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A COMPARATIVE ANALYSIS AMONG THE WELDED Al-6061 PLATES JOINED BY FSW, MIG AND TIG WELDING METHODS 摘要对FSW、MIG和TIG三种焊接方法对Al-6061钢板的焊接效果进行了对比分析
IF 1 Q3 Materials Science Pub Date : 2023-06-20 DOI: 10.36547/ams.29.2.1778
Aaluri Praveen Reddy, Saurabh Dewangan
The present work deals with assessment of tensile strength, hardness, fracture behavior and microstructural changes in welded Al-6061 plates. MIG welding has been done with filler rod whereas no filler metal has been applied during TIG welding for comparing the results with FSW, a filler-less solid-state welding. The ultimate tensile strength (UTS) of MIGW sample has been found 75% and 111% higher than that of FSW and TIGW samples respectively. Also, the elongation shown by MIG joint is nearly 50% higher than that of other two welds. The tensile properties of two non-filler welds, i.e., FSW and TIG have been found similar. The fractography results have established the ductile behavior of all the three joints. The primary phase (bright Al-grains) of base metal zone (BM) with thin solid boundary has changed into thick dendritic shapes in the welded zone (WZ). Also, the coarse secondary phase of BM has converted into fine particle in WZ under the influence of rapid cooling. The WZ has been reported harder than HAZ in MIG and FSW plates whereas the HAZ of TIGW plate has been found harder than WZ due to accumulation of fine equiaxed secondary phase.         
本工作对焊接的Al-6061板的抗拉强度、硬度、断裂行为和微观结构变化进行了评估。MIG焊接是用填充棒进行的,而在TIG焊接过程中没有使用填充金属,以将结果与FSW(一种无填充物的固态焊接)进行比较。MIGW试样的极限抗拉强度分别比FSW和TIGW试样高75%和111%。MIG焊接接头的伸长率比其他两种焊缝高出近50%。FSW和TIG两种非填充焊缝的拉伸性能相似。断口分析结果确定了所有三个接头的韧性行为。在焊接区(WZ),具有薄固体边界的母材区(BM)的初生相(亮Al晶粒)已转变为厚树枝状。此外,在快速冷却的影响下,BM的粗二次相在WZ中转化为细颗粒。据报道,MIG和FSW板中的WZ比HAZ更硬,而TIGW板的HAZ由于细小的等轴二次相的积累而比WZ更硬。
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引用次数: 1
Metallurgical investigation of direct drive friction welded joint for austenitic stainless steel (AISI 316) 奥氏体不锈钢(AISI 316)直接驱动摩擦焊接接头的冶金学研究
IF 1 Q3 Materials Science Pub Date : 2023-06-20 DOI: 10.36547/ams.29.2.1802
Ammar JABBAR HASSAN, B. Cheniti, B. Belkessa, T. Boukharouba, D. Miroud, N. Titouche
The present study investigates the metallurgical behavior of direct-drive friction-welded (DDFW) joints for high Cr, Ni, and Mo steel (AISI 316). Macro-microscopic, microhardness, and X-ray diffraction (XRD) were conducted. The results for the macroscopic view showed that the narrow welding center did not exceed 600 µm and there were no macro cracks or defects, indicating a uniform structure. The microstructure exhibited a significant welded joint interface with microcavities and a grain refinement of 10 µm, about three times smaller than the grain size of AISI 316, due to the creation of a highly plastically deformed zone (HPDZ), while the thermo-mechanically affected zone (TMAZ) formed in the neighboring area with a grain growth of about 100 µm, relatively enlarged three times compared to AISI 316 and time time related HPDZ. Thus, the high level of microhardness was investigated at the welding center and low values in the neighboring area were caused by the formation of the HPDZ and TMAZ, respectively. XRD also illustrated the concentration of gamma iron at the 111 level due to the grain refinement resulting from high plastic deformation.
