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Characterization of laser-induced damage by picosecond pulses on multi-layer dielectric coatings for petawatt-class lasers 皮秒脉冲对多层介质涂层激光致损伤的表征
Pub Date : 2015-11-23 DOI: 10.1117/12.2195528
R. Negres, C. Carr, I. Bass, D. Alessi, T. Laurence, K. Stanion, G. Guss, D. Cross, P. Wegner, C. Stolz
We investigate the optical damage performance of multi-layer dielectric (MLD) coatings suitable for use in high energy, large-aperture petawatt-class lasers. We employ small-area damage test methodologies to evaluate the damage resistance of various coatings as a function of deposition methods and coating materials under simulated use conditions. In addition, we demonstrate that damage initiation by raster scanning at lower fluences and growth threshold testing are required to estimate large-aperture optics’ performance.
研究了适用于高能、大孔径千瓦级激光器的多层介质(MLD)涂层的光学损伤性能。在模拟使用条件下,我们采用小区域损伤测试方法来评估各种涂层的抗损伤性,作为沉积方法和涂层材料的函数。此外,我们还证明,在较低的影响下,需要光栅扫描和生长阈值测试来评估大孔径光学系统的性能。
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引用次数: 5
Scaling of laser-induced contamination growth at 266nm and 355nm 266nm和355nm激光诱导污染生长的标度
Pub Date : 2015-11-23 DOI: 10.1117/12.2194083
M. Liessmann, L. Jensen, I. Balasa, M. Hunnekuhl, A. Büttner, P. Wessels, J. Neumann, D. Ristau
The growth of laser-induced contamination (LIC) on optical components in extraterrestrial missions is a known issue especially for the UV spectral region. The Laser Zentrum Hannover e.V. is responsible for the development of a pulsed laser-system operating at a wavelength of 266 nm for the ExoMars mission and for the qualification of used optics and materials regarding LIC. In this context, toluene was utilized which is an often used model contaminant in LIC studies. Test cycles based on the application of the two UV wavelengths 355 nm and 266 nm on fused silica substrates and ARcoated optics are conducted and the observed contamination effects are compared. This scaling allows for a rough estimate of the destructive influence of LIC on space optics degradation at 266 nm. Further tests will be performed with materials integrated into the ExoMars-laser-head under near-operation environmental conditions.
在地外任务中,光学元件的激光诱导污染(LIC)的增长是一个众所周知的问题,特别是在紫外光谱区域。汉诺威激光中心(Laser Zentrum Hannover e.V.)负责为ExoMars任务开发波长为266纳米的脉冲激光系统,并对使用过的光学器件和材料进行LIC认证。在这种情况下,使用了甲苯,这是在LIC研究中经常使用的模型污染物。将355nm和266nm两种紫外波长分别应用于熔融二氧化硅基片和ararcoated光学器件上进行了测试循环,并比较了观察到的污染效应。这种缩放可以粗略估计在266nm处LIC对空间光学退化的破坏性影响。在接近操作的环境条件下,将对集成到exomars -激光头中的材料进行进一步的测试。
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引用次数: 7
Laser damage resistance of optical components in sub-picosecond regime in the infrared 红外亚皮秒区光学元件的抗激光损伤性能
Pub Date : 2015-11-23 DOI: 10.1117/12.2194286
M. Sozet, J. Néauport, E. Lavastre, N. Roquin, L. Gallais, L. Lamaignère
A rasterscan procedure is set to determine laser-induced damage densities in sub-picosecond regime at 1053nm on high-reflective coatings. Whereas laser-induced damage is usually considered deterministic in this regime, damage events occur on these structures for fluences lower than their intrinsic Laser-Induced Damage Threshold (LIDT). Damage densities are found to be high even for fluences as low as 20% of the LIDT. Scanning Electron Microscope observations of these “under threshold” damage sites evidence ejections of defects, embedded in the dielectric stack. It brings a new viewpoint for the qualification of optical components and for the optimization of manufacturing processes of coatings.
