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Effect of microwave-assisted extraction and autoclave extraction on the physicochemical properties of holy basil (Ocimum sanctum L.) by-product powder 微波萃取与蒸压萃取对圣罗勒副产物粉末理化性质的影响
IF 6.6 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2026-01-14 DOI: 10.1016/j.lwt.2026.119026
Papawarin Lowleraha , Pitiporn Ritthiruangdej , Nantawan Therdthai , Udomlak Sukatta , Phatcharee Kittisuban , Thanaphon Chonburom
This study investigated the potential to valorize Holy Basil (Ocimum sanctum L.) processing by-products into a functional powder by comparing the effects of two novel extraction methods, Microwave-Assisted Extraction (MAE) and Autoclave Extraction (AE), applied for 10, 20, and 30 min. While employing standard, non-comparable solid-to-liquid ratios optimized for each technology (MAE 1:0.4 w/v, AE 1:10 w/v), the experiment aimed to determine the optimal conditions for enhancing physicochemical and antioxidant properties through distinct thermal modification mechanisms. Results showed that both MAE and AE treatments significantly improved the nutritional profile, achieving a substantial increase in crude fiber and total dietary fiber by reducing non-fiber components. Crude fiber peaked at 42.90 % (AE-30). Both methods significantly increased antioxidant activity (DPPH, ABTS, FRAP) and the concentration of Total Phenolic Compounds (TPC) and Total Flavonoids (TF) (p < 0.05). Crucially, the methods exhibited divergent functional effects: MAE-30 was superior for maximizing TPC (103.21 mg GAE/g sample) and Water Solubility Index (WSI) (98.21 %), linked to the large, irregular pores observed via microstructural analysis. Conversely, AE-30 optimized Water Holding Capacity (WHC) (6.18 g/g) and Insoluble Dietary Fiber content due to better structural integrity. Both methods successfully transform agricultural by-products into valuable, high-fiber, antioxidant-rich ingredients, with MAE-30 providing the optimal conditions for a highly soluble, bioactive powder.
本研究通过比较微波辅助提取(MAE)和高压灭菌提取(AE)两种新型提取方法,分别应用10、20和30 min,研究了将圣罗勒(Ocimum sanctum L.)加工副产物转化为功能性粉末的潜力。实验采用标准的、不可比较的固液比(MAE:0.4 w/v, AE:10 w/v),旨在通过不同的热改性机制确定提高物理化学和抗氧化性能的最佳条件。结果表明,MAE和AE处理均显著改善了饲料的营养状况,通过减少非纤维成分,显著提高了粗纤维和总膳食纤维含量。粗纤维最高达42.90% (AE-30)。两种方法均显著提高了抗氧化活性(DPPH、ABTS、FRAP)和总酚类化合物(TPC)、总黄酮(TF)的浓度(p < 0.05)。重要的是,这些方法表现出不同的功能效果:MAE-30在最大TPC (103.21 mg GAE/g样品)和水溶性指数(WSI)(98.21%)方面优于MAE-30,这与通过微观结构分析观察到的大而不规则的孔隙有关。相反,由于AE-30具有较好的结构完整性,因此具有较高的持水能力(WHC) (6.18 g/g)和不溶性膳食纤维含量。这两种方法都成功地将农业副产品转化为有价值的、高纤维的、富含抗氧化剂的成分,MAE-30为高可溶性、生物活性粉末的生产提供了最佳条件。
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引用次数: 0
Isolation, identification, and binding mechanism of selenium-binding peptides from peanut protein hydrolysate 花生蛋白水解物中硒结合肽的分离、鉴定及结合机制研究
IF 6.6 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2026-01-14 DOI: 10.1016/j.lwt.2026.119043
Meiyue Wang , Xiaoling Zhao , Guanhao Bu , Jia Liu , Yan Du , Xiaojie Duan , Chenyang Yang , Qing Hao , Jinrong Zhu
Peptide-selenium complexes have become an important form of organic selenium. In this study, peanut peptide (PP) was prepared using peanut meal as the raw material. The high-binding peptide segments were isolated and purified, and their amino acid sequence were then identified by mass spectrometry and confirmed by solid-phase synthesis. The binding mechanism between PP and Na2SeO3 was further explored using particle size analysis, Zeta potential measurements, X-ray diffraction, Raman spectroscopy and molecular dynamics simulations. The results showed that a fraction with a high selenium binding rate of 92.5 % was obtained after purification. After identification by mass spectrometry and validation through solid-phase synthesis, six peptide segments with high binding activity were screened, among which the three peptides (SPQTQPKQEDRE, QVDDRQIVQ, and NLRGENESEEE) had the highest activity. Structural analysis verified that a new substance was formed through the binding of PP and selenium. Molecular dynamics simulations revealed that serine, glutamine, arginine, and asparagine in peptides could act as main binding sites for SeO32−. This study provides an important theoretical basis for the development of peanut peptide selenium supplements.