本研究研究了高Cr、Ni、Mo钢(AISI 316)直接驱动摩擦焊接(DDFW)接头的冶金行为。进行了宏观显微镜、显微硬度和x射线衍射(XRD)分析。宏观观察结果表明,狭窄的焊接中心不超过600µm,无宏观裂纹和缺陷,结构均匀。由于形成了高塑性变形区(HPDZ),其晶粒细化约为10µm,比AISI 316的晶粒尺寸小3倍,而在邻近区域形成了热机械影响区(TMAZ),晶粒长大约为100µm,相对于AISI 316和与时间相关的HPDZ增大了3倍。因此,焊接中心的显微硬度较高,而邻近区域的显微硬度较低分别是由HPDZ和TMAZ的形成引起的。XRD还表明,由于高塑性变形导致晶粒细化,γ铁的浓度达到111水平。
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引用次数: 0
Mg2Si INTERMETALLIC ALLOYS: PHASE GROWTH AND MICROSTRUCTURE Mg2Si金属间合金:相生长和显微组织
IF 1 Q3 Materials Science Pub Date : 2023-06-20 DOI: 10.36547/ams.29.2.1840
Septian Adi Chandra, R. Roberto, Dedi Pria Utama, Dhany Zulkarnain, Delfiarina Salsabila Putri Bratawan, Mila Saprila Suherman, Annisfiah Gayatri, A. Tjahjono, Muhammad Yunan Hasbi, S. Dwi Yudanto
The Mg2Si intermetallic alloys have been prepared by using a powder metallurgy process. The milling treatment of silicon powder as a raw material to improve the formation of the Mg2Si phase was investigated in this research. The un-milled and milled silicon powder was mixed with magnesium powder and milled for 2 hours. The milled powders were compacted in stainless steel tubes and sintered at 500 and 600°C for 6 hours. The phase formation and crystal structure were identified using the X-ray diffractometer (XRD), while the fracture surface was observed under the scanning electron microscope (SEM). The XRD results show that the Mg2Si phase is the dominant phase, with the highest mass fraction of 86.31%. The lattice parameter calculated from the Mg2Si cubic phase is 0.6355 nm. As a result, we might derive the conclusion that the Mg2Si intermetallic alloys can be produced with atmospheric mechanical milling under air and powder sintering techniques in a tube.
采用粉末冶金法制备了Mg2Si金属间合金。本文研究了以硅粉为原料进行磨铣处理,以改善Mg2Si相的形成。将未磨和磨后的硅粉与镁粉混合,磨2小时。研磨后的粉末在不锈钢管中压实,在500和600℃下烧结6小时。采用x射线衍射仪(XRD)对试样的物相组成和晶体结构进行了表征,并用扫描电镜(SEM)对试样的断口形貌进行了观察。XRD结果表明,Mg2Si相为主要相,质量分数最高,为86.31%。由Mg2Si立方相计算得到的晶格参数为0.6355 nm。结果表明,在空气和粉末烧结的条件下,可以在管内用常压机械铣切法制备Mg2Si金属间合金。
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引用次数: 0
MODEL DECISION-MAKING SYSTEM IN THE TASK OF CHOOSING THE OPTIMAL COMPOSITION OF THE BLAST FURNACE BURDEN UNDER SPECIFIC OPERATING CONDITIONS OF BF 模型决策系统的任务是选择高炉在特定运行条件下炉料的最优组成
IF 1 Q3 Materials Science Pub Date : 2023-06-20 DOI: 10.36547/ams.29.2.1764
A. Belkova, Daria Togobitska, D. Stepanenko
This paper presents the methodological basis for creating a model system for selecting the optimum composition of blast furnace burden, providing the required technical and economic performance and the melting of pig iron of the required composition. The system implements a new systematic approach to modeling the processes of directed formation of blast-furnace melts. Description of composition and properties of metallurgical systems in different states is based on an original concept of directional chemical bonding using integral parameters of interatomic interaction of components in the system. The developed complex of mathematical and physical-chemical models and criteria provides a solution to the direct problem of predicting the composition of pig iron and properties of blast furnace slag, depending on burden and technological conditions. Determination of the optimal burden composition is carried out using vector optimization methods with mandatory verification of compliance with the technological requirements of high-temperature properties of the burden. The results of testing the model system on actual industrial data of blast furnace operation are illustrated, which made it possible to formulate recommendations on the composition of the loaded feed, taking into account the available raw material and energy resources.