采用光栅扫描程序确定高反射涂层在1053nm处亚皮秒范围内的激光损伤密度。然而,在这种情况下,激光诱导损伤通常被认为是确定性的,损伤事件发生在这些结构上的影响低于其固有的激光诱导损伤阈值(LIDT)。发现即使影响低至LIDT的20%,损伤密度也很高。扫描电子显微镜观察到的这些“阈值以下”的损伤部位证明了嵌入在电介质堆栈中的缺陷的弹射。这为光学元件的质量鉴定和镀膜工艺的优化提供了新的视角。
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引用次数: 0
Analysis of cumulative versus ISO-recommended calculation of damage probability using a database of real S-on-1 tests 使用实际S-on-1试验数据库对累积与iso推荐的损伤概率计算进行分析
Pub Date : 2015-11-23 DOI: 10.1117/12.2194303
A. Zorila, A. Stratan, I. Dumitrache, L. Rusen, G. Nemeş
Data collected in real S-on-1 LIDT experiments performed with a nanosecond, 1064 nm automated station are used to calculate the damage probability with the ISO-recommended (conventional) method and the recently-suggested cumulative method. The damage probability points versus fluence for each type of calculation are fitted using both, linear and nonlinear curves. The resultant four data sets corresponding to each real experiment are used to compare important parameters as: statistical uncertainty of damage probability points, fitting errors, damage threshold fluences for actual number of pulses, and the extrapolated threshold fluences for very large number of pulses. We suggest and analyze also a limit case of the cumulative method, when the damage probability points are calculated for each interrogated site. Both, the recently-suggested cumulative method, and our limit case, look very promising.
利用在纳秒1064 nm自动站进行的实际S-on-1 LIDT实验中收集的数据,采用iso推荐的(传统)方法和最近提出的累积方法计算损伤概率。用线性曲线和非线性曲线拟合了每种计算类型的损伤概率点与影响的关系。每个实际实验对应的四个数据集用于比较损伤概率点的统计不确定性、拟合误差、实际脉冲数的损伤阈值影响以及非常大脉冲数的外推阈值影响等重要参数。我们还提出并分析了累积法的一种极限情况,即计算每个被询问部位的损伤概率点。最近提出的累积法和我们的极限情况看起来都很有前途。
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引用次数: 2
Improved parametric spectroscopic performance of an optical fiber doped with erbium 掺铒光纤参数光谱性能的改进
Pub Date : 2015-11-23 DOI: 10.1117/12.2194077
M. Ghoumazi, N. Demagh, A. Adouane, B. Boubir, A. Daoui
In recent years, the rare earth ions and primarily Er played a crucial role in the development of the technology of optical telecommunications. The Emission of erbium ions at 1.53 microns is important for optical telecommunications because this emission corresponds to minimum mitigation of silica fibers which used as purpose to transport information. At first, we study the evolution of the signal powers and the pump powers along the propagation in the optical fiber amplifier Erbium doped. In addition, we study the variation of Erbium ions concentration for different spectroscopic parameters such as signal strength with (0, 1μW, 1mW) and the power of the pump going up 200 mW.
近年来,稀土离子(主要是铒)在光通信技术的发展中发挥了至关重要的作用。铒离子在1.53微米的发射对光通信很重要,因为这种发射对应于用于传输信息的硅纤维的最小减缓。首先,我们研究了掺铒光纤放大器中信号功率和泵浦光功率在传输过程中的演化规律。此外,我们还研究了信号强度为(0、1μW、1mW)和泵浦功率达到200 mW时不同光谱参数下铒离子浓度的变化。
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引用次数: 0
Calculation of nonlinear optical damage from space-time-tailored pulses in dielectrics 介质中时空定制脉冲非线性光学损伤的计算
Pub Date : 2015-11-23 DOI: 10.1117/12.2195299
T. Lanier, J. Gulley
Control of the time duration of a laser pulse as it focuses spatially in a material provides a means for delaying the onset of nonlinear effects during propagation. We investigate simultaneous space-time focusing (SSTF) of femtosecond radially-chirped annular pulses in Kerr dielectrics. The energy and temporal chirp of pulses incident upon a grating-grating-lens system are varied in simulations that solve the unidirectional pulse propagation equation. This system is modeled by inserting transformations that act on the electric field obtained from propagation from one component to the next. The propagation is coupled to the time evolution of the free charge density as a function of space. The resulting “ionization tracks” are taken as a metric for predicting material modification and/or damage in bulk fused silica. As expected from linear-optical considerations, the temporal pre-chirp determines the overall pulse duration as the focusing annulus closes. We find in addition that, for a given pulse energy, the temporal pre-chirp also determines the on-axis intensity distribution as energy collapses onto the propagation axis. This effect determines how the local ionization-induced decrease in refractive index shifts energy in time relative to energy arriving on-axis from the spatially collapsing beam. The magnitude of the pre-chirp can thus control the spatial structure of ionization that may lead to material modification and/or damage.