肽硒复合物已成为有机硒的一种重要形式。本研究以花生粕为原料制备花生肽(PP)。分离纯化高结合肽段,质谱鉴定其氨基酸序列,固相合成鉴定其氨基酸序列。通过粒径分析、Zeta电位测量、x射线衍射、拉曼光谱和分子动力学模拟等手段进一步探讨了PP与Na2SeO3的结合机理。结果表明,经纯化后得到了硒结合率达92.5%的高分离产物。经质谱鉴定和固相合成验证,筛选出6个具有高结合活性的肽段,其中SPQTQPKQEDRE、QVDDRQIVQ、NLRGENESEEE 3个肽段的结合活性最高。结构分析证实PP与硒结合形成了一种新的物质。分子动力学模拟表明,肽中的丝氨酸、谷氨酰胺、精氨酸和天冬酰胺可能是SeO32−的主要结合位点。本研究为开发花生肽硒补充剂提供了重要的理论依据。
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引用次数: 0
The deterioration law of pre-proofed frozen dough for the southern steamed bread and the improvement mechanism using hydroxypropyl distarch phosphate as the main improvers 研究了南方馒头用预冻面变质规律及以磷酸羟丙基二淀粉为主要改良剂的改善机理
IF 6.6 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2026-01-08 DOI: 10.1016/j.lwt.2026.119016
Guozhen Wang , Jiejun Zhou , Zhuang Liu , Sifan Liu , Guoyong Xu , Peng Yuan , Dongzhang Ying , Xianhui Chang , Kun Zhuang , Wenping Ding
This study investigated the deterioration patterns and underlying mechanisms of the pre-proofed frozen dough (PPFD) for the southern steamed bread (PPFD-SSB) during frozen storage, as well as the effects and the action mechanisms of two improvers primarily composed of hydroxypropyl distarch phosphate (HPDP). The southern steamed bread is characterized by its high sugar content. Two different improvers were applied to the PPFD. And the behavior of the moisture and the gluten proteins were evaluated in the fresh, frozen and frozen stored dough (after 7, 14, 21, and 28 days). The results indicated that freezing increased the freezable water content and decreased the bound water content in the dough. The ice crystals formed from freezable water damaged the microstructure of the dough. Frozen also disrupted the gluten protein structure. The HPDP-based improver was able to bind water, which was important to mitigate the accumulation of large ice crystals and reduce the structural damage caused by ice formation. It also improved the fermentation height and the viscoelasticity of the dough. These findings provided theoretical supports for enhancing the quality of the PPFD-SSB and established a basis for developing novel improvers aimed at optimizing the gluten protein structure.
