首页 > 最新文献

Jsme International Journal Series A-solid Mechanics and Material Engineering最新文献

英文 中文
Experimental and Analytical Characterization of β-Tricalcium Phosphate Particle Reinforced Poly-L-Lactide Composites β-磷酸三钙颗粒增强聚l -丙交酯复合材料的实验与分析表征
Satoshi Kobayashi, Kazuki Sakamoto
Bioactive ceramics, β-tricalcium phosphate (β-TCP), particles reinforced bioabsorbable plastics poly-L lactide (PLLA) composites have been expected to apply for the fracture fixations which have more biocompatibility than monolithic PLLA. In this study, β-TCP/PLLA composites containing three different β-TCP contents (4.8, 9.5, 14.3wt%) were prepared by injection molding. The results of bending tests show bending strength decreases with increasing β-TCP contents. On the other hand, bending modulus increases with increasing β-TCP contents. After immersion tests in PBS at 37°C up to 8 weeks, the mechanical properties were hardly degraded in all specimens. The results of fracture surface observation by scanning electron microscopy indicated that microscopic damage such as debonding between β-TCP and PLLA initiates at β-TCP agglomeration and grows with increasing loading. Analytical predictions of the relationship between stress and strain based on micromechanics considering the progress of debonding between β-TCP and PLLA were in good agreement with experimental results.
生物活性陶瓷、β-磷酸三钙(β-TCP)、颗粒增强生物可吸收塑料聚乳酸(PLLA)复合材料具有比单片PLLA更好的生物相容性,有望应用于骨折固定。本研究通过注射成型制备了三种不同β-TCP含量(4.8、9.5、14.3wt%)的β-TCP/PLLA复合材料。抗弯试验结果表明,随着β-TCP含量的增加,抗弯强度降低。另一方面,弯曲模量随β-TCP含量的增加而增加。在37°C的PBS中浸泡8周后,所有试件的力学性能几乎没有退化。扫描电镜观察断口形貌结果表明,β-TCP与PLLA之间的脱粘等微观损伤始于β-TCP团聚,并随着载荷的增加而扩大。考虑β-TCP与PLLA脱粘过程的细观力学应力应变关系分析预测与实验结果吻合较好。
{"title":"Experimental and Analytical Characterization of β-Tricalcium Phosphate Particle Reinforced Poly-L-Lactide Composites","authors":"Satoshi Kobayashi, Kazuki Sakamoto","doi":"10.1299/JSMEA.49.314","DOIUrl":"https://doi.org/10.1299/JSMEA.49.314","url":null,"abstract":"Bioactive ceramics, β-tricalcium phosphate (β-TCP), particles reinforced bioabsorbable plastics poly-L lactide (PLLA) composites have been expected to apply for the fracture fixations which have more biocompatibility than monolithic PLLA. In this study, β-TCP/PLLA composites containing three different β-TCP contents (4.8, 9.5, 14.3wt%) were prepared by injection molding. The results of bending tests show bending strength decreases with increasing β-TCP contents. On the other hand, bending modulus increases with increasing β-TCP contents. After immersion tests in PBS at 37°C up to 8 weeks, the mechanical properties were hardly degraded in all specimens. The results of fracture surface observation by scanning electron microscopy indicated that microscopic damage such as debonding between β-TCP and PLLA initiates at β-TCP agglomeration and grows with increasing loading. Analytical predictions of the relationship between stress and strain based on micromechanics considering the progress of debonding between β-TCP and PLLA were in good agreement with experimental results.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"4 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2006-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"125989001","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 11
Approach to Analysis of Mechanical Behavior of Textile Composites by Inclusion Element Method 包合元法分析纺织复合材料力学性能的探讨
T. Tsujikami, T. Horikawa, Satoru Hirosawa, M. Zako
The inclusion element method with a simple grid model has been proposed as one of the analytical techniques of the mechanical behavior of textile composites, and the effectiveness of this method has been verified. The inclusion element method is applicable to the analysis of all types of textile composites because the element stiffness obtained by the inclusion method through cooperation with a fabric structure simulator is used. From the result of the analysis by the inclusion element method, it has been confirmed that the peculiar crimp-interchange of woven composites occurs and high tensile stress arises at the elements with fiber bundles oriented in the load direction. A comparison between the analyses using a real model and the inclusion element model has shown relatively good agreement. Although the analytical result is greatly dependent on the grid pattern, the inclusion element method can provide a sufficient accuracy of results even when the number of elements in the model is lower than that in the real model.
