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The behavior of different clays subjected to a fast-drying cycle for traditional ceramic manufacturing 传统陶瓷制造中不同粘土在快速干燥循环中的表现
Q1 Chemical Engineering Pub Date : 2024-07-01 DOI: 10.1016/j.jksues.2022.05.003

Studies have been widely carried out on drying techniques and equipment. The behavior of clays subjected to drying stages requires further research. This study aims to evaluate the behavior of the clay ceramic body during the different stages of the drying cycle and match the characteristics of the raw materials with the final quality of the pieces. In this work, the behavior of three different clays in terms of drying performance was studied. The clays were selected, and their chemical, mineralogical, and particle size characteristics were measured. The mixture design (DoE) developed 10 formulations and was processed through vacuum extrusion. The samples were subjected to forced drying cycles of 180 min by varying the temperature from 30 to 90 °C and air speed from 1.5 to 4.0 m/s. At the end of the cycle, the retraction was a determining factor for the crack probability indicator, where formulations that obtained ∼10% retraction in the dry zone showed losses >25%. On the other hand, it is could be stated that claystone assists the drying process of the ceramic piece, minimizing losses. The drying sensitivity coefficient (k-factor) presented values that reproduce the number of losses during drying, proving to be a valid tool to relate clay properties, drying conditions, and losses in this process. In this case, drying process losses >25% were observed when the k-factor was from 1.6.

有关干燥技术和设备的研究已广泛开展。粘土在干燥阶段的行为需要进一步研究。本研究旨在评估粘土陶瓷体在干燥周期不同阶段的行为,并将原材料的特性与作品的最终质量相匹配。在这项工作中,研究了三种不同粘土在干燥性能方面的表现。选定了粘土,并测量了它们的化学、矿物学和粒度特征。混合物设计(DoE)开发了 10 种配方,并通过真空挤压进行处理。通过改变温度(30 至 90 °C)和风速(1.5 至 4.0 m/s),对样品进行了 180 分钟的强制干燥循环。在循环结束时,回缩率是裂纹概率指标的决定性因素,在干燥区回缩率为 10% 的配方显示出 25% 的损失。另一方面,可以说粘土岩有助于陶瓷片的干燥过程,将损失降至最低。干燥灵敏度系数(K 系数)显示的数值再现了干燥过程中的损耗数量,证明它是将粘土特性、干燥条件和干燥过程中的损耗联系起来的有效工具。在这种情况下,当 k 系数为 1.6 时,干燥过程中的损耗为 25%。
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引用次数: 0
Development of Dioscorea alata stem fibers as eco-friendly reinforcement for composite materials 开发薯蓣茎纤维作为复合材料的生态友好型增强材料
Q1 Chemical Engineering Pub Date : 2024-07-01 DOI: 10.1016/j.jksues.2022.02.003

The use of natural fibers instead of synthetic fibers has become a hot topic in the reinforced composite manufacturing industry. However, there are considerable differences in the mechanical properties of natural fibers cited in the literature. These differences could be due to the prevalent use of monothetic analysis. In this paper, the use of a simplified Taguchi technique in novel Dioscorea alata stems fiber processing is proposed to allow for simultaneous evaluation of control parameters such as treatment type, harvest condition, gauge length and chemical treatment temperature to determine the optimal conditions for fiber tensile properties. These fibers were extracted from the stem by means of water retting method before chemical treatment. The tensile properties were determined as per ASTM D3822/D3822M-14. Non-destructive examinations were employed to look into the chemical make-up, thermal, crystalline and morphological characteristics of the fibers. The test results showed an optimum tensile strength of 151 MPa and tensile modulus of 5709.5 MPa. Density was 0.4 g/cm3 while cellulose, lignin, moisture, hemicellulose and ash contents were 13.1 %, 10.3 %, 9.7 %, 5.0 % and 8.2 % respectively. The treated fibers were thermally stable till 320 °C. The properties of Dioscorea alata stem fiber (DASF) were found to be promising when compared to existing natural fibers, making it a viable candidate for composite material reinforcement.

