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PRELIMINARY INVESTIGATION INTO MECHANICAL PROPERTIES AND MICROSTRUCTURAL BEHAVIOUR OF INCONEL ALLOY UNDER WELDED AND UNWELDED CONDITIONS 焊接和非焊接条件下铬镍铁合金力学性能和显微组织行为的初步研究
IF 1 Q3 Materials Science Pub Date : 2023-03-23 DOI: 10.36547/ams.29.1.1664
Saurabh Dewangan, Sharath Narayanan, Gurbaaz Singh Gill, Utkarsh Chadha
This work focusses on analysing mechanical properties and microscopic assessment into Inconel-718 plates in welded and unwelded conditions. Welding was performed by tungsten inert gas welding technique. Two mechanical tests such as tensile test and hardness were performed on both the types of plates to compare the properties of welded joint and unwelded plate. Although Inconel 718 possesses good weldability, the strength, ductility, and hardness of welded joint were reported lesser than these of Unwelded plate. The microstructural images revealed that metal carbides present in Inconel plate had reduced after welding. The ultimate tensile stress and elongation before breaking of welded joint were 16% and 72% lower than Unwelded plate. The fractography analysis of the ruptured part revealed that Unwelded plate possessed higher ductility than welded plate.
这项工作的重点是分析Inconel-718板材在焊接和非焊接条件下的力学性能和微观评估。焊接采用钨极惰性气体焊接技术。对两种类型的板材进行了拉伸试验和硬度试验,以比较焊接接头和未焊接板材的性能。尽管铬镍铁合金718具有良好的可焊性,但据报道,焊接接头的强度、延展性和硬度低于未焊板。显微结构图像显示,铬镍铁合金板中存在的金属碳化物在焊接后减少。焊接接头断裂前的极限拉伸应力和伸长率分别比未焊板低16%和72%。断裂部位的断口分析表明,未焊板比焊接板具有更高的延性。
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引用次数: 1
improvement of tensile properties of low-carbon steels via short-time intercritical annealing 短时临界间退火对低碳钢拉伸性能的改善
IF 1 Q3 Materials Science Pub Date : 2023-03-23 DOI: 10.36547/ams.29.1.1709
M. S. Mohsenzadeh
The effect of low volume fraction formation of martensite on the tensile properties of low carbon steel was evaluated. First, steel samples with ferrite-cementite microstructure were produced. The thermomechanical treatment used included austenitizing at 1000 °C and then quenching in ice brine solution, tempering the obtained martensitic structure for 1 h at 650 °C, 80% cold rolling, and re-tempering for 2 h at 650 °C. In order to form a low volume fraction of martensite, steel samples with ferrite-cementite microstructure were intercritically annealed for 30 seconds at 740 °C. As a result of intercritical annealing treatment, 6.2% martensite was formed. The results of tensile test showed that the formation of 6.2% martensite led to the elimination of yield point phenomenon and Lüders banding, decrease of yield stress and increase of true stress at maximum load, while true uniform strain did not change significantly. The work hardening rate also increased significantly. Based on the results of modeling of the flow behavior with the Holloman equation, the work hardening capability of the steel sample including ferrite-cementite decreased after a certain plastic strain, while the work hardening capacity remained constant with the formation of a low volume fraction of martensite in the microstructure.
研究了低体积分数马氏体形成对低碳钢拉伸性能的影响。首先,制备具有铁素体-渗碳体微观结构的钢样品。采用的热处理包括1000℃奥氏体化,然后在冰盐水中淬火,650℃回火1 h, 80%冷轧,650℃再回火2 h。为了形成低体积分数的马氏体,将铁素体-渗碳体组织的钢样品在740℃下进行了30秒的临界退火。经临界间退火处理,形成6.2%的马氏体。拉伸试验结果表明,6.2%马氏体的形成消除了屈服点现象和 ders带状带,最大载荷下屈服应力降低,真应力增加,而真均匀应变变化不显著。加工硬化率也显著提高。基于Holloman方程的流动行为模拟结果表明,含铁素体-渗碳体的钢试样在达到一定塑性应变后加工硬化能力下降,而在微观组织中形成小体积分数的马氏体后加工硬化能力保持不变。
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引用次数: 0
Case study of advanced processed OFHC copper by dry sliding wear test 先进加工OFHC铜干式滑动磨损试验研究
IF 1 Q3 Materials Science Pub Date : 2023-03-23 DOI: 10.36547/ams.29.1.1734
R. Bidulský, J. Bidulská, T. Kvačkaj, M. Grande
The wear behaviour of copper material processed by ECAP (Equal Channel Angular Pressing) and orbital forging (OF) is presented in this study. Dry sliding wear tests were carried out for the wear behaviour of the investigated system. Oxygen-free high thermal conductivity (OFHC) copper was used for testing. The new combination of metal forming processes was used because of ease of fabrication. Additionally, wear rate, friction coefficient and wears mechanisms were observed. The friction resistance is caused by the destruction of the adhesion between surface asperities in metal friction. Moreover, increased asperity interactions connected with wear particle entrapment gradually increase the friction coefficient. These results show the metal forming process's positive influence in reducing interfacial adhesion and asperity deformation. Finally, the combinations of newly used advanced processing demonstrated excellent wear characteristics of copper.