提出了基于简单网格模型的包含元法作为纺织复合材料力学行为的分析方法之一,并验证了该方法的有效性。由于采用的是与织物结构模拟器配合使用的包含单元刚度,因此包含单元法适用于各类纺织复合材料的分析。包合元法分析结果表明,织物复合材料发生了特殊的卷曲交换现象,纤维束在载荷方向上的单元产生了较高的拉应力。用真实模型和包含元素模型进行的分析比较表明,两者具有较好的一致性。虽然分析结果很大程度上依赖于网格模式,但即使模型中的元素数量低于实际模型中的元素数量,包含元素方法也能提供足够的结果精度。
{"title":"Approach to Analysis of Mechanical Behavior of Textile Composites by Inclusion Element Method","authors":"T. Tsujikami, T. Horikawa, Satoru Hirosawa, M. Zako","doi":"10.1299/JSMEA.49.418","DOIUrl":"https://doi.org/10.1299/JSMEA.49.418","url":null,"abstract":"The inclusion element method with a simple grid model has been proposed as one of the analytical techniques of the mechanical behavior of textile composites, and the effectiveness of this method has been verified. The inclusion element method is applicable to the analysis of all types of textile composites because the element stiffness obtained by the inclusion method through cooperation with a fabric structure simulator is used. From the result of the analysis by the inclusion element method, it has been confirmed that the peculiar crimp-interchange of woven composites occurs and high tensile stress arises at the elements with fiber bundles oriented in the load direction. A comparison between the analyses using a real model and the inclusion element model has shown relatively good agreement. Although the analytical result is greatly dependent on the grid pattern, the inclusion element method can provide a sufficient accuracy of results even when the number of elements in the model is lower than that in the real model.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"40 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2006-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"125049324","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
Gigacycle Fatigue Properties of V-Added Steel with an Application of Modified Ausforming 加v钢的千兆周疲劳性能及其改进的应用
H. Hirukawa, Y. Furuya, S. Matsuoka
This report reveals gigacycle fatigue properties for a modified-ausformed V-added steel with the chemical composition of 0.3C-0.3Si-1.0Cr-0.7Mo-0.3V in mass %. Modified-ausformed and oil-quenched steels were prepared for fatigue tests, followed by tempering at 400°C and 600°C. The tensile strengths of the 600°C tempered steels were almost equal to those of the 400°C tempered versions because of secondary hardening due to fine precipitation of vanadium carbides. The fatigue properties of the 600°C tempered version of oil-quenched steel (QT600) showed little difference from the 400°C tempered version (QT400) in spite of the fine precipitation of vanadium carbides. The modified-ausformed steels (AF400 and AF600) revealed higher fatigue limits at 5× 109 cycles than the oil-quenched versions (QT400 and QT600), although the difference between AF400 and AF600 was small. The remarkable difference between AF400 and AF600 was fatigue strengths at around 106 cycles, i.e. the fatigue strength of AF600 at those cycles was higher than that of AF400. Based on the above results, the effect of the fine precipitation of vanadium carbides was small on the gigacycle fatigue properties, while modified-ausforming could improve those properties. On the other hand, the multiple effects of the fine precipitation and modified-ausforming was large on the fatigue strength at around 106 cycles.
