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Direct absorption measurements in thin rods and optical fibers 细棒和光纤的直接吸收测量
Pub Date : 2015-11-23 DOI: 10.1117/12.2192579
C. Mühlig, S. Bublitz, M. Lorenz
We report on the first realization of direct absorption measurements in thin rods and optical fibers using the laser induced deflection (LID) technique. Typically, along the fiber processing chain more or less technology steps are able to introduce additional losses to the starting material. After the final processing, the fibers are commonly characterized regarding losses using the so-called cut-back technique in combination with spectrometers. This, however, only serves for a total loss determination. For optimization of the fiber processing, it would be of great interest to not only distinguish between different loss mechanisms but also have a better understanding of possible causes. For measuring the absorption losses along the fiber processing, a particular concept for the LID technique is introduced and requirements, calibration procedure as well as first results are presented. It allows to measure thin rods, e.g. during preform manufacturing, as well as optical fibers. In addition, the results show the prospects to also apply the new concept to topics like characterizing unwanted absorption after fiber splicing or Bragg grating inscription.
我们报道了利用激光诱导偏转(LID)技术在细棒和光纤中首次实现直接吸收测量。通常,沿着纤维加工链或多或少的技术步骤会给起始材料带来额外的损失。在最后的处理之后,通常使用所谓的回切技术与光谱仪结合来表征光纤的损耗。然而,这只适用于总损失的确定。为了优化光纤的加工,不仅要区分不同的损耗机制,而且要更好地了解可能的原因。为了测量光纤加工过程中的吸收损耗,介绍了LID技术的概念,并给出了要求、校准过程和初步结果。它允许测量细棒,例如在预制件制造过程中,以及光纤。此外,结果还显示了将新概念应用于光纤拼接或布拉格光栅刻字后的非期望吸收表征等主题的前景。
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引用次数: 0
Energetic laser cleaning of metallic particles and surface damage on silica optics: investigation of the underlying mechanisms 金属颗粒的高能激光清洗和二氧化硅光学表面损伤:潜在机制的研究
Pub Date : 2015-11-23 DOI: 10.1117/12.2195593
N. Shen, S. Demos, R. Negres, A. Rubenchik, C. Harris, M. Matthews
Surface particulate contamination on optics can lead to laser-induced damage hence limit the performance of high power laser system. In this work we focus on understanding the fundamental mechanisms that lead to damage initiation by metal contaminants. Using time resolved microscopy and plasma spectroscopy, we studied the dynamic process of ejecting ~30 μm stainless steel particles from the exit surface of fused silica substrate irradiated with 1064 nm, 10 ns and 355 nm, 8 ns laser pulses. Time-resolved plasma emission spectroscopy was used to characterize the energy coupling and temperature rise associated with single, 10-ns pulsed laser ablation of metallic particles bound to transparent substrates. Plasma associated with Fe(I) emission lines originating from steel microspheres was observe to cool from <24,000 K to ~15,000 K over ~220 ns as τ-0.22, consistent with radiative losses and adiabatic gas expansion of a relatively free plasma. Simultaneous emission lines from Si(II) associated with the plasma etching of the SiO2 substrate were observed yielding higher plasma temperatures, ~35,000 K, relative to the Fe(I) plasma. The difference in species temperatures is consistent with plasma confinement at the microsphere-substrate interface as the particle is ejected, and is directly visualized using pump-probe shadowgraphy as a function of pulsed laser energy.
