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The construction of yeast β-glucan coated-edible dock protein nanomicelles for the encapsulation and sustained release of apigenin 构建用于包裹和持续释放芹菜素的酵母β-葡聚糖包被可食用对接蛋白纳米微囊
IF 5.5 2区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-14 DOI: 10.1016/j.jfoodeng.2024.112136
Qian Zhou , Xiao-Jie Wang , Yu-Ru Wu , Weinan Zhang , Jing Li , Wei Wang , Ying-Nan Liu , Zhen-Yu Yu , Ming-Ming Zheng , Yi-Bin Zhou , Kang Liu

In this study, yeast β-glucan (YG) and edible dock protein (EDP) were used to develop the nanomicelles for delivering apigenin (Api) via self-assembly. Results showed that a stable and uniform Api-EDP-YG composite nanomicelles could be formed when the additive amount of YG was 0.5 wt%, giving the particle size of 351.2 nm and the zeta-potential of −22.59 mV. The composite nanomicelles exhibited a core-shell structure, wherein Api-EDP was a core and YG was a shell. Moreover, hydrogen bonding and van der Waals forces drove the formation of Api-EDP-YG nanomicelles. Meanwhile, the composite nanomicelles can delay the degradation of apigenin in SSF and make it slowly release in SIF, which is benefit for improving its stability and bioavailability. Importantly, the apigenin within the composite nanomicelles displayed a good storage stability and cellular compatibility. These results indicated that the Api-EDP-YG nanomicelles might have a potential application in precision nutritional and healthy foods.

本研究利用酵母β-葡聚糖(YG)和可食性码头蛋白(EDP)通过自组装开发了可递送芹菜素(Api)的纳米微孔。结果表明,当YG的添加量为0.5 wt%时,可形成稳定、均匀的Api-EDP-YG复合纳米微孔,其粒径为351.2 nm,zeta电位为-22.59 mV。复合纳米微孔呈现出核壳结构,其中 ApiEDP 为核,YG 为壳。此外,氢键和范德华力推动了 Api-EDP-YG 纳米簇的形成。同时,复合纳米微孔能延缓芹菜苷在 SSF 中的降解,使其在 SIF 中缓慢释放,有利于提高芹菜苷的稳定性和生物利用度。重要的是,复合纳米微孔中的芹菜苷具有良好的储存稳定性和细胞相容性。这些结果表明,Api-EDP-YG 纳米微孔有可能应用于精准营养和健康食品。
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引用次数: 0
Rapid screening of tuna samples for food safety issues related to histamine content using fourier-transform mid-infrared (FT-MIR) and chemometrics 利用傅立叶变换中红外(FT-MIR)和化学计量学快速筛查金枪鱼样品中组胺含量的食品安全问题
IF 5.5 2区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-13 DOI: 10.1016/j.jfoodeng.2024.112129
Mónica Sánchez-Parra , Juan Antonio Fernández Pierna , Vincent Baeten , José Manuel Muñoz-Redondo , José Luis Ordóñez-Díaz , José Manuel Moreno-Rojas

Biogenic amines (BAs) generally result from the decarboxylation reaction of free amino acids as a result of the activity of different microorganisms. A build-up of these compounds can result in food being spoilt. Therefore, the rapid and precise detection of BAs like histamine is an important task for food safety. This research aimed to explore the potential of Fourier-Transform Mid-Infrared (FT-MIR) spectroscopy combined with chemometric methods to assess histamine in fresh tuna quantitatively. Based on the FT-MIR data, partial least squares regression models for the prediction of histamine were successfully constructed with R2 > 0.90. Machine learning algorithms (partial least squares-discrimination analysis, k-nearest neighbors, and support vector machine) were applied, and excellent discrimination results were achieved based on the limits specified in two different legislations (EU and FDA). The results support the use of a rapid, economic and reliable approach for the discrimination of samples that could pose a health risk to consumers.