使用天然纤维代替合成纤维已成为增强复合材料制造业的热门话题。然而,文献中提到的天然纤维的机械性能存在很大差异。这些差异可能是由于普遍使用的单一分析法造成的。本文建议在新型薯蓣茎纤维加工中使用简化的田口技术,以便同时评估处理类型、收获条件、规格长度和化学处理温度等控制参数,从而确定纤维拉伸性能的最佳条件。在进行化学处理之前,先用水甑法从茎中提取这些纤维。拉伸性能按照 ASTM D3822/D3822M-14 标准测定。此外,还采用了非破坏性检测方法来研究纤维的化学成分、热、结晶和形态特征。测试结果表明,最佳拉伸强度为 151 兆帕,拉伸模量为 5709.5 兆帕。密度为 0.4 克/立方厘米,纤维素、木质素、水分、半纤维素和灰分含量分别为 13.1%、10.3%、9.7%、5.0% 和 8.2%。处理后的纤维热稳定性可达 320 °C。与现有的天然纤维相比,发现薯蓣茎纤维(DASF)的性能很有前途,使其成为复合材料加固的可行候选材料。
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引用次数: 0
Influence of multiproduct pipeline telescopicity design on the process of mixing during sequential pumping 多产品管道伸缩性设计对连续泵送过程中混合过程的影响
Q1 Chemical Engineering Pub Date : 2024-07-01 DOI: 10.1016/j.jksues.2022.05.002

In the present paper, the research of the processes of mixture formation is carried out using the method of transportation of light petroleum products — sequential pumping by direct contact. Modeling of the processes of mixture formation is carried out taking into account the influence of parametric factors. This paper is based on a previously published work on non-isothermal pumping of petroleum products in a pipeline. It is also worth noting that in this work, a mathematical model has been finalized to consider the increase in accuracy, namely, accounting in a telescopic pipeline. To perform numerical simulation, a software package was developed that is capable of not only modeling and calculating the parameters of the petroleum product pipeline operation in real time, followed by graphical visualization, but also comparing the obtained data with the real data processed by operators at industrial facilities.

本文采用轻质石油产品的运输方法--直接接触式顺序泵送,对混合物的形成过程进行了研究。考虑到参数因素的影响,对混合物的形成过程进行了建模。本文基于之前发表的关于管道中石油产品非等温抽吸的研究成果。值得注意的是,在这项工作中,还最终确定了一个数学模型,以考虑精度的提高,即在伸缩管道中进行核算。为了进行数值模拟,开发了一个软件包,该软件包不仅能够实时建模和计算石油产品管道运行的参数,然后进行图形可视化,还能将获得的数据与工业设施操作员处理的真实数据进行比较。
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引用次数: 0
Modeling and simulation of the startup of the coupling reactor for Industrial-Scale production of Diethyl oxalate 草酸二乙酯工业规模生产耦合反应器的启动建模与模拟
Q1 Chemical Engineering Pub Date : 2024-07-01 DOI: 10.1016/j.jksues.2022.05.007

A one-dimensional homogeneous reactor model was developed to simulate the dynamic behavior of a fixed-bed reactor for a catalytic coupling reactor of carbon monoxide and ethyl nitrite to diethyl oxalate. Reactor modeling was performed using a comprehensive numerical model that was simulated using Simulink. The power law kinetic model was applied for simulating the catalytic coupling reaction considering the main and side reactions. The heat of reaction was calculated with respect to the reacted moles of ethyl nitrite for each reaction. When the simulated model reached a steady state, the predicted results were in agreement with the actual data that was collected from an already established pilot plant fixed bed reactor. The startup dynamic behavior of hypothetical industrial-scale production of diethyl oxalate at 78,000 tons per year was simulated. The system reached steady-state within 14–16 min at a space velocity of 1400 h−1.

开发了一种一维均相反应器模型,用于模拟一氧化碳和亚硝酸乙酯催化耦合反应器中固定床反应器的动态行为。反应器建模是通过使用 Simulink 模拟的综合数值模型进行的。在模拟催化偶联反应时,考虑到了主反应和副反应,采用了幂律动力学模型。计算了每个反应的反应热与亚硝酸乙酯的反应摩尔数。当模拟模型达到稳定状态时,预测结果与已建立的中试装置固定床反应器收集的实际数据一致。模拟了年产 78,000 吨草酸二乙酯的假设工业规模生产的启动动态行为。系统在 14-16 分钟内达到稳态,空间速度为 1400 h-1。
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引用次数: 0
CO2 sequestration using a novel Belt Conveyor Reactor with rotating sieve trays compared with Airlift Bubble Column as photobioreactors 将带有旋转筛盘的新型带式输送反应器与气升泡柱作为光生物反应器进行二氧化碳封存比较
Q1 Chemical Engineering Pub Date : 2024-07-01 DOI: 10.1016/j.jksues.2021.12.007

The present work aims to evaluate the performance of a novel three-phase reactor Belt Conveyor Reactor BCR (with rotating sieve trays patent GB2567340B) as a photobioreactor compared with a traditional Airlift Bubble Column ALR, both influenced by the flow of the gas. Chlorella vulgaris was cultivated in these two photobioreactors using ambient air has a CO2 concentration of 0.038% with different aeration flowrates 0.145, 0.195, 0.24, and 0.29 vvm (gas volume per minute/liquid volume in the reactor).

