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Recycling of metallic values from discarded tantalum capacitors 从废弃钽电容器中回收金属价值
IF 1.2 Q2 Earth and Planetary Sciences Pub Date : 2023-02-14 DOI: 10.1080/25726641.2023.2177243
Shaila Mir, N. Dhawan
ABSTRACT The generation of electronic waste generation has led to significant attention towards metal recovery from urban sources. Due to scarcity, finite resources, and geopolitical constraints, tantalum recycling from capacitors is essential. In this study, sequential separation involving the removal of tightly bound epoxy resin and metallic impurities is carried out. Pyrolysis as a pre-treatment and its response on phase transformation, resin decomposition and metal enrichment are investigated. Pyrolysis effectively liberates the tantalum–rich sintered core from outer resin which is followed by mild organic acid leaching. The manganese impurity was removed from the core to obtain Ta recovery of ∼94.8% with ∼96% purity in the leach residue. The separated resin component was subjected to conventional sink-float separation for the recovery of metallic values (silver, tantalum). It is found that 100 g (666 units) of Ta capacitors can yield 34 g of Ta, equivalent to 0.28 tons of primary ore.
摘要电子垃圾的产生引起了人们对从城市来源回收金属的极大关注。由于稀缺、资源有限和地缘政治限制,从电容器中回收钽至关重要。在本研究中,进行了顺序分离,包括去除紧密结合的环氧树脂和金属杂质。研究了作为预处理的热解及其对相变、树脂分解和金属富集的响应。热解有效地将富含钽的烧结芯从外部树脂中释放出来,然后进行温和的有机酸浸出。从岩心中去除锰杂质,以获得约94.8%的Ta回收率,浸出残渣中的纯度为约96%。将分离的树脂组分进行常规的沉浮分离以回收金属值(银、钽)。发现100 g(666个单位)的Ta电容器可以产生34 g钽,相当于0.28吨原矿。
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引用次数: 1
Assessment of Physiochemical Qualities of Soil at Kataeregi Mining Site, Niger State, Nigeria 尼日利亚尼日尔州Kataeregi矿区土壤理化性质评价
IF 1.2 Q2 Earth and Planetary Sciences Pub Date : 2023-02-04 DOI: 10.11648/j.ijmpem.20220704.11
J. Shehu, Usman Defyan Alhassan, Abdulwaheed Adewuyi Rafiu, A. Idris-Nda, A. Alkali
: Soil samples were analysed to determine the heavy metals (pH, Cd, Zn, Ar, Cr, Cu, Pb, Hg, Fe and Ni) at Kataeregi mining site, Niger State, Nigeria. Ten soil samples were collected from four soil pits and control site were collected 100 m away from mining site. The results of the analysed soil samples are as follows: Soil pH values of various locations ranged from 6.08 to 8.12 which is indicative of moderately alkaline, Ar values ranged from 4.23 mg/kg to 12.05 mg/kg, Ni values ranged between 4.00 mg/kg and 70.0 mg/kg and is above the standard set for agricultural and human health, Fe ranged from 0.72 mg/kg to 16.03 mg/kg, Hg values ranged between 0.11 and 1.01, Cd values ranged from 4.76 mg/kg to 9.32 mg/kg which is indicative of high concentration of chemical parameters and Cr ranged between 9.89 mg/kg and 27.00 mg/kg. Cu values ranged from 99.78 mg/kg to 111.9 mg/kg while Pb values ranged between 1.0 mg/kg and 6.07 mg/kg and Zn values ranged from 9.91 mg/kg to 13.0 mg/kg. It is observed that concentrations of Ar, Ni, Hg, Cd and Cr are above the CSQG standard while that of Fe is found to be below the standard set by CSQG & WHO and Cu, Pb, and Zn are within the permissible range.