本报告揭示了一种化学成分为质量%为0.3C-0.3Si-1.0Cr-0.7Mo-0.3V的变质型加v钢的千兆周疲劳性能。制备了变形钢和油淬钢进行疲劳试验,然后分别在400℃和600℃回火。600°C回火钢的抗拉强度与400°C回火钢的抗拉强度几乎相等,这是由于碳化钒的细析出引起的二次硬化。600℃调质油淬钢(QT600)的疲劳性能与400℃调质钢(QT400)相比差异不大,但碳化钒析出较多。AF400和AF600在5× 109次循环下的疲劳极限高于油淬钢(QT400和QT600),但两者之间的差异很小。AF400与AF600在106次循环时的疲劳强度差异显著,即AF600在106次循环时的疲劳强度高于AF400。综上所述,碳化钒的细析出对合金的千兆周疲劳性能影响不大,而改性奥氏体可以改善合金的千兆周疲劳性能。另一方面,在106次循环时,细析出和变质变形的多重影响对疲劳强度影响较大。
{"title":"Gigacycle Fatigue Properties of V-Added Steel with an Application of Modified Ausforming","authors":"H. Hirukawa, Y. Furuya, S. Matsuoka","doi":"10.1299/JSMEA.49.337","DOIUrl":"https://doi.org/10.1299/JSMEA.49.337","url":null,"abstract":"This report reveals gigacycle fatigue properties for a modified-ausformed V-added steel with the chemical composition of 0.3C-0.3Si-1.0Cr-0.7Mo-0.3V in mass %. Modified-ausformed and oil-quenched steels were prepared for fatigue tests, followed by tempering at 400°C and 600°C. The tensile strengths of the 600°C tempered steels were almost equal to those of the 400°C tempered versions because of secondary hardening due to fine precipitation of vanadium carbides. The fatigue properties of the 600°C tempered version of oil-quenched steel (QT600) showed little difference from the 400°C tempered version (QT400) in spite of the fine precipitation of vanadium carbides. The modified-ausformed steels (AF400 and AF600) revealed higher fatigue limits at 5× 109 cycles than the oil-quenched versions (QT400 and QT600), although the difference between AF400 and AF600 was small. The remarkable difference between AF400 and AF600 was fatigue strengths at around 106 cycles, i.e. the fatigue strength of AF600 at those cycles was higher than that of AF400. Based on the above results, the effect of the fine precipitation of vanadium carbides was small on the gigacycle fatigue properties, while modified-ausforming could improve those properties. On the other hand, the multiple effects of the fine precipitation and modified-ausforming was large on the fatigue strength at around 106 cycles.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"84 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2006-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"124339704","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
Synthesis and Characterization of SiC Ceramics for High Temperature Resistant Coatings and Matrix 耐高温涂层和基体用SiC陶瓷的合成与表征
H. Watanabe, Satoshi Kobayashi, M. Fukushima, S. Wakayama
SiC ceramics are expected as oxidation resistant coating material for Carbon/Carbon (C/C) composites. In the present study, SiC ceramics were synthesized through Sol-Gel method with low environmental impact. The gels were synthesized from ethylalcohol, methyltriethoxysilane (MTES), hydrochloric acid (HCl) and purified water (H2O), and it was pyrolyzed at 1 000, 1 500 and 1 700◦C. The structures of gels after heat treatment were analyzed by X-ray diffraction (XRD). XRD results indicated that β-SiC were obtained in the present method and crystallization was increased with increasing heat treatment temperature. There was little weight change in synthesized SiC obtained at 1 000◦C in air, which results in lower weight changes in SiC coated C/C composites comparing with bare C/C composites. However, SiC coated C/C composites were also oxidized because of the generation of cracks during heat treatment at 1 000◦C. Residual tensile strength of SiC coated C/C composites were also higher than that of bare C/C composites after 5 minutes oxidation.
