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Collinear double-pulse laser-induced breakdown spectroscopy using Nd:YAG laser generating two nanosecond pulses of regulated energy ratios 共线双脉冲激光诱导击穿光谱利用Nd:YAG激光器产生两个纳秒脉冲的调节能量比
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-08-28 DOI: 10.24425/mms.2023.144872
W. Skrzeczanowski, M. Skórczakowski, W. Zendzian
In the paper results of single-and double-pulse LIBS (Laser-Induced Breakdown Spectroscopy) measurements in collinear geometry are described. The experiments were performed using a unique self-made Nd:YAG laser operating in the Q-switching regime, where the laser transmission losses are switched. Such a laser allowed for an easy and quick change of the operating mode (one and two pulses), free shaping of the energy ratio of the two pulses (division of the energy of a single pulse into two parts) and a smooth change of the delay time between pulses in the range from 200 ns to 10 μ s. To our knowledge, such a laser was used in LIBS measurements for the first time. LIBS experiments revealed strong self-absorption depending on energy ratios carried out in the first and second laser pulse in the double-pulse mode. This was confirmed also by statistical factorial analysis of LIBS spectra. Plasma temperature and LIBS signal enhancement were measured both for energy proportions between the first and the second laser pulse and for the first-to-second-pulse delay.
本文描述了共线几何中单脉冲和双脉冲激光诱导击穿光谱测量的结果。实验采用了一种独特的自制Nd:YAG激光器,工作在q开关状态下,激光传输损耗被切换。这种激光器可以轻松快速地改变工作模式(单脉冲和双脉冲),自由地改变两个脉冲的能量比(将单个脉冲的能量分成两部分),并且在200 ns到10 μ s的范围内平滑地改变脉冲之间的延迟时间。据我们所知,这种激光器首次用于LIBS测量。LIBS实验显示,在双脉冲模式下,第一和第二激光脉冲的能量比决定了材料的自吸收强度。LIBS光谱的统计因子分析也证实了这一点。等离子体温度和LIBS信号增强测量了第一和第二激光脉冲之间的能量比例和第一到第二脉冲延迟。
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引用次数: 0
Quantitative analysis of reaction gases or exhaust using an online process mass spectrometer 使用在线过程质谱仪对反应气体或废气进行定量分析
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-08-28 DOI: 10.24425/mms.2023.144874
Fu-Qiang Wei, Zejian Huang, X. Dai, Xiang Fang, Shang-Zhong Jin
Online quantitative analysis of reaction gases or exhaust in industrial production is of great significance to improve the production capacity and process. A novel method is developed for the online quantitative analysis of reaction gases or exhaust using quantitative mathematical models combined with the linear regression algorithm of machine learning. After accurately estimating the component gases and their contents in the reaction gases or exhaust, a ratio matrix is constructed to separate the relevant overlapping peaks. The ratio andcalibrationstandardgasesaredetected,filtered,normalized,andlinearlyregressedwithanonlineprocess massspectrometertocorrecttheratiomatricesandobtaintherelativesensitivitymatrices.Aquantitative mathematicalmodelcanbeestablishedtoobtainthecontentofeachcomponentofthereactiongasesor exhaustinrealtime.Themaximumquantificationerrorandrelativestandarddeviationofthemethodare within0.3%and1%,afteronlinequantificationoftherepresentativeyeastfermentertailgas.
工业生产中反应气体或废气的在线定量分析对提高生产能力和工艺具有重要意义。利用定量数学模型和机器学习的线性回归算法,开发了一种在线定量分析反应气体或废气的新方法。在准确估计反应气体或废气中的组分气体及其含量后,构建比率矩阵以分离相关重叠峰。用非线性过程质谱仪对比率和校准标准气体进行检测、过滤、归一化和线性回归,以校正治疗基质,并保持相对灵敏度。可以建立一个定量的数学模型,以实时绘制反应气体或排气中各成分的含量。在对代表年的废气进行在线定量后,该方法的最大定量误差和相对标准偏差在0.3%和1%之间。
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引用次数: 0
Analysis of impact of atmospheric attenuation and measurement uncertainties on laser hazard distances in navigable airspace for visible cw laser radiation 大气衰减和测量不确定性对可航空域可见连续波激光危害距离的影响分析
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-08-28 DOI: 10.24425/mms.2023.144869
J. Młyńczak
ThisdocumentprovidesasimplifiedsolutiontotheproblemofcalculationoflaserhazarddistancesdefinedintheAdvisoryCircular70-1BbytheU.S.FederalAviationAdministrationregardingatmosphericattenuation (assumingitsconstantvalue)andmeasurementuncertainties.Thecalculationapproachesandexamples presentedinthisdocumentdonotspecifytheprocedurethatshouldbefollowedinthecaseofatmospheric attenuation,nordotheytakeintoaccounttheuncertaintiesassociatedwiththemeasuredparameters.The analysispresentedinthearticlecomplementstosomeextentAC70-1Bandcanbeusedbythosewhoneed suchasimplifiedsolutionregardingilluminationoflandingortakingoffaircrafts.Thearticlepresentsa sampleanalysisforatypicallaserpointer,wherethenecessaryparametersofthelaserbeamalongwiththe appropriateuncertaintiesweredeterminedinaccordancewiththemethodsaccreditedbythePolishCentre forAccreditationwhiletheappropriatelaserhazarddistanceswerecalculatedtakingintoaccountdifferent atmosphericattenuationcoefficients.