生物胺(BA)通常是游离氨基酸在不同微生物的作用下发生脱羧反应而产生的。这些化合物的积累会导致食物变质。因此,快速准确地检测组胺等生物碱是食品安全的一项重要任务。本研究旨在探索傅立叶变换中红外光谱(FT-MIR)结合化学计量学方法定量评估新鲜金枪鱼中组胺的潜力。基于傅立叶变换中红外光谱数据,成功构建了预测组胺含量的偏最小二乘回归模型,R2 > 0.90。应用机器学习算法(偏最小二乘判别分析、k-近邻和支持向量机),根据两个不同法规(欧盟和美国食品药物管理局)规定的限值,取得了极佳的判别结果。这些结果支持使用一种快速、经济、可靠的方法来鉴别可能对消费者健康造成危害的样品。
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引用次数: 0
A feature extractor for temporal data of electronic nose based on parallel long short-term memory network in flavor discrimination of Chinese vinegars 基于并行长短期记忆网络的电子鼻时间数据特征提取器在中国醋风味鉴别中的应用
IF 5.5 2区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-12 DOI: 10.1016/j.jfoodeng.2024.112132
Yufei Chen , Jun Fu , Xin Weng , Jiaoni Chen , Ruifen Hu , Yunfang Zhu

Volatile flavor is a key indicator of food quality which can directly affect consumer preference and purchase intention. Electronic nose is considered as a promising intelligent sensory analysis tool for food flavor assessment, however, extracting effective features from the gas sensor array is still a major challenge, which largely determines the performance of subsequent classifiers. Here, a parallel long short-term memory (LSTM) network is proposed as a feature extractor for automatically extracting features from the whole time series of sensor responses in flavor discrimination of five Chinese vinegars. The network was trained by the temporal data from the sensor array and yielded different feature patterns corresponding to different vinegars, which were then fed to other conventional classifiers for pattern recognition. We also evaluated the influence of the extracted feature dimension that is related to the dimension of the hidden state of the LSTM layer on the classification performance. The results indicate that a larger dimension of extracted feature is unnecessary for promoting classification accuracy, instead, the optimum dimension 4 of the hidden state gives the highest accuracy of 95.8% in this application under the softmax evaluator. Moreover, much higher accuracies were obtained when combined with other sophisticated classifiers such as support vector machine. The results demonstrate that the proposed network is competent to extract features directly and automatically from the temporal data of the electronic nose.

挥发性风味是食品质量的一个关键指标,会直接影响消费者的偏好和购买意向。电子鼻被认为是用于食品风味评估的一种前景广阔的智能感官分析工具,然而,从气体传感器阵列中提取有效特征仍是一大挑战,这在很大程度上决定了后续分类器的性能。本文提出了一种并行长短期记忆(LSTM)网络作为特征提取器,用于从传感器响应的整个时间序列中自动提取五种中国醋风味鉴别中的特征。该网络通过来自传感器阵列的时间数据进行训练,得出了与不同醋相对应的不同特征模式,然后将其输入其他传统分类器进行模式识别。我们还评估了与 LSTM 层隐藏状态维度相关的提取特征维度对分类性能的影响。结果表明,提取特征的维度越大,对提高分类准确率越无必要,相反,在软最大评估器下,隐藏状态的最佳维度 4 在该应用中的准确率最高,达到 95.8%。此外,在与支持向量机等其他复杂分类器相结合时,也能获得更高的准确率。结果表明,所提出的网络能够直接自动地从电子鼻的时间数据中提取特征。
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引用次数: 0
Online sorting of surface defective walnuts based on deep learning 基于深度学习的核桃表面缺陷在线分拣技术
IF 5.5 2区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-12 DOI: 10.1016/j.jfoodeng.2024.112133
Jingwei Wang , Xiaopeng Bai , Daochun Xu , Wenbin Li , Siyuan Tong , Jiaming Zhang

To address concerns regarding walnut shell damage and inadequate sorting precision during the mechanized sorting of walnuts, a walnut automatic sorting machine was designed based on deep learning and experimental research. Initially, the rationality of the design was verified through experiment. Then, three deep learning semantic segmentation algorithms, namely PSPnet, U-net, and Deeplabv3+, were selected to train walnut detection models. Results indicated that the U-net algorithm proved to be the most effective, achieving a Mean Intersection over Union of 96.71% and a Mean Pixel Accuracy value of 98.52%. Finally, performance tests were conducted on the prototype machine, yielding results with an average sorting efficiency of 51.70 kg/h, an average loss rate of 6.50%, and an average accuracy of sorting walnuts of 92.98%. The findings can provide insights for future structural improvements and operational parameter optimization of walnut automatic sorting machines.