光学元件表面颗粒污染会导致激光损伤,从而限制了高功率激光系统的性能。在这项工作中,我们的重点是了解导致金属污染物引发损伤的基本机制。利用时间分辨显微镜和等离子体光谱技术,研究了1064 nm (10 ns)和3555 nm (8 ns)激光脉冲辐照下,熔融石英衬底出口表面喷射出~30 μm不锈钢颗粒的动态过程。利用时间分辨等离子体发射光谱研究了单次10ns脉冲激光烧蚀与透明基底结合的金属颗粒的能量耦合和温升。观察到与铁(I)发射线相关的等离子体在~220 ns内从< 24000 K冷却到~ 15000 K, τ-0.22与相对自由等离子体的辐射损失和绝热气体膨胀一致。与Fe(I)等离子体相比,Si(II)等离子体腐蚀SiO2衬底的同时发射线产生了更高的等离子体温度,约35000 K。当粒子喷射时,物质温度的差异与微球-衬底界面上的等离子体约束一致,并且可以使用泵浦探针阴影成像作为脉冲激光能量的函数直接可视化。
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引用次数: 2
Laser damage threshold: useful idea or dangerous misconception? 激光损伤阈值:有用的想法还是危险的误解?
Pub Date : 2015-11-23 DOI: 10.1117/12.2195271
J. Arenberg
The concept of a laser damage threshold as a safe operating level is both useful and confounding. This paper examines and analyzes the power of the concept of a laser damage threshold, identifying the good and the danger in its use. The history of the definition and concept of the laser damage threshold is traced from the earliest days of the laser through to the present day. Criteria for an accurate threshold measurement are presented and distribution of the weakest site on an optic is derived to provide a basis of analysis. Using a pedagogically selected defect distribution, the statistics of the weakest site are derived. The dependence of the weakest site on the area of the test is shown explicitly. It is argued that typical small area tests, characteristic of most main stream damage tests have insufficient area to include the true weakest site, and are therefore generally inaccurate. The paper concludes with some ideas on how to redefine the threshold measurement technique resulting in a more accurate test procedure.
激光损伤阈值作为安全操作水平的概念既有用又令人困惑。本文对激光损伤阈值的概念进行了检验和分析,指出了激光损伤阈值在使用中的好处和危险。激光损伤阈值的定义和概念的历史可以追溯到最早的激光时代,直到今天。提出了精确阈值测量的标准,并推导了光学器件上最弱点的分布,为分析提供了基础。利用教学方法选择的缺陷分布,得出了最薄弱部位的统计数据。最弱部位对试验面积的依赖性得到了明确的显示。有人认为,典型的小区域试验,即大多数主流损伤试验的特点,没有足够的面积包括真正最薄弱的部位,因此通常是不准确的。最后,对如何重新定义阈值测量技术,以获得更准确的测试程序提出了一些看法。
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引用次数: 2
Ultrafast beam dump materials and mirror coatings tested with the ELI beamlines LIDT test station 用ELI光束线LIDT测试站测试了超快光束转储材料和反射镜涂层
Pub Date : 2015-11-23 DOI: 10.1117/12.2194970
M. Ďurák, D. Kramer, P. Velpula, J. Cupal, T. Medřík, J. Hrebicek, J. Golasowski, D. Peceli, L. Fekete, V. Stepan, M. Kozlová, B. Rus
The ELI Beamlines project will deliver ultrafast laser pulses with peak powers up to 10PW available every minute and PW class beams at 10Hz complemented by a 10TW 1kHz beamline. To properly determine damage thresholds of involved optical components in conditions similar to the operational environment and with expected laser parameters, a high vacuum LIDT test station was constructed at PALS facility. Our study presents results of ISO based S-on-1 and R-on-1 tests in femtosecond regime (50fs, 800nm, 10Hz/1kHz) performed on two different types of coatings: a) highabsorption black coatings with low outgassing rates, intended for use as a beam dump surface; and b) high-reflectivity, low-dispersion 45° AOI ultrafast mirror coatings. Testing of absorptive coatings was accompanied with QMS residual gas analysis to verify, that high intensity laser radiation approaching the damage threshold does not increase concentration of volatile organic compounds in the vacuum chamber. In case of HR mirror coatings, we also investigate the effect of cleaning on LIDT value, comparing characteristic S-on-1 curves of given sample with values obtained after 12h immersion in ethanol-water solution.