The maximum growth rate achieved on the 14th day of culture was 2.120 and 1.420 g/L for BCR, ALR respectively, with initial biomass concentrations of 0.2 g/L and aeration flow of 0.29 vvm. Moreover, the removal efficiency of carbon dioxide sequestration by the two photobioreactors is 40% for BCR and 25% for ALR. The innovative design succeeded in operational quality of agitation with high gas holdup inside the sieve trays to increase the biomass growth up to 50% higher than in the ALR. The maximum CO2 fixation for ALR was at about 18% at a specific aeration rate of 0.145 vvm in the bubbly regime. Whereas in the BCR can be reached about 38% with wide range operation condition of airflow rate 0.145–0.24 vvm due to well-distributed liquid due to rotating trays, and good gas–liquid mass transfer surface area.

本研究旨在评估新型三相反应器带式输送反应器 BCR(带旋转筛盘,专利号:GB2567340B)作为光生物反应器与传统气升式气泡塔 ALR 的性能比较,两者都受到气体流量的影响。用二氧化碳浓度为 0.038% 的环境空气和 0.145、0.195、0.24 和 0.29 vvm(反应器中每分钟的气体体积/液体体积)的不同曝气流量在这两种光生物反应器中培养小球藻。此外,两种光生物反应器对二氧化碳的吸收效率分别为:BCR 40%,ALR 25%。创新设计成功地提高了搅拌的运行质量,筛盘内的气体保持率高,使生物量的增长比 ALR 高出 50%。在气泡曝气条件下,当特定曝气率为 0.145 vvm 时,ALR 的二氧化碳最大固定率约为 18%。而在 BCR 中,气流速率为 0.145-0.24 vvm 的宽范围运行条件下,二氧化碳固定率可达到约 38%,这得益于旋转托盘使液体分布均匀,以及良好的气液传质表面积。
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引用次数: 0
Augmented hunger games search algorithm using logarithmic spiral opposition-based learning for function optimization and controller design 使用对数螺旋对立学习的增强型饥饿游戏搜索算法,用于函数优化和控制器设计
Q1 Chemical Engineering Pub Date : 2024-07-01 DOI: 10.1016/j.jksues.2022.03.001

This paper explains the construction of a novel augmented hunger games search algorithm using a logarithmic spiral opposition-based learning technique. The proposed algorithm (LsOBL-HGS) is used as an efficient tool for both function optimization and controller design. To assess the performance of the algorithm for function optimization, benchmark functions from the CEC2017 test suite were employed and comparisons were made with available and good performing algorithms. In terms of controller design, the proposed LsOBL-HGS algorithm was utilized to design a FOPID controlled magnetic ball suspension system. Comparative assessments were also performed for FOPID controller design, as well using other state-of-the-art methods reported for the magnetic ball suspension system. The results showed that the proposed LsOBL-HGS algorithm has good capability for FOPID controller design employed in a magnetic ball suspension system as it provided an improvement of more than 13% in terms of the transient response-related parameters and more than 34% in terms of bandwidth compared to the best-reported approach used for comparisons.

本文阐述了利用对数螺旋对立学习技术构建的新型增强饥饿游戏搜索算法。所提出的算法(LsOBL-HGS)被用作函数优化和控制器设计的有效工具。为了评估该算法在函数优化方面的性能,采用了 CEC2017 测试套件中的基准函数,并与现有的性能良好的算法进行了比较。在控制器设计方面,利用提出的 LsOBL-HGS 算法设计了一个 FOPID 控制的磁球悬挂系统。此外,还对 FOPID 控制器设计进行了比较评估,并采用了其他已报道的磁球悬挂系统的最新方法。结果表明,所提出的 LsOBL-HGS 算法在磁球悬挂系统的 FOPID 控制器设计方面具有良好的能力,因为与用于比较的最佳报告方法相比,它在瞬态响应相关参数方面提高了 13% 以上,在带宽方面提高了 34% 以上。
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引用次数: 0
Accurate finite element modelling of knots and related fibre deviations in structural timber 结构木材节疤及相关纤维偏差的精确有限元建模
Q1 Chemical Engineering Pub Date : 2024-07-01 DOI: 10.1016/j.jksues.2022.01.005