本文介绍了建立高炉炉料最佳成分选择模型系统的方法基础,提供了所需的技术经济性能和所需成分的生铁熔炼。该系统为高炉熔体定向形成过程的建模提供了一种新的系统方法。描述不同状态下的冶金系统的组成和性能是基于一个原始的定向化学键概念,使用系统中组分的原子间相互作用的积分参数。发展起来的数学和物理化学模型和标准的复合体,为根据炉料和工艺条件预测生铁成分和高炉炉渣性能的直接问题提供了解决方案。采用矢量优化方法确定最优炉料组成,并对炉料高温性能的工艺要求进行强制性验证。通过对高炉实际工业运行数据的测试,说明了该模型系统的测试结果,从而可以在考虑到现有原料和能源的情况下,对加载料的组成提出建议。
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引用次数: 0
CHANGE IN MICROSTRUCTURE AND HARDNESS OF ADDITIVELY MANUFACTURED AISI H13 STEEL BY HEAT TREATMENT AND NITRIDING PROCESSES 添加aisih13钢经热处理和氮化处理后组织和硬度的变化
IF 1 Q3 Materials Science Pub Date : 2023-06-20 DOI: 10.36547/ams.29.2.1790
Trung Van Trinh, Son Anh Nguyen, K. Pham, C. Seidel, A. H. Pham, Cuong Nhu Phung
AISI H13 steel samples were additively manufactured using a laser powder bed fusion (LPBF) system. The effect of annealing tem-perature, quenching & tempering, and nitriding were determined. The microstructure and properties of the samples were investigated using optical microscopy, scanning electron microscopy, electron backscattered diffraction, electron probe micro-analysis, X-ray diffraction, roughness measurement, and a hardness tester. The results show that the as-built AISI H13 steel sample had a roughness on the surface and pores inside. The microstructure consisted of martensite and retained austenite. The average hardness was 460 HV, and the porosity was 0.086 %. The annealing process helped homogenize the microstructure, increase the density, and reduce the porosity and hardness of the LPBF-manufactured sample. The quenching process helped increase the hardness of the steel to the maximum of 787 HV, then the tempering process reduced the hardness to 572 HV. Heat treatment and nitriding processes tended to increase the martensite block size, reduce the retained austenitic content, and precipitate the V-Mo-rich carbide in the LPBF-manufactured AISI H13 steel. After nitriding was conducted, the nitriding case depth was 87 um, and the surface hardness increased up to higher than 1020 HV due to the formation of CrN and Fe3-4N.