ELI光束线项目将提供峰值功率高达每分钟10PW的超快激光脉冲和10Hz的PW级光束,并辅以10TW的1kHz光束线。为了在接近操作环境和预期激光参数的条件下正确确定相关光学元件的损伤阈值,在PALS设施建立了高真空LIDT试验站。我们的研究展示了基于ISO的S-on-1和R-on-1在飞秒范围内(50fs, 800nm, 10Hz/1kHz)对两种不同类型的涂层进行的测试结果:a)具有低放气率的高吸收率黑色涂层,用于光束卸载表面;b)高反射率、低色散45°AOI超快反射镜涂层。对吸收涂层进行测试,并结合QMS残余气体分析验证,接近损伤阈值的高强度激光辐射不会增加真空室中挥发性有机化合物的浓度。对于HR镜面涂层,我们还研究了清洗对LIDT值的影响,将给定样品的特征S-on-1曲线与在乙醇水溶液中浸泡12h后获得的值进行了比较。
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引用次数: 3
Tunable laser source based on storage device using Bragg grating 基于Bragg光栅存储装置的可调谐激光源
Pub Date : 2015-11-23 DOI: 10.1117/12.2197183
Chinmayee V Prabhu Dessai, I. Reddy, S. Parne, G. R. Reddy
Tunable LASER source is a device which emits a particular light wavelength based on the tuning done. The tuning depends on certain characteristic of the LASER source which makes it customised within a gamut of wavelengths. Most Conventional LASER sources in the market are bulky and complex. The Tunable LASER source designed is established on the simple idea that Optical Amplifier can act as a broadband source, and temperature and strain sensitive Fiber Bragg Grating can be used to filter the required wavelength. This makes the design very light and elementary.
可调谐激光光源是一种基于调谐而发出特定波长光的装置。调谐取决于激光源的某些特性,使其在波长范围内定制。市场上大多数传统的激光光源体积庞大,结构复杂。所设计的可调谐激光源是建立在光放大器作为宽带源的简单思想上的,温度和应变敏感的光纤布拉格光栅可以过滤所需的波长。这使得设计非常轻和基本。
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引用次数: 0
Comparative STEREO-LID (Spatio-TEmporally REsolved Optical Laser-Induced Damage) studies of critical defect distributions in IBS, ALD, and electron-beam coated dielectric films 比较STEREO-LID(时空分辨光学激光诱导损伤)研究IBS、ALD和电子束镀膜介质薄膜的临界缺陷分布
Pub Date : 2015-11-23 DOI: 10.1117/12.2196548
Yejia Xu, A. Khabbazi, T. Day, A. Brown, L. Emmert, J. Talghader, E. Field, D. Kletecka, J. Bellum, D. Patel, C. Menoni, W. Rudolph
The laser damage behavior of high quality coatings under nanosecond pulse illumination is controlled by statistically distributed defects, whose physical nature and defect mechanisms are still largely unknown. Defect densities are often retrieved by modeling the fluence dependence of the damage probability measured by traditional damage test (TDT) methods, based on ‘damage’ or ‘no damage’ observations. STEREO-LID (Spatio-TEmporally REsolved Optical LaserInduced Damage) allows the determination of the damage fluence (and intensity) in a single test by identifying the initiation of damage both temporally and spatially. The advantages of this test method over the TDT are discussed. In particular, its ability to retrieve detailed defect distribution functions is demonstrated by comparison of results from HfO2 films prepared by ion-assisted electron beam evaporation, ion-beam sputtering, and atomic layer deposition.