为了解决核桃机械化分拣过程中核桃外壳损坏和分拣精度不足的问题,我们在深度学习和实验研究的基础上设计了一种核桃自动分拣机。首先,通过实验验证了设计的合理性。然后,选择了 PSPnet、U-net 和 Deeplabv3+ 三种深度学习语义分割算法来训练核桃检测模型。结果表明,U-net 算法被证明是最有效的,其平均联合交叉率达到 96.71%,平均像素准确率达到 98.52%。最后,对原型机进行了性能测试,结果显示平均分拣效率为 51.70 公斤/小时,平均损失率为 6.50%,核桃平均分拣准确率为 92.98%。研究结果可为核桃自动分拣机未来的结构改进和运行参数优化提供启示。
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引用次数: 0
Acoustic signals associated with the multifractal breakage patterns of brittle and crispy foods 与脆性和酥性食品的多分形破损模式相关的声学信号
IF 5.5 2区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-11 DOI: 10.1016/j.jfoodeng.2024.112130
Carla Acosta-Ramírez , Evangelina García-Armenta , Georgina Calderón-Domínguez , Maribel Cornejo-Mazón , Hugo S. García , Humberto Hernández-Sánchez , Gustavo F. Gutiérrez-López

Food breakage is an important issue in industry and is coupled to acoustic signals. The aim of this work was to analyse the breakage phenomenon with time in commercial crispy and brittle foods, using acoustic techniques and mechanical-textural features using Digital Image Analysis (DIA) and fractal analysis. Breakage patterns were coupled to the acoustic signals of six brittle foods by capturing the audio during breaking and then, applying DIA to audio signals and breakage patterns, which depicted multifractal spectra. Results showed that samples with less irregular acoustic patterns presented higher spectrum amplitudes and low generalised fractal dimension (GFD) (1.245 ± 0.045) and lacunarity (Ʌ) (0.269 ± 0.209) while materials presenting the largest irregularity had shorter spectrum amplitudes and depicted high GFD (1.656 ± 0.177) and Ʌ(0.745 ± 0.007). For global analysis of the transverse and longitudinal rupture pattern, four breakage zones were defined. In all cases, multifractal breakage patterns were associated to multifractal acoustic signals.

食品破损是工业中的一个重要问题,与声学信号有关。这项工作的目的是利用声学技术以及数字图像分析(DIA)和分形分析的机械纹理特征,分析商业脆皮食品的破损现象。通过捕捉六种脆性食品破损过程中的音频信号,将破损模式与音频信号进行耦合,然后对音频信号和破损模式应用数字图像分析(DIA),从而描绘出多分形光谱。结果表明,不规则声学模式较少的样品频谱振幅较高,广义分形维度(GFD)(1.245 ± 0.045)和裂隙度(Ʌ)(0.269 ± 0.209)较低,而不规则程度最大的材料频谱振幅较短,广义分形维度(GFD)(1.656 ± 0.177)和裂隙度(Ʌ)(0.745 ± 0.007)较高。为全面分析横向和纵向断裂模式,定义了四个断裂带。在所有情况下,多分形断裂模式都与多分形声学信号有关。
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引用次数: 0
Differentiation between fresh and frozen-thawed mackerel fish using low-cost portable near infrared spectrometry devices 利用低成本便携式近红外光谱仪区分新鲜和冷冻解冻的鲭鱼
IF 5.5 2区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-11 DOI: 10.1016/j.jfoodeng.2024.112131
Mar Giró-Candanedo , Jordi Cruz , Josep Comaposada , Clara Barnés-Calle , Pere Gou , Elena Fulladosa

Mislabelling frozen-thawed fish fillets as fresh is one of the most important fraudulent practices during commercialisation. This study aimed to determine the ability of two portable miniaturised low-cost near-infrared spectroscopy (NIR) devices intended for consumers to discriminate between fresh and thawed mackerel (submitted to one or two frozen-thawed cycles) and between different freezing systems. The effect of different fish seasonal characteristics on the performance of the model was also evaluated. The low-cost NIR devices were able to discriminate between fresh and thawed samples with a classification rate of 90.3% and 94.1% and the freezing system to which they were submitted with a classification rate of 91.2% and 89.7%. These findings suggest that low-cost portable NIR spectroscopy can be a valuable tool for detecting mislabeled frozen-thawed products sold as fresh, providing consumers with a rapid and affordable method for fraud detection.