研究了南方馒头冷冻面团(PPFD- ssb)在冷藏过程中的变质规律和变质机理,以及以磷酸羟丙基二淀粉(HPDP)为主的两种改良剂的保鲜效果和作用机理。南方馒头的特点是含糖量高。两种不同的改善剂应用于PPFD。并对新鲜、冷冻和冷冻保存面团(7、14、21和28天)的水分和面筋蛋白的行为进行了评价。结果表明,冷冻提高了面团的可冻水含量,降低了面团的束缚水含量。冻水形成的冰晶破坏了面团的微观结构。冷冻也破坏了面筋蛋白的结构。基于hdp的改进剂能够结合水,这对于减轻大冰晶的积聚和减少冰形成造成的结构破坏非常重要。提高了面团的发酵高度和粘弹性。这些研究结果为提高PPFD-SSB的质量提供了理论支持,并为开发旨在优化面筋蛋白结构的新型改良剂奠定了基础。
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引用次数: 0
Effects of packaging methods and storage duration on yak meat flavor profiles during chilled storage: GC-IMS and GC-MS evaluation 包装方式和贮藏时间对牦牛肉冷藏风味特征的影响:GC-IMS和GC-MS评价
IF 6.6 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2026-01-08 DOI: 10.1016/j.lwt.2026.119002
Shaoke Guo , Chao Chen , Mengli Cao , Jie Pei , Lin Xiong , Xian Guo
Yak meat is valued for its unique flavor and nutrition, but refrigerated storage packaging affects its flavor quality. This study focuses on longissimus thoracis et lumborum (LTL) of yaks and compares the regulatory effects of tray packaging (aerobic environment) and vacuum packaging (low oxygen environment) on the taste and metabolic characteristics of meat products at 3 days (mid-term of short-term storage) and 7 days (end of short-term storage, upper limit of conventional shelf life) under 4 °C refrigeration conditions. The relevant mechanisms are analyzed by combining gas chromatography-ion mobility spectrometry (GC-IMS) and gas chromatography-mass spectrometry (GC-MS) techniques. The results showed that GC-IMS detection revealed that tray packaging had significantly higher fresh flavor compounds (alcohols, aldehydes, esters) than vacuum at 3 days, better retaining initial aroma. However, when storage was extended to 7 days, substances imparting undesirable flavors (2-methylbutanal-D, 1-hydroxy-2-propanone, 2-propanethiol, and 2-ethylfuran) accumulated significantly in tray packaging meat, while vacuum packaging effectively inhibited the formation of such substances. GC-MS analysis indicated that the contents of fumaric acid and glutamine in the vacuum packaging groups (3/7 days) were consistently higher than those in tray packaging groups. After 7 days of storage, the content of free amino acids (L-cysteine, L-lysine) in vacuum packaging meat was significantly increased. Furthermore, glyceraldehyde 3-phosphate, formamide, and 1-methoxy-2-methylprop-1-en-1-ol were identified as the key differential metabolites between the two packaging methods. KEGG pathway enrichment analysis showed that amino acid metabolism was the core driving pathway for changes in the composition of flavor compounds during the oxidation of yak meat under chilled storage. The selection of yak meat packaging should be adjusted according to storage duration: tray packaging is more suitable for short-term storage (within 3 days) to retain fresh flavor, while vacuum packaging can more effectively maintain meat flavor quality during long-term storage (7 days) by inhibiting oxidative reactions and regulating umami-related metabolism. The results of this study provide experimental support for the targeted optimization of fresh yak meat packaging schemes and the extension of its flavor shelf life.
牦牛肉因其独特的风味和营养价值而受到重视,但冷藏包装会影响其风味品质。本研究以牦牛胸腰最长肌(LTL)为研究对象,比较了托盘包装(有氧环境)和真空包装(低氧环境)在4℃冷藏条件下对肉制品3天(短期储存中期)和7天(短期储存结束,常规保质期上限)的口感和代谢特性的调节作用。结合气相色谱-离子迁移谱法(GC-IMS)和气相色谱-质谱法(GC-MS)分析了相关机理。结果表明,气相色谱- ims检测结果表明,托盘包装在3 d时的新鲜风味化合物(醇类、醛类、酯类)含量明显高于真空包装,能更好地保留初始香气。然而,当储存时间延长至7天时,托盘包装肉类中产生不良风味的物质(2-甲基丁醇- d、1-羟基-2-丙烷酮、2-丙硫醇和2-乙基呋喃)显著积累,而真空包装有效地抑制了这些物质的形成。GC-MS分析表明,真空包装组(3/7 d)富马酸和谷氨酰胺含量均高于托盘包装组。贮藏7 d后,真空包装肉中游离氨基酸(l -半胱氨酸、l -赖氨酸)含量显著提高。此外,3-磷酸甘油醛、甲酰胺和1-甲氧基-2-甲基丙烯-1-烯-1-醇被确定为两种包装方法之间的关键差异代谢物。KEGG途径富集分析表明,氨基酸代谢是牦牛肉冷藏氧化过程中风味物质组成变化的核心驱动途径。牦牛肉包装的选择应根据储存期限进行调整:托盘包装更适合短期储存(3天以内)以保持鲜味,而真空包装可以通过抑制氧化反应和调节鲜味相关代谢,在长期储存(7天)中更有效地保持肉的风味品质。本研究结果为有针对性地优化鲜肉包装方案,延长鲜肉风味保质期提供了实验支持。
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引用次数: 0
Cutting boards as a source of high histamine-producing bacteria: Persistence and transfer to fish fillets 砧板作为高组胺产生细菌的来源:持久性和转移到鱼片
IF 6.6 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2026-01-07 DOI: 10.1016/j.lwt.2026.119017