高质量涂层在纳秒脉冲照射下的激光损伤行为是由统计分布缺陷控制的,这些缺陷的物理性质和缺陷机制在很大程度上仍然是未知的。缺陷密度通常通过对传统损伤试验(TDT)方法测量的损伤概率的影响依赖性建模来检索,该方法基于“损伤”或“无损伤”观察结果。STEREO-LID(时空分辨光学激光诱导损伤)通过识别时间和空间上的损伤起始,允许在一次测试中确定损伤影响(和强度)。讨论了该测试方法相对于TDT的优点。特别是,通过比较离子辅助电子束蒸发、离子束溅射和原子层沉积制备的HfO2薄膜的结果,证明了其检索详细缺陷分布函数的能力。
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引用次数: 0
How reduced vacuum pumping capability in a coating chamber affects the laser damage resistance of HfO2/SiO2 antireflection and high-reflection coatings 涂层腔内真空度的降低如何影响HfO2/SiO2增透和高反射涂层的激光损伤抗力
Pub Date : 2015-11-23 DOI: 10.1117/12.2194131
E. Field, J. Bellum, D. Kletecka
Optical coatings with the highest laser damage thresholds rely on clean conditions in the vacuum chamber during the coating deposition process. A low base pressure in the coating chamber, as well as the ability of the vacuum system to maintain the required pressure during deposition, are important aspects of limiting the amount of defects in an optical coating that could induce laser damage. Our large optics coating chamber at Sandia National Laboratories normally relies on three cryo pumps to maintain low pressures for e-beam coating processes. However, on occasion, one or more of the cryo pumps have been out of commission. In light of this circumstance, we decided to explore how deposition under compromised vacuum conditions resulting from the use of only one or two cryo pumps affects the laser-induced damage thresholds of optical coatings. The coatings of this study consist of HfO2 and SiO2 layer materials and include antireflection coatings for 527 nm at normal incidence, and high reflection coatings for 527 nm, 45° angle of incidence (AOI), in P-polarization (P-pol).
具有最高激光损伤阈值的光学涂层依赖于涂层沉积过程中真空室的清洁条件。镀膜腔内的低底压以及真空系统在沉积过程中保持所需压力的能力是限制光学镀膜中可能引起激光损伤的缺陷数量的重要方面。我们在桑迪亚国家实验室的大型光学镀膜室通常依靠三个低温泵来维持电子束镀膜过程的低压。然而,有时,一个或多个低温泵已经停止使用。鉴于这种情况,我们决定探索仅使用一个或两个冷冻泵导致的受损真空条件下的沉积如何影响激光诱导光学涂层的损伤阈值。本研究的涂层由HfO2和SiO2层材料组成,包括527 nm的法向增透涂层和45°入射角(AOI)的p偏振(P-pol) 527 nm的高反射涂层。
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引用次数: 2
Study of laser-induced damage at 1064nm in fused silica samples in vacuum environment 真空环境下熔融石英样品1064nm激光致损伤研究
Pub Date : 2015-11-23 DOI: 10.1117/12.2195471
R. Diaz, M. Chambonneau, P. Grua, J. Rullier, J. Natoli, L. Lamaignère
The influence of vacuum on nanosecond laser-induced damage at the exit surface of fused silica components is investigated at 1064 nm. In the present study, as previously observed in air, ring patterns surrounding laserinduced damage sites are systematically observed on a plane surface when initiated by multiple longitudinal modes laser pulses. Compared to air, the printed pattern is clearly more concentrated. The obtained correlation between the damage morphology and the temporal structure of the pulses suggests a laser-driven ablation mechanism resulting in a thorough imprint of energy deposit. The ablation process is assumed to be subsequent to an activation of the surface by hot electrons related to the diffusive expansion of a plasma formed from silica. This interpretation is strongly reinforced with additional experiments performed on an optical grating in vacuum on which damage sites do not show any ring pattern. Qualitatively, in vacuum, the intensity-dependent ring appearance speed V ∝ I1/2 is shown to be different than in air where V ∝ I1/3 . This demonstrates that the mechanisms of formation of ring patterns are different in vacuum than in air. Moreover, the mechanism responsible of the propagation of the activation front in vacuum is shown to be outdone when experiments are performed in air.