ThisdocumentprovidesasimplifiedsolutiontotheproblemofcalculationoflaserhazarddistancesdefinedintheAdvisoryCircular70-1BbytheU.S。FederalAviationAdministrationregardingatmosphericattenuation andmeasurementuncertainties (assumingitsconstantvalue)。本文件中提出的计算方法和示例没有具体说明在大气衰减情况下应遵循的程序,也没有考虑到与测量参数相关的不确定性。本文所做的分析在一定程度上可以为那些需要这种关于飞机着陆或飞行照明的简化解决方案的人所用。本文介绍了对非典型激光指示器的样品分析,其中激光光束的必要参数以及适当的不确定度是根据波兰认证中心认可的方法确定的,同时考虑到不同的大气衰减系数,计算了适当的激光危害距离。
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引用次数: 0
An experimental device for evaluation of hydrogen sorption 一种评价氢气吸附性能的实验装置
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-08-28 DOI: 10.24425/mms.2023.144875
J. Leyko, K. Surmiński, D. Batory, K. Jastrzębski, Ł. Kaczmarek, W. Kaczorowski, P. Kula
Hydrogen storage for the purposes of the automotive industry in a form other than under high pressure or cryo conditions has been under careful investigation by researchers over past decades. One of the arising methods is the usage of powdered/granulated beds that contain metal hydrides and/or carbon materials to take advantage of the “spillover” phenomenon. Handling and characterization of such material can be troublesome, which is why the experimental setup needs careful investigation. The apparatus for the analysis of hydrogen sorption/desorption characteristics has been successfully designed and described based on the constructed unit within the scope of this article. The full functionality of that setup covered fuelling the bed as well as the examination of sorption/desorption potential. Moreover, the proposed experimental device can clarify many uncertainties about further development and optimization of hydrogen storage materials.
在过去的几十年里,研究人员一直在仔细研究以高压或低温条件以外的形式用于汽车工业的氢储存。新出现的方法之一是使用含有金属氢化物和/或碳材料的粉状/颗粒状床,以利用“溢出”现象。处理和表征这种材料可能是麻烦的,这就是为什么实验设置需要仔细调查。在本文所构建的单元的基础上,成功地设计和描述了用于氢吸附/解吸特性分析的装置。该装置的全部功能包括给床加油以及检查吸附/解吸电位。此外,所提出的实验装置可以澄清进一步开发和优化储氢材料的许多不确定性。
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引用次数: 0
Development and performance test of a novel solar tracking sensor 一种新型太阳能跟踪传感器的研制与性能测试
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-08-28 DOI: 10.24425/mms.2023.144870
Jianjun Lan
A new solar tracking sensor based on image recognition is proposed and designed to solve the problem of low accuracy of photoelectric tracking in photovoltaic power generation. The sensor can directly output its angular deviation from the sun, and its mechanical structure and working principle are analysed in detail. We use a high-precision camera to collect the image of the two slots on the projector surface and use the Hough transform to identify the image of the light seam. After obtaining the linear equation for the two slots, the coordinate of the intersection point is found, and the calculation of the solar altitude and azimuth can be realized. We have improved the Hough transform scheme by using the skeleton image of the slots instead of the edge image. The improvement of the scheme has been proved to effectively improve the detection accuracy. A calibration test board is used to test the sensor and experimental results show that the scheme can achieve the measurement of azimuth and altitude with the accuracy of be 0.05 ° , which can meet the detection accuracy requirements of the solar tracking in photovoltaic power generation and many other photoelectric tracking implementations.
