首页 > 最新文献

Applied Composite Materials最新文献

英文 中文
A Novel Construct to Perform In Situ Deformation Measurements of Material Extrusion-Fabricated Structures 对材料挤压成型结构进行现场变形测量的新结构
IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-12-03 DOI: 10.1007/s10443-024-10283-4
Daniel Nelson, Valeria La Saponara

Material extrusion is an additive manufacturing modality that continues to show great promise in the ability to create low cost, highly intricate, and exceedingly useful structural elements. As more capable and versatile filament materials are devised and the resolution of manufacturing systems continues to increase, the need to understand and predict manufacturing-induced warping will gain ever greater importance. The following study presents a novel in situ remote sensing and data analysis construct that allows for the in situ mapping and quantification of surface displacements induced by residual stresses on specified test structures. This proof-of-concept experimental process shows that it is possible to provide designers and manufacturers with insight into the manufacturing parameters that lead to these deformations, with a greater understanding of the behavior of these warping events over the course of the manufacturing process.

{"title":"A Novel Construct to Perform In Situ Deformation Measurements of Material Extrusion-Fabricated Structures","authors":"Daniel Nelson,&nbsp;Valeria La Saponara","doi":"10.1007/s10443-024-10283-4","DOIUrl":"10.1007/s10443-024-10283-4","url":null,"abstract":"<div><p>Material extrusion is an additive manufacturing modality that continues to show great promise in the ability to create low cost, highly intricate, and exceedingly useful structural elements. As more capable and versatile filament materials are devised and the resolution of manufacturing systems continues to increase, the need to understand and predict manufacturing-induced warping will gain ever greater importance. The following study presents a novel in situ remote sensing and data analysis construct that allows for the in situ mapping and quantification of surface displacements induced by residual stresses on specified test structures. This proof-of-concept experimental process shows that it is possible to provide designers and manufacturers with insight into the manufacturing parameters that lead to these deformations, with a greater understanding of the behavior of these warping events over the course of the manufacturing process.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"32 2","pages":"395 - 413"},"PeriodicalIF":2.3,"publicationDate":"2024-12-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s10443-024-10283-4.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143778003","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Tensile Properties of Scarf-Repaired Composite Laminates with Bonding Defects
IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-11-29 DOI: 10.1007/s10443-024-10286-1
Jinxin DENG, Wenjun HUANG, Xiaoquan CHENG

Scarf repair is a common repair method for composite laminate structures. Poor workmanship may cause bonding defects in the repair area. In this paper, the tensile properties of scarf-repaired composite laminates with three types of adhesive pore defects were studied by finite element method, and the effects of defect type, area and location were discussed. The results indicate that adhesive pores lead to local stress concentrations, significantly reducing the damage initiation load of the adhesive and laminate, but have limited influence on the initial stiffness and ultimate load of the structure. Pore defects alter the adhesive damage propagation mode but do not change the ultimate failure mode of the structure. Larger defect areas (porosity) result in lower structural tensile performance, and defects located in high-stress regions cause earlier damage initiation. ‌Different types of adhesive defects exhibit varying effects on structural tensile performance.‌.

{"title":"Tensile Properties of Scarf-Repaired Composite Laminates with Bonding Defects","authors":"Jinxin DENG,&nbsp;Wenjun HUANG,&nbsp;Xiaoquan CHENG","doi":"10.1007/s10443-024-10286-1","DOIUrl":"10.1007/s10443-024-10286-1","url":null,"abstract":"<div><p>Scarf repair is a common repair method for composite laminate structures. Poor workmanship may cause bonding defects in the repair area. In this paper, the tensile properties of scarf-repaired composite laminates with three types of adhesive pore defects were studied by finite element method, and the effects of defect type, area and location were discussed. The results indicate that adhesive pores lead to local stress concentrations, significantly reducing the damage initiation load of the adhesive and laminate, but have limited influence on the initial stiffness and ultimate load of the structure. Pore defects alter the adhesive damage propagation mode but do not change the ultimate failure mode of the structure. Larger defect areas (porosity) result in lower structural tensile performance, and defects located in high-stress regions cause earlier damage initiation. ‌Different types of adhesive defects exhibit varying effects on structural tensile performance.‌.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"32 2","pages":"575 - 597"},"PeriodicalIF":2.3,"publicationDate":"2024-11-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143778073","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Applied Composite Materials Special Memorial Issue on Structural Integrity of Engineering Composite Materials 应用复合材料工程复合材料结构完整性专题纪念刊
IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-11-21 DOI: 10.1007/s10443-024-10287-0
Maria Kashtalyan, Costas Soutis, Anoush Poursartip
{"title":"Applied Composite Materials Special Memorial Issue on Structural Integrity of Engineering Composite Materials","authors":"Maria Kashtalyan,&nbsp;Costas Soutis,&nbsp;Anoush Poursartip","doi":"10.1007/s10443-024-10287-0","DOIUrl":"10.1007/s10443-024-10287-0","url":null,"abstract":"","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"31 6","pages":"1791 - 1793"},"PeriodicalIF":2.3,"publicationDate":"2024-11-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142790345","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A Review of Structural Health Monitoring for Flexible Composite Materials
IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-11-16 DOI: 10.1007/s10443-024-10285-2
Xiangli Hu, Jiangxing Wu, Yantao Gao