对尼日利亚尼日尔州Kataeregi矿区的土壤样品进行了分析,以确定重金属(pH、Cd、Zn、Ar、Cr、Cu、Pb、Hg、Fe和Ni)。在4个土坑中采集10个土样,在距矿区100 m处采集对照场地。土样分析结果如下:不同地点土壤pH值在6.08 ~ 8.12之间,为中等碱性,Ar值在4.23 ~ 12.05 mg/kg之间,Ni值在4.00 ~ 70.0 mg/kg之间,高于农业和人体健康标准,Fe值在0.72 ~ 16.03 mg/kg之间,Hg值在0.11 ~ 1.01之间,Cd值为4.76 mg/kg至9.32 mg/kg,表明化学参数浓度较高,Cr值为9.89 mg/kg至27.00 mg/kg。Cu值在99.78 ~ 111.9 mg/kg之间,Pb值在1.0 ~ 6.07 mg/kg之间,Zn值在9.91 ~ 13.0 mg/kg之间。其中,Ar、Ni、Hg、Cd、Cr高于CSQG标准,Fe低于CSQG和WHO标准,Cu、Pb、Zn在允许范围内。
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引用次数: 0
Removal of Fe2+ and Mn2+ from Water by Using Mining Rock Wastes and Their Synthesized Zeolites 利用采煤废石及其合成沸石去除水中铁锰离子
IF 1.2 Q2 Earth and Planetary Sciences Pub Date : 2023-02-04 DOI: 10.11648/j.ijmpem.20220704.12
Walaa Ali Hassan, Mohamed Abdel-Moneim Mohamed, Ezzat Abdalla Ahmed, Mohamed Said Shaban, Mostafa Ragab Abukhadra
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引用次数: 0
Microindentation testing as a means of predicting lump iron ore physical properties 微压痕试验作为预测块状铁矿物理性质的一种方法
IF 1.2 Q2 Earth and Planetary Sciences Pub Date : 2023-01-28 DOI: 10.1080/25726641.2023.2165292
Michael Peterson
ABSTRACT This study utilised Vickers and Knoop microindentation testing to characterise the physical and chemical properties of a range of iron ore material types and lump ore samples. Lump ore composite microhardness (CH) and fracture toughness (CFT) correlated best with Tumble and Abrasion Indices and with Fe-total, Al2O3 and LOI contents. General trends were evident between CH/CFT and other common metallurgical indices, e.g. higher Reduction Degradation Index with lower CH. Correlations between ore group CH/CFT and the metallurgical data were generally similar, but relatively stronger, than those for the lump ores. The chemistry of mineralogical-textural sub-sets of ore groups correlated with lump ore CH/CFT. Calculating ore group CH/CFT using a textural method is therefore capable of capturing differences in ore group chemistry that relate in part to texture. A textural database of microhardness and fracture toughness can be utilised with automated optical image analysis to provide geometallurgical characterisation of iron ores.
本研究利用维氏和努氏微压痕测试来表征一系列铁矿石材料类型和块状矿石样品的物理和化学性质。块状矿石复合显微硬度(CH)和断裂韧性(CFT)与翻滚指数、磨损指数、总fe、Al2O3和LOI含量相关性最好。CH/CFT与其他常见冶金指标之间存在明显的总体趋势,即还原降解指数越高,CH越低。矿石组CH/CFT与冶金数据之间的相关性基本相似,但相对于块状矿石的相关性更强。与块状矿CH/CFT相关的矿群矿物结构亚组化学特征。因此,使用结构方法计算矿石组的CH/CFT能够捕捉到部分与结构有关的矿石组化学差异。显微硬度和断裂韧性的纹理数据库可以与自动光学图像分析相结合,提供铁矿石的地质冶金特征。
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引用次数: 1
New Directions in Mineral Processing, Extractive Metallurgy, Recycling and Waste Minimization: An EPD Symposium in Honor of Patrick R. Taylor 矿物加工、萃取冶金、回收和废物最小化的新方向:环保署纪念帕特里克·r·泰勒的研讨会
IF 1.2 Q2 Earth and Planetary Sciences Pub Date : 2023-01-01 DOI: 10.1007/978-3-031-22765-3
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引用次数: 1
Investigation of transformations of low-grade manganese ore during the roasting process 低品位锰矿在焙烧过程中的转化研究
IF 1.2 Q2 Earth and Planetary Sciences Pub Date : 2022-12-28 DOI: 10.1080/25726641.2022.2161736
H. Ali, M. El-Sadek, H. Ahmed
ABSTRACT The transformations of low-grade manganese ore were investigated during roasting in the air at different temperatures up to 1200°C. The transformations were followed up by XRD and TGA-DTA. Moreover, the morphology and magnetic properties were determined by SEM and VSM. It was observed that MnO2 transformed to the lower oxide Mn5O8 at 500°C and then to bixbyite (Mn2O3) at 600°C. Finally, the bixbyite decomposed to hausmannite (Mn3O4) at 800°C. Increasing the roasting temperature to 900°C induced a reaction between hematite and hausmannite and led to the formation of a small amount of solid solution of the ferrite spinel MnFe2O4. Further increase in temperature to 1000°C led to the formation of a solid solution of braunite (Mn7SiO12) which decomposed to rhodonite (MnSiO3) at 1200°C. The magnetic susceptibility of the original ore gradually increased with the roasting temperature, from 0.119 × 10−3 at ambient temperature to a maximum value of 80 × 10−3 at 1200°C.