控制激光脉冲在材料中的空间聚焦时的持续时间提供了一种延迟传播过程中非线性效应发生的手段。研究了飞秒径向啁啾环形脉冲在克尔介质中的同步时空聚焦(SSTF)特性。在求解脉冲单向传播方程的仿真中,入射到光栅-光栅-透镜系统的脉冲的能量和时间啁啾是不同的。该系统通过插入作用于从一个分量传播到下一个分量的电场的变换来建模。该传播与自由电荷密度随时间的演化作为空间的函数相耦合。由此产生的“电离轨迹”被用作预测材料改性和/或块状熔融二氧化硅损伤的度量。正如线性光学考虑所期望的那样,时间预啁啾决定了聚焦环闭合时的总脉冲持续时间。此外,我们发现,对于给定的脉冲能量,时间预啁啾也决定了能量坍缩到传播轴上时的轴上强度分布。这一效应决定了局部电离引起的折射率下降如何在时间上转移能量,相对于从空间坍缩光束到达轴上的能量。因此,预啁啾的大小可以控制可能导致材料修饰和/或损坏的电离的空间结构。
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引用次数: 1
Measurement and compensation of wavefront deformations and focal shifts in high-power laser optics 高功率激光光学中波前变形和焦移的测量与补偿
Pub Date : 2015-11-23 DOI: 10.1117/12.2196160
Klaus Mann, B. Schäfer, M. Stubenvoll, K. Hentschel, M. Zenz
We demonstrate the feasibility of passive compensation of the thermal lens effect in fused silica optics, placing suitable optical materials with negative dn/dT in the beam path of a high power near IR fiber laser. Following a brief overview of the involved mechanisms, photo-thermal absorption measurements with a Hartmann-Shack sensor are described, from which coefficients for surface/coating and bulk absorption in various materials are determined. Based on comprehensive knowledge of the 2D wavefront deformations resulting from absorption, passive compensation of thermally induced aberrations in complex optical systems is possible, as illustrated for an F-Theta objective. By means of caustic measurements during high-power operation we are able to demonstrate a 60% reduction of the focal shift in F-Theta lenses through passive compensation.