Flexible composite materials find extensive utilization in diverse applications. However, during the use of fiber-reinforced flexible composite materials, various types of damage may occur due to aging, improper use, and incorrect manufacturing and assembly, necessitating real-time monitoring of the health status of flexible composite materials to prevent accidents. This article first introduces the main monitoring methods and principles of structural health monitoring, further elaborates and summarizes the research status of structural detection of fiber-reinforced flexible composite materials, and prospects for future development directions.

{"title":"A Review of Structural Health Monitoring for Flexible Composite Materials","authors":"Xiangli Hu,&nbsp;Jiangxing Wu,&nbsp;Yantao Gao","doi":"10.1007/s10443-024-10285-2","DOIUrl":"10.1007/s10443-024-10285-2","url":null,"abstract":"<div><p>Flexible composite materials find extensive utilization in diverse applications. However, during the use of fiber-reinforced flexible composite materials, various types of damage may occur due to aging, improper use, and incorrect manufacturing and assembly, necessitating real-time monitoring of the health status of flexible composite materials to prevent accidents. This article first introduces the main monitoring methods and principles of structural health monitoring, further elaborates and summarizes the research status of structural detection of fiber-reinforced flexible composite materials, and prospects for future development directions.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"32 2","pages":"431 - 471"},"PeriodicalIF":2.3,"publicationDate":"2024-11-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143778005","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Structural Behaviour of TPU Based Hybrid Laminated Structures Subjected to Static and Dynamic Perforation Loading 静态和动态射孔载荷作用下TPU基复合层合结构的结构性能
IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-11-14 DOI: 10.1007/s10443-024-10282-5
Muhd Azimin bin Ab Ghani, Qingyuan Wang, Zhongwei Guan

This paper presents a study on manufacturing a range of hybrid laminated structures made of thermoplastic polyurethan (TPU), glass fibre reinforced plastic (GFRP), styrene-butadiene rubber (SBR) and metal mesh materials, and further on investigating the structural response of the TPU based composite sandwich laminated structures. These laminated structures were tested under quasi-static perforation and low velocity impact loading to determine their structural responses and energy absorption characteristics. It has been shown that three-layer and five-layer laminates with lay-ups of GFRP-TPU-GFRP or TPU-GFRP-TPU and GFRP-TPU-GFRP-TPU-GFRP or TPU-GFRP-TPU-GFRP-TPU subjected to quasi-static perforation demonstrate an increased peak load and stiffness with the core thickness from 1 to 4 mm. Also, the TPU core laminates show a superior ductility in comparison to their GFRP core counterparts. The energy absorption values of the three-layer and five-layer TPU and GFRP based laminated structures under low velocity impact are higher than those under quasi-static loading due to strain-rate effect. However, the hybrid laminates with SBR and wire mesh as a core do not give much improvement on the impact perforation resistance of the laminates with the different size of wire mesh, as metal mesh plays a less important role in the laminated structures to resist perforation. In overall, TPU-GFRP-TPU-GFRP-TPU structure with 4mm thick GFRP core demonstrates the highest peak force, and the GFRP-TPU-GFRP-TPU-GFRP structure with 4mm thick TPU core offers the highest energy absorption.