Sahar Elmi Anvari, Mehdi Zarei, Maryam Ghaderi Ghahfarokhi
Microbial contamination of food contact surfaces, particularly cutting boards, poses a significant risk for secondary contamination and foodborne illness, with histamine-producing bacteria (HPB) being a key concern due to their association with scombroid poisoning. This study examined the prevalence, biofilm formation, persistence, and cross-contamination potential of high histamine-producing (HHP) bacteria isolated from cutting boards in fish retail markets. Out of 288 isolates, two Gram-negative strains—Morganella morganii and Raoultella planticola—were identified as high histamine producers. Both strains demonstrated biofilm-forming ability under different nutrient conditions (TSB, diluted TSB, distilled water) and temperatures (22 °C and 35 °C). Persistence assays revealed that surface-associated M. morganii cells declined to undetectable levels by day 8, whereas R. planticola remained viable until day 14. Biofilm cells exhibited prolonged survival, with R. planticola persisting for 20 days under dry, nutrient-deprived conditions. Bacterial transfer was found to occur at varying contamination levels (4–6 log CFU/cm2) and contact times (2–10 min). Bacterial transfer was found to increase significantly with higher initial contamination levels (P < 0.05). However, no significant variation in transfer efficiency was observed across different contamination levels or contact times (P > 0.05). Furthermore, transfer rates were observed to decrease progressively with consecutive fillet contacts, regardless of the initial inoculum level or contact duration. The demonstrated potential for cross-contamination to fish fillets, even after sequential contacts, underscores a substantial risk for scombroid poisoning and highlights the need for stringent hygiene protocols targeting biofilm removal in fish retail markets.
食品接触表面的微生物污染,特别是砧板,造成二次污染和食源性疾病的重大风险,产生组胺的细菌(HPB)是一个关键问题,因为它们与鲭鱼中毒有关。本研究调查了从鱼类零售市场的砧板中分离出的高组胺生成(HHP)细菌的流行率、生物膜形成、持久性和交叉污染潜力。288株分离株中,两株革兰氏阴性菌株——摩氏摩根菌和足底拉乌尔菌——被鉴定为高组胺产生菌。两株菌株在不同的营养条件(TSB、稀释TSB、蒸馏水)和温度(22°C和35°C)下均表现出生物膜形成能力。持久性测试显示,表面相关的摩根氏分枝杆菌细胞在第8天下降到无法检测到的水平,而足底分枝杆菌在第14天仍然存活。生物膜细胞表现出较长的存活时间,在干燥、缺乏营养的条件下,车前草可存活20天。发现细菌转移发生在不同的污染水平(4-6 log CFU/cm2)和接触时间(2-10分钟)。发现细菌转移随着初始污染水平的增加而显著增加(P < 0.05)。然而,在不同的污染水平或接触时间内,转移效率没有显著变化(P > 0.05)。此外,无论初始接种水平或接触时间如何,观察到随着连续的鱼片接触,转移率逐渐降低。已证明的鱼片交叉污染的可能性,即使在连续接触之后,也强调了鲭鱼中毒的巨大风险,并强调了在鱼类零售市场针对生物膜去除的严格卫生协议的必要性。
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引用次数: 0
Mitigation of cyanide formation in Jiangxiangxing Baijiu brewing sorghum during grain hydration: Effects of abscisic acid and γ-irradiation 姜香星白酒酿造高粱籽粒水化过程中氰化物的形成:脱落酸和γ辐照的影响
IF 6.6 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2026-01-07 DOI: 10.1016/j.lwt.2026.119015
Yuxuan Zhu , Yehui Han , Shuang Chen , Yan Xu
Cyanide converts to carcinogenic ethyl carbamate upon reaction with ethanol in distilled spirits, raising safety concerns in using cyanogenic crops for fermentation and distillation. Thus, control of cyanide in cyanogenic sorghum-based liquors, such as baijiu, represents a scientific and industrial challenge. This study introduced a novel enzymatic–alkaline method to quantify total cyanide in sorghum used for baijiu brewing. Results showed that dhurrin is the primary source of cyanide in sorghum. Additionally, dhurrin is produced during grain hydration, as it mimics germination conditions. High levels of dhurrin were detected in intact hydrated kernels, whereas crushing limited dhurrin synthesis. Two additional interventions, abscisic acid (ABA) spraying and γ-irradiation, were evaluated to test their ability to reduce dhurrin production during sorghum hydration. Both methods reduced total cyanide levels by approximately 80 %. Importantly, neither approach compromised starch structure or nutritional value. However, ABA was more effective at preserving starch crystallinity and structural stability, whereas γ-irradiation offered advantages in speed and simplicity.
