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The Study of Temperature-Dependent Magnetic Properties Variation in CoCr2O4 Nanoparticles with (y = 0.8) and Without Coating Concentration of Non-Magnetic (SiO2)y 含有 (y = 0.8) 和不含有非磁性 (SiO2)y 涂层的 CoCr2O4 纳米粒子随温度变化的磁性能研究
IF 0.7 Q3 Engineering Pub Date : 2023-12-01 DOI: 10.2478/ama-2023-0062
Ghazanfar Mehboob, K. Nadeem, A. Iqbal, Gohar Mehboob, Shahnawaz Hussain, Mohamed Ragab, Mazhar Iqbal, S. Ajmal, Adel El-Marghany
Abstract The present study investigates the temperature-dependent magnetic (MT) properties of CoCr2O4/(SiO2)y (y = 0 and 0.8) nanoparticles. Nanoparticles were synthesised by using the conventional sol–gel technique. The X-ray diffraction (XRD) method confirmed the normal spinel structure of CoCr2O4 nanoparticles. The main peak analysis of the XRD pattern using Debye–Scherrer’s formula probes the mean crystallite sizes for coated and uncoated nanoparticles, and the sizes based on which the probes have been carried out amount to 19 nm and 28 nm, respectively. The transmission electron microscopy (TEM) image showed the non-spherical shape of these nanoparticles. Field-cooled (FC) and zero field-cooled (ZFC) MT plots were taken by using a superconducting quantum interference device (SQUID) magnetometer. Pure CoCr2O4 nanoparticles showed the ferrimagnetic transition at Curie temperature (Tc = 99 K) on an applied field (H) of 50 Oe. Tc decreased up to 95 K with the increase in 80% SiO2 concentration in CoCr2O4 nanoparticles. For pure samples, conical spiral temperature (TS) and lock-in transition temperature (TL) remain unchanged with increasing magnetic field because of strong spin–lattice coupling. However, for 80% SiO2 impurity, the decrease in Tc was attributed to the reduction in surface disorder with a minor decline in TS and TL. The Ms declined with a decrease in temperature because of the existence of stiffed/strong conical spin-spiral and lock-in states in pure CoCr2O4 nanoparticles, while nanoparticles with 80% coating SiO2 concentration showed abnormal behavior. The coercivity increases with a decrease in temperature due to a decrease in thermal fluctuations at low temperatures for both samples. The fitting of coercivity (Hc) versus temperature plot by using Kneller’s law has given the values of coercivity constant (α) and coercivity at average blocking temperature (TB) for both samples, which are α = 0.54, TB = 75 K and α = 1.59, TB = 81 K, respectively. Hence, the increase in the concentration of SiO2 decreased nanoparticles size and surface disorder in CoCr2O4 nanoparticles while enhancing Ms below spin-spiral state ordering.
摘要 本研究探讨了 CoCr2O4/(SiO2)y(y = 0 和 0.8)纳米粒子随温度变化的磁性(MT)特性。纳米粒子采用传统的溶胶-凝胶技术合成。X 射线衍射(XRD)方法证实了 CoCr2O4 纳米粒子的正尖晶石结构。利用 Debye-Scherrer 公式对 X 射线衍射图的主峰进行分析,可探测出涂层和未涂层纳米粒子的平均晶粒尺寸,探测所依据的尺寸分别为 19 nm 和 28 nm。透射电子显微镜(TEM)图像显示了这些纳米颗粒的非球形形状。使用超导量子干涉装置(SQUID)磁力计绘制了场冷(FC)和零场冷(ZFC)MT 图。纯 CoCr2O4 纳米粒子在外加磁场 (H) 为 50 Oe 时,在居里温度 (Tc = 99 K) 出现铁磁转变。随着 CoCr2O4 纳米粒子中 80% SiO2 浓度的增加,Tc 下降到 95 K。对于纯样品,由于自旋-晶格耦合很强,锥螺旋温度(TS)和锁相转变温度(TL)随磁场的增加而保持不变。然而,对于二氧化硅杂质含量为 80% 的样品,Tc 的降低是由于表面无序性的降低,而 TS 和 TL 则略有下降。由于纯 CoCr2O4 纳米粒子中存在刚性/强锥形自旋螺旋态和锁入态,Ms 随温度降低而下降,而含有 80% 镀层 SiO2 的纳米粒子则表现出异常行为。由于两种样品在低温下的热波动减小,矫顽力随温度的降低而增加。利用克奈勒定律拟合矫顽力(Hc)与温度的关系图,得出了两种样品的矫顽力常数(α)和平均阻滞温度(TB)下的矫顽力值,分别为α = 0.54,TB = 75 K和α = 1.59,TB = 81 K。因此,SiO2 浓度的增加减小了 CoCr2O4 纳米粒子的尺寸和表面无序度,同时增强了自旋螺旋态有序度以下的 Ms。
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引用次数: 0
A New Approach to Designing Control of Dissolved Oxygen and Aeration System in Sequencing Batch Reactor by Applied Backstepping Control Algorithm 应用反步进控制算法设计控制序批式反应器中溶解氧和曝气系统的新方法
IF 0.7 Q3 Engineering Pub Date : 2023-12-01 DOI: 10.2478/ama-2023-0070
Michał Kolankowski, Michał Banach, R. Piotrowski, Tomasz Ujazdowski
