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量子ドットを活用した冷間圧延時のロールバイト油膜厚さ分布の測定 利用量子点测定冷轧时的滚压和油膜厚度分布
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-01 DOI: 10.2355/tetsutohagane.tetsu-2023-040
Masahiro Shimura, Daisuke Kasai, Takayuki Otsuka, Naoki Yamashita, Tomoko Hirayama
During the cold rolling of flat steel products, lubrication is critical to achieve stable rolling. However, the oil film thickness distribution in the roll bite and its effect on friction between the work roll and strip have not been clarified thus far. This study aimed to elucidate the relationship between the oil film thickness distribution and friction by focusing on the rolling oil viscosity and steel grades, because they significantly affect the friction between the work roll and strip. Rolling oil was prepared with quantum dots as the fluorescent additive and used in rolling experiments to identify its distribution. Furthermore, cold rolling experiments were conducted using two types of oil with different viscosities and three different steel grades, namely low-carbon steel (LCS), high-strength steel (HSS), and advanced high-strength steel (AHSS) with tensile strengths of 270, 590, and 1180 MPa. Subsequently, the oil film thickness distribution on the steel strip surface was visualized using quantum dots by fluorescence microscopy. It was demonstrated that the higher the tensile strength of the steel or the higher the oil viscosity, the wider the rolling oil distribution on the strip surface. Numerical analyses revealed that the rolling oil distribution on the steel sheet surface was more widespread for AHSS and HSS than for LCS. The high surface pressure between the roll and steel plate may have increased the oil leaching area by increasing the oil viscosity. These findings demonstrate that rolling oil permeation from the oil-pits reduces the friction between the work rolls and strip.
在扁钢冷轧过程中,润滑是保证轧制稳定的关键。然而,对轧辊咬口的油膜厚度分布及其对工作辊与带材间摩擦的影响,目前还没有明确的认识。由于油膜厚度分布对工作辊与带材之间的摩擦有显著影响,本研究旨在通过重点研究轧制油粘度和钢种来阐明油膜厚度分布与摩擦之间的关系。以量子点为荧光添加剂制备了轧制油,并进行了轧制实验,以确定其分布。在此基础上,采用抗拉强度分别为270、590和1180 MPa的低碳钢(LCS)、高强钢(HSS)和高级高强钢(AHSS)三种不同钢种,采用两种不同粘度的油进行了冷轧试验。随后,利用量子点荧光显微镜观察钢带表面的油膜厚度分布。结果表明,钢的抗拉强度越高或油的粘度越高,轧制油在带钢表面的分布越广。数值分析表明,与LCS相比,AHSS和HSS的轧制油在钢板表面的分布更为广泛。轧辊与钢板之间的高表面压力可能通过增加油的粘度而增加了油的浸出面积。这些结果表明,从油坑中渗透的轧制油减少了工作辊与带材之间的摩擦。
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引用次数: 0
Flow Stress of Duplex Stainless Steel by Inverse Analysis with Dynamic Recovery and Recrystallization Model 双相不锈钢流动应力动态恢复与再结晶模型反演分析
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-01 DOI: 10.2355/tetsutohagane.tetsu-2023-048
Kyunghyun Kim, Hyung-Won Park, Sheng Ding, Hyeon-Woo Park, Jun Yanagimoto
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引用次数: 0
電気抵抗率測定を用いた塑性変形に伴うBCC鉄中の格子欠陥密度変化の定量 利用电阻率测量BCC铁中伴随塑性变形的晶格缺陷密度变化的定量
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-01 DOI: 10.2355/tetsutohagane.tetsu-2023-050
Soichiro Takenaka, Ryohei Takahashi, Kazuhiro Ishikawa, Yoji Miyajima
Change in lattice defects density in bcc pure iron due to tensile deformation was quantified by using both electrical resistivity measurements and X-ray diffraction (XRD). As bcc pure irons, ultra-low carbon steel (ULCS) and interstitial free (IF) steel are used as the model specimen. Dislocation density evaluated using Williamson Hall method with XRD shows the saturation with the value of around 3.7×1015 m−1 for ULCS and around 1.4×1015 m−1 for IF steel after plastic strain after ~5%. Increase in electrical resistivity was observed with increasing plastic strain. Consequently, increase in vacancy concentration occurs with increasing plastic strain of around 0.3, such as, 2.6×10−5 for ULCS and 3.4×10−5 for IF steel. Additionally, the migration of carbon atoms from grain interior to grain boundary via dislocation might occur at the initial stage of plastic deformation in ULCS.