通过在高功率近红外光纤激光器的光束路径中放置合适的dn/dT为负的光学材料,证明了在熔融石英光学中无源补偿热透镜效应的可行性。在简要概述所涉及的机制之后,描述了使用哈特曼-夏克传感器进行光热吸收测量,由此确定了各种材料的表面/涂层和体吸收系数。基于对由吸收引起的二维波前变形的全面了解,复杂光学系统中热致像差的被动补偿是可能的,如F-Theta物镜所示。通过高功率操作期间的苛性测量,我们能够通过被动补偿证明F-Theta透镜的焦移减少60%。
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引用次数: 3
Improved laser damage threshold performance of calcium fluoride optical surfaces via Accelerated Neutral Atom Beam (ANAB) processing 通过加速中性原子束(ANAB)处理提高氟化钙光学表面激光损伤阈值性能
Pub Date : 2015-11-23 DOI: 10.1117/12.2196545
S. Kirkpatrick, M. Walsh, R. Svrluga, M. Thomas
Optics are not keeping up with the pace of laser advancements. The laser industry is rapidly increasing its power capabilities and reducing wavelengths which have exposed the optics as a weak link in lifetime failures for these advanced systems. Nanometer sized surface defects (scratches, pits, bumps and residual particles) on the surface of optics are a significant limiting factor to high end performance. Angstrom level smoothing of materials such as calcium fluoride, spinel, magnesium fluoride, zinc sulfide, LBO and others presents a unique challenge for traditional polishing techniques. Exogenesis Corporation, using its new and proprietary Accelerated Neutral Atom Beam (ANAB) technology, is able to remove nano-scale surface damage and particle contamination leaving many material surfaces with roughness typically around one Angstrom. This surface defect mitigation via ANAB processing can be shown to increase performance properties of high intensity optical materials. This paper describes the ANAB technology and summarizes smoothing results for calcium fluoride laser windows. It further correlates laser damage threshold improvements with the smoothing produced by ANAB surface treatment. All ANAB processing was performed at Exogenesis Corporation using an nAccel100TM Accelerated Particle Beam processing tool. All surface measurement data for the paper was produced via AFM analysis on a Park Model XE70 AFM, and all laser damage testing was performed at Spica Technologies, Inc. Exogenesis Corporation’s ANAB processing technology is a new and unique surface modification technique that has demonstrated to be highly effective at correcting nano-scale surface defects. ANAB is a non-contact vacuum process comprised of an intense beam of accelerated, electrically neutral gas atoms with average energies of a few tens of electron volts. The ANAB process does not apply mechanical forces associated with traditional polishing techniques. ANAB efficiently removes surface contaminants, nano-scale scratches, bumps, particles and other asperities under low energy physical sputtering conditions. ANAB may be used to remove a precisely controlled, uniform thickness of material without any increase of surface roughness, regardless of the total amount of material removed. The ANAB process does not involve the use of slurries or other abrasive polishing compounds and therefore does not require any post process cleaning. ANAB can be integrated as an in-situ surface preparation method for other process steps in the uninterrupted fabrication of optical devices.
光学没有跟上激光的发展步伐。激光工业正在迅速提高其功率能力和减少波长,这暴露了光学器件作为这些先进系统寿命失效的薄弱环节。光学器件表面的纳米级表面缺陷(划痕、凹坑、凹凸和残余颗粒)是影响其高端性能的重要限制因素。氟化钙、尖晶石、氟化镁、硫化锌、LBO等材料的埃级平滑对传统抛光技术提出了独特的挑战。Exogenesis公司使用其专有的加速中性原子束(ANAB)技术,能够去除纳米级表面损伤和颗粒污染,使许多材料表面粗糙度通常在1埃左右。这种通过ANAB处理的表面缺陷缓解可以提高高强度光学材料的性能。本文介绍了ANAB技术,总结了氟化钙激光窗的平滑效果。它进一步将激光损伤阈值的改善与ANAB表面处理产生的平滑联系起来。所有ANAB处理均在Exogenesis Corporation使用nAccel100TM加速粒子束处理工具进行。论文的所有表面测量数据都是通过在Park型号XE70 AFM上进行AFM分析产生的,所有激光损伤测试都是在Spica Technologies公司进行的。Exogenesis公司的ANAB加工技术是一种新的、独特的表面改性技术,已被证明在纠正纳米级表面缺陷方面非常有效。ANAB是一种非接触真空过程,由一束加速的、平均能量为几十电子伏特的电中性气体原子组成。ANAB工艺不应用与传统抛光技术相关的机械力。ANAB在低能量物理溅射条件下有效去除表面污染物、纳米级划痕、凹凸、颗粒和其他凹凸。ANAB可用于去除精确控制的均匀材料厚度,而不增加表面粗糙度,无论去除的材料总量如何。ANAB工艺不涉及使用浆料或其他研磨抛光化合物,因此不需要任何后处理清洁。ANAB可以作为一种原位表面制备方法集成到光学器件的不间断制造的其他工艺步骤中。
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引用次数: 2
Analysis of energy deposition and damage mechanisms in single layers of HfO2 and Nb2O5 submitted to 500fs pulses 500fs脉冲下HfO2和Nb2O5单层能量沉积及损伤机理分析
Pub Date : 2015-11-23 DOI: 10.1117/12.2195005
Dam-be Douti, M. Chrayteh, S. Monneret, M. Commandré, L. Gallais
Laser Induced Damage Thresholds and morphologies of damage sites on thin films samples irradiated by sub-ps pulses are studied based on experimental and numerical studies. Experiments are conducted with 500fs pulses at 1030nm and 343nm and the irradiated sites are analyzed with phase imaging, AFM and SEM. The results are compared to simulations of energy deposition in the films based on the Single Rate Equation taking account transient optical properties of the films. Results suggest that a critical absorbed energy as a damage criterion give consistent results both with the measured LIDT and the observed damage morphologies.