SiC陶瓷有望成为碳/碳复合材料的抗氧化涂层材料。本研究采用溶胶-凝胶法制备了低环境影响的SiC陶瓷。以乙醇、甲基三乙氧基硅烷(MTES)、盐酸(HCl)和纯净水(H2O)为原料合成凝胶,分别在1 000、1 500和1 700℃下进行热解。用x射线衍射(XRD)分析了热处理后凝胶的结构。XRD结果表明,本方法制备的β-SiC晶化程度随热处理温度的升高而提高。在1 000◦C空气中合成的SiC重量变化很小,这导致SiC涂层C/C复合材料的重量变化比裸C/C复合材料小。然而,SiC涂层的C/C复合材料也被氧化,因为在1 000◦C的热处理过程中产生裂纹。SiC涂层C/C复合材料氧化5 min后的残余抗拉强度也高于裸C/C复合材料。
{"title":"Synthesis and Characterization of SiC Ceramics for High Temperature Resistant Coatings and Matrix","authors":"H. Watanabe, Satoshi Kobayashi, M. Fukushima, S. Wakayama","doi":"10.1299/JSMEA.49.237","DOIUrl":"https://doi.org/10.1299/JSMEA.49.237","url":null,"abstract":"SiC ceramics are expected as oxidation resistant coating material for Carbon/Carbon (C/C) composites. In the present study, SiC ceramics were synthesized through Sol-Gel method with low environmental impact. The gels were synthesized from ethylalcohol, methyltriethoxysilane (MTES), hydrochloric acid (HCl) and purified water (H2O), and it was pyrolyzed at 1 000, 1 500 and 1 700◦C. The structures of gels after heat treatment were analyzed by X-ray diffraction (XRD). XRD results indicated that β-SiC were obtained in the present method and crystallization was increased with increasing heat treatment temperature. There was little weight change in synthesized SiC obtained at 1 000◦C in air, which results in lower weight changes in SiC coated C/C composites comparing with bare C/C composites. However, SiC coated C/C composites were also oxidized because of the generation of cracks during heat treatment at 1 000◦C. Residual tensile strength of SiC coated C/C composites were also higher than that of bare C/C composites after 5 minutes oxidation.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"45 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2006-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"115120311","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Nonlinear Dynamic Bending and Domain Wall Motion in Functionally Graded Piezoelectric Actuators under AC Electric Fields: Simulation and Experiment 交流电场作用下功能梯度压电驱动器的非线性动态弯曲和畴壁运动:仿真与实验
Y. Shindo, F. Narita, M. Mikami, Fumitoshi Saito
This paper describes the results of our numerical and experimental studies of the nonlinear bending behavior due to domain wall motion in functionally graded piezoelectric actuator under alternating current electric fields. A nonlinear three-dimensional finite element method is employed to simulate the dynamic response of cantilever functionally graded piezoelectric actuator. A phenomenological model of domain wall motion is used in computation, and the effects of ac electric field amplitude and frequency, number of layers, and property gradation on the deflection and internal stresses of the functionally graded bimorphs are examined. It is shown that the predicted deflection results, obtained from the numerical model, agree well with the corresponding experimental results.
本文介绍了在交流电场作用下,功能梯度压电执行器的畴壁运动引起的非线性弯曲行为的数值和实验研究结果。采用非线性三维有限元法对悬臂式功能梯度压电作动器的动态响应进行了仿真。采用畴壁运动的现象学模型进行计算,考察了交流电场振幅和频率、层数和性质梯度对功能梯度双晶的挠度和内应力的影响。结果表明,数值模型预测的挠度结果与相应的试验结果吻合较好。
{"title":"Nonlinear Dynamic Bending and Domain Wall Motion in Functionally Graded Piezoelectric Actuators under AC Electric Fields: Simulation and Experiment","authors":"Y. Shindo, F. Narita, M. Mikami, Fumitoshi Saito","doi":"10.1299/JSMEA.49.188","DOIUrl":"https://doi.org/10.1299/JSMEA.49.188","url":null,"abstract":"This paper describes the results of our numerical and experimental studies of the nonlinear bending behavior due to domain wall motion in functionally graded piezoelectric actuator under alternating current electric fields. A nonlinear three-dimensional finite element method is employed to simulate the dynamic response of cantilever functionally graded piezoelectric actuator. A phenomenological model of domain wall motion is used in computation, and the effects of ac electric field amplitude and frequency, number of layers, and property gradation on the deflection and internal stresses of the functionally graded bimorphs are examined. It is shown that the predicted deflection results, obtained from the numerical model, agree well with the corresponding experimental results.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"103 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2006-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"132528274","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 21
Photodiode Camera Measurement of Surface Strains on Tendons during Multiple Cyclic Tests 多次循环试验中肌腱表面应变的光电二极管相机测量
K. Chun, R. Hubbard
The objectives of this study are to introduce the use of a photodiode camera for measuring surface strain on soft tissue and to present some representative responses of the tendon. Tendon specimens were obtained from the hindlimbs of canines and frozen to -70°C. After thawing, specimens were mounted in the immersion bath at a room temperature (22°C), preloaded to 0.13N and then subjected to 3% of the initial length at a strain rate of 2%/sec. In tendons which were tested in two blocks of seven repeated extensions to 3% strain with a 120 seconds wait period between, the surface strains were measured with a photodiode camera and near the gripped ends generally were greater than the surface strains in the middle segment of the tendon specimens. The recovery for peak load after the rest period was consistent but the changes in patterns of surface strains after the rest period were not consistent. The advantages of a photodiode measurement of surface strains include the followings: 1) it is a noncontacting method which eliminates errors and distortions caused by clip gauges or mechanical/electronic transducers; 2) it is more accurate than previous noncontact methods, e.g. the VDA and the high speed photographic method; 3) it is a fully automatic, thus reducing labor for replaying video tapes or films and potential errors from human judgement which can occur during digitizing data from photographs. Because the photodiode camera, employs a solid state photodiode array to sense black and white images, scan targets (black image) on the surface of the tendon specimen and back lighting system (white image), and stored automatically image data for surface strains of the tendon specimen on the computer during cyclic extensions.