本文研究了由热塑性聚氨酯(TPU)、玻璃纤维增强塑料(GFRP)、丁苯橡胶(SBR)和金属网材料制成的复合层合结构,并进一步研究了TPU基复合夹层层合结构的结构响应。在准静态射孔和低速冲击载荷作用下,测试了复合材料的结构响应和吸能特性。研究表明,当芯层厚度为1 ~ 4mm时,GFRP-TPU-GFRP、TPU-GFRP-TPU、GFRP-TPU-GFRP- gfrp或TPU-GFRP-TPU- gfrp - tpu层合板的峰值载荷和刚度均有所增加。此外,与GFRP芯板相比,TPU芯层压板具有优越的延展性。由于应变率效应,三层和五层TPU和GFRP复合结构在低速冲击下的能量吸收值高于准静态载荷作用下的能量吸收值。然而,以SBR和钢丝网为核心的混合层合板对不同钢丝网尺寸层合板的抗冲击穿孔性能并没有太大的提高,因为金属网在层合结构中的抗穿孔作用较小。总体而言,GFRP芯厚为4mm的TPU-GFRP-TPU-GFRP-TPU结构的峰值力最大,tfrp芯厚为4mm的GFRP-TPU-GFRP- GFRP结构的吸能最大。
{"title":"Structural Behaviour of TPU Based Hybrid Laminated Structures Subjected to Static and Dynamic Perforation Loading","authors":"Muhd Azimin bin Ab Ghani,&nbsp;Qingyuan Wang,&nbsp;Zhongwei Guan","doi":"10.1007/s10443-024-10282-5","DOIUrl":"10.1007/s10443-024-10282-5","url":null,"abstract":"<div><p>This paper presents a study on manufacturing a range of hybrid laminated structures made of thermoplastic polyurethan (TPU), glass fibre reinforced plastic (GFRP), styrene-butadiene rubber (SBR) and metal mesh materials, and further on investigating the structural response of the TPU based composite sandwich laminated structures. These laminated structures were tested under quasi-static perforation and low velocity impact loading to determine their structural responses and energy absorption characteristics. It has been shown that three-layer and five-layer laminates with lay-ups of GFRP-TPU-GFRP or TPU-GFRP-TPU and GFRP-TPU-GFRP-TPU-GFRP or TPU-GFRP-TPU-GFRP-TPU subjected to quasi-static perforation demonstrate an increased peak load and stiffness with the core thickness from 1 to 4 mm. Also, the TPU core laminates show a superior ductility in comparison to their GFRP core counterparts. The energy absorption values of the three-layer and five-layer TPU and GFRP based laminated structures under low velocity impact are higher than those under quasi-static loading due to strain-rate effect. However, the hybrid laminates with SBR and wire mesh as a core do not give much improvement on the impact perforation resistance of the laminates with the different size of wire mesh, as metal mesh plays a less important role in the laminated structures to resist perforation. In overall, TPU-GFRP-TPU-GFRP-TPU structure with 4mm thick GFRP core demonstrates the highest peak force, and the GFRP-TPU-GFRP-TPU-GFRP structure with 4mm thick TPU core offers the highest energy absorption.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"31 6","pages":"2047 - 2069"},"PeriodicalIF":2.3,"publicationDate":"2024-11-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142790378","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Structure Design and Performance Evaluation of Fibre Reinforced Composite Honeycombs: A Review 纤维增强复合材料蜂窝结构设计与性能评价综述
IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-11-07 DOI: 10.1007/s10443-024-10281-6
Ao Liu, Aoxin Wang, Qian Jiang, Yanan Jiao, Liwei Wu, Youhong Tang

With the widespread application of sandwich composites, the performance of the core structure in the sandwich composites has received particular attention. As the typical representative of lightweight core structure, honeycombs have excellent designability and are widely used. The emerging fibre reinforced composite honeycombs have incomparable performance advantages over traditional metal or chopped fibre honeycombs. This means that design, manufacturing technologies and performance evaluation of composite honeycombs are important. In this review, grid, hexagonal, Kagome, corrugated and origami structure honeycombs and their associated manufacturing strategies have been summarised. In addition, more attention has been paid to textile structure composite honeycombs fabricated by weaving, braiding, or knitting techniques. Their mechanical performances have been extensively reviewed to clarify the relationship between structure and properties. Based on existing studies, the damage mechanisms of composite honeycomb structures are found to be insufficient; especially for the load-bearing mechanisms and predicting methods for honeycombs, which is a challenge for further development. This review hopes to inspire the innovation in fibre reinforced composite honeycombs from the view of structure design and performance evaluation.

