance. The purpose of this study is to establish a mass production method for these double thread bolts (DTBs) by thread rolling. The pitch ratio of the coarse thread and the fine thread of the target DTB is set as 2 to 1. A two-die roller with a plunge feed is employed as the rolling method due to its fine processing precision. The roller dies used in the experiments have special grooves on the external surface which follow the same outline as the thread profiles of the DTB. Using these special dies, the DTB can be successfully formed in the same process as single thread bolts. The deformation of a workpiece during rolling is examined, and the examination shows that the formed material smoothly fills the die grooves in each cross section. The rolled DTBs completely pass the loosening test with extremely severe vibration and impact, as specified in NAS3354. The tensile fatigue strength of the rolled DTB is about 100% greater than that of the cutting DTB.
实践证明,基于双螺纹机构的螺栓紧固件具有优异的防松性能。本研究的目的是建立一种螺纹滚压生产双螺纹螺栓(dtb)的方法。将目标DTB的粗螺纹和细螺纹的螺距比设置为2比1。由于其加工精度高,采用了双模滚轮插入式进给作为轧制方法。实验中使用的滚子模具外表面有特殊的凹槽,凹槽的轮廓与DTB的螺纹轮廓相同。使用这些专用模具,DTB可以在与单螺纹螺栓相同的工艺中成功成形。对轧制过程中工件的变形进行了检测,检测结果表明成形材料平滑地填充了各截面的模槽。轧制后的dtb完全通过了NAS3354中规定的极端剧烈振动和冲击的松动试验。轧制DTB的拉伸疲劳强度比切削DTB高100%左右。
{"title":"Development of Thread Rolled Anti-Loosening Bolts Based on the Double Thread Mechanism and a Performance Evaluation","authors":"T. Takemasu, H. Miyahara","doi":"10.1299/JSMEA.48.305","DOIUrl":"https://doi.org/10.1299/JSMEA.48.305","url":null,"abstract":"It has already been proven that bolt fasteners based on the double thread mechanism have an excellent anti-loosening performance. The purpose of this study is to establish a mass production method for these double thread bolts (DTBs) by thread rolling. The pitch ratio of the coarse thread and the fine thread of the target DTB is set as 2 to 1. A two-die roller with a plunge feed is employed as the rolling method due to its fine processing precision. The roller dies used in the experiments have special grooves on the external surface which follow the same outline as the thread profiles of the DTB. Using these special dies, the DTB can be successfully formed in the same process as single thread bolts. The deformation of a workpiece during rolling is examined, and the examination shows that the formed material smoothly fills the die grooves in each cross section. The rolled DTBs completely pass the loosening test with extremely severe vibration and impact, as specified in NAS3354. The tensile fatigue strength of the rolled DTB is about 100% greater than that of the cutting DTB.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"91 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2005-10-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"126020242","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 7
Crystal Structure Formed in Mechanical Alloying Process of Mg-Al-Zn Powder Mixture Using Magnesium Alloy Machined Chips 镁合金加工芯片机械合金化Mg-Al-Zn混合粉末过程中形成的晶体结构
H. Oginuma, E. Yuasa
For making the functional alloy powder from magnesium alloy scrap, Mg-Zn and Mg-Al-Zn powder mixtures, which aluminum and zinc powder were added with various contents to machined chips of AZ31 alloy, were mechanically alloyed for various milling times using planetary ball mill. Crystal phase formed in the obtained powder was investigated by X-ray di ff raction and Vickers hardness of the powder particles was measured for confirmations of the formed phases. In the case of Mg-2.5 mol%Zn powder mechanically alloyed for long milling time, super-saturated α -Mg phase with 2.5 mol%Zn concentration forms. The structures of Mg-28 and 52 mol%Zn powder consist of Mg 2 Zn 2 or MgZn 2 , Mg 7 Zn 3 phases and then these phases become to amorphous phase by milling for prolonged time. In the ternary Mg-Al-Zn system of composition range, which were (30-50) mol%Mg with Al / Zn = (90 / 10-60 / 40) molar ratio, Mg-(30-50) mol%Al-20 mol%Zn and Mg-(10-30) mol%Al-40 mol%Zn, icosahedron Mg 49 (Al,Zn) 32 phase as called the quasi crystal forms by the mechanical alloying for 72 ks.