Abstract The wastewater treatment plant (WWTP) is a complex system due to its non-linearity, time-variance and multiple time scales in its dynamics among others. The most important control parameter in a WWTP is the dissolved oxygen (DO) concentration. The tracking problem of the DO concentration is one of the most fundamental issues in biological wastewater treatment. Proper control of DO concentration is necessary to achieve adequate biological conditions for microorganisms in the WWTP. Aeration is an important process to achieve those conditions, but it is expensive. It was performed using an aeration system, which includes blowers, pipelines and diffusers. This paper presents a new approach to designing a non-linear control system for controlling DO concentration using an adaptive backstepping algorithm. A model of biological processes and aeration system were applied in designing the control system. Simulation tests of the control system were performed and very good results on control were obtained. The proposed solution has proved to be effective and computationally efficient.
摘要 污水处理厂(WWTP)是一个复杂的系统,因为其动态具有非线性、时变性和多时间尺度等特点。污水处理厂最重要的控制参数是溶解氧(DO)浓度。溶解氧浓度的跟踪问题是生物废水处理中最基本的问题之一。要使污水处理厂中的微生物获得充足的生物条件,就必须对溶解氧浓度进行适当控制。曝气是实现这些条件的一个重要过程,但成本高昂。曝气系统包括鼓风机、管道和扩散器。本文提出了一种新的方法,利用自适应反步进算法设计非线性控制系统来控制溶解氧浓度。在设计控制系统时应用了生物过程和曝气系统模型。对控制系统进行了仿真测试,取得了非常好的控制效果。事实证明,所提出的解决方案不仅有效,而且计算效率高。
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引用次数: 0
Numerical Analysis of the Boiling Heat Transfer Coefficient in the Flow in Mini-Channels 微型通道流动中沸腾传热系数的数值分析
IF 0.7 Q3 Engineering Pub Date : 2023-12-01 DOI: 10.2478/ama-2023-0069
Beata Maciejewska, S. Hożejowska, M. Grabowski, M. Poniewski
Abstract This paper deals with boiling heat transfer in the flow of water through an asymmetrically heated horizontal rectangular mini-channel. The mini-channel was made by gluing three transparent glass plates and a copper block. Through the glass window, the variable along the length of the mini-channel two-phase flow structures were recorded to determine local values of the void fraction. Four resistance heaters were attached to the copper block, powered by direct current, generating the heat initiating the flow boiling inside the channel. During the experiment, the following were measured: water volumetric flow rate, inlet pressure with pressure drop, inlet and outlet water temperature, copper block temperatures at three points inside its body, voltage and current supplied to the heaters. Stationary and laminar fluid flow with low Reynolds numbers were assumed in the mathematical model of heat transfer in selected elements of the measuring module. The temperature distributions in the copper block and flowing water were described by the appropriate energy equations: the Laplace equation for the copper block and the Fourier–Kirchhoff equation with parabolic fluid velocity for the flowing water. These equations were supplemented with a set of boundary conditions based on measurement data; moreover, data from experimental studies were the basis for numerical calculations and their verification. Two-dimensional temperature distributions of the copper block and water were calculated with the Trefftz method (TM). The main objective of this study was to determine the heat transfer coefficient on the contact surface of the copper block and water, which was calculated from the Robin boundary condition. The results of the calculations were compared with the results of numerical simulations performed using the Simcenter STAR-CCM+ software, obtaining consistent values. Computational fluid dynamics (CFD) simulations were verified based on experimental data including void fraction and temperature measurements of the copper block and flowing water.