The primary purpose of the pursued research presented in this article was to propose a new technique to create the actual three-dimensional geometry of knots and related fibre deviations and eliminate the inconsistency between modelling the knots as openings or solids. The geometrical and mechanical characteristics of knots and related local disturbed fibre patterns were numerically modelled. The numerical models were experimentally validated by four-point bending tests performed on six timber beams made of Nordic spruce (Picea abies). Tested specimens were sliced up into several strips parallel to the grains in the vicinity of the knot to numerically generate the actual geometrical model of the knots and related fibre deviations for creating the three-dimensional fibre paradigm. The validated numerical models can also be used based on visual inspections. The user needs only to define the position and size of the knot within the timber element required for the 3D finite element model. Moreover, the model allows defining different fibre patterns in the knot vicinity. Results proved that openings can represent knots when found in the tension zone with careful adjustment of the related three-dimensional fibre deviations. Moreover, the results emphasize the need for accurate modelling for the fibre deviations rather than the knot itself.

本文所介绍的研究的主要目的是提出一种新技术,以创建纤维结和相关纤维偏差的实际三维几何形状,并消除将纤维结建模为开口或实体之间的不一致性。本文对纤维节的几何和机械特性以及相关的局部纤维扰动模式进行了数值建模。通过对六根北欧云杉(Picea abies)木材横梁进行四点弯曲试验,对数值模型进行了实验验证。测试后的试样被切成若干条,平行于木节附近的纹理,以数值方法生成木节的实际几何模型和相关的纤维偏差,从而创建三维纤维范例。经过验证的数值模型也可用于目测。用户只需在三维有限元模型所需的木材元素中定义木结的位置和大小。此外,该模型还允许在木结附近定义不同的纤维模式。结果证明,当在张力区发现木结时,只要仔细调整相关的三维纤维偏差,就可以用开口来表示木结。此外,结果还强调了对纤维偏差而非绳结本身进行精确建模的必要性。
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引用次数: 0
Study on the friction and wear properties of zinc oxide/silicon dioxide composite-coated paper mulch film 氧化锌/二氧化硅复合涂层纸地膜的摩擦和磨损特性研究
Q1 Chemical Engineering Pub Date : 2024-05-01 DOI: 10.1016/j.jksues.2021.12.004
Anling Li , Yangyang Jia , Zhen Li , Shuaiyang Ren , Fengwei Zhang , Qiang He

Paper mulching films are affected by wind and rain in the field, which lead to the problems of water absorption, shrinkage, and friction with the soil surface. In order to achieve better hydrophobic durability and wear resistance of paper mulching films, a paper mulching film with ZnO/SiO2 composite coating was prepared by the brush coating method. Taking ceramic balls as friction pairs, reciprocating friction tests were carried out with two kinds of paper mulching films at different temperatures. The morphology of the raw paper mulch film and the ZnO/SiO2 composite-coated paper mulch film after rubbing at different temperatures and the reason of the hydrophobic durability of the coated paper mulch film were analyzed using a scanning electron microscope and a three-dimensional topography instrument. The results show that ZnO/SiO2 composite coating can improve the wear resistance and hydrophobic durability of the paper mulch film. Through surface morphology analysis, it can be found that the composite coating plays a role in modification and filling and improves the adhesion between the fibers by reducing the pores on the surface of the paper mulch film, finally improving the wear resistance and hydrophobic durability of the paper mulch film.

纸地膜在田间受到风雨的影响,会出现吸水、收缩以及与土壤表面摩擦等问题。为了使纸地膜具有更好的疏水耐久性和耐磨性,采用刷涂法制备了一种具有 ZnO/SiO2 复合涂层的纸地膜。以陶瓷球为摩擦副,在不同温度下对两种纸地膜进行了往复摩擦试验。使用扫描电子显微镜和三维形貌仪分析了原纸地膜和 ZnO/SiO2 复合涂层纸地膜在不同温度下摩擦后的形貌以及涂层纸地膜疏水耐久性的原因。结果表明,ZnO/SiO2 复合涂层能提高纸地膜的耐磨性和疏水耐久性。通过表面形貌分析可以发现,复合涂层起到了改性和填充的作用,并通过减少纸地膜表面的孔隙提高了纤维间的粘附力,最终提高了纸地膜的耐磨性和疏水耐久性。
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引用次数: 0
Optimal dynamic balancing of a hybrid serial-parallel robotic manipulator through bio-inspired computing 通过生物启发计算优化串并联混合机器人机械手的动态平衡
Q1 Chemical Engineering Pub Date : 2024-05-01 DOI: 10.1016/j.jksues.2021.10.008
Ricardo Mejia-Rodriguez, Miguel Gabriel Villarreal-Cervantes, Josué Nathán Martínez-Castelán, José Saúl Muñoz-Reina, Víctor Manuel Silva-García