为制备功能合金粉末,采用行星球磨机将不同含量的铝和锌粉加入到AZ31合金的加工切屑中,进行不同磨次的Mg-Zn和Mg-Al-Zn混合粉的机械合金化。用x射线分光光度法研究了粉末中形成的晶相,并测定了粉末颗粒的维氏硬度以确定形成的相。在Mg-2.5 mol%Zn机械合金化较长时间的情况下,形成了具有2.5 mol%Zn浓度的过饱和α -Mg相。Mg-28和52 mol%Zn粉末的结构由mg2zn2或mgzn2、mg7zn2相组成,经过长时间的研磨,这些相变成非晶相。在Al / Zn =(90 / 10-60 / 40)摩尔比为(30-50)mol%Mg的三元Mg-Al-Zn体系中,Mg-(30-50) mol%Al-20 mol%Zn和Mg-(10-30) mol%Al-40 mol%Zn,经过72 k的机械合金化形成了二十面体mg49 (Al,Zn) 32相的准晶体。
{"title":"Crystal Structure Formed in Mechanical Alloying Process of Mg-Al-Zn Powder Mixture Using Magnesium Alloy Machined Chips","authors":"H. Oginuma, E. Yuasa","doi":"10.1299/JSMEA.48.381","DOIUrl":"https://doi.org/10.1299/JSMEA.48.381","url":null,"abstract":"For making the functional alloy powder from magnesium alloy scrap, Mg-Zn and Mg-Al-Zn powder mixtures, which aluminum and zinc powder were added with various contents to machined chips of AZ31 alloy, were mechanically alloyed for various milling times using planetary ball mill. Crystal phase formed in the obtained powder was investigated by X-ray di ff raction and Vickers hardness of the powder particles was measured for confirmations of the formed phases. In the case of Mg-2.5 mol%Zn powder mechanically alloyed for long milling time, super-saturated α -Mg phase with 2.5 mol%Zn concentration forms. The structures of Mg-28 and 52 mol%Zn powder consist of Mg 2 Zn 2 or MgZn 2 , Mg 7 Zn 3 phases and then these phases become to amorphous phase by milling for prolonged time. In the ternary Mg-Al-Zn system of composition range, which were (30-50) mol%Mg with Al / Zn = (90 / 10-60 / 40) molar ratio, Mg-(30-50) mol%Al-20 mol%Zn and Mg-(10-30) mol%Al-40 mol%Zn, icosahedron Mg 49 (Al,Zn) 32 phase as called the quasi crystal forms by the mechanical alloying for 72 ks.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"282 2 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2005-10-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"131786734","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
Evaluation of Mechanical Properties and Microstructure in Ion-Irradiated Surface Layer 离子辐照表面层的力学性能和微观结构评价
T. Naoe, M. Futakawa, A. Naito, H. Kogawa, Y. Ikeda, Y. Motohashi
Target vessel materials used in spallation neutron source will be exposed to proton and neutron irradiation and mercury immersion environments. In order to evaluate the surface degradation of the vessel candidate materials due to such environment, the triple-ion beam irradiation taking the spallation reaction into account and mercury immersion tests were carried out. Mechanical properties of the gradient surface layer were evaluated by the inverse analysis with multi-layer model that considers distribution of surface characteristic was applied to the load and depth curves measured by using the instrumented indentation machine. Transmission electron microscopic observations were performed to evaluate the changes of microstructure in irradiated surface layer using focused ion-beam cut micro-specimen. The mechanical properties distributions in the surface layer were evaluated quantitatively and the changes in microstructures were correspondent to the property distribution. It was confirmed that the ductility loss is enhanced by the irradiation and mercury immersion, and simulated stress and strain curves of the ion-irradiated surface layer were adequately in good agreement with the curves of experimental equivalent neutron-irradiated material.
散裂中子源靶容器材料将暴露在质子、中子辐照和汞浸环境中。为了评估这种环境对容器候选材料表面降解的影响,进行了考虑碎裂反应的三离子束辐照和浸汞试验。采用考虑表面特性分布的多层模型,对仪器压痕机测得的载荷和深度曲线进行逆分析,评价了梯度面层的力学性能。采用聚焦离子束切割微试样,通过透射电镜观察辐照面层微结构的变化。定量评价了表层的力学性能分布,微观组织的变化与性能分布相对应。结果表明,辐照和汞浸均能增强材料的延性损失,模拟的离子辐照面层应力应变曲线与实验等效中子辐照材料的应力应变曲线吻合较好。
{"title":"Evaluation of Mechanical Properties and Microstructure in Ion-Irradiated Surface Layer","authors":"T. Naoe, M. Futakawa, A. Naito, H. Kogawa, Y. Ikeda, Y. Motohashi","doi":"10.1299/JSMEA.48.280","DOIUrl":"https://doi.org/10.1299/JSMEA.48.280","url":null,"abstract":"Target vessel materials used in spallation neutron source will be exposed to proton and neutron irradiation and mercury immersion environments. In order to evaluate the surface degradation of the vessel candidate materials due to such environment, the triple-ion beam irradiation taking the spallation reaction into account and mercury immersion tests were carried out. Mechanical properties of the gradient surface layer were evaluated by the inverse analysis with multi-layer model that considers distribution of surface characteristic was applied to the load and depth curves measured by using the instrumented indentation machine. Transmission electron microscopic observations were performed to evaluate the changes of microstructure in irradiated surface layer using focused ion-beam cut micro-specimen. The mechanical properties distributions in the surface layer were evaluated quantitatively and the changes in microstructures were correspondent to the property distribution. It was confirmed that the ductility loss is enhanced by the irradiation and mercury immersion, and simulated stress and strain curves of the ion-irradiated surface layer were adequately in good agreement with the curves of experimental equivalent neutron-irradiated material.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"24 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2005-10-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"129807655","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Influence of Heat Treatment on Mechanical Properties of DLC Deposited by FIB-CVD 热处理对FIB-CVD沉积DLC力学性能的影响
N. Sakamoto, Y. Kogo, T. Yasuno, J. Taniguchi, I. Miyamoto
The influence of heat treatment on the mechanical properties of DLC deposited by FIB-CVD was examined. To evaluate the mechanical properties, Young’s modulus and Vickers hardness were measured by the nano indentation tester. For the characterization of DLC structure, Raman scattering was used. The microstructures of samples were characterized by HRTEM equipped with EELS. From results of the indentation experiments, it was found that Young’s modulus and Vickers hardness decreased with increasing heat treatment temperature. Analysis of Raman and EELS spectra indicated that the decrease of Young’s modulus and hardness was caused by the decrease of sp3 fraction.