随着夹层复合材料的广泛应用,夹层复合材料芯结构的性能受到了人们的特别关注。蜂窝结构作为轻量化核心结构的典型代表,具有优良的可设计性和广泛的应用前景。新型纤维增强复合材料蜂窝具有传统金属或短切纤维蜂窝无法比拟的性能优势。这意味着复合材料蜂窝的设计、制造技术和性能评价是非常重要的。本文综述了网格结构、六边形结构、Kagome结构、瓦楞结构和折纸结构蜂窝及其相关的制造策略。此外,通过编织、编织或针织技术制造的纺织结构复合材料蜂窝也受到了更多的关注。为了阐明结构与性能之间的关系,对其力学性能进行了广泛的综述。基于已有的研究,发现复合材料蜂窝结构的损伤机理研究不足;特别是蜂窝的承载机理和预测方法,这是一个有待进一步发展的挑战。本文希望从结构设计和性能评价两个方面对纤维增强复合材料蜂窝的创新有所启发。
{"title":"Structure Design and Performance Evaluation of Fibre Reinforced Composite Honeycombs: A Review","authors":"Ao Liu,&nbsp;Aoxin Wang,&nbsp;Qian Jiang,&nbsp;Yanan Jiao,&nbsp;Liwei Wu,&nbsp;Youhong Tang","doi":"10.1007/s10443-024-10281-6","DOIUrl":"10.1007/s10443-024-10281-6","url":null,"abstract":"<div><p>With the widespread application of sandwich composites, the performance of the core structure in the sandwich composites has received particular attention. As the typical representative of lightweight core structure, honeycombs have excellent designability and are widely used. The emerging fibre reinforced composite honeycombs have incomparable performance advantages over traditional metal or chopped fibre honeycombs. This means that design, manufacturing technologies and performance evaluation of composite honeycombs are important. In this review, grid, hexagonal, Kagome, corrugated and origami structure honeycombs and their associated manufacturing strategies have been summarised. In addition, more attention has been paid to textile structure composite honeycombs fabricated by weaving, braiding, or knitting techniques. Their mechanical performances have been extensively reviewed to clarify the relationship between structure and properties. Based on existing studies, the damage mechanisms of composite honeycomb structures are found to be insufficient; especially for the load-bearing mechanisms and predicting methods for honeycombs, which is a challenge for further development. This review hopes to inspire the innovation in fibre reinforced composite honeycombs from the view of structure design and performance evaluation.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"31 6","pages":"2019 - 2045"},"PeriodicalIF":2.3,"publicationDate":"2024-11-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142790412","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Damage Resistance of Honeycomb Sandwich Composites under Low-Energy Impact 蜂窝夹层复合材料在低能量冲击下的抗破坏性
IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-29 DOI: 10.1007/s10443-024-10278-1
Bohan He, Xiaoxia Zheng, Qiao Yang, Yu Zou, Kai Wu, Zhengdong Liu, Jiangxu Gong, Zhiqiang Li

Due to advantages of light-weight, high-strength, and superior energy absorption, honeycomb sandwich composites (HSC) are widely used in the aerospace industry. However, HSC are prone to damage from low-energy impacts, posing a threat to the overall safety of components. This paper presents a comprehensive analysis of the damage resistance of the HSC synergistic approach of experimental validation and finite element (FE) simulation. A drop hammer impact experiment was conducted on specimens with varying upper and lower panels thicknesses, utilizing Digital Image Correlation (DIC) technology to monitor the deformation and strain of the impacted panels. The study identified the upper panel as the initial failure point, characterized by matrix cracking, fiber fracture, and interlayer delamination, with the honeycomb core primarily experiencing crushing damage. A critical impact energy threshold of 40 J was established for upper panel penetration, with lower panel damage becoming evident at energies exceeding 80 J. The quantity of panel layers significantly enhances the damage resistance of the structure. Investigated the damage characteristics of the lower panel under impact load. An FE model was meticulously constructed, incorporating the Hashin failure criterion and damage evolution, and was calibrated to reflect the experimental conditions precisely. The simulation results were found to be in excellent agreement with experimental data, with discrepancies within a 5% margin, thereby validating the predictive capabilities of FE model. The interlayer damage of finite element model, leading to the identification of delamination characteristics. This insight is advantageous for the analysis of the residual strength. Subsequent analysis explored the impact of various design parameters on damage resistance, providing valuable insights for the structural design and material selection in aerospace applications.