采用激光粉末床熔合(LPBF)系统对AISI H13钢样品进行了增材制造。研究了退火温度、调质温度和渗氮温度对合金性能的影响。采用光学显微镜、扫描电镜、电子背散射衍射、电子探针显微分析、x射线衍射、粗糙度测量和硬度计对样品的显微组织和性能进行了研究。结果表明:AISI H13钢试样表面粗糙,内部有气孔;显微组织由马氏体和残余奥氏体组成。平均硬度为460 HV,孔隙率为0.086%。退火工艺有助于均匀化lpbf制备的样品的微观结构,增加密度,降低孔隙率和硬度。淬火工艺使钢的硬度提高到787 HV,回火工艺使钢的硬度降低到572 HV。在lpbf制备的AISI H13钢中,热处理和渗氮工艺增加了马氏体块尺寸,降低了残余奥氏体含量,析出了富v - mo碳化物。渗氮后,渗层深度为87 um,由于CrN和Fe3-4N的形成,表面硬度提高到1020 HV以上。
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引用次数: 0
SIMULATION TOOL FOR MATERIAL BEHAVIOUR PREDICTION IN ADDITIVE MANUFACTURING 增材制造中材料行为预测的仿真工具
IF 1 Q3 Materials Science Pub Date : 2023-06-20 DOI: 10.36547/ams.29.2.1846
Ľ. Kaščák, J. Varga, J. Bidulská, R. Bidulský, M. Grande
Simulation tools play an important role not only in terms of understanding the processes taking place in the production, and the possibility to prevent failures, but ultimately, and most importantly, to optimize the production process. Thus, simulation tools should be able to work with many input parameters. The processes in which many parameters influence the final quality of the part, and its properties is metal additive manufacturing (AM). The volume of support material used in the metal AM process is also of importance, as its reduction plays an important role in terms of cost-effectiveness, which can be increased by minimizing support structures. The paper deals with the numerical simulation of the metal AM process. The simulation analyses with the same input parameters were performed, comparing each other the support material distribution, volume fraction or shape deviation with respect to the conventional support generation method and the function allowing the support generation by means of the optimization mode. Less variation in the shape of the part, variation in its volume fraction, variation in the density of the generated support structures as well as variation in the spacing of the generated support structure was achieved by using the support generation optimization mode.
模拟工具不仅在理解生产过程中发生的过程和防止故障的可能性方面发挥着重要作用,而且最终也是最重要的是,在优化生产过程方面发挥着至关重要的作用。因此,模拟工具应该能够使用许多输入参数。许多参数影响零件最终质量及其性能的工艺是金属增材制造(AM)。金属AM工艺中使用的支撑材料的体积也很重要,因为其减少在成本效益方面起着重要作用,成本效益可以通过最小化支撑结构来增加。本文对金属AM工艺进行了数值模拟。使用相同的输入参数进行模拟分析,相互比较相对于传统支撑生成方法的支撑材料分布、体积分数或形状偏差以及允许通过优化模式生成支撑的函数。通过使用支撑生成优化模式,实现了零件形状的较小变化、其体积分数的变化、生成的支撑结构的密度的变化以及生成的支持结构的间距的变化。
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引用次数: 1
Effect of SiO2 Surface Oxidation Coating of Silicon Carbide Particles Reinforcement on the Mechanical Properties of Al-2.5%Mg/xSiCp Developed by Stir Casting Method 碳化硅颗粒表面氧化涂层对搅拌铸造Al-2.5%Mg/xSiCp力学性能的影响
IF 1 Q3 Materials Science Pub Date : 2023-03-23 DOI: 10.36547/ams.29.1.1692
A. Ambali, O. A. Oyelaran, Bukola Olalekan Bolaji, I. Abdulmalik, Olayiwola Abdulrafiu Suleiman, Usman Hamza Ibrahim
The literature revealed that composites developed through stir casting process suffer some limitations such as low wettability and insufficient bonding between the molten Al and SiCp and the formation of aluminium carbide (Al4C3) at the interface which degrades mechanical performances of the composites. To overcome these challenges, this study used magnesium for improved wettability, heat treatment of reinforcement particles (SiCp) and application of metallic (SiO2) coating on the SiCp before addition to melt to improve Al-SiCp wettability in the manufacture of Al-2.5%Mg/xSiCp composites. The SiCp coating reduce direct interaction and promote wetting between SiCp and molten Al to developed Al-2.5%Mg/xSiCp composites. The percentage weight of SiCp varied from 5 wt% to 20 wt% (uncoated and coated) at 5 % intervals. The mechanical properties tests were conducted to examined the effects of coating and variation of volume percentage of SiCp on the composites developed. The results obtained showed that the reinforced alloy with both uncoated and coated SiCp performed favorably well compared to the control sample with 0% SiCp. The improvement of interfacial strength was observed in the composites developed with coated SiCp as the coating of SiCp enhanced its diffusion with Al-2.5%Mg.