摘要 本文研究水流通过不对称加热的水平矩形微型通道时的沸腾传热。微型通道由三块透明玻璃板和一个铜块粘合而成。通过玻璃窗记录迷你通道两相流结构沿长度方向的变量,以确定空隙率的局部值。铜块上安装了四个电阻加热器,由直流电源供电,产生的热量引发通道内的流动沸腾。在实验过程中,测量了以下数据:水的体积流量、带有压降的入口压力、入口和出口水温、铜块内部三点的温度、加热器的电压和电流。在测量模块选定元件的传热数学模型中,假设流体为静止层流,雷诺数较低。铜块和流水中的温度分布用相应的能量方程来描述:铜块用拉普拉斯方程,流水用具有抛物线流体速度的傅立叶-基尔霍夫方程。这些方程根据测量数据补充了一组边界条件;此外,实验研究数据也是数值计算及其验证的基础。铜块和水的二维温度分布采用 Trefftz 方法 (TM) 计算。这项研究的主要目的是确定铜块和水接触面上的传热系数,该系数是根据罗宾边界条件计算得出的。计算结果与使用 Simcenter STAR-CCM+ 软件进行的数值模拟结果进行了比较,得出了一致的数值。计算流体动力学 (CFD) 模拟根据实验数据(包括铜块和流水的空隙率和温度测量值)进行了验证。
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引用次数: 0
Semi-Analytical Analysis of a Rigid Rotor Mounted on Four-Pad Hydrostatic Squeeze Film Damper with Single-Action Membrane-Type Restrictors 对安装在带有单作用膜式限制器的四垫静压挤压膜阻尼器上的刚性转子的半解析分析
IF 0.7 Q3 Engineering Pub Date : 2023-12-01 DOI: 10.2478/ama-2023-0059
Ahmed Kechra, Ahmed Bouzidaine
Abstract The current study is a semi-analytical analysis of the vibratory behaviour of a rigid vertical rotor, supported by a new hydrostatic squeeze film damper (HSFD), consisting of four hydrostatic pads fed through four single-action membrane-type variable-flow restrictors. The Reynolds equation based on the Newtonian theory of lubrication is used and then adapted to our work, which is solved semi-analytically. In this paper, we study the effect of different parameters, the eccentricity, membrane geometry coefficient, pressure ratio and rotational speed, on the main characteristics of a four-pad HSFD. From the simulation results, we observed that at the critical speed, the rigid rotor fed by membrane restrictor shows a decrease in transmitted forces, a decrease in vibration response and good system stability as compared with a similar rotor fed by capillary restrictor. From the results reported in this work, we observed good agreement between our study and other works.