研究了热处理对FIB-CVD沉积DLC力学性能的影响。采用纳米压痕仪测量了材料的杨氏模量和维氏硬度,以评价材料的力学性能。对于DLC结构的表征,采用了拉曼散射。利用电子能谱仪(EELS)对样品的微观结构进行了表征。压痕实验结果表明,随着热处理温度的升高,合金的杨氏模量和维氏硬度呈下降趋势。Raman和EELS光谱分析表明,sp3分数的降低是杨氏模量和硬度降低的主要原因。
{"title":"Influence of Heat Treatment on Mechanical Properties of DLC Deposited by FIB-CVD","authors":"N. Sakamoto, Y. Kogo, T. Yasuno, J. Taniguchi, I. Miyamoto","doi":"10.1299/JSMEA.48.275","DOIUrl":"https://doi.org/10.1299/JSMEA.48.275","url":null,"abstract":"The influence of heat treatment on the mechanical properties of DLC deposited by FIB-CVD was examined. To evaluate the mechanical properties, Young’s modulus and Vickers hardness were measured by the nano indentation tester. For the characterization of DLC structure, Raman scattering was used. The microstructures of samples were characterized by HRTEM equipped with EELS. From results of the indentation experiments, it was found that Young’s modulus and Vickers hardness decreased with increasing heat treatment temperature. Analysis of Raman and EELS spectra indicated that the decrease of Young’s modulus and hardness was caused by the decrease of sp3 fraction.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"39 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2005-10-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"132863524","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 6
Effects of Powder Size and Initial Arrangement on Cold Compaction 粉末粒度和初始排列对冷压成型的影响
W. Tanwongwan, A. Manonukul, J. Carmai
In the past, the most common assumption in every explicit modelling of individual powders for compaction is that powders have only one single size which are arranged uniformly. However, all powders used in practice have a distribution of particle size and random initial arrangement. In this work, a systematic theoretical study of the effects of initial powder arrangement and distribution of size has been investigated using numerical analysis tool. Various types of elements have been considered first. Considering the accuracy and the effort required, the two-dimensional plane strain element has been employed for the rest of the investigation. The initial arrangement of powder and the distribution of powder size were considered separately. The results show that the initial arrangement has significant influence on the macroscopic behaviour while the powder size has little influence. Both factors have noticeable influence on the microscopic behaviour.
在过去,最常见的假设,在每一个明确的模型的单个粉末压实是粉末只有一个单一的尺寸是均匀排列。然而,实际使用的所有粉末都具有粒径分布和随机初始排列。本文采用数值分析工具,对粉末初始排列和粒度分布的影响进行了系统的理论研究。首先考虑了各种类型的元素。考虑到精度和所需的努力,在接下来的研究中采用二维平面应变单元。粉末的初始排列和粉末粒度的分布是分开考虑的。结果表明,初始排列对宏观行为有显著影响,而粉末粒度对宏观行为影响较小。这两个因素对微观行为都有显著的影响。
{"title":"Effects of Powder Size and Initial Arrangement on Cold Compaction","authors":"W. Tanwongwan, A. Manonukul, J. Carmai","doi":"10.1299/JSMEA.48.376","DOIUrl":"https://doi.org/10.1299/JSMEA.48.376","url":null,"abstract":"In the past, the most common assumption in every explicit modelling of individual powders for compaction is that powders have only one single size which are arranged uniformly. However, all powders used in practice have a distribution of particle size and random initial arrangement. In this work, a systematic theoretical study of the effects of initial powder arrangement and distribution of size has been investigated using numerical analysis tool. Various types of elements have been considered first. Considering the accuracy and the effort required, the two-dimensional plane strain element has been employed for the rest of the investigation. The initial arrangement of powder and the distribution of powder size were considered separately. The results show that the initial arrangement has significant influence on the macroscopic behaviour while the powder size has little influence. Both factors have noticeable influence on the microscopic behaviour.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"16 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2005-10-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"130582952","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
期刊
Jsme International Journal Series A-solid Mechanics and Material Engineering
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1