在蒸馏酒中,氰化物与乙醇反应后会转化为致癌的氨基甲酸乙酯,这引起了使用含氰作物进行发酵和蒸馏的安全问题。因此,控制以高粱为原料的白酒中的氰化物是一项科学和工业挑战。介绍了一种新的酶碱法测定白酒用高粱中总氰化物的方法。结果表明,苦胆素是高粱中氰化物的主要来源。此外,苦胆素在谷物水化过程中产生,因为它模拟发芽条件。在完整的水合果仁中检测到高水平的苦胆素,而粉碎则限制了苦胆素的合成。另外两种干预措施,脱落酸(ABA)喷洒和γ辐照,测试了它们在高粱水化过程中减少苦胆素产量的能力。这两种方法都能将总氰化物含量降低约80%。重要的是,这两种方法都不会损害淀粉的结构或营养价值。然而,ABA在保持淀粉结晶度和结构稳定性方面更有效,而γ-辐照在速度和简单性方面具有优势。
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引用次数: 0
Influence of roasted and unroasted berry seed oils on the formation of Maillard reaction products in model gluten-free rice bread 烘培和未烘培浆果籽油对模型无麸质米面包中美拉德反应产物形成的影响
IF 6.6 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2026-01-07 DOI: 10.1016/j.lwt.2026.119012
Maria Barbara Różańska , Joanna Zembrzuska , Sylwia Mildner-Szkudlarz
This study examines the impact of oils from unconventional sources — chokeberry, blackcurrant, raspberry, and strawberry seeds — applied with or without prior roasting, on the formation of Maillard reaction products in a model gluten-free rice bread. The addition of oils from roasted chokeberry and blackcurrant seeds significantly reduced furosine levels in the crumb by 32 % and 25 %, respectively. In contrast, only the oil from roasted strawberry seeds increased furosine content, by 42 % in the crust and 49 % in the crumb. The use of oils from roasted seeds resulted in an average 23 % reduction of free fluorescent advanced glycation end-products (AGEs) in the crust. However, the addition of roasted blackcurrant seed oil was associated with a 48 % increase in free fluorescent AGEs in the crumb. Roasting-induced changes in berry seed oils had no significant effect on the mitigation of 5-hydroxymethylfurfural (5-HMF) formation in the crust. No significant differences were observed in N-ε-(carboxymethyl)lysine (CML) levels in crust when comparing oils from roasted and unroasted seeds. Higher concentrations of N-ε-(carboxyethyl)lysine (CEL) relative to CML in the crust suggest a dominant role of lipid-derived glycation pathways in this food system.