研究了等通道角挤压(ECAP)和轨道锻造(of)对铜材料的磨损行为。对所研究的系统的磨损行为进行了干滑动磨损试验。使用无氧高导热性(OFHC)铜进行测试。由于易于制造,采用了金属成型工艺的新组合。此外,还观察了磨损率、摩擦系数和磨损机理。摩擦阻力是由金属摩擦中表面微凸体之间的粘附力被破坏引起的。此外,与磨损颗粒截留相关的凹凸相互作用的增加逐渐增加了摩擦系数。这些结果表明,金属成形工艺在减少界面粘附和凹凸变形方面具有积极影响。最后,新使用的先进工艺组合展示了铜优异的磨损特性。
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引用次数: 0
COMPARISON OF FINISHING MILLING STRATEGIES USING TOPOGRAPHY OF THE MACHINED SURFACE 利用加工表面形貌的精铣策略比较
IF 1 Q3 Materials Science Pub Date : 2023-03-23 DOI: 10.36547/ams.29.1.1763
J. Varga, Peter Ižol, Ľ. Kaščák, M. Vrabeľ, A. Kubit
The plastics processing and injection molding industry is known for the fact that the future molded part contains a variety of geometric shapes and, in some cases, free surfaces. To produce these shapes, knowledge of CAM systems is required to enable the programmer to select the necessary milling strategies designed to achieve the best possible quality and dimensional accuracy. However, it is equally necessary to understand and appreciate the effect of each strategy and which strategy is best suited for a given type of surface. The paper compares finishing milling strategies by evaluating the topography of the machined surface. The material was AlCu4Mg aluminium alloy, where Constant-Z and Spiral strategy – circle-type finishing strategies were selected for the production process. Surface topography analysis was evaluated and compared at three different heights of the produced part with respect to the tool contact with the machined surface, which showed a variation in toolpaths and therefore also in the quality of machining. The surface topography results demonstrated the Constant Z strategy to be the more suitable strategy for producing the shaped surface, which achieved uniform toolpaths over the whole height of the part.
众所周知,塑料加工和注塑行业的未来成型零件包含各种几何形状,在某些情况下,自由表面。为了生产这些形状,需要CAM系统的知识,使程序员能够选择必要的铣削策略,以实现最佳的质量和尺寸精度。然而,同样有必要理解和欣赏每种策略的效果,以及哪种策略最适合给定类型的表面。通过对加工表面形貌的评价,对精加工策略进行了比较。材料为AlCu4Mg铝合金,生产工艺选择Constant-Z和螺旋策略-圆型精加工策略。根据刀具与加工表面接触的不同高度,对所生产零件的表面形貌分析进行了评估和比较,这表明了刀具路径的变化,因此也表明了加工质量的变化。表面形貌结果表明,恒定Z策略更适合于生产异形表面,该策略在零件的整个高度上实现了均匀的刀具轨迹。
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引用次数: 1
EFFECT OF ULTRAFAST HEATING ON AISI 441 FERRITIC STAINLESS STEEL 超快加热对aisi 441铁素体不锈钢的影响
IF 1 Q3 Materials Science Pub Date : 2023-03-23 DOI: 10.36547/ams.29.1.1713
G. Stornelli, L. Albini, P. E. Di Nunzio, Giulia Tiracorrendo, B. R. Rodriguez vargas, A. Di schino
The use of the ultrafast heating (UFH) heat treatment process attracted great attention in the last few years, following the requirements of CO2 emissions reduction. The effect of ultrafast heating (UFH) treatment an AISI 441 ferritic stainless steels is reported in this paper. Results show that a minimum temperature of 975 °C is required in order to achieve a fully recrystallized microstructure. The study highlights the effect of ultrarapid annealing on grain size evolution as a function of different adopted process parameters. The obtained microstructure is related to mechanical properties in terms of ultimate tensile stress and hardness.