在实验和数值研究的基础上,对亚ps脉冲辐照下薄膜样品的激光损伤阈值和损伤部位形貌进行了研究。实验采用500fs脉冲在1030nm和343nm处进行,用相位成像、原子力显微镜和扫描电镜对辐照部位进行了分析。将所得结果与考虑薄膜瞬态光学特性的基于单速率方程的薄膜能量沉积模拟结果进行了比较。结果表明,临界吸收能作为损伤判据,其结果与实测的LIDT和观察到的损伤形态相一致。
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引用次数: 0
Morphology of ejected debris from laser super-heated fused silica following exit surface laser-induced damage 激光过热熔融二氧化硅出口表面激光损伤后喷射碎片的形貌
Pub Date : 2015-11-23 DOI: 10.1117/12.2195501
S. Demos, R. Negres, R. Raman, M. Feit, K. Manes, A. Rubenchik
Laser induced damage (breakdown) initiated on the exit surface of transparent dielectric materials using nanosecond pulses creates a volume of superheated material reaching localized temperatures on the order of 1 eV and pressures on the order of 10 GPa or larger. This leads to material ejection and the formation of a crater. The volume of this superheated material depends largely on the laser parameters such as fluence and pulse duration. To elucidate the material behaviors involved, we examined the morphologies of the ejected superheated material particles and found distinctive morphologies. We hypothesize that these morphologies arise from the difference in the structure and physical properties (such as the dynamic viscosity and presence of instabilities) of the superheated material at the time of ejection of each individual particle. Some of the ejected particles are on the order of 1 µm in diameter and appear as “droplets”. Another subgroup appears to have stretched, foam-like structure that can be described as material globules interconnected via smaller in diameter columns. Such particles often contain nanometer size fibers attached on their surface. In other cases, only the globules have been preserved suggesting that they may be associated with a collapsed foam structure under the dynamic pressure as it traverses in air. These distinct features originate in the structure of the superheated material during volume boiling just prior to the ejection of the particles.
利用纳秒脉冲在透明介质材料的出口表面引发激光诱导损伤(击穿),使材料体积过热,局部温度达到1 eV,压力达到10 GPa或更大。这导致了物质的喷射和陨石坑的形成。这种过热材料的体积在很大程度上取决于激光的参数,如能量流和脉冲持续时间。为了阐明所涉及的材料行为,我们检查了喷出的过热材料颗粒的形态,并发现了独特的形态。我们假设这些形态是由每个粒子喷射时过热材料的结构和物理性质(如动态粘度和不稳定性)的差异引起的。喷射出的一些颗粒直径约为1 μ m,呈“液滴”状。另一个亚群似乎具有拉伸的泡沫状结构,可以将其描述为通过直径较小的柱相互连接的材料球体。这种颗粒表面通常含有纳米大小的纤维。在其他情况下,只有小球体被保存下来,这表明它们可能与泡沫结构在空气中移动时受到动压而坍塌有关。这些明显的特征源于在颗粒喷射之前的体积沸腾期间过热材料的结构。
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引用次数: 1
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SPIE Laser Damage
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