本研究考察了非常规来源的油——蔓越莓、黑加仑子、覆盆子和草莓籽——在事先烘烤或不烘烤的情况下对无麸质大米面包中美拉德反应产物形成的影响。加入烤过的蔓越莓和黑加仑籽油后,面包屑中的糠氨酸含量分别显著降低了32%和25%。相比之下,只有烤草莓籽的油增加了糠氨酸的含量,在面包皮中增加了42%,在面包屑中增加了49%。使用烘焙种子的油导致外壳中游离荧光晚期糖基化终产物(AGEs)平均减少23%。然而,加入烤黑加仑籽油与面包屑中游离荧光AGEs增加48%有关。烘烤引起的浆果籽油含量变化对减缓果皮中5-羟甲基糠醛(5-HMF)的形成没有显著影响。烤制和未烤制籽油籽皮中N-ε-(羧甲基)赖氨酸(CML)含量无显著差异。相对于CML,地壳中N-ε-(羧乙基)赖氨酸(CEL)浓度较高,表明脂质衍生的糖基化途径在该食物系统中起主导作用。
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引用次数: 0
A novel strategy for β-glucan enrichment during oat germination: Low temperature stress combined with slightly acidic electrolyzed water 低温胁迫结合微酸性电解水对燕麦萌发过程中β-葡聚糖富集的新策略
IF 6.6 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2026-01-07 DOI: 10.1016/j.lwt.2026.119014
Shaokang Liu, Hongrui Ren, Yu Quan, Ziyue Wang, Jianxiong Hao
The treatment of germinating seeds with slightly acidic electrolyzed water (SAEW) is a promising sustainable agricultural technology, but there is limited research on its effect on enriching β-glucan in germinating oat seeds. In this study, the effects of SAEW treatments at two different temperatures (25 °C and 4 °C) on the β-glucan content in germinating oat seeds were investigated by assessing morphological indicators, as well as changes in substances related to the β-glucan content, functional characteristics, and the structural characteristics of β-glucan during germination. Although the β-glucan content in germinating oat seeds continued to increase at 36 h, 24 h was selected as the optimal interval for comparing treatment effects. The results showed that the enrichment of β-glucan in germinating oat seeds was highest with the 4 °C + SAEW treatment. At 24 h of germination after 4 °C + SAEW treatment, the β-glucan content was 9.69 ± 0.30 mg/g, the β-glucanase activity was 24003.22 ± 242.52 U/mL, the soluble sugars content was 40.46 ± 0.72 mg/g, the reducing sugars content was 5.25 ± 0.01 mg/g, the total saponin content was 186.48 ± 7.01 mg/g, the glucose content (indicative of monosaccharide composition) was 14.22 mg/L, and the molecular weight of β-glucan was 163.10 kDa. These index values in the 4 °C + SAEW treatment group were significantly different from those in the tap water (TW) control group and the 25 °C + SAEW treatment group (p < 0.05), indicating that the 4 °C + SAEW treatment was the most effective. We also evaluated the ability of extracts from oat seeds in the different groups to adsorb glucose, inhibit glucose diffusion, inhibit α-glucosidase activity, and inhibit pancreatic amylase activity. The extract from oat seeds under the 4 °C + SAEW treatment had significantly stronger effects on these factors compared with extracts from oat seeds in the TW control group and the 25 °C + SAEW treatment group (p < 0.05). Treatment with SAEW at low temperature is a novel strategy for the efficient enrichment of oat β-glucan.