随着二氧化碳减排的要求,超快加热(UFH)热处理工艺的使用在过去几年引起了极大的关注。本文报道了AISI441铁素体不锈钢的超快速加热(UFH)处理效果。结果表明,为了获得完全再结晶的微观结构,需要975°C的最低温度。该研究强调了超快退火对晶粒尺寸演变的影响,这是不同工艺参数的函数。所获得的微观结构与极限拉伸应力和硬度方面的机械性能有关。
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引用次数: 2
NUMERICAL AND EXPERIMENTAL STUDIES ON CLINCH-BONDED HYBRID JOINING OF STEEL SHEET DX53D+Z dx53d + z钢板夹接复合连接的数值与试验研究
IF 1 Q3 Materials Science Pub Date : 2022-12-13 DOI: 10.36547/ams.28.4.1657
Ľ. Kaščák, Denis Cmorej, J. Slota, E. Spišák, J. Varga
The automotive industry is characterized by the fact that it uses an entire range of materials. These are materials with different mechanical properties, thicknesses, and even different combinations. A variety of joining methods, such as clinching, is used to join this range of materials. However, sometimes it is necessary to combine several methods of joining materials. The paper deals with the evaluation of the properties of joints, which are created by a combination of mechanical joining and adhesive bonding. Two types of adhesives were used: adhesive based on epoxy resin and adhesive based on acrylate polymers. Double-sided hot-dip galvanized steel sheets DX53D+Z with a thickness of 0.8 mm were used to join with this combination of joining techniques. Numerical simulation tools were used to assess the joinability of materials. The simulation results were verified by the results from the experiments of real test samples. Samples joined by the clinching method combined with epoxy resin adhesives achieved higher load-bearing values and no cracks or any other type of failures were observed in these joints.
汽车工业的特点是它使用了各种各样的材料。这些材料具有不同的机械性能、厚度,甚至不同的组合。各种连接方法,如夹紧,用于连接该范围的材料。然而,有时需要将几种连接材料的方法结合起来。本文讨论了机械连接与胶粘接相结合形成的接头的性能评价问题。采用了两种胶粘剂:环氧树脂胶粘剂和丙烯酸酯聚合物胶粘剂。采用双面热镀锌钢板DX53D+Z,厚度为0.8 mm,采用这种组合连接技术进行连接。采用数值模拟工具评估材料的接合性。仿真结果与实际测试样品的实验结果相吻合。结合环氧树脂胶粘剂的粘接方法连接的样品具有更高的承载值,并且在这些接缝中没有观察到裂缝或任何其他类型的破坏。
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引用次数: 0
Effects of aluminium addition and austempering temperatures on Al-alloyed ductile iron microstructure and mechanical properties 铝添加和等温淬火温度对铝合金球墨铸铁组织和力学性能的影响
IF 1 Q3 Materials Science Pub Date : 2022-12-13 DOI: 10.36547/ams.28.4.1598
A. Adebayo, O. Ajibola, O. Falodun, Sunday G. Borisade, A. Owa, Oluwole D Adigun, A. Oyetunji, K. Alaneme
The research investigates the effect of varying amounts of aluminium (1.05, 1.575, 2.29, 3.02 and 3.74 wt.%) addition and heat treatment (austempering at 300, 350, 400 oC) on the microstructure and mechanical properties of ductile cast iron alloys. The graphitizing effects of the Al alloy and varied austempering temperatures on hardness, tensile strength, and impact toughness of the ductile cast iron (DCI) were evaluated. The results of the influences of Al addition and heat treatment on the properties of the DCI determined were presented as graphical data while the microstructures were done by using a scanning electron microscope (SEM). The microstructures revealed that the addition of Al into the matrix brings about the precipitation of ferrite around the graphite nodules. The combined effects of the increase Al content and austempering temperatures produced greater hardness values on the Al-alloyed DCI samples than the as-cast sample. The hardness value for the entire sample ranged between 27.25 to 57.03 BHN. Tensile strength increased with an increase in Al content and lower austempering temperatures, whereas, the impact toughness increased with an increase in Al content and higher austempering temperature.