针对光伏发电中光电跟踪精度低的问题,提出并设计了一种基于图像识别的太阳能跟踪传感器。该传感器可以直接输出与太阳的角度偏差,并详细分析了其机械结构和工作原理。我们使用高精度摄像机采集投影仪表面两个槽的图像,并使用霍夫变换识别光缝的图像。得到两个槽的线性方程后,求出交点坐标,实现太阳高度和方位角的计算。我们改进了Hough变换方案,使用凹槽的骨架图像代替边缘图像。经实践证明,该方案的改进有效地提高了检测精度。利用标定测试板对传感器进行了测试,实验结果表明,该方案可以实现方位角和高度的测量,精度为0.05°,可以满足光伏发电等多种光电跟踪实现中太阳能跟踪的检测精度要求。
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引用次数: 0
Fabricated electromechanical resonator sensor for liquid viscosity measurement 用于液体粘度测量的装配式机电共振传感器
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-08-28 DOI: 10.24425/mms.2023.144868
Amin Eidi
The properties of a mechanical resonator provide a valuable ability to measure liquid density and viscosity. The viscosity of liquids is of interest to researchers in both industry and medicine. In this paper, a viscosity sensor for liquids is proposed, which is designed based on an electromechanical resonator. In the proposed sensor, a capacitor is used as an electrostatic actuator. The capacitor is also used to monitor the frequency changes of the proposed resonator. The range of displacement of the resonator and capacitor in response to different fluids under test varies according to their viscosity. The design of the proposed sensor and its electrostatic and mechanical simulations are reported in this paper. Also, the effect of viscosity of several different liquids on its performance has been analyzed and presented experimentally using a prototype.
机械谐振器的特性提供了测量液体密度和粘度的有价值的能力。液体的粘度引起了工业和医学研究人员的兴趣。本文提出了一种基于机电谐振器的液体粘度传感器。在所提出的传感器中,电容器被用作静电致动器。电容器还用于监测所提出的谐振器的频率变化。谐振器和电容器响应测试中不同流体的位移范围因其粘度而异。本文报道了所提出的传感器的设计及其静电和机械模拟。此外,还分析了几种不同液体的粘度对其性能的影响,并使用原型进行了实验。
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引用次数: 2
Accuracy of drying selected products using a moisture analyzer method based on infrared radiation 使用基于红外辐射的水分分析仪方法干燥选定产品的准确性
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-08-28 DOI: 10.24425/mms.2023.144873
Sławomir Janas, M. Kowalska
Trueness and precision of a method for determining the water content (%) of food and chemical products based on infrared radiation with a wavelength in the range (2 . 70 ÷ 7 . 21 μ m) was evaluated. The most accurate measurements for food products were obtained when the heat source was a radiant heater with a radiation wavelength of 7 . 21 μ m, a trueness deviation of 0.01%. When heated with radiation with wavelengths (from 3 . 32 μ m to 7 . 21 μ m), the trueness of the measurement ranged (0 . 03% ÷ 0 . 13%) for chemical products. The shortest analysis time for food products was found when the analysis was carried out using an IR source with a wavelength of 7 . 21 μ m, while for chemical products, a heat source with a wavelength of 2 . 70 ÷ 7 . 21 μ m was optimal. According to the results of the analysis, the use of IR radiation with a wavelength range of 3 . 32 ÷ 7 . 21 μ m is an alternative for accurate measurements.
评价了一种基于波长在(2.70÷7.21μm)范围内的红外辐射测定食品和化工产品含水量(%)的方法的真实性和准确性。当热源是辐射波长为7。21μm,准确度偏差为0.01%。当用波长为3.22μm至7.21μm的辐射加热时,化学产品的测量准确度范围为(0.03%÷0.13%)。当使用波长为7的IR源进行分析时,发现食品的分析时间最短。21μm,而对于化学产品,使用波长为2的热源。70÷7。μm为最佳。根据分析结果,利用红外辐射的波长范围为3。32÷7。21μm是精确测量的替代方案。
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引用次数: 0
An accurate and stable pose estimation method for planar cases considering the line constraints between every two points 一种考虑两点间线约束的平面情况下精确稳定的位姿估计方法
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-08-28 DOI: 10.24425/mms.2023.144871
Zimiao Zhang, Zhang Hao, Zhang Fumin, Shihai Zhang
The current solutions for pose estimation problems using coplanar feature points (PnP problems) can be divided into non-iterative and iterative solutions. The accuracy, stability, and efficiency of iterative methods are unsatisfactory. Therefore, non-iterative methods have become more popular. However, the non-iterative methods only consider the correspondence of the feature points with their 2D projections. They ignore the constraints formed between feature points. This results in lower pose estimation accuracy and stability. In this work, we proposed an accurate and stable pose estimation method considering the line constraints between every two feature points. Our method has two steps. In the first step, we solved the pose non-iteratively, considering the correspondence of the 3D feature points with their 2D projections and the line constraints formed by every two feature points. In the second step, the pose was refined by minimizing the re-projection errors with one iteration, further improving accuracy and stability. Simulation and actual experiment results show that our method’s accuracy, stability, and computational efficiency are better than the other existing pose estimation methods. In the − 45 ◦ to + 45 ◦ measuring range, the maximum angle measurement error is no more than 0 . 039 ◦ , and the average angle measurement error is no more than 0 . 016 ◦ . In the 0 mm to 30 mm measuring range, the maximum displacement measurement error is no more than 0.049 mm, and the average displacement measurement error is no more than 0.012 mm. Compared to other current pose estimation methods, our method is the most efficient based on guaranteeing measurement accuracy and stability.