微酸性电解水(SAEW)处理发芽种子是一种很有前途的可持续农业技术,但对其在发芽燕麦种子中富集β-葡聚糖的效果研究有限。本研究以25°C和4°C两种不同温度下SAEW处理对萌发期燕麦种子中β-葡聚糖含量的影响为研究对象,通过形态指标、萌发期β-葡聚糖含量相关物质的变化、β-葡聚糖的功能特征、结构特征等进行研究。虽然在36 h时萌发的燕麦种子中β-葡聚糖含量继续增加,但选择24 h作为比较处理效果的最佳间隔。结果表明,在4℃+ SAEW处理下,萌发中的燕麦种子中β-葡聚糖的富集量最高。4℃+ SAEW处理后萌发24 h, β-葡聚糖含量为9.69±0.30 mg/g, β-葡聚糖酶活性为24003.22±242.52 U/mL,可溶性糖含量为40.46±0.72 mg/g,还原糖含量为5.25±0.01 mg/g,总皂苷含量为186.48±7.01 mg/g,葡萄糖含量(单糖组成指标)为14.22 mg/L, β-葡聚糖分子量为163.10 kDa。4°C + SAEW处理组与自来水(TW)对照组和25°C + SAEW处理组相比,这些指数值均有显著差异(p < 0.05),说明4°C + SAEW处理效果最好。我们还评估了不同组燕麦种子提取物吸附葡萄糖、抑制葡萄糖扩散、抑制α-葡萄糖苷酶活性和抑制胰淀粉酶活性的能力。与TW对照组和25°C + SAEW处理组相比,4°C + SAEW处理组燕麦种子提取物对这些因素的影响均显著增强(p < 0.05)。低温SAEW处理是一种高效富集燕麦β-葡聚糖的新方法。
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引用次数: 0
Electron beam pretreatment to enhance Schiff base of watermelon seed shell nanocellulose with tannic acid-decylamine: The complex's universality for various emulsion systems 单宁酸-癸胺电子束预处理增强西瓜籽壳纳米纤维素席夫碱的研究:该配合物适用于各种乳液体系
IF 6.6 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2026-01-06 DOI: 10.1016/j.lwt.2025.118960
Li Niu , Yupeng Fan , Yanliang Guo , Qian Lin , Hanlin Guan , Xiangrui Ren , Wenqing Zhao , Wenhao Li , Huijun Zhang
Nanocellulose has shown great potential and practical applicability across numerous fields, but its inherent hydrophilicity is a major limitation for its use in non-aqueous environments. In this work, electron beam irradiation pretreatment at 40, 80, and 120 kGy accelerated the Schiff base reaction of watermelon seed shell nanocellulose (WNC) with tannic acid and decylamine. Consequently, hydrophobic WNC with a DS of 0.42–0.72 was synthesized, up to 40 %–140 % higher than untreated WNC (0.30). A decreased hydrophilic-lipophilic balance and contact angle confirmed the improved lipophilicity. FTIR confirmed the successful formation of imine (-C=N-) linkages, indicating effective Schiff base grafting. Morphological observations revealed that a transformation of WNC from elongated ribbons into aggregated granules with more crystal defects formed after modification. Hydrophobic WNC exhibited enhanced oil-holding capacity and radical-scavenging activity. A cascade strategy was developed to fabricate stable low-oil emulsions and high internal phase emulsion (HIPE) gels using the hydrophobic WNC. Notably, the HIPE gels showed strong oil entrapment and effectively retarded lipid oxidation. This work unlocks the value of agricultural byproducts as a source of nanocellulose and offers a streamlined and sustainable strategy for producing highly functional nanocellulose.
纳米纤维素在许多领域显示出巨大的潜力和实用性,但其固有的亲水性是其在非水环境中应用的主要限制。在40、80和120 kGy的辐照条件下,电子束预处理加速了西瓜籽壳纳米纤维素(WNC)与单宁酸和癸胺的希夫碱反应。因此,合成的疏水WNC的DS为0.42-0.72,比未处理的WNC(0.30)高出40% - 140%。亲水亲脂平衡和接触角的降低证实了亲脂性的提高。FTIR证实亚胺(- c =N-)键成功形成,表明席夫碱接枝有效。形态学观察表明,改性后的WNC由细长的带状转变为聚集的颗粒,形成了更多的晶体缺陷。疏水性WNC具有较强的持油能力和自由基清除能力。采用疏水WNC制备了稳定的低油乳液和高内相乳液(HIPE)凝胶。值得注意的是,HIPE凝胶表现出很强的油包裹性,有效地延缓了脂质氧化。这项工作揭示了农业副产品作为纳米纤维素来源的价值,并为生产高功能纳米纤维素提供了一种精简和可持续的策略。
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引用次数: 0
Kinetic characteristics and energy efficiency analysis of microwave-dried fresh ginger: Impacts of key process parameters 微波干燥鲜姜的动力学特性及能效分析:关键工艺参数的影响
IF 6.6 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2026-01-06 DOI: 10.1016/j.lwt.2026.118999
Yaping Wang , Boyu Li , Yu Xi , Longwei Zheng , Wenhua Zi
Microwave drying has emerged as an energy-efficient and environmentally benign alternative to conventional methods. Given the considerable nutritional and medicinal value of ginger, this study systematically investigates the effects of key parameters, such as microwave power (600–1800 W), slice thickness (1–7 mm), and loading amount (200–500 g), on drying kinetics and energy consumption of microwave-dried ginger. The mechanisms of key parameters on moisture migration and energy changes are discussed. The results reveal that the Page model best characterizes power-dependent drying, while the Midilli model better fits loading and thickness variations. Increasing microwave power considerably increases moisture diffusivity (Deff) and drying efficiency from 26.46 % to 40.56 % but reduces the specific energy consumption (Es) from 16.89 to 9.01 MJ/kg. Thickness exhibits dual effects—it improves Deff but decreases drying efficiency from 43.31 % to 26.58 % while increasing Es from 5.41 to 15.24 MJ/kg. Higher loading amounts improve drying efficiency from 30.05 % to 42.43 % and Es from 12.43 to 6.23 MJ/kg, despite slight reduction in Deff. The optimal parameters are identified as 1200–1300 W power, 350 g loading, and 2–4 mm thickness. These findings establish theoretical foundations and provide technical guidance for precision drying of high-moisture agricultural products.