研究了不同量的铝(1.05、1.575、2.29、3.02和3.74 wt.%)添加量和热处理(300、350、400℃等温回火)对球墨铸铁合金组织和力学性能的影响。研究了不同等温淬火温度对球墨铸铁(DCI)硬度、抗拉强度和冲击韧性的影响。结果表明,Al添加和热处理对DCI性能的影响以图形形式呈现,并通过扫描电子显微镜(SEM)对其进行了显微组织分析。显微组织分析表明,Al的加入使石墨结核周围有铁素体析出。Al含量的增加和等温回火温度的共同作用使Al- DCI试样的硬度值高于铸态试样。整个试样的硬度值在27.25 ~ 57.03 BHN之间。拉伸强度随Al含量的增加和等温温度的降低而增加,冲击韧性随Al含量的增加和等温温度的升高而增加。
{"title":"Effects of aluminium addition and austempering temperatures on Al-alloyed ductile iron microstructure and mechanical properties","authors":"A. Adebayo, O. Ajibola, O. Falodun, Sunday G. Borisade, A. Owa, Oluwole D Adigun, A. Oyetunji, K. Alaneme","doi":"10.36547/ams.28.4.1598","DOIUrl":"https://doi.org/10.36547/ams.28.4.1598","url":null,"abstract":"The research investigates the effect of varying amounts of aluminium (1.05, 1.575, 2.29, 3.02 and 3.74 wt.%) addition and heat treatment (austempering at 300, 350, 400 oC) on the microstructure and mechanical properties of ductile cast iron alloys. The graphitizing effects of the Al alloy and varied austempering temperatures on hardness, tensile strength, and impact toughness of the ductile cast iron (DCI) were evaluated. The results of the influences of Al addition and heat treatment on the properties of the DCI determined were presented as graphical data while the microstructures were done by using a scanning electron microscope (SEM). The microstructures revealed that the addition of Al into the matrix brings about the precipitation of ferrite around the graphite nodules. The combined effects of the increase Al content and austempering temperatures produced greater hardness values on the Al-alloyed DCI samples than the as-cast sample. The hardness value for the entire sample ranged between 27.25 to 57.03 BHN. Tensile strength increased with an increase in Al content and lower austempering temperatures, whereas, the impact toughness increased with an increase in Al content and higher austempering temperature.","PeriodicalId":44511,"journal":{"name":"Acta Metallurgica Slovaca","volume":null,"pages":null},"PeriodicalIF":1.0,"publicationDate":"2022-12-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46342927","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
MICROSTRUCTURE AND TENSILE PROPERTIES OF A RECENT INTER-CRITICALLY AUSTENITIZED QUENCHED AND PARTITIONED STEEL 一种新型临界间奥氏体淬火分区钢的组织和拉伸性能
IF 1 Q3 Materials Science Pub Date : 2022-12-13 DOI: 10.36547/ams.28.4.1578
Hoda Refaiy, Mai Fouad, Hoda Nasr El-Din, Eman H. El-shenawy
Quenched and partitioned steel is a promising grade of advanced high-strength steel "Third Generation" for industrial applications such as the automotive industry. This research aimed to develop a novel ultra-high-strength quenched and partitioned steel with good ductility from a novel alloy with the composition of 0.37C- 3.65Mn- 0.65Si- 0.87Al- 1.5Ni-0.05P, wt.% which is non-standard. This quenched and partitioned steel was developed by inter-critical austenitization followed by quenching to a temperature below Martensite start temperature (80 and 120 oC), then partitioning at 450 oC for different times (20, 40, 60, 100, 140, and 180 s). Scanning electron microscope and X-Ray diffraction were utilized to investigate the microstructure and retained austenite characteristics. The tensile properties of developed Q&P specimens were also investigated. The results demonstrated that the specimen quenched at 120 oC and partitioned for 180s achieved a maximum strength elongation balance of 26 GPa.%. Both the specimens quenched at 80 and 120 oC displayed a decrease in strength values with extending holding time due to the tempering of primary martensite. Increasing partitioning time for the specimens quenched at 120 oC led to enhancing elongation, where a maximum total elongation of 19.7% was achieved for the partitioning time of 180s.  