利用电阻率测量和x射线衍射(XRD)分析了bcc纯铁在拉伸变形过程中晶格缺陷密度的变化。作为bcc纯铁,采用超低碳钢(ULCS)和无间隙钢(IF)作为模型试样。采用Williamson Hall法和XRD对位错密度进行了评价,结果表明,在~5%的塑性应变后,ULCS的位错密度约为3.7×1015 m−1,IF钢的位错密度约为1.4×1015 m−1。电阻率随塑性应变的增大而增大。因此,当塑性应变增加到0.3左右时,空位浓度增加,如ULCS为2.6×10−5,IF钢为3.4×10−5。此外,在ULCS塑性变形的初始阶段,碳原子可能通过位错从晶粒内部向晶界迁移。
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引用次数: 0
An Optimization for Ore Stockyard Layout Operation Schedules Using Multi-Start Greedy Algorithm 基于多起点贪心算法的堆场布置作业调度优化
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-01 DOI: 10.2355/tetsutohagane.tetsu-2023-043
Akira Kumano, Yusuke Yoshinari, Osamu Yamaguchi, Toru Miyazawa
We have developed an optimal scheduling method for the highly efficient management of multiple stockpiles of iron ore in the stockyard to significantly improve both yard logistics and the operational stability of steelworks.
我们开发了一种最优调度方法,对堆场的多个铁矿石库存进行高效管理,显著提高了堆场物流和钢厂的运行稳定性。
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引用次数: 0
単結晶Al<sub>2</sub>O<sub>3</sub>板を通した液体金属中のAl<sub>2</sub>O<sub>3</sub>粒子/単結晶Al<sub>2</sub>O<sub>3</sub>板間の焼結界面のその場観察 单晶体al&lt;sub & gt;2 &爱尔蒂;/ sub & gt;o &爱尔蒂;sub & gt;3 &爱尔蒂;/ sub & gt;穿过板的液态金属中的al&lt;sub & gt;2 &爱尔蒂;/ sub & gt;o &爱尔蒂;sub & gt;3 &爱尔蒂;/ sub & gt;粒子/单晶al&lt;sub & gt;2 &爱尔蒂;/ sub & gt;o &爱尔蒂;sub & gt;3 &爱尔蒂;/ sub & gt;对木板间的烧结面的当场观察
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-01 DOI: 10.2355/tetsutohagane.tetsu-2023-025
Masashi Nakamoto, Toshihiro Tanaka
In a continuous casting process, the clogging of the immersion nozzle with inclusions occurs as a result of the adhesion, agglomeration, and coalescence of inclusions. The most effective way to understand the behavior of inclusions, i.e. oxide particles, in a liquid steel is the in-situ observation. To our knowledge, however, there is no research on the in-situ observation of the behavior of oxide particles in a liquid steel. In the present work, therefore, the in-situ observation method for sintering interface between Al2O3 particle / single crystalline Al2O3 plate by laser microscope through single crystalline Al2O3 plate is proposed. First, the in-situ observation of sintering interface between Al2O3 particle and single crystalline Al2O3 in Ar atmosphere is conducted to verify the observation method for the interface through single crystalline Al2O3 plate. Then, the in-situ observation of sintering interface between Al2O3 particle and single crystalline Al2O3 in a liquid Ag is challenged. The observations for sintering interface between Al2O3 particle and single crystalline Al2O3 plate in Ar gas atmosphere and a liquid Ag are achieved by our proposed method. It is verified that the growth of sintering interface in liquid Ag is faster than that in an Ar gas atmosphere. This finding indicates that the non-wetting by liquid Ag of alumina particles promotes the growth of sintering interface in liquid Ag.