{"title":"Damage Resistance of Honeycomb Sandwich Composites under Low-Energy Impact","authors":"Bohan He,&nbsp;Xiaoxia Zheng,&nbsp;Qiao Yang,&nbsp;Yu Zou,&nbsp;Kai Wu,&nbsp;Zhengdong Liu,&nbsp;Jiangxu Gong,&nbsp;Zhiqiang Li","doi":"10.1007/s10443-024-10278-1","DOIUrl":"10.1007/s10443-024-10278-1","url":null,"abstract":"<div><p>Due to advantages of light-weight, high-strength, and superior energy absorption, honeycomb sandwich composites (HSC) are widely used in the aerospace industry. However, HSC are prone to damage from low-energy impacts, posing a threat to the overall safety of components. This paper presents a comprehensive analysis of the damage resistance of the HSC synergistic approach of experimental validation and finite element (FE) simulation. A drop hammer impact experiment was conducted on specimens with varying upper and lower panels thicknesses, utilizing Digital Image Correlation (DIC) technology to monitor the deformation and strain of the impacted panels. The study identified the upper panel as the initial failure point, characterized by matrix cracking, fiber fracture, and interlayer delamination, with the honeycomb core primarily experiencing crushing damage. A critical impact energy threshold of 40 J was established for upper panel penetration, with lower panel damage becoming evident at energies exceeding 80 J. The quantity of panel layers significantly enhances the damage resistance of the structure. Investigated the damage characteristics of the lower panel under impact load. An FE model was meticulously constructed, incorporating the Hashin failure criterion and damage evolution, and was calibrated to reflect the experimental conditions precisely. The simulation results were found to be in excellent agreement with experimental data, with discrepancies within a 5% margin, thereby validating the predictive capabilities of FE model. The interlayer damage of finite element model, leading to the identification of delamination characteristics. This insight is advantageous for the analysis of the residual strength. Subsequent analysis explored the impact of various design parameters on damage resistance, providing valuable insights for the structural design and material selection in aerospace applications.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"32 2","pages":"703 - 732"},"PeriodicalIF":2.3,"publicationDate":"2024-10-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143778054","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Experimental Investigation οf Bio-Based Polymers Reinforced with Graphene Oxide 石墨烯氧化物增强生物基聚合物的实验研究
IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-28 DOI: 10.1007/s10443-024-10274-5
Aikaterini N. Gargala, Panagiota V. Polydoropoulou, Konstantinos Tserpes

Graphene oxide (GO) is a commonly used additive to enhance the mechanical properties of epoxy polymers. The quality of GO and the homogeneity of its dispersion into epoxy can notably improve the mechanical properties of multifunctional polymers. This work aims to clarify contradictory results of the effect of GO on the mechanical properties of bio-based polymers by synthesizing high-quality and low-cost GO. To this end, we investigated the effect of adding solvents (acetone, THF) on the mechanical behavior of polymers subjected to several types of static loading. Five different types of materials were examined: neat epoxy (reference material), enhanced epoxy without solvent, enhanced epoxy with acetone solvent, enhanced epoxy with THF solvent, and epoxy enhanced with pure graphite powder. The concentration of GO or graphite was 0.5 wt%. The findings were analyzed using Scanning Electron Microscope (SEM), Thermogravimetric Analysis (TGA), and Raman Spectroscopy. A significant increase in the tensile strength and fracture toughness of polymers filled with GO without solvent was observed compared to the enhanced materials with solvents. SEM analysis of the fracture surfaces revealed resin penetration into the graphene sheets, indicating strong bonding between amino groups and graphene oxide in the case of the enhanced epoxy without solvent. In contrast, in the enhanced epoxies with solvents, the GO-epoxy bonding appeared to be either deteriorated or destroyed. TGA analysis revealed that both neat and GO-reinforced resins without solvent were thermally stable up to 360 °C. Raman spectra showed epoxy ring vibrations during the curing process, indicating the quantity of free epoxides in the samples.