将冷冻解冻的鱼片误标为新鲜鱼片是商业化过程中最重要的欺诈行为之一。本研究旨在确定两款面向消费者的便携式微型低成本近红外光谱(NIR)设备区分新鲜和解冻鲭鱼(经过一个或两个冷冻解冻周期)以及不同冷冻系统的能力。此外,还评估了不同鱼类季节性特征对模型性能的影响。低成本近红外设备能够区分新鲜样品和解冻样品,分类率分别为 90.3% 和 94.1%,区分冷冻系统的分类率分别为 91.2% 和 89.7%。这些研究结果表明,低成本的便携式近红外光谱仪可以成为检测将冷冻解冻产品误标为新鲜产品的重要工具,为消费者提供一种快速、经济的欺诈检测方法。
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引用次数: 0
Fabrication of chitosan-based smart film by the O/W emulsion containing curcumin for monitoring pork freshness 利用含有姜黄素的水包油型乳液制备壳聚糖基智能薄膜,用于监测猪肉新鲜度
IF 5.5 2区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-08 DOI: 10.1016/j.jfoodeng.2024.112115
Yanhong Liu , Guangrao Chen , Yajiao Yang , Ruonan Wu , Lingling Zhang , Xiwang Mu , Shuo Wang

In this research, curcumin (Cur) was encapsulated in succinylated soy protein isolate (SSPI) emulsion and combined with chitosan (CS) to prepare a smart film. The good adsorption ability of SSPI at the oil-water interface provides good physical stability for preparing Cur-loaded emulsion. These CS smart films containing SSPI emulsions with different curcumin content were evaluated on the structure, mechanical, barrier, antioxidant, antibacterial properties, and controlled release behavior. SEM and FT-IR results showed that the Cur-loaded emulsion was compatible with the CS matrix. By adding the emulsion, the film blocked 97.11% of ultraviolet radiation, reduced the water vapor transmission rate by 42%, and improved the swelling degree (32.26%), water solubility (12%), thermal stability and elongation at break (70.79 %) (p < 0.05). In addition, the film has a high antibacterial effect on Staphylococcus aureus and Escherichia coli (Bacterial inhibition zone diameter: 19.59 mm and 18.66 mm) and the release rate of curcumin in the film reaches 82.60%, mainly following the Fickian diffusion. The film gradually turns red under alkaline conditions, a property that makes the films successful in monitoring the deterioration of pork during storage. Adding SSPI emulsions and curcumin to films has great potential for food freshness monitoring and packaging.

本研究将姜黄素(Cur)封装在琥珀酰化大豆分离蛋白(SSPI)乳液中,并与壳聚糖(CS)结合制备智能薄膜。SSPI 在油水界面的良好吸附能力为制备姜黄素乳液提供了良好的物理稳定性。研究人员对这些含有不同姜黄素含量的 SSPI 乳化液的 CS 智能薄膜的结构、机械、阻隔、抗氧化、抗菌性能和控释行为进行了评估。扫描电子显微镜(SEM)和傅立叶变换红外光谱(FT-IR)结果表明,含有姜黄素的乳液与 CS 基质相容。加入该乳液后,薄膜阻隔了 97.11% 的紫外线辐射,水蒸气透过率降低了 42%,溶胀度(32.26%)、水溶性(12%)、热稳定性和断裂伸长率(70.79 %)均得到改善(p <0.05)。此外,该薄膜对金黄色葡萄球菌和大肠杆菌具有很高的抗菌效果(抑菌区直径分别为 19.59 毫米和 18.66 毫米),姜黄素在薄膜中的释放率达到 82.60%,主要是通过费克扩散作用释放的。在碱性条件下,薄膜会逐渐变红,这一特性使薄膜能成功监测猪肉在储存过程中的变质情况。在薄膜中添加 SSPI 乳液和姜黄素在食品保鲜监测和包装方面具有很大的潜力。
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引用次数: 0
Corrigendum to ‘Low-density foreign body detection in food products using single-shot grid-based dark-field X-ray imaging’ [J. Food Eng. 129 (2022) 111189] 利用单次网格暗场 X 射线成像检测食品中的低密度异物"[J. Food Eng. 129 (2022) 111189] 更正
IF 5.5 2区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-08 DOI: 10.1016/j.jfoodeng.2024.112108
Hyunwoo Lim, Jonghyeok Lee, Soohyun Lee, Hyosung Cho, Hunwoo Lee, Duhee Jeon
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引用次数: 0
Transformation of quinoa seeds to nanoscale flour by ball milling: Influence of ball diameter and milling time on the particle sizing, microstructure, and rheology 通过球磨将藜麦种子转化为纳米级面粉:球直径和研磨时间对颗粒大小、微观结构和流变学的影响
IF 5.5 2区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-08 DOI: 10.1016/j.jfoodeng.2024.112127
Jasim Ahmed , Abdullah Alazemi , Poornima Ponnumani , Bini T. B. , Mahmoud Soliman , Lidia Emmanuval , Nickey M. Thomas