摘要研究了低品位锰矿在1200°C以下不同温度下的空气焙烧过程中的转化过程。通过XRD和TGA-DTA对转化进行了跟踪。此外,通过扫描电镜和VSM测定了其形貌和磁性能。观察到MnO2在500°C时转化为较低的氧化物Mn5O8,然后在600°C时转变为二氧化二钒(Mn2O3)。最后,在800°C下,方镁石分解为锰铝石(Mn3O4)。将焙烧温度提高到900°C会引发赤铁矿和hausmannite之间的反应,并导致形成少量铁氧体尖晶石MnFe2O4的固溶体。温度进一步升高至1000°C,形成了在1200°C分解为菱铁矿(MnSiO3)的黑柱石(Mn7SiO12)固溶体。原始矿石的磁化率随着焙烧温度的升高而逐渐增加,从0.119 × 环境温度为10−3,最大值为80 × 1200°C时为10−3。
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引用次数: 0
CFD modelling of copper flash smelting furnace – reaction shaft 铜闪速熔炼炉-反应轴的CFD建模
IF 1.2 Q2 Earth and Planetary Sciences Pub Date : 2022-12-28 DOI: 10.1080/25726641.2022.2160081
S. Nirmal Kumar, B. Desai, V. Tathavadkar, Yogesh Patel, Jayesh Patel, Anil Singh, Ka Vakil, Sokkuraj Kanakanand
ABSTRACT Flash smelting furnace (FSF) technology by Outokumpu is one of the most widely employed methods for copper smelting. Developing an understanding of the impact of the process parameters on smelting operation through modelling is the key to improve the smelting efficiency. Though several numerical approaches for modelling the FSF have been reported, this paper focuses on a detailed approach of computational fluid dynamics (CFD) modelling which overcomes the limitations of the earlier models by incorporating feed mineralogy and smelting reaction kinetics. The FSF based at Birla Copper, Dahej was modelled considering the reaction shaft and settler freeboard as the domain, where most of the gas-solid phase reactions occur. This model provides an exhaustive information on the FSF operation which aids in visualizing the phenomena occurring inside the furnace. A parametric study was done to validate and demonstrate the impact of various process parameters on smelting.
Outokumpu公司的闪速熔炼炉(FSF)技术是目前应用最广泛的铜冶炼方法之一。通过建模来了解工艺参数对冶炼操作的影响是提高冶炼效率的关键。虽然已经报道了几种模拟FSF的数值方法,但本文重点介绍了计算流体动力学(CFD)建模的详细方法,该方法通过结合进料矿物学和冶炼反应动力学克服了早期模型的局限性。在Dahej Birla Copper的FSF模型中,考虑了反应轴和沉降器干舷作为主要发生气固相反应的区域。该模型提供了FSF操作的详尽信息,有助于可视化炉内发生的现象。进行了参数化研究,验证和论证了各工艺参数对冶炼的影响。
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引用次数: 1
Use of cavitation to enhance the leaching kinetics of refractory gold ores 利用空化提高难浸金矿的浸出动力学
IF 1.2 Q2 Earth and Planetary Sciences Pub Date : 2022-12-07 DOI: 10.1080/25726641.2022.2153484
Jean Jacques Kalombo Mbayo, H. Simonsen, S. Ndlovu
ABSTRACT The cyanidation process for refractory gold ores has been the subject of numerous investigations aimed at improving gold recovery and leaching kinetics. From recent literature investigations, hydrodynamic cavitation has been found to be a promising new approach which may modify the cyanidation processes. In this study, this approach results in the enhancement of mass transfer kinetics in multiphase fluid streams due to impacting two pulps streams against one another in a vessel called the Jetleach reactor. In this work, the Jetleach reactor was applied to a flotation concentrate from a South African gold tailings processing plant (Ergo) where an improvement of almost 10% in gold recovery was obtained while decreasing cyanide and oxygen consumption by almost 8% and 50%, respectively. The main reason for the improvement is surmised to be due to the generation of micro-cavitation which improves the mass transfer of oxygen and cyanide within the slurry.