本研究的目的是介绍使用光电二极管相机测量软组织的表面应变,并提出肌腱的一些代表性反应。取犬科动物后肢肌腱标本,冷冻至-70℃。解冻后,将试样置于室温(22℃)浸泡浴中,预加载至0.13N,然后以2%/秒的应变速率承受初始长度的3%。在两组肌腱中进行测试,每组7次重复拉伸至3%应变,间隔120秒,用光电二极管相机测量表面应变,在抓握端附近的表面应变通常大于肌腱标本中间部分的表面应变。静息期后峰值荷载恢复一致,但静息期后表面应变变化规律不一致。光电二极管测量表面应变的优点包括:1)它是一种非接触的方法,消除了夹片计或机械/电子传感器引起的误差和扭曲;2)比以往的非接触方法(如VDA和高速照相法)精度更高;3)它是全自动的,因此减少了重放录像带或电影的劳动,以及在将照片数据数字化过程中可能出现的人为判断错误。由于光电二极管相机采用固态光电二极管阵列感测黑白图像,扫描肌腱试件表面的目标(黑色图像)和背光系统(白色图像),并在循环拉伸过程中将肌腱试件表面应变的图像数据自动存储在计算机上。
{"title":"Photodiode Camera Measurement of Surface Strains on Tendons during Multiple Cyclic Tests","authors":"K. Chun, R. Hubbard","doi":"10.1299/JSMEA.49.282","DOIUrl":"https://doi.org/10.1299/JSMEA.49.282","url":null,"abstract":"The objectives of this study are to introduce the use of a photodiode camera for measuring surface strain on soft tissue and to present some representative responses of the tendon. Tendon specimens were obtained from the hindlimbs of canines and frozen to -70°C. After thawing, specimens were mounted in the immersion bath at a room temperature (22°C), preloaded to 0.13N and then subjected to 3% of the initial length at a strain rate of 2%/sec. In tendons which were tested in two blocks of seven repeated extensions to 3% strain with a 120 seconds wait period between, the surface strains were measured with a photodiode camera and near the gripped ends generally were greater than the surface strains in the middle segment of the tendon specimens. The recovery for peak load after the rest period was consistent but the changes in patterns of surface strains after the rest period were not consistent. The advantages of a photodiode measurement of surface strains include the followings: 1) it is a noncontacting method which eliminates errors and distortions caused by clip gauges or mechanical/electronic transducers; 2) it is more accurate than previous noncontact methods, e.g. the VDA and the high speed photographic method; 3) it is a fully automatic, thus reducing labor for replaying video tapes or films and potential errors from human judgement which can occur during digitizing data from photographs. Because the photodiode camera, employs a solid state photodiode array to sense black and white images, scan targets (black image) on the surface of the tendon specimen and back lighting system (white image), and stored automatically image data for surface strains of the tendon specimen on the computer during cyclic extensions.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"59 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2006-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"132144145","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Evaluation of Ferroelectric Properties of Piezoelectric Ceramics Based on Crystallographic Homogenization Method and Crystal Orientation Analysis by SEM·EBSD Technique 基于晶体均质法和SEM·EBSD技术的压电陶瓷铁电性能评价
Y. Uetsuji, Toshihiro Yoshida, T. Yamakawa, K. Tsuchiya, S. Ueda, E. Nakamachi
Macroscopic ferroelectric properties of piezoelectric polycrystals are strongly affected by microscopic inhomogeneous crystal structure. In our previous study, a multi-scale finite element method based on crystallographic homogenization method has been developed to estimate macroscopic properties considering microscopic crystal morphology. In this paper, the crystal orientation distribution of polycrystalline barium titanate has been measured by SEM·EBSD technique, and the measured crystal orientation distribution has been introduced to the microscopic finite element model. As the prediction of macroscopic properties depends on the sampling conditions of the measured crystal orientations, the effects of number of sampling points and sampling area have been investigated. As a result, the effective sampling conditions have been clarified to estimate macroscopic ferroelectric properties.