摘要 当前的研究是对刚性垂直转子的振动行为进行半分析,该转子由新型静压挤压膜阻尼器(HSFD)支撑,HSFD 由四个静压垫组成,通过四个单作用膜式可变流量限制器输入。我们使用了基于牛顿润滑理论的雷诺方程,并对其进行了半分析求解。本文研究了偏心率、膜几何系数、压力比和转速等不同参数对四垫片 HSFD 主要特性的影响。模拟结果表明,在临界转速下,与采用毛细管限流器的类似转子相比,采用膜限流器的刚性转子的传动力减小,振动响应降低,系统稳定性良好。从这项工作所报告的结果中,我们发现我们的研究与其他工作之间存在良好的一致性。
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引用次数: 0
Energy Conversion in Systems-Contained Laser-Irradiated Metallic Nanoparticles – Comparison of Results from Analytical Solutions and Numerical Methods 包含激光照射金属纳米粒子的系统中的能量转换--分析解决方案与数值方法结果的比较
IF 0.7 Q3 Engineering Pub Date : 2023-12-01 DOI: 10.2478/ama-2023-0063
Piotr Radomski, Paweł Ziółkowski, Dariusz Mikielewicz
Abstract This work introduces the theoretical method of metallic nanoparticles’ (NPs’) heat and mass transfer where the particles are coated on a surface (base), together with considering the case wherein nanoparticles move freely in a pipe. In order to simulate the heat transfer, energy and radiative transfer equations are adjusted to the considered issue. NPs’ properties are determined following the nanofluidic theories, whereas absorption and scattering coefficients are described using either Mie-Lorenz theory or Rayleigh-Drude approximation. Thermal boundary conditions are implemented based on the microscale heat transfer and Smoluchowski theory. Results are compared with the classical Fourier transport differential solutions that have been adjusted to laser irradiation.
摘要 本研究介绍了金属纳米粒子(NPs)传热和传质的理论方法,即在粒子表面(基底)镀膜,同时考虑纳米粒子在管道中自由移动的情况。为了模拟热量传递,对能量和辐射传递方程进行了调整,以适应所考虑的问题。纳米粒子的特性根据纳米流体理论确定,而吸收和散射系数则使用 Mie-Lorenz 理论或 Rayleigh-Drude 近似值来描述。热边界条件是根据微尺度传热和斯莫卢霍夫斯基理论实现的。研究结果与根据激光辐照进行调整的经典傅里叶传输微分解法进行了比较。
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引用次数: 0
An Innovative Approach to Fabrication With Photo-Cured Resins by Shell-Printed-Core-Casting 一种创新的光固化树脂壳印芯铸造制造方法
IF 0.7 Q3 Engineering Pub Date : 2023-08-17 DOI: 10.2478/ama-2023-0056
Emil Szymczyk, M. Rećko, K. Dzierżek, K. Sapiołko
Abstract Modified LCD-based method was used to print three-dimensional (3D) elements. This innovative method combines printing the external shell and filling, thus obtaining mould by casting resin. In order to compare the properties of prints obtained with this method with the ones fabricated in a standard procedure, we conducted bending tests of vertically/horizontally printed and shell-printed cast specimens. The shell-cast samples showed higher flexural strength and larger values of apparent Young’s modulus. The presented results also concern the kinetics of curing samples obtained with different fabrication routes.
摘要:采用改进的液晶显示技术打印三维元件。这种创新的方法将打印外壳和填充相结合,从而通过铸造树脂获得模具。为了将用这种方法获得的打印件的性能与用标准程序制造的打印件进行比较,我们对垂直/水平打印和壳打印的铸造样品进行了弯曲测试。铸壳试样具有较高的抗弯强度和较大的表观杨氏模量。所提出的结果也涉及到不同制造路线获得的固化样品的动力学。
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引用次数: 0
Experimental Investigation of a Uniaxial Dielectric Elastomer Generator 单轴介质弹性体发生器的实验研究
IF 0.7 Q3 Engineering Pub Date : 2023-08-17 DOI: 10.2478/ama-2023-0058
W. Sikora
Abstract The widespread use of battery-powered electronic devices creates the need to develop methods to extend their maximum operating time. This can be achieved by using ambient energy, which would otherwise be dissipated. The conversion of energy, usually mechanical energy, into electric energy takes place in energy harvesters. Energy harvester systems based on a dielectric elastomer (DE) are a relatively new field that is being constantly developed. Due to their features, dielectric elastomer generators (DEGs) may complement the currently dominant piezoelectric harvesters. The major feature of employing a hyperelastic material is that it allows relatively large displacements to be utilised for generating energy, which is impossible in the case of piezoceramics. This article presents a DEG designed to operate under uniaxial tensile loads and which has a multilayer structure, describes the general operating principles of a DEG, explains the construction and assembly process of the investigated design and shows the electric circuit necessary to properly direct current flow during the DEG operation. The experimental part consists of two series of tests based on a central composite design (CCD). The objective of the first part was to map a capacitance response surface of the DEG in the selected range of the cyclic mechanical load. The second part concerned the amount of generated energy for the specific load case as a function of operating voltages. The result of the work is the formulation of regression models that allow the characteristics of the presented DEG design to be identified.