微波干燥已成为传统方法的一种节能环保的替代方法。鉴于生姜具有丰富的营养价值和药用价值,本研究系统地考察了微波功率(600 ~ 1800 W)、薄片厚度(1 ~ 7 mm)、添加量(200 ~ 500 g)等关键参数对微波干燥生姜的干燥动力学和能量消耗的影响。讨论了关键参数对水分迁移和能量变化的影响机理。结果表明,Page模型最能表征功率依赖性干燥,而Midilli模型更适合负载和厚度变化。增加微波功率可显著提高水分扩散率(Deff)和干燥效率,从26.46%提高到40.56%,但可将比能量消耗(Es)从16.89降低到9.01 MJ/kg。厚度具有双重作用,使干燥效率从43.31%降低到26.58%,使干燥效率从5.41 MJ/kg提高到15.24 MJ/kg。较高的装载量使干燥效率从30.5%提高到42.43%,Es从12.43提高到6.23 MJ/kg,尽管Deff略有降低。确定最佳参数为:功率1200 ~ 1300w,负载350g,厚度2 ~ 4mm。研究结果为高水分农产品的精密干燥提供了理论基础和技术指导。
{"title":"Kinetic characteristics and energy efficiency analysis of microwave-dried fresh ginger: Impacts of key process parameters","authors":"Yaping Wang ,&nbsp;Boyu Li ,&nbsp;Yu Xi ,&nbsp;Longwei Zheng ,&nbsp;Wenhua Zi","doi":"10.1016/j.lwt.2026.118999","DOIUrl":"10.1016/j.lwt.2026.118999","url":null,"abstract":"<div><div>Microwave drying has emerged as an energy-efficient and environmentally benign alternative to conventional methods. Given the considerable nutritional and medicinal value of ginger, this study systematically investigates the effects of key parameters, such as microwave power (600–1800 W), slice thickness (1–7 mm), and loading amount (200–500 g), on drying kinetics and energy consumption of microwave-dried ginger. The mechanisms of key parameters on moisture migration and energy changes are discussed. The results reveal that the Page model best characterizes power-dependent drying, while the Midilli model better fits loading and thickness variations. Increasing microwave power considerably increases moisture diffusivity (<em>Deff</em>) and drying efficiency from 26.46 % to 40.56 % but reduces the specific energy consumption (Es) from 16.89 to 9.01 MJ/kg. Thickness exhibits dual effects—it improves <em>Deff</em> but decreases drying efficiency from 43.31 % to 26.58 % while increasing Es from 5.41 to 15.24 MJ/kg. Higher loading amounts improve drying efficiency from 30.05 % to 42.43 % and Es from 12.43 to 6.23 MJ/kg, despite slight reduction in <em>Deff</em>. The optimal parameters are identified as 1200–1300 W power, 350 g loading, and 2–4 mm thickness. These findings establish theoretical foundations and provide technical guidance for precision drying of high-moisture agricultural products.</div></div>","PeriodicalId":382,"journal":{"name":"LWT - Food Science and Technology","volume":"240 ","pages":"Article 118999"},"PeriodicalIF":6.6,"publicationDate":"2026-01-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145941359","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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LWT - Food Science and Technology
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