压电多晶的宏观铁电性能受到微观非均匀晶体结构的强烈影响。在我们之前的研究中,基于晶体均匀化方法的多尺度有限元方法已经发展到考虑微观晶体形态的宏观性能估计。本文采用SEM·EBSD技术对多晶钛酸钡的晶体取向分布进行了测量,并将测量到的晶体取向分布引入微观有限元模型。由于宏观性质的预测依赖于被测晶体取向的采样条件,因此研究了采样点数和采样面积的影响。从而明确了估算宏观铁电性能的有效取样条件。
{"title":"Evaluation of Ferroelectric Properties of Piezoelectric Ceramics Based on Crystallographic Homogenization Method and Crystal Orientation Analysis by SEM·EBSD Technique","authors":"Y. Uetsuji, Toshihiro Yoshida, T. Yamakawa, K. Tsuchiya, S. Ueda, E. Nakamachi","doi":"10.1299/JSMEA.49.209","DOIUrl":"https://doi.org/10.1299/JSMEA.49.209","url":null,"abstract":"Macroscopic ferroelectric properties of piezoelectric polycrystals are strongly affected by microscopic inhomogeneous crystal structure. In our previous study, a multi-scale finite element method based on crystallographic homogenization method has been developed to estimate macroscopic properties considering microscopic crystal morphology. In this paper, the crystal orientation distribution of polycrystalline barium titanate has been measured by SEM·EBSD technique, and the measured crystal orientation distribution has been introduced to the microscopic finite element model. As the prediction of macroscopic properties depends on the sampling conditions of the measured crystal orientations, the effects of number of sampling points and sampling area have been investigated. As a result, the effective sampling conditions have been clarified to estimate macroscopic ferroelectric properties.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"29 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2006-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"115454643","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
Fabrication of Smart Material PZT Thin Films by RF Magnetron Sputtering Method in Micro Actuators
K. Tsuchiya, T. Kitagawa, Y. Uetsuji, E. Nakamachi
PZT piezoelectric thin films can be promising candidates for microactuators or microsensors in MEMS (Micro Electro Mechanical Systems) or NEMS (Nano Electro Mechanical Systems) because of the quick response. In this research, the RF magnetron sputtering method is used for PZT thin films deposition. The sputtering conditions to control the crystalline plane (111) of perovskite structure for PZT to influence the piezoelectric constant can be proposed. Those sputtering conditions such as substrate angle and temperature, Ar/O2 pressure and flow rate were investigated by the heuristic and experimental design method to fabricate optimum PZT perovskite crystal thin film. The condition of substrate temperature was the most important factor to improve piezoelectric constant. The crystalline structure, surface topography and piezoelectric constant of the deposited PZT were observed by X-ray diffraction structural analysis, atomic force microscope and piezoelectric constant evaluation equipment. PZT thin films with only perovskite structure were obtained. PZT (111) was grown with the increase in substrate temperature, and the piezoelectric property was improved. The elastic modulus of 70GPa for the deposited PZT found a good agreement with the quoted value for commercial based bulk PZT. We obtained a piezoelectric constant d31=-28pm/V and a high performance of bimorph actuator.