{"title":"Experimental Investigation οf Bio-Based Polymers Reinforced with Graphene Oxide","authors":"Aikaterini N. Gargala,&nbsp;Panagiota V. Polydoropoulou,&nbsp;Konstantinos Tserpes","doi":"10.1007/s10443-024-10274-5","DOIUrl":"10.1007/s10443-024-10274-5","url":null,"abstract":"<div><p>Graphene oxide (GO) is a commonly used additive to enhance the mechanical properties of epoxy polymers. The quality of GO and the homogeneity of its dispersion into epoxy can notably improve the mechanical properties of multifunctional polymers. This work aims to clarify contradictory results of the effect of GO on the mechanical properties of bio-based polymers by synthesizing high-quality and low-cost GO. To this end, we investigated the effect of adding solvents (acetone, THF) on the mechanical behavior of polymers subjected to several types of static loading. Five different types of materials were examined: neat epoxy (reference material), enhanced epoxy without solvent, enhanced epoxy with acetone solvent, enhanced epoxy with THF solvent, and epoxy enhanced with pure graphite powder. The concentration of GO or graphite was 0.5 wt%. The findings were analyzed using Scanning Electron Microscope (SEM), Thermogravimetric Analysis (TGA), and Raman Spectroscopy. A significant increase in the tensile strength and fracture toughness of polymers filled with GO without solvent was observed compared to the enhanced materials with solvents. SEM analysis of the fracture surfaces revealed resin penetration into the graphene sheets, indicating strong bonding between amino groups and graphene oxide in the case of the enhanced epoxy without solvent. In contrast, in the enhanced epoxies with solvents, the GO-epoxy bonding appeared to be either deteriorated or destroyed. TGA analysis revealed that both neat and GO-reinforced resins without solvent were thermally stable up to 360 °C. Raman spectra showed epoxy ring vibrations during the curing process, indicating the quantity of free epoxides in the samples.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"32 2","pages":"473 - 492"},"PeriodicalIF":2.3,"publicationDate":"2024-10-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143778070","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Basalt Fiber-Reinforced Epoxy Laminates: Improvement in Quasi-Static and Fatigue Properties with Modified Matrices and Fiber Surfaces Using Silica Nanoparticles
IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-28 DOI: 10.1007/s10443-024-10273-6
Mayank Agrawal, R T Durai Prabhakaran, Puneet Mahajan

The performance of composite materials is influenced largely by adding organic or inorganic nanoparticles. The composite properties also depend on the fiber/matrix interface bonding. The present article focuses on the influence of basalt fiber surface modifications using hybrid sizings (silane/and silica nanoparticles (SNPs)) and matrix modifications by adding SNPs in the epoxy resin are studied. Vacuum-assisted resin infusion molding (VARIM) was used to fabricate the basalt fiber/epoxy composites. First, the commercial fibers were washed in acetone to remove the commercial sizing; thereafter, a hybrid sizing (3-Glycidyloxypropyl) trimethoxysilane (GPMS)/SNP was applied using the dip-coating method. The SNPs were dispersed using homogenization and probe sonication before infusion. There is an improvement of about 9.05% and 11.33% in the tensile strength and 2.40% and 4.13% in the tensile modulus of as-received basalt fibers with modified epoxy (ABF/EPSNP) and sized basalt fibers with as-received epoxy resin (SBF/EP) composites, respectively. The flexural strength and modulus have improved by about 30% and 8.5%, respectively. Failure mechanisms were analyzed using scanning electron microscopy. From the current study, it was found that surface modifications could result in better composite performance.

Graphical Abstract

{"title":"Basalt Fiber-Reinforced Epoxy Laminates: Improvement in Quasi-Static and Fatigue Properties with Modified Matrices and Fiber Surfaces Using Silica Nanoparticles","authors":"Mayank Agrawal,&nbsp;R T Durai Prabhakaran,&nbsp;Puneet Mahajan","doi":"10.1007/s10443-024-10273-6","DOIUrl":"10.1007/s10443-024-10273-6","url":null,"abstract":"<div><p>The performance of composite materials is influenced largely by adding organic or inorganic nanoparticles. The composite properties also depend on the fiber/matrix interface bonding. The present article focuses on the influence of basalt fiber surface modifications using hybrid sizings (silane/and silica nanoparticles (SNPs)) and matrix modifications by adding SNPs in the epoxy resin are studied. Vacuum-assisted resin infusion molding (VARIM) was used to fabricate the basalt fiber/epoxy composites. First, the commercial fibers were washed in acetone to remove the commercial sizing; thereafter, a hybrid sizing (3-Glycidyloxypropyl) trimethoxysilane (GPMS)/SNP was applied using the dip-coating method. The SNPs were dispersed using homogenization and probe sonication before infusion. There is an improvement of about 9.05% and 11.33% in the tensile strength and 2.40% and 4.13% in the tensile modulus of as-received basalt fibers with modified epoxy (ABF/EPSNP) and sized basalt fibers with as-received epoxy resin (SBF/EP) composites, respectively. The flexural strength and modulus have improved by about 30% and 8.5%, respectively. Failure mechanisms were analyzed using scanning electron microscopy. From the current study, it was found that surface modifications could result in better composite performance.</p><h3>Graphical Abstract</h3><div><figure><div><div><picture><img></picture></div></div></figure></div></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"32 2","pages":"659 - 679"},"PeriodicalIF":2.3,"publicationDate":"2024-10-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143778080","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Advancing Lower Limb Prosthetics: Custom Design, Simulation, and Experimental Evaluation 推进下肢修复术:定制设计、模拟和实验评估
IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-24 DOI: 10.1007/s10443-024-10271-8
Felipe Eduardo Ribeiro Silva, Antonio Carlos Ancelotti Jr., Guilherme Ferreira Gomes