随着电池供电电子设备的广泛使用,需要开发延长其最大工作时间的方法。这可以通过利用周围的能量来实现,否则这些能量会被消耗掉。能量(通常是机械能)在能量采集器中转换成电能。基于介电弹性体(DE)的能量收集系统是一个相对较新的领域,正在不断发展。由于其特点,介电弹性体发电机(DEGs)可以补充目前占主导地位的压电收集器。采用超弹性材料的主要特点是,它允许利用相对较大的位移来产生能量,这在压电陶瓷的情况下是不可能的。本文介绍了一种在单轴拉伸载荷下工作的多层结构的DEG,描述了DEG的一般工作原理,解释了所研究设计的结构和组装过程,并展示了在DEG工作时适当直流流动所必需的电路。实验部分包括基于中心复合设计(CCD)的两个系列测试。第一部分的目的是在循环机械载荷的选定范围内绘制DEG的电容响应面。第二部分涉及特定负载情况下作为工作电压函数的发电量。工作的结果是制定回归模型,允许提出的DEG设计的特点被识别。
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引用次数: 0
Effectiveness of Friction Force Reduction in Sliding Motion Depending on the Frequency of Longitudinal Tangential Vibrations, Sliding Velocity and Normal Pressure 根据纵向切向振动频率、滑动速度和法向压力降低滑动摩擦力的有效性
IF 0.7 Q3 Engineering Pub Date : 2023-08-17 DOI: 10.2478/ama-2023-0057
Mariusz Leus, P. Gutowski, Marta Rybkiewicz
Abstract The article presents the results of experimental research and simulation analyses of the influence of slip velocity, normal pressures and vibration frequency on the effectiveness of friction force reduction carried out in sliding motion in the presence of forced tangential vibrations. In experimental studies, changes in the driving force were measured during the slip of the upper body over the vibrating lower body. The direction of these vibrations was parallel both to the contact plane and to the direction of movement of the shifted body. The simulation tests were carried out in the Matlab/Simulink environment through the use of numerical procedures that were specially created for this purpose. Dynamic friction models considering the tangential compliance of contact and the phenomenon of pre-sliding displacement were used for calculations. The paper presents the designated values of the so-called coefficient of average friction force reduction in sliding motion for the following friction pairs: steel C45–steel C45, steel C45–cast iron GGG40 and steel C45–polytetrafluoroethy-lene PTFE (Teflon). The results of numerical analyses were in good agreement with those of experimental tests. A significant dependence of the level of average friction force reduction on the frequency of forced vibrations, sliding velocity as well as the kind of sliding pair material, and normal pressures was shown.
摘要本文介绍了滑移速度、法向压力和振动频率对存在强迫切向振动的滑动运动中减小摩擦力有效性影响的实验研究和仿真分析结果。在实验研究中,测量了上半身在振动的下半身上滑动时驱动力的变化。这些振动的方向与接触面和被移物体的运动方向平行。仿真测试在Matlab/Simulink环境中通过使用为此目的专门创建的数值程序进行。采用考虑接触切向柔度和预滑位移现象的动力摩擦模型进行计算。本文提出了C45 - C45钢、C45 -铸铁GGG40钢和C45 -聚四氟乙烯聚四氟乙烯(Teflon)钢三种摩擦副在滑动运动中所谓平均摩擦力减小系数的定值。数值分析结果与试验结果吻合较好。结果表明,平均摩擦力减小水平与受迫振动频率、滑动速度以及滑动副材料的种类和法向压力有关。
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引用次数: 0
Effect of Dam–Rock Foundation Interaction Modeling on the Modal Ratio-Related Quantity of Beni Behdel and ‘El Mefrouch Multi-Arch Dams 坝岩基础相互作用模型对贝尼贝德尔和梅弗洛奇多拱坝模态比相关量的影响
IF 0.7 Q3 Engineering Pub Date : 2023-07-16 DOI: 10.2478/ama-2023-0052
A. Berrabah, A. Attia, Daoudi Mohammed Habib, D. Ouzandja
Abstract Using the Beni Behdel dam and the El Mefrouch dam as example studies, this paper intends to clearly demonstrate how modeling of the interactions between rock foundations and dams impacts the modal behavior of these two multi-arch dams. The uniqueness of this study is that the modal behavior of each dam is represented in terms of related parameters (period, participation factor, ratio, and effective mass), and more precisely in terms of ratio (defined as the ratio between the participation factor of the mode i and the maximum participation factor), as opposed to other works that have expressed this behavior in terms of frequency. In this article, stiff rock foundation, massless rock foundation, and massed rock foundation are the three methods used to simulate dynamic interactions. The investigated dams are three-dimensionally simulated using the ANSYS finite elements code. The modeling of the rock foundation–dam interaction has an effect on the fundamental mode value, its location, and the related parameters, according to the results. Furthermore, it is found that the upstream–downstream direction is not always the most important direction for dams and that interaction modeling influences the resonance bandwidth, which affects the forecast of the resonance phenomenon.