PZT压电薄膜由于响应速度快,可以作为MEMS(微电子机械系统)或NEMS(纳米电子机械系统)中的微致动器或微传感器。本研究采用射频磁控溅射法沉积PZT薄膜。提出了控制钙钛矿结构的晶面(111)以影响压电常数的溅射条件。采用启发式和实验设计的方法,考察了衬底角度和温度、Ar/O2压力和流速等溅射条件,以制备最佳的PZT钙钛矿晶体薄膜。衬底温度条件是提高压电常数的最重要因素。利用x射线衍射结构分析、原子力显微镜和压电常数评价设备对沉积的PZT的晶体结构、表面形貌和压电常数进行了观察。得到了仅具有钙钛矿结构的PZT薄膜。PZT(111)随着衬底温度的升高而生长,压电性能得到改善。沉积的PZT弹性模量为70GPa,与商用大块PZT的报价值吻合较好。我们得到了一个压电常数d31=-28pm/V和高性能的双晶圆作动器。
{"title":"Fabrication of Smart Material PZT Thin Films by RF Magnetron Sputtering Method in Micro Actuators","authors":"K. Tsuchiya, T. Kitagawa, Y. Uetsuji, E. Nakamachi","doi":"10.1299/JSMEA.49.201","DOIUrl":"https://doi.org/10.1299/JSMEA.49.201","url":null,"abstract":"PZT piezoelectric thin films can be promising candidates for microactuators or microsensors in MEMS (Micro Electro Mechanical Systems) or NEMS (Nano Electro Mechanical Systems) because of the quick response. In this research, the RF magnetron sputtering method is used for PZT thin films deposition. The sputtering conditions to control the crystalline plane (111) of perovskite structure for PZT to influence the piezoelectric constant can be proposed. Those sputtering conditions such as substrate angle and temperature, Ar/O2 pressure and flow rate were investigated by the heuristic and experimental design method to fabricate optimum PZT perovskite crystal thin film. The condition of substrate temperature was the most important factor to improve piezoelectric constant. The crystalline structure, surface topography and piezoelectric constant of the deposited PZT were observed by X-ray diffraction structural analysis, atomic force microscope and piezoelectric constant evaluation equipment. PZT thin films with only perovskite structure were obtained. PZT (111) was grown with the increase in substrate temperature, and the piezoelectric property was improved. The elastic modulus of 70GPa for the deposited PZT found a good agreement with the quoted value for commercial based bulk PZT. We obtained a piezoelectric constant d31=-28pm/V and a high performance of bimorph actuator.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2006-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"131070345","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 7
Theoretical Investigation on the Contact Duration in Elastic and Inelastic Collision of a Circular Plate to a Planar Surface 圆板与平面弹性与非弹性碰撞接触时间的理论研究
Zhong-Lan Lu, Koichi Tanaka, M. Nishida, F. Huang
In this paper a new theoretical method is proposed for calculating the normalized contact duration and indentation depth in elastic, elastic-plastic and plastic collision of circular plates. The contact duration is composed of total loading time and unloading time that are dependent on the relationship between the interaction force and normal indentation. For plastic collision, the contact duration relates to the coe ffi cient of restitution (COR) of the collision. Considering the actual thickness of a circular plate, a coe ffi cient of indentation (COI) is newly introduced in theoretical analyses of the COR. According to experimental results of COR, a hybrid nonlinear model is also proposed to describe the COR of circular plates for obtaining the unloading time of the plastic collision. Contact force history during collision can be expressed approximately by a half-sine wave and the force and contact duration is calculated numerically.