Among various size reduction techniques, high-energy ball milling is one of the most attractive means for plant-based foods. The objectives of the work were to investigate the influence of ball diameters (3, 6, and 13 mm) and milling time (2, 4, and 6 h) on particle size and microstructural properties of quinoa flours. Particle size analysis demonstrated that ball-milled particles were mostly in the range of nanoscales (122–295 nm). A longer milling time with larger balls significantly increased the particles to microscale (3.58 μm). The scanning electron microscopy displayed the conversion of quinoa starch granules into flakes after ball milling, however, the X-ray diffraction crystallinity peak observed at a 2θ value of 19–20° did not change. The AFM roughness parameters, arithmetic and squared mean heights of flours increased with increasing ball diameters. These results provided new insights for the application of ball milling, in particular in functional foods and pickering emulsion.

在各种减小粒度的技术中,高能球磨是对植物性食品最有吸引力的方法之一。这项工作的目的是研究球直径(3、6 和 13 毫米)和研磨时间(2、4 和 6 小时)对藜麦粉粒度和微观结构特性的影响。粒度分析表明,球磨颗粒大多在纳米级(122-295 纳米)范围内。用更大的球进行更长时间的研磨后,颗粒明显增加到微米级(3.58 μm)。扫描电子显微镜显示,球磨后藜麦淀粉颗粒转化为片状,但在 2θ 值为 19-20° 处观察到的 X 射线衍射结晶峰没有变化。淀粉的原子力显微镜粗糙度参数、算术平均高度和平方平均高度随球直径的增加而增加。这些结果为球磨的应用,特别是功能性食品和挑拣乳液的应用提供了新的见解。
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引用次数: 0
Extrusion-controlled lipid retention and distribution of wheat germ and its application combining exogenous starch 挤压控制小麦胚芽的脂质保留和分布及其结合外源淀粉的应用
IF 5.5 2区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-07 DOI: 10.1016/j.jfoodeng.2024.112128
Ruihao Niu , Jingyi Wang , Jianwei Zhou , Huan Cheng , Jianle Chen , Wenjun Wang , Donghong Liu , Enbo Xu

Wheat germ is an agricultural but low-economic by-product for animal feed or waste due to its susceptibility of hydrolytic/oxidative rancidities. Here, we use controllable extrusion to treat wheat germ, and with assistance of exogenous starch as lipid protective factor at different ratios (0:10 2:8, 3:7, 4:6). Oxidation of optimized germ extrudate was slowed down during storage, with total lipid retention rate reach up to ∼88.3%. Extrusion dynamic analysis showed that relatively high screw speed (100–150 rpm) significantly shortened mean residence time, increased axial diffusion velocity and reduced the loss of free and bound lipid. Type Ⅱ starch-lipid complex was changed to type Ⅰ during extrusion, with thermal transition peak declined. Wheat germ lipid was most evenly distributed under 100 rpm extrusion. The hydrogen bonding interaction between exogenous starch and lipids in wheat germ was strengthened, with significant modification in water absorption, water solubility, expansion and textual indexes.

小麦胚芽是一种农业副产品,但由于其易水解/氧化酸败,因此可用作动物饲料或废物,经济效益较低。在此,我们采用可控挤压法处理小麦胚芽,并辅以不同比例(0:10、2:8、3:7、4:6)的外源淀粉作为脂质保护因子。优化后的胚芽挤压物在贮藏过程中氧化速度减慢,总脂质保留率高达 88.3%。挤压动态分析表明,相对较高的螺杆转速(100-150 rpm)可明显缩短平均停留时间,提高轴向扩散速度,减少游离脂质和结合脂质的损失。在挤压过程中,Ⅱ型淀粉-脂质复合物转变为Ⅰ型,热转变峰值下降。在 100 rpm 挤压条件下,小麦胚芽脂质分布最均匀。小麦胚芽中外源淀粉和脂质之间的氢键作用得到加强,吸水性、水溶性、膨胀性和质构指标均有显著改变。
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引用次数: 0
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Journal of Food Engineering
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