淬火和分区钢是一种很有前途的高级高强度钢“第三代”,用于汽车工业等工业应用。本研究旨在由成分为0.37C-3.65Mn-0.65Si-0.87Al-1.5Ni-0.05P,wt.%的新型非标合金,开发出一种具有良好延展性的新型超高强度调质钢。这种淬火和分区钢是通过临界间奥氏体化,然后淬火到低于马氏体起始温度(80和120℃)的温度,然后在450℃下分区不同的时间(20、40、60、100、140和180 s)来开发的。利用扫描电子显微镜和X射线衍射仪对其显微组织和残余奥氏体特性进行了研究。还研究了开发的Q&P试样的拉伸性能。结果表明,在120℃下淬火并分配180 s的试样获得了26GPa.%的最大强度-伸长率平衡。由于初生马氏体的回火,在80和120℃下淬火的两个试样的强度值都随着保温时间的延长而降低。增加在120℃下淬火的试样的分配时间会提高伸长率,其中在180s的分配时间内,最大总伸长率达到19.7%。
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引用次数: 0
CIRCULAR ECONOMY APPLIED TO METHANE PRODUCTION FROM NATURAL GAS HYDRATE RESERVOIRS: POTENTIALITIES OF RESIDUAL DUST COMING FROM STEEL PLANTS 循环经济在天然气水合物甲烷生产中的应用:钢铁厂残余粉尘的潜力
IF 1 Q3 Materials Science Pub Date : 2022-12-13 DOI: 10.36547/ams.28.4.1632
G. Stornelli, A. Gambelli, A. Di schino, G. Zucca, F. Rossi
Natural gas hydrate represents one of the most promising solutions to answer to the constantly increasing energy demand; in addition, the possibility of recover methane via carbon dioxide injection, with a theoretical exchange ratio equal to 1, makes it a potential carbon neutral energy source. Among them, energetical costs associated to practical operations in marine deposits. The use of chemical inhibitors and or promoters to improve the exchange process is gaining increasing interest and researchers are mainly focused on finding less environmental unfriendly additives and on reducing their costs. In that direction, the present work deals with the possible use of waste dust, produced during steel mill processes, as promoter of the CO2/CH4 replacement process. That sand commonly contains a great variety of compounds, such as metal oxides, alumina, salts, and so on. Some of them have a chemical composition close to well-known hydrate inhibitors/promoters. Moreover, that application could be a further energetic cycle for a waste product. In this work, both methane and carbon dioxide hydrate formation were tested in absence and in presence of cupper oxides, with different concentrations. Hydrate formation and dissociation results where then compared among each other and with hydrate equilibrium values for those compounds.
天然气水合物是应对不断增长的能源需求的最有希望的解决方案之一;此外,通过注入二氧化碳回收甲烷的可能性,其理论交换比等于1,使其成为潜在的碳中性能源。其中,与海洋矿床实际作业有关的能源成本。使用化学抑制剂和/或促进剂来改善交换过程正引起越来越多的兴趣,研究人员主要集中在寻找对环境不太友好的添加剂和降低其成本。在这个方向上,目前的工作涉及在炼钢过程中产生的废粉尘作为CO2/CH4替代过程的促进剂的可能性。这种沙子通常含有各种各样的化合物,如金属氧化物、氧化铝、盐等。其中一些化合物的化学组成接近于众所周知的水合物抑制剂/促进剂。此外,这种应用可能是废物的进一步能量循环。在这项工作中,在不同浓度的氧化铜存在和不存在的情况下,测试了甲烷和二氧化碳水合物的形成。然后将水合物形成和解离的结果相互比较,并与这些化合物的水合物平衡值进行比较。
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引用次数: 0
EFFECT OF RETAINED AUSTENITE ON PLASTIC CHARACTERISTICS OF DUAL PHASE STEELS 残余奥氏体对双相钢塑性特性的影响
IF 1 Q3 Materials Science Pub Date : 2022-12-13 DOI: 10.36547/ams.28.4.1653
Peter Prislupcak, T. Kvačkaj, J. Bidulská, S. Németh, M. Demčáková, R. Gburík, Vladimír Kundracík
In terms of the current trend of research and development of new materials and optimization of current materials in the automotive industry, the greatest attention is paid to progressive high-strength dual-phase (DP) steels with increased stampability, which are designed for cold stamping for specific internal car body components of the current market. New grades of DP steels provide a combination of high strength and good formability and contribute to the weight savings of vehicle parts by 10 to 20 %, compared to current DP grades. Thanks to their top properties, DP steels with increased formability can absorb more crash energy using less steel. As a result, high-strength DP780GI and DP780GI-HF materials of first generation (hereinfater DP780GI-HF) were analyzed. The stampability improvement of DP steels was demonstrated by the experimentally determined Forming Limit Curves for both steels.
就目前汽车行业新材料的研发和现有材料的优化趋势而言,最受关注的是可冲压性提高的渐进式高强度双相(DP)钢,它是为当前市场的特定内部车身部件设计的冷冲压。与目前的DP等级相比,新等级的DP钢提供了高强度和良好成形性的结合,并有助于车辆零件的重量节省10%至20%。由于其顶级性能,可成形性增强的DP钢可以用更少的钢材吸收更多的碰撞能量。结果,分析了第一代高强度DP780GI和DP780GI-HF材料(下文称为DP780GI-HF)。实验确定的DP钢和DP钢的成形极限曲线证明了DP钢的压模性能的提高。
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引用次数: 0
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Acta Metallurgica Slovaca
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