One of the most challenging robotic manipulator designs is finding an appropriate balance between the shaking force and shaking moment because this reduces vibrations. Several approaches have been introduced in the last decades; nevertheless, some assumptions must be established to make such a balance. In this paper, a dynamic balancing approach is proposed. The main novelty is the no dependence on specific trajectories to be executed by the manipulator, which allows finding a design with a similar tradeoff in the balancing under robot configuration changes. Also, the proposal incorporates mass distribution and link shape in a single design procedure. The proposal is stated as a constrained nonlinear optimization problem and applied to a hybrid serial-parallel robotic manipulator. The use of different bio-inspired algorithms and one gradient one in the solution of the balancing problem reveals that differential evolution finds the most suitable design. Besides, comparative simulation results of the obtained design with other design approaches show that the obtained design presents the most suitable tradeoff between the shaking force and the shaking moment when the manipulator executes tasks with different operating velocities.

机器人机械手设计中最具挑战性的问题之一是如何在晃动力和晃动力矩之间找到适当的平衡,因为这样可以减少振动。在过去的几十年里,已经推出了多种方法;然而,要实现这种平衡,必须建立一些假设。本文提出了一种动态平衡方法。该方法的主要创新点在于不依赖于机械手执行的特定轨迹,因此可以在机器人配置变化的情况下找到具有类似平衡权衡的设计。此外,该提案还将质量分布和链接形状纳入了单一设计程序。该建议被表述为一个约束非线性优化问题,并应用于一个串行-并行混合机械手。在平衡问题的求解过程中,使用了不同的生物启发算法和一种梯度算法,结果表明微分进化算法能找到最合适的设计方案。此外,将所获得的设计与其他设计方法进行比较的模拟结果表明,当机械手以不同的操作速度执行任务时,所获得的设计能在晃动力和晃动力矩之间做出最合适的权衡。
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引用次数: 0
Electric vehicle speed tracking control using an ANFIS-based fractional order PID controller 使用基于 ANFIS 的分数阶 PID 控制器实现电动汽车速度跟踪控制
Q1 Chemical Engineering Pub Date : 2024-05-01 DOI: 10.1016/j.jksues.2022.01.001
Mary Ann George , Dattaguru V. Kamat , Ciji Pearl Kurian

Electric vehicles (EVs) have assumed prominence due to their enhanced performance, efficiency, and zero carbon emission. This paper proposes an efficient adaptive neuro-fuzzy inference system (ANFIS) based fractional order PID (FOPID) controller for an EV speed tracking control driven by a DC motor. The optimal controller parameters of the FOPID controller are found via an Ant Colony Optimization (ACO) method. The ANFIS controllers are well trained, tested, and validated using the data set sextracted from the fuzzy-based controllers. The performance and accuracy of the ANFIS model are evaluated using statistical parameters such as mean square error (MSE), coefficient of correlation (R), and root mean square error (RMSE). The controller performance, energy consumption, and robustness are tested using the new European drive cycle (NEDC) test. The efficacy of the ANFIS-based controller is demonstrated by comparing its performance with properly tuned fuzzy-based controllers. The proposed controller shows robustness towards external disturbances and offers promising EV speed regulation control. The comparative results illustrate the superior performance of ANFIS-based FOPID controller with high prediction and low error rates. MATLAB- Simulink platform is used for system modeling, controller design, and numerical simulation.

电动汽车(EV)因其更高的性能、效率和零碳排放而备受瞩目。本文针对直流电机驱动的电动汽车速度跟踪控制,提出了一种基于分数阶 PID(FOPID)控制器的高效自适应神经模糊推理系统(ANFIS)。FOPID 控制器的最佳控制器参数是通过蚁群优化(ACO)方法找到的。利用从基于模糊的控制器中提取的数据集,对 ANFIS 控制器进行了良好的训练、测试和验证。ANFIS 模型的性能和准确性通过均方误差 (MSE)、相关系数 (R) 和均方根误差 (RMSE) 等统计参数进行评估。控制器的性能、能耗和鲁棒性通过新欧洲行驶循环(NEDC)测试进行了检验。通过将基于 ANFIS 的控制器的性能与经过适当调整的基于模糊的控制器进行比较,证明了该控制器的功效。所提出的控制器对外部干扰具有鲁棒性,并能对电动汽车进行速度调节控制。比较结果表明,基于 ANFIS 的 FOPID 控制器性能优越,预测准确率高,误差率低。MATLAB- Simulink 平台用于系统建模、控制器设计和数值模拟。
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引用次数: 0
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Journal of King Saud University, Engineering Sciences
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