研究表明,采用搅拌铸造工艺制备的复合材料存在一定的局限性,如润湿性低,Al与SiCp之间的结合不充分,在界面处形成碳化物(Al4C3),从而降低了复合材料的力学性能。为了克服这些挑战,本研究在制造Al-2.5%Mg/xSiCp复合材料时,使用镁来改善润湿性,对增强颗粒(SiCp)进行热处理,并在SiCp上涂上金属(SiO2)涂层,然后加入熔体,以改善Al-SiCp的润湿性。SiCp涂层减少了SiCp与熔融Al之间的直接相互作用,促进了其润湿,形成了Al-2.5% mg /xSiCp复合材料。SiCp的重量百分比以5%的间隔从5wt %变化到20wt %(未包覆和包覆)。通过力学性能试验考察了涂层和SiCp体积百分比变化对复合材料力学性能的影响。结果表明,与未涂覆SiCp和涂覆SiCp的对照样品相比,未涂覆SiCp的增强合金的性能都优于未涂覆SiCp的增强合金。SiCp涂层增强了其在Al-2.5%Mg中的扩散,从而提高了复合材料的界面强度。
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引用次数: 0
CRITICAL ANALYSIS OF MATERIAL BEHAVIOUR IN WELDED PLATES OF AISI 0.2%-C STEEL UNDER AS-WELDED, QUENCHED AND ANNEALED CONDITIONS aisi0.2%C钢焊接板在AS-weld、淬火和退火条件下材料行为的临界分析
IF 1 Q3 Materials Science Pub Date : 2023-03-23 DOI: 10.36547/ams.29.1.1719
Saurabh Dewangan, Vedant Vinod Nemade, Kanad Harshal Nemade
AISI 1020 grade of steel is well known for its good combination of high strength and fair ductility. Therefore, it is widely demanded in construction sectors. It possesses a good weldability too in both arc and gas welding conditions. In the present work four pairs of AISI 1020-0.2%C steel plates were welded by shielded arc welding method. Except one welded plate, other three were heat treated. Based on the heat treating, three different physical conditions were achieved- water quenched, oil quenched and annealed. All the samples were tested for tensile strength, hardness, and microstructure. The annealed specimen has showed a significantly improved tensile strength of 439 MPa which is 85% higher than as-welded specimen. Water and oil quenched specimens showed lesser strength than that of as-welded specimen. With regard to hardness, there were two different observations. The as-welded and annealed specimens indicated the highest hardness at welded joint whereas the lower values were reported in base metal part. In contrary, the water and oil quenched specimens were harder in base metal zone as compared to welded zone. Both, strength, and hardness were found in good correlation with microstructural appearance of the plates.
AISI 1020级钢以其高强度和良好延展性的良好结合而闻名。因此,它在建筑行业有着广泛的需求。它在电弧焊和气焊条件下都具有良好的可焊性。本工作采用保护电弧焊方法焊接了4对AISI 1020-0.2%C钢板。除一块焊接板外,其余三块均经过热处理。在热处理的基础上,实现了三种不同的物理条件——水淬火、油淬火和退火。对所有样品进行拉伸强度、硬度和微观结构测试。退火试样的抗拉强度显著提高,达到439MPa,比焊接试样高85%。水和油淬火试样的强度低于焊接试样的强度。关于硬度,有两种不同的观察结果。焊接和退火试样表明焊接接头处的硬度最高,而基底金属部分的硬度较低。相反,水淬和油淬试样在基体金属区比焊接区更硬。强度和硬度都与板材的微观结构外观有很好的相关性。
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引用次数: 1
ASSESSMENT OF TRIBOLOGICAL PROPERTIES OF STIR CAST Al6063 ALLOY REINFORCED WITH OKABA COAL ASH 冈叶粉煤灰增强搅拌铸造Al6063合金摩擦学性能的评价
IF 1 Q3 Materials Science Pub Date : 2023-03-23 DOI: 10.36547/ams.29.1.1750
J. Odusote, A. A. Adeleke, P. Ikubanni, Samuel Adeiza, Qudus Badrudeen, Olalekan Ogunniyi, T. Ogedengbe
Composite are multi-phase materials made up of matrix and reinforcement. This paper assesses the tribological property of Al6063 alloy (AMCs) reinforced with Okaba coal ash (OCA) using the stir casting method. By using a constant speed of 1000 rpm and two different loads (250 g and 750 g) on Taber wear apparatus, the tribological properties of the produced composite are contrasted with those of an unreinforced Al6063 alloy. The results show a reduction in wear index and the highest abrasion resistance at 4 wt.% coal ash at 500 g and 1000 rpm, as well as at 0, 2, and 6 wt.% with 8.688, 5.878, and 5.813 at 500g and 8.688, 5.878, 4.125, and 5.813 at 750g, respectively. Therefore, for all composite products compared to metal, there is an increase in abrasion resistance with a decrease in wear index, but this decreases when the load is increased to 750g, showing that the higher the load, the higher the wear index, which results in a reduction in abrasion resistance. Load is taken into greater consideration when using the AMCs manufactured in engineering applications. Additionally, SEM images revealed uniform distribution of the OCA reinforcement in the matrix alloy; thereby, improving its wear resistance.