摘要难浸金矿石的氰化工艺一直是众多研究的主题,旨在提高金的回收率和浸出动力学。从最近的文献研究来看,流体动力学空化是一种很有前途的新方法,可以改变氰化过程。在这项研究中,由于在一个称为Jetleach反应器的容器中两股纸浆流相互碰撞,这种方法增强了多相流体流中的传质动力学。在这项工作中,Jetleach反应器被应用于南非黄金尾矿处理厂(Ergo)的浮选精矿,在该厂,黄金回收率提高了近10%,同时氰化物和氧气消耗分别减少了近8%和50%。据推测,改善的主要原因是由于微空化的产生,微空化改善了浆料中氧气和氰化物的传质。
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引用次数: 0
Microhardness-compositional relationship of Fe3O4-Mn3O4 series spinels from ferromanganese sinter and its relationship to sinter strength 锰铁烧结矿中Fe3O4-Mn3O4系列尖晶石的显微硬度-成分关系及其与烧结矿强度的关系
IF 1.2 Q2 Earth and Planetary Sciences Pub Date : 2022-10-08 DOI: 10.1080/25726641.2022.2130522
M. Peterson, S. Hapugoda, J. Manuel
ABSTRACT Fe-Mn spinels are common bonding phases in ferromanganese sinter and play an important role in determining sinter strength. This study analysed spinel phases from ferromanganese sinter to determine the range of compositions present and examine the relationship between phase composition and microhardness. Spinels with α-vredenburgite and jacobsite compositions had notably increased mean Al content compared to that of end-member Fe- or Mn-spinels. There was a strong negative correlation between the Fe+Al content and the Mn/Fe ratio of sinter jacobsite and of α-vredenburgite, indicating the likely substitution of Al3+ for Mn3+ in the vredenburgite structure. Mixed Fe-Mn spinels had higher Vickers and Knoop microhardness and fracture toughness than end-member Fe- or Mn-spinels. It is likely that the presence of Al in the octahedral site in the α-vredenburgite structure is related to the increased microhardness and, therefore, should have a positive effect on sinter strength if vredenburgite is present in sufficient quantities.
铁锰尖晶石是锰铁烧结矿中常见的结合相,在决定烧结矿强度方面起着重要作用。本研究分析了锰铁烧结矿中的尖晶石相,以确定存在的成分范围,并研究了相组成与显微硬度之间的关系。与端元Fe或Mn尖晶石相比,具有α-辉橄榄岩和雅各布岩成分的尖晶石的平均Al含量显著增加。Fe+Al含量与烧结Jacobite和α-辉橄榄岩的Mn/Fe比呈强负相关,表明在辉橄榄岩结构中Al3+可能取代Mn3+。混合铁锰尖晶石比端元铁锰尖晶石具有更高的维氏和努氏显微硬度以及断裂韧性。铝在α-辉橄榄岩结构中八面体位置的存在可能与显微硬度的增加有关,因此,如果辉橄榄岩存在足够的量,则应对烧结强度产生积极影响。
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引用次数: 0
Improving the Morrell C-model's accuracy in predicting the ball mills’ power draw based on calculating the dynamic voidage of grinding media 基于磨矿介质动态空隙率计算提高Morrell C模型预测球磨机功率消耗的精度
IF 1.2 Q2 Earth and Planetary Sciences Pub Date : 2022-08-30 DOI: 10.1080/25726641.2022.2116363
Mohammad Hasan Golpayegani, B. Rezai
ABSTRACT This paper investigates grinding media's dynamic voidage to improve the Morrell-C model's accuracy in predicting the ball mills' power draw. Using a three-level factorial design, we provided an empirical model to determine the voidage of each ball size distribution proposed by Bond for ball mills' first filling in various ranges of fractional mill filling and mill rotating speed. Moreover, by employing the multiple regression method, a general model was developed to predict the balls' dynamic voidage by calculating the mean absolute deviation (MAD) of the balls' diameter. Results revealed that the balls' dynamic voidage increases with increasing the rotating speed and decreasing the fractional filling and MAD of the balls' diameter. The evaluation of the grinding media's voidage prediction models' performance in improving the Morrell-C model's accuracy indicated an increase in the model's predictive power by calculating the ball mills' load bulk density based on the dynamic voidage of grinding media.
为了提高莫雷尔- c模型预测球磨机功率消耗的精度,研究了磨矿介质的动态空隙。利用三水平析因设计,我们提供了一个经验模型来确定Bond提出的球磨机在不同分级机填充和球磨机转速范围内首次填充的每个球粒度分布的空隙率。此外,采用多元回归方法,通过计算球直径的平均绝对偏差(MAD),建立了预测球动态空隙的通用模型。结果表明:随着转速的增加、填充分数和直径的减小,球的动态空隙增大;通过评价磨矿介质空隙率预测模型对Morrell-C模型精度的提高,发现基于磨矿介质动态空隙率计算球磨机负荷容重,提高了模型的预测能力。
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引用次数: 0
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Mineral Processing and Extractive Metallurgy-Transactions of the Institutions of Mining and Metallurgy
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