在1064 nm处研究了真空对熔融石英组件出口表面纳秒激光损伤的影响。在本研究中,正如先前在空气中观察到的那样,当多个纵向模式激光脉冲引发时,在平面表面上系统地观察到激光诱导损伤部位周围的环状图案。与空气相比,印刷的图案明显更集中。得到的损伤形态与脉冲时间结构之间的相关性表明,激光驱动的烧蚀机制导致能量沉积的彻底印记。烧蚀过程被认为是由二氧化硅形成的等离子体的扩散膨胀引起的热电子对表面的激活。在真空中对光学光栅进行的额外实验有力地加强了这一解释,在该实验中,损坏部位没有显示出任何环状图案。定性地说,在真空中,与强度相关的环出现速度V∝I1/2不同于在空气中,V∝I1/3。这表明在真空中环形图案的形成机制与在空气中不同。此外,在空气中进行的实验表明,真空中激活锋传播的机制是不完善的。
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引用次数: 0
Transmittance measurements of laser components using a combination of cavity ring-down and photometry 结合腔衰荡和光度法测量激光元件的透光率
Pub Date : 2015-11-23 DOI: 10.1117/12.2197779
H. Cui, Y. Han, C. Gao, Y. Wang, B. Li
A combined cavity ring-down (CRD) and photometry technique is employed to measure the transmittance of optical laser components in a range extending from below 0.01% to over 99.99%. In this combined technique, the conventional photometric configuration is used to measure, by ratioing the transmitted light power to the input power, the transmittance ranging from below 0.01% to over 99% with a typical relative uncertainty below 0.3%, and the CRD configuration is used to measure the transmittance higher than 99% with an uncertainty below 0.01%. Eight test samples with transmittance in the range of nearly 99.99% to approximately 0.013% are experimentally measured. Uncertainties of approximately 0.0001% for the transmittance of 99.9877% and of 0.003% for the transmittance of 0.013% are achieved with respectively the CRD and photometric schemes of a simple experimental apparatus. The experimental results showed that the combined technique is capable of measuring the transmittance of any practically fabricated optical laser components.
采用腔衰荡(CRD)和光度测量相结合的方法,测量了激光光学元件在0.01%到99.99%以上范围内的透射率。在该组合技术中,采用传统的光度测量配置,通过透射光功率与输入功率的比值,测量从0.01%到99%以上的透光率,典型的相对不确定度小于0.3%;采用CRD配置,测量高于99%的透光率,典型的相对不确定度小于0.01%。实验测量了透光率在99.99% ~ 0.013%之间的8种样品。采用简单实验装置的CRD方案和光度方案,在透过率为99.987%和0.013%的情况下,不确定度分别为0.0001%和0.003%。实验结果表明,该组合技术能够测量任何实际制造的光学激光元件的透射率。
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引用次数: 1
Multipulse degradation of fused silica surfaces at 351 nm 熔融二氧化硅表面在351nm处的多脉冲降解
Pub Date : 2015-11-23 DOI: 10.1117/12.2195595
S. Ly, T. Laurence, N. Shen, B. Hollingsworth, M. Norton, J. Bude
We investigate the multipulse degradation of fused silica surfaces exposed at 351 nm for up to 109 pulses at pulse fluences greater than 10 J/cm2. In vacuum, the transmission loss increases as a function of the number of shots at low pulse intensity. However, as the pulse intensity increases, the transmission loss decreases and is not measureable above a certain intensity. Transmission loss is highest when measured at shorter wavelengths, and decreases towards the IR. Absorption is the primary mechanism that leads to transmission loss and is from photo-reduction of the silica surface.
我们研究了暴露在351nm下的熔融二氧化硅表面的多脉冲降解,脉冲影响大于10j /cm2。在真空中,在低脉冲强度下,传输损耗随发射次数的增加而增加。但随着脉冲强度的增大,传输损耗减小,超过一定强度时传输损耗不可测量。传输损耗在较短波长测量时最高,向红外方向减小。吸收是导致传输损失的主要机制,是由二氧化硅表面的光还原引起的。
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引用次数: 0
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SPIE Laser Damage
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