复合材料是由基体和增强材料组成的多相材料。采用搅拌铸造法对冈巴粉煤灰增强Al6063合金的摩擦学性能进行了评价。通过在Taber磨损装置上使用1000rpm的恒定速度和两种不同的载荷(250g和750g),将所制备的复合材料的摩擦学性能与未增强Al6063合金的摩擦学性能进行了对比。结果表明,在500g和1000rpm下,在4wt.%的煤灰下,以及在0、2和6wt.%时,磨损指数降低,耐磨性最高,分别为8.688、5.878和5.813,在750g下分别为8.68、5.878、4.125和5.813。因此,与金属相比,对于所有复合材料产品,耐磨性随着磨损指数的降低而增加,但当负载增加到750g时,耐磨性降低,这表明负载越高,磨损指数越高,这导致耐磨性降低。在使用工程应用中制造的AMC时,应更多地考虑荷载。此外,SEM图像显示OCA增强剂在基体合金中均匀分布;从而提高其耐磨性。
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引用次数: 0
High entropy coating from AlCoCrCuFeNi alloy, obtained by laser alloying 激光合金化法制备高熵涂层
IF 1 Q3 Materials Science Pub Date : 2023-03-23 DOI: 10.36547/ams.29.1.1710
V. Girzhon, V. Yemelianchenko, O. Smolyakov
The structural-phase state of the Al-Co-Cr-Cu-Fe-Ni system high-entropy alloy obtained by laser alloying of technically pure aluminium surface layers was investigated by XRD, EDX and metallographic analyses. It is shown that in the process of laser alloying the formation of an an ordered multicomponent substitution solid solution based on BCC lattice took place, which is typical for high-entropy alloys. The process of heterogeneous crystallization of high-entropy alloys AlCoCrCuFeNi and Al3CoCrCuFeNi was modeled taking into account cooling rates of the melt. It is established that the formation of the obtained structure is a consequence of high cooling rates of the melt and high content of aluminum in the laser alloying zone. The microhardness of the alloyed surface was higher compared to high-entropy alloys of this system obtained under equilibrium conditions and was equal to 6.59 GPa. Additional reasons that may affect the high values of microhardness are analysed.
采用XRD、EDX和金相分析研究了激光合金化工艺纯铝表层制备的Al-Co-Cr-Cu-Fe-Ni体系高熵合金的组织相态。结果表明,在激光合金化过程中,形成了高熵合金典型的基于BCC晶格的有序多组分取代固溶体。考虑熔体冷却速率,模拟了高熵合金AlCoCrCuFeNi和Al3CoCrCuFeNi的非均相结晶过程。结果表明,该组织的形成是熔体冷却速度快和激光合金化区铝含量高的结果。在平衡条件下获得的合金表面显微硬度高于该体系的高熵合金,达到6.59 GPa。分析了影响显微硬度高值的其他原因。
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引用次数: 0
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Acta Metallurgica Slovaca
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