摘要以Beni Behdel大坝和El Mefrouch大坝为例,本文旨在清楚地展示岩石基础和大坝之间的相互作用建模如何影响这两座连拱坝的模态行为。本研究的独特性在于,每个大坝的模态行为都是用相关参数(周期、参与因子、比率和有效质量)来表示的,更准确地说,是用比率(定义为模式i的参与因子和最大参与因子之间的比率)来表示,与其他在频率方面表达这种行为的作品相反。本文中,刚性岩石基础、无质量岩石基础和块状岩石基础是用于模拟动力相互作用的三种方法。利用ANSYS有限元程序对所研究的大坝进行了三维模拟。根据结果,岩石-基础-大坝相互作用的建模对基本模态值、位置和相关参数有影响。此外,研究发现,上下游方向并不总是大坝最重要的方向,相互作用建模会影响共振带宽,从而影响共振现象的预测。
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引用次数: 0
Material Characteristic of an Innovative Stent for the Treatment of Urethral Stenosis 用于治疗尿道狭窄的新型支架的材料特性
IF 0.7 Q3 Engineering Pub Date : 2023-07-16 DOI: 10.2478/ama-2023-0055
Jagoda Kurowiak, A. Mackiewicz, T. Klekiel, R. Będziński
Abstract The appropriate development and customisation of the stent to the urethral tissues requires the determination of many factors such as strength and degradation. Given the distinctive conditions of urethral tissues, it is important that the design of the stent be properly developed. The selection of a stent material requires knowing its material characteristics and verifying that they are suitable for the future implantation site. In the present study, the development of a polydioxanone (PDO)-based stent was undertaken. The PDO material was fabricated using an additive technique – 3D printing. Then, in vitro tests were performed to determine the degradation time of the material under conditions simulating an aggressive urinary environment. The changes in the parameters of mechanical properties before and after the degradation period were determined, and the changes in the structure of the material before and after degradation were observed. Numerical analysis was performed for the proposed stent design. The results showed that PDO has good mechanical properties, but its degradation time is too short to be used in a urethral stent. Among the innovations of the studies conducted are bending strength tests, which is not a frequently considered aspect so far.
摘要尿道组织支架的适当开发和定制需要确定许多因素,如强度和降解。鉴于尿道组织的特殊情况,正确开发支架的设计是很重要的。支架材料的选择需要了解其材料特性,并验证其是否适合未来的植入部位。在本研究中,开发了一种基于聚二氧烷酮(PDO)的支架。PDO材料是使用添加技术(3D打印)制造的。然后,进行体外测试,以确定在模拟侵蚀性尿液环境的条件下材料的降解时间。测定了降解前后机械性能参数的变化,并观察了降解前后材料结构的变化。对所提出的支架设计进行了数值分析。结果表明,PDO具有良好的力学性能,但降解时间太短,不能用于尿道支架。在所进行的研究的创新中,弯曲强度测试是一个迄今为止还不是经常考虑的方面。
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引用次数: 1
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Acta Mechanica et Automatica
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