在连铸过程中,夹杂物堵塞浸没喷嘴是由于夹杂物的粘附、结块和聚并造成的。了解钢液中夹杂物(即氧化物颗粒)行为的最有效方法是现场观察。然而,据我们所知,还没有对钢液中氧化物颗粒的行为进行现场观察的研究。因此,本文提出了用激光显微镜通过单晶Al2O3板对Al2O3颗粒/单晶Al2O3板之间烧结界面进行原位观察的方法。首先,在Ar气氛中对Al2O3颗粒与单晶Al2O3烧结界面进行了原位观察,验证了通过单晶Al2O3板观察界面的方法。然后,对液态银中Al2O3颗粒与Al2O3单晶之间的烧结界面进行了原位观察。用该方法对Al2O3颗粒与单晶Al2O3板在氩气气氛和液态银中烧结界面进行了观察。结果表明,在液态Ag中烧结界面的生长速度比在氩气中快。这一发现表明,液态银对氧化铝颗粒的不润湿作用促进了液态银中烧结界面的生长。
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引用次数: 0
Mechanism of Al Coordination Change in Alkaline-earth Aluminosilicate Glasses: An Application of Bond Valence Model 碱土铝硅酸盐玻璃中Al配位变化机理:键价模型的应用
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-01 DOI: 10.2355/tetsutohagane.tetsu-2023-056
Sohei Sukenaga, Koji Kanehashi, Hiroki Yamada, Koji Ohara, Toru Wakihara, Hiroyuki Shibata
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引用次数: 0
Thermodynamic Analysis of Precipitation Behaviors in Hot-Rolled Ti-stabilized Interstitial-Free Steel Sheets 热轧无间隙钛稳定钢板析出行为的热力学分析
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-01 DOI: 10.2355/tetsutohagane.tetsu-2023-032
Michitoshi Saeki, Takako Yamashita
Thermodynamic calculations were performed on the precipitation behavior in the hot-rolled Ti-stabilized Interstitial Free (IF) steel sheets. By combining the thermodynamic parameters of Ti4C2S2 evaluated by first-principles calculations with previously reported parameters, parameters were developed that allow the calculation of the precipitation behavior of IF steels during hot rolling. The calculated precipitation behavior using those thermodynamic parameters is in relatively good agreement with the TEM observation results in hot-rolled IF steel sheets. The results of thermodynamic calculations suggest that the precipitation behavior of IF steel sheets during hot rolling depends on the amounts of Mn. These results are considered to be due to the decreased excess S in steel sheets as a result of the increase in precipitation of sulfides containing Mn.
对热轧ti稳定无间隙(IF)钢板的析出行为进行了热力学计算。通过将第一性原理计算评估的Ti4C2S2热力学参数与先前报道的参数相结合,开发了用于计算IF钢在热轧过程中析出行为的参数。利用这些热力学参数计算的析出行为与热轧中频钢板的透射电镜观察结果吻合较好。热力学计算结果表明,中频钢板在热轧过程中的析出行为取决于Mn的含量。这些结果被认为是由于含有Mn的硫化物的析出增加导致钢板中过量S的减少。
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引用次数: 0
深層学習と相変態モデルの融合による微細組織推定 深度学习和相变态模型融合的微细组织推测
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-01 DOI: 10.2355/tetsutohagane.tetsu-2023-045
Satoshi Noguchi, Syuji Aihara, Junya Inoue
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引用次数: 0
Changes in the Heterogeneous Deformation Structure and Texture with Cold Rolling Reduction in {110}<110> Oriented Coarse Grained 3% Silicon Steel {110}&lt;110&gt冷轧压下非均质变形组织和织构的变化取向粗晶3%硅钢
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-10-01 DOI: 10.2355/tetsutohagane.tetsu-2023-037
Tesshu Murakawa, Hiroshi Fujimura, Kenichi Murakami, Kohsaku Ushioda
We systematically investigated changes in crystal orientation due to the cold rolling of a {110}<110> single crystal, which had not been researched to date, in a reduction range of 10–70%. The results allowed for a classification of the changes into the following three reduction cases. The first was a 10–20% reduction. For this reduction, there was almost no change in the matrix orientation, and a shear band slightly appeared near the surface layer. The second was a 30–50% reduction, at which many shear bands were introduced, and the crystal orientation inside the shear bands was rotated from the initial {110}<110> orientation to the {100}<001> orientation around the TD axis. There are cells in the shear band. And {100}<001> orientation cells are considered having lower strain than around cells to having lower GAM. Additionally, the {111}<211> orientation was also confirmed in a small area that was thought to be surrounded by shear bands. The third was a 60–70% reduction, at which the matrix rotated to {111}<110>, but there were some areas with a {111}<211> orientation. Furthermore, the shear bands increased with increasing reduction, and more inner orientations were observed for {111}<211> than for {100}<001>. {111}<211> bands and {100}<001> bands are considered different origins to change discontinuously.