目前基于共面特征点的位姿估计问题的解可分为非迭代解和迭代解。迭代法的精度、稳定性和效率都不理想。因此,非迭代方法变得越来越流行。而非迭代方法只考虑特征点与其二维投影的对应关系。它们忽略了特征点之间形成的约束。这导致姿态估计精度和稳定性降低。在这项工作中,我们提出了一种考虑每两个特征点之间的线约束的准确稳定的姿态估计方法。我们的方法有两个步骤。在第一步中,我们考虑三维特征点与其二维投影的对应关系以及每两个特征点形成的线约束,非迭代地求解姿态。第二步,通过一次迭代最小化重投影误差对姿态进行细化,进一步提高姿态精度和稳定性。仿真和实际实验结果表明,该方法的精度、稳定性和计算效率均优于现有的姿态估计方法。−45◦~ + 45◦测量范围内,最大角度测量误差不大于0。039◦,平均角度测量误差不大于0。016◦在0 mm ~ 30 mm测量范围内,最大位移测量误差不大于0.049 mm,平均位移测量误差不大于0.012 mm。与现有的姿态估计方法相比,该方法在保证测量精度和稳定性的基础上是最有效的。
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引用次数: 0
Testing of the delay time of wireless communication of CNC machine tools’ probes and controller 数控机床探头与控制器无线通信延迟时间的测试
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-07-20 DOI: 10.24425/119559
M. Jankowski, A. Woźniak
Touch-trigger probes for CNC milling machines usually use wireless communication in the radio or IR band. Additionally they enable triggering signal filtering in order to avoid false triggers of the probe. These solutions cause a delay in trigger signal transmission from the probe to the machine tool controller. This delay creates an additional pre-travel component, which is directly proportional to the measurement speed and which is the cause of a previously observed but not explained increase of the pre-travel with the increase of the measurement speed. In the paper, a method of testing the delay time of triggering signal is described, an example of delay time testing results is presented and the previous, unexplained results of other researchers are analysed in terms of signal transmission delay.
数控铣床的触摸触发探头通常使用无线电或红外波段的无线通信。此外,它们启用触发信号过滤,以避免探针的错误触发。这些解决方案导致从探针到机床控制器的触发信号传输延迟。该延迟产生了额外的预行程分量,该分量与测量速度成正比,并且是先前观察到但未解释的预行程随着测量速度的增加而增加的原因。本文介绍了一种测试触发信号延迟时间的方法,给出了延迟时间测试结果的一个例子,并从信号传输延迟的角度分析了以前其他研究人员无法解释的结果。
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引用次数: 1
A study on the calibration of an HPM meter based on a D-dot sensor and logarithmic RF power detector 基于d点传感器和对数射频功率检测器的HPM计标定研究
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-07-20 DOI: 10.24425/mms.2020.134846
J. Jakubowski
HPM meters are required for the assessment of fields generated by sources of high-power microwaves. Finding the inverse calibration curves for such instruments is important for ensuring accuracy. The procedure is relatively simple for meters consisting of linear devices but there can also be hardware solutions implementing nonlinear ones. The objective of the present work was to develop a convenient procedure to allow finding such a curve when the meter uses a D-dot probe and a power detector. For that purpose, the results of low voltage measurements describing the properties of the detector were first analysed. Then a software code was developed to estimate the RMS value of an incident field based on measured output and frequency response. The response was estimated with very low electric field. And finally, the performance of the proposed procedure was verified by tests conducted with high electric field in a TEM cell. High conformity of the output of the meter with fields of known values was demonstrated. The maximum error related to the meter range did not exceed 4%.
HPM计用于评估高功率微波源产生的场。找到这类仪器的反校准曲线对保证精度很重要。对于由线性器件组成的仪表,该过程相对简单,但也可以采用实现非线性器件的硬件解决方案。本工作的目的是开发一种方便的程序,允许在仪表使用d点探针和功率检测器时找到这样的曲线。为此,首先分析了描述探测器特性的低电压测量结果。然后开发了一个软件代码,根据测量输出和频率响应估计入射场的均方根值。用很低的电场估计了响应。最后,在TEM电池中进行了高电场测试,验证了该方法的性能。证明了该仪表的输出与已知值场的高度一致性。与仪表量程相关的最大误差不超过4%。
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引用次数: 1
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Metrology and Measurement Systems
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