Addressing the rehabilitation needs of individuals with lower limb amputations, prostheses play a crucial role in providing comfort and functionality, facilitating walking and daily activities. Prostheses for transtibial amputon specifically cater to the area below the knee joint, encompassing the tibia, fibula, and foot. Conventionally, prosthetic feet are mass-produced through molding techniques using the autoclave process, resulting in standardized designs lacking personalization. In pursuit of a tailored and cost-effective solution, this study endeavors to conceptualize, fabricate, and assess the feasibility of a novel prosthetic foot design. The methodology involves 3D scanning of a real human foot to obtain an editable design model, subsequently utilized in crafting the structural component of the foot from carbon fiber/epoxy composite. Finite element analysis is employed to evaluate structural integrity, encompassing stress analysis, deformations, and the Tsai-Wu failure criterion. Full-scale models are then 3D printed using thermoplastic polyurethane (TPU) filament, augmented with an internally fabricated reinforcement structure comprising a polymer matrix composite reinforced with carbon fiber. Mechanical testing, in accordance with ISO 10328:2016 standards, is conducted to validate the proposed structures. Correlation between numerical simulations and experimental results demonstrates satisfactory agreement. Notably, mechanical tests reveal a 358% over performance in the heel region, surpassing standard requirements. Conversely, the forefoot segment exhibits failure under a 20% load due to defects inherent in the composite manufacturing process. The findings underscore the potential of the proposed concept as a promising alternative in lower limb prosthetics, offering both customization and affordability.

{"title":"Advancing Lower Limb Prosthetics: Custom Design, Simulation, and Experimental Evaluation","authors":"Felipe Eduardo Ribeiro Silva,&nbsp;Antonio Carlos Ancelotti Jr.,&nbsp;Guilherme Ferreira Gomes","doi":"10.1007/s10443-024-10271-8","DOIUrl":"10.1007/s10443-024-10271-8","url":null,"abstract":"<div><p>Addressing the rehabilitation needs of individuals with lower limb amputations, prostheses play a crucial role in providing comfort and functionality, facilitating walking and daily activities. Prostheses for transtibial amputon specifically cater to the area below the knee joint, encompassing the tibia, fibula, and foot. Conventionally, prosthetic feet are mass-produced through molding techniques using the autoclave process, resulting in standardized designs lacking personalization. In pursuit of a tailored and cost-effective solution, this study endeavors to conceptualize, fabricate, and assess the feasibility of a novel prosthetic foot design. The methodology involves 3D scanning of a real human foot to obtain an editable design model, subsequently utilized in crafting the structural component of the foot from carbon fiber/epoxy composite. Finite element analysis is employed to evaluate structural integrity, encompassing stress analysis, deformations, and the Tsai-Wu failure criterion. Full-scale models are then 3D printed using thermoplastic polyurethane (TPU) filament, augmented with an internally fabricated reinforcement structure comprising a polymer matrix composite reinforced with carbon fiber. Mechanical testing, in accordance with ISO 10328:2016 standards, is conducted to validate the proposed structures. Correlation between numerical simulations and experimental results demonstrates satisfactory agreement. Notably, mechanical tests reveal a 358% over performance in the heel region, surpassing standard requirements. Conversely, the forefoot segment exhibits failure under a 20% load due to defects inherent in the composite manufacturing process. The findings underscore the potential of the proposed concept as a promising alternative in lower limb prosthetics, offering both customization and affordability.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"32 2","pages":"543 - 573"},"PeriodicalIF":2.3,"publicationDate":"2024-10-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143778055","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
期刊
Applied Composite Materials
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1