我们系统地研究了{110}单晶冷轧后晶体取向的变化,这是迄今为止尚未研究过的,在10-70%的还原范围内。结果允许将变化分类为以下三种减少情况。第一个是减少10-20%。在此还原过程中,基体取向几乎没有变化,在表层附近出现了轻微的剪切带。第二次是30-50%的还原,此时引入了许多剪切带,剪切带内的晶体取向围绕TD轴从最初的{110}取向旋转到{100}取向。剪切带中有细胞。{100}取向细胞被认为比周围细胞具有更低的应变,从而具有更低的GAM。此外,{111}取向也在一个被认为被剪切带包围的小区域得到证实。第三种是60-70%的减少,此时矩阵旋转到{111},但仍有一些区域具有{111}方向。剪切带随着还原度的增加而增加,{111}比{100}有更多的内取向。{111}带和{100}带被认为是不连续变化的不同起源。
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引用次数: 0
低合金鋼の焼戻しマルテンサイトにおける耐水素脆性に及ぼす転位密度の影響 位错密度对低合金钢的回火马氏体的耐水脆性的影响
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-10-01 DOI: 10.2355/tetsutohagane.tetsu-2023-047
Shinji Yoshida, Yuji Arai, Tomohiko Omura, Ken Cho, Hiroyuki Yasuda
The effect of dislocation density on hydrogen embrittlement resistance of tempered martensite in low alloy steels was investigated quantitatively. The various samples of which dislocation density was from 0.7×1014 m−2 to 4.5×1014 m−2 were prepared by changing tempering temperature and C content. Then, the yield stress of the samples was between 780 MPa and 1020 MPa. Especially, the change of the C content made various dislocation density samples even though the yield stress is almost same. The hydrogen embrittlement resistance was estimated with four-point bend test. The hydrogen embrittlement resistance decreases with increasing the dislocation density and the yield stress. Although the critical yield stress was changed dramatically by changing C content, the critical dislocation density was almost same (about 2.0×1014 m−2) even though the C content was different. In addition, the absorbed hydrogen content correlated with the dislocation density, and did not depend on the C content in this research. This means that the dislocation density is higher, the hydrogen trapping ability is higher. As the result, when the absorbed hydrogen content reach the critical diffusible hydrogen content, hydrogen embrittlement cracking occurs probably.
定量研究了位错密度对低合金钢回火马氏体抗氢脆性能的影响。通过改变回火温度和C含量,制备了位错密度在0.7×1014 m−2 ~ 4.5×1014 m−2之间的不同样品。试样的屈服应力在780 ~ 1020 MPa之间。特别是,C含量的变化使屈服应力几乎相同的位错密度试样也发生了变化。用四点弯曲试验估计了其抗氢脆性能。随着位错密度和屈服应力的增大,抗氢脆性能降低。随着C含量的变化,临界屈服应力发生了较大的变化,但在C含量不同的情况下,临界位错密度几乎相同(约为2.0×1014 m−2)。此外,吸附氢含量与位错密度相关,而不依赖于本研究中的C含量。这意味着位错密度越高,俘获氢的能力越强。因此,当吸收氢含量达到临界扩散氢含量时,可能发生氢脆开裂。
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引用次数: 0
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Tetsu To Hagane-journal of The Iron and Steel Institute of Japan
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