本文提出了一种计算圆板弹性、弹塑性和塑性碰撞归一化接触时间和压痕深度的新理论方法。接触持续时间由总加载时间和卸载时间组成,这取决于相互作用力与法向压痕之间的关系。对于塑性碰撞,接触时间与碰撞的恢复系数(COR)有关。考虑到圆板的实际厚度,在圆板压痕系数的理论分析中引入了新的压痕系数,并根据压痕系数的实验结果,提出了一种描述圆板压痕系数的混合非线性模型,用于计算塑性碰撞的卸载时间。碰撞过程中的接触力历史可以用半正弦波近似表示,并对碰撞过程中的力和接触时间进行了数值计算。
{"title":"Theoretical Investigation on the Contact Duration in Elastic and Inelastic Collision of a Circular Plate to a Planar Surface","authors":"Zhong-Lan Lu, Koichi Tanaka, M. Nishida, F. Huang","doi":"10.1299/JSMEA.49.258","DOIUrl":"https://doi.org/10.1299/JSMEA.49.258","url":null,"abstract":"In this paper a new theoretical method is proposed for calculating the normalized contact duration and indentation depth in elastic, elastic-plastic and plastic collision of circular plates. The contact duration is composed of total loading time and unloading time that are dependent on the relationship between the interaction force and normal indentation. For plastic collision, the contact duration relates to the coe ffi cient of restitution (COR) of the collision. Considering the actual thickness of a circular plate, a coe ffi cient of indentation (COI) is newly introduced in theoretical analyses of the COR. According to experimental results of COR, a hybrid nonlinear model is also proposed to describe the COR of circular plates for obtaining the unloading time of the plastic collision. Contact force history during collision can be expressed approximately by a half-sine wave and the force and contact duration is calculated numerically.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"19 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2006-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"131571108","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
Non-Contact Evaluation for Articular Cartilage Using Ultrasound 超声对关节软骨的非接触评价
K. Mori, Y. Nakagawa, H. Kuroki, Keisuke Nakashima, K. Ikeuchi, T. Mine, Takashi Nakamura, S. Kawai, Takashi Saito
In orthopedic field, various new treatments of articular cartilage defect, for example autogenous osteochondral grafts, have been developed. With the spread of these treatments, orthopedists began to focus on the mechanical properties of recovered articular cartilage. The quantitative evaluation of articular cartilage before and after these treatments gives orthopedists the important information to improve these treatments and develop new treatments. We have been investigating the non-contact ultrasonic evaluation for articular cartilage under arthroscopy. In this paper, it was hypothesized that the ultrasonic evaluation depended on the collagen fiber in cartilage. The enzymatically degradation of collagen fiber in cartilage surface was performed. The effect of the degradation on sound velocity, attenuation coefficient and signal intensity, which is the index of cartilage stiffness calculated from the proposed method, was measured. The numerical analysis was performed to clear the relation between the cartilage character and ultrasonic parameters. Experimental and numerical results suggest that the present method can be expanded the sensitive evaluation for cartilage disease in clinical field.
在骨科领域,自体骨软骨移植等治疗关节软骨缺损的新方法已经发展起来。随着这些治疗方法的普及,骨科医生开始关注恢复关节软骨的力学特性。关节软骨在这些治疗前后的定量评估为骨科医生提供了重要的信息,以改进这些治疗和开发新的治疗方法。我们一直在研究关节镜下关节软骨的非接触超声评估。本文假设超声评价依赖于软骨中的胶原纤维。研究了软骨表面胶原纤维的酶解作用。测量了退化对声速、衰减系数和信号强度的影响,信号强度是根据该方法计算的软骨刚度指标。通过数值分析,明确了超声参数与软骨特性之间的关系。实验和数值结果表明,该方法可在临床领域扩大对软骨疾病的敏感评价。
{"title":"Non-Contact Evaluation for Articular Cartilage Using Ultrasound","authors":"K. Mori, Y. Nakagawa, H. Kuroki, Keisuke Nakashima, K. Ikeuchi, T. Mine, Takashi Nakamura, S. Kawai, Takashi Saito","doi":"10.1299/JSMEA.49.242","DOIUrl":"https://doi.org/10.1299/JSMEA.49.242","url":null,"abstract":"In orthopedic field, various new treatments of articular cartilage defect, for example autogenous osteochondral grafts, have been developed. With the spread of these treatments, orthopedists began to focus on the mechanical properties of recovered articular cartilage. The quantitative evaluation of articular cartilage before and after these treatments gives orthopedists the important information to improve these treatments and develop new treatments. We have been investigating the non-contact ultrasonic evaluation for articular cartilage under arthroscopy. In this paper, it was hypothesized that the ultrasonic evaluation depended on the collagen fiber in cartilage. The enzymatically degradation of collagen fiber in cartilage surface was performed. The effect of the degradation on sound velocity, attenuation coefficient and signal intensity, which is the index of cartilage stiffness calculated from the proposed method, was measured. The numerical analysis was performed to clear the relation between the cartilage character and ultrasonic parameters. Experimental and numerical results suggest that the present method can be expanded the sensitive evaluation for cartilage disease in clinical field.","PeriodicalId":170519,"journal":{"name":"Jsme International Journal Series A-solid Mechanics and Material Engineering","volume":"43 5","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2006-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"132501310","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 6
期刊
Jsme International Journal Series A-solid Mechanics and Material Engineering
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1