The hygrothermal aging of vinylester resin and its carbon fiber fabric-reinforced composite structures is examined here, focusing on moisture absorption and the consequent degradation of mechanical properties. Specifically, resin casting and CFRP (carbon fiber reinforced polymer) specimens were prepared and immersed into the deionized water and artificial seawater, respectively, at a temperature of 70 °C. Regular weight measurements were taken, accompanied by surface morphology observations using scanning electron microscopy (SEM) and identification of variations in functional groups through Fourier-transform infrared (FTIR) spectroscopy. Meanwhile, the mechanical properties of resin and CFRP were periodically checked. The gravimetric analysis results indicate that resin immersed in deionized water exhibits non-Fickian diffusion due to strong hydrolysis, while CFRP obeys approximately Fickian diffusion because of the embedded carbon fiber inhibiting the hydrolysis. The examination of mechanical properties for CFRP reveals that moisture absorption significantly influences interlaminar shear strength, resulting in a maximum reduction of 13.5%.
{"title":"Hygrothermal Behavior of Carbon Fiber Fabric Reinforced Vinylester Resin Composite Structures","authors":"Jincheng Gao, Xu Li, Jianhui Wei, Yuheng Zhang, Jihui Wang, Anxin Ding","doi":"10.1007/s10443-024-10216-1","DOIUrl":"https://doi.org/10.1007/s10443-024-10216-1","url":null,"abstract":"<p>The hygrothermal aging of vinylester resin and its carbon fiber fabric-reinforced composite structures is examined here, focusing on moisture absorption and the consequent degradation of mechanical properties. Specifically, resin casting and CFRP (carbon fiber reinforced polymer) specimens were prepared and immersed into the deionized water and artificial seawater, respectively, at a temperature of 70 °C. Regular weight measurements were taken, accompanied by surface morphology observations using scanning electron microscopy (SEM) and identification of variations in functional groups through Fourier-transform infrared (FTIR) spectroscopy. Meanwhile, the mechanical properties of resin and CFRP were periodically checked. The gravimetric analysis results indicate that resin immersed in deionized water exhibits non-Fickian diffusion due to strong hydrolysis, while CFRP obeys approximately Fickian diffusion because of the embedded carbon fiber inhibiting the hydrolysis. The examination of mechanical properties for CFRP reveals that moisture absorption significantly influences interlaminar shear strength, resulting in a maximum reduction of 13.5%.</p>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"131 1","pages":""},"PeriodicalIF":2.3,"publicationDate":"2024-03-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140128909","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-09DOI: 10.1007/s10443-024-10217-0
Abstract
The effects of service temperatures on the mechanical properties of self-piercing riveting (SPR) joints of carbon fiber reinforced polymer (CFRP) sheets and AA5754 aluminum alloy sheets were investigated in this study. Three different thicknesses of 0°/90° lay-up sequences of CFRP sheets and aluminum alloy sheets were selected for the SPR joints, and these three joints were subjected to static tensile tests at four different temperatures of 25 °C, 50 °C, 80 °C and 125 °C. A noncontact strain measurement DIC-3D system was used to record changes in the strain field and scanning electron microscopy (SEM) was used to observe the failure area at the rivet hole of the CFRP sheet to study the damage forms and mechanisms of the joints. The results of the tests showed an average reduction of 35.4% in maximum load and an average degradation of 21.9% in energy absorption for the three joints at 125 °C compared to room temperature conditions.
{"title":"Effects of Service Temperature on the Mechanical Properties of CFRP/Aluminum Alloy Self-Piercing Riveting Joints","authors":"","doi":"10.1007/s10443-024-10217-0","DOIUrl":"https://doi.org/10.1007/s10443-024-10217-0","url":null,"abstract":"<h3>Abstract</h3> <p>The effects of service temperatures on the mechanical properties of self-piercing riveting (SPR) joints of carbon fiber reinforced polymer (CFRP) sheets and AA5754 aluminum alloy sheets were investigated in this study. Three different thicknesses of 0°/90° lay-up sequences of CFRP sheets and aluminum alloy sheets were selected for the SPR joints, and these three joints were subjected to static tensile tests at four different temperatures of 25 °C, 50 °C, 80 °C and 125 °C. A noncontact strain measurement DIC-3D system was used to record changes in the strain field and scanning electron microscopy (SEM) was used to observe the failure area at the rivet hole of the CFRP sheet to study the damage forms and mechanisms of the joints. The results of the tests showed an average reduction of 35.4% in maximum load and an average degradation of 21.9% in energy absorption for the three joints at 125 °C compared to room temperature conditions.</p>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"133 1","pages":""},"PeriodicalIF":2.3,"publicationDate":"2024-03-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140098704","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-09DOI: 10.1007/s10443-024-10213-4
G. Romano, Y. N. Rao, C. Liu, K. B. Katnam, Z. Zou, P. Potluri
This paper investigates the effect of intra-laminar fibre hybridisation, i.e., primary and secondary fibres within a matrix, on the homogenised properties and micro-stress fields in uni-directional polymer composite laminae. The study is focused on S-glass/epoxy laminae which are hybridised with secondary fibres (e.g., polypropylene). Two-dimensional repeating unit cells (2D RUCs) with periodic microstructures are developed to conduct the micro-mechanical analyses under transverse tensile and transverse shear loading conditions. Uni-directional fibre-hybrid S-glass/epoxy laminae with different secondary fibres are studied by varying (a) the periodic microstructure and (b) the material properties of the constituent fibres to assess the effect of such geometric and material variations on the homogenised elastic lamina properties and intra-lamina micro-stress fields. The results show that intra-laminar fibre hybridisation significantly affects the elastic lamina properties and micro-stress fields. Notably, the presence of the secondary fibres significantly increases or reduces the stress fields in the matrix and at the fibre-matrix interfaces (i.e. normal and shears stress components)–depending on the microstructure and the stiffness of the secondary fibres–which could be explored to manipulate the damage modes and thus energy dissipation mechanisms.
本文研究了层内纤维杂化(即基体中的一次纤维和二次纤维)对单向聚合物复合材料层板的均匀特性和微应力场的影响。研究重点是与次生纤维(如聚丙烯)杂化的 S 玻璃/环氧层压板。开发了具有周期性微结构的二维重复单元格(2D RUC),用于在横向拉伸和横向剪切加载条件下进行微观力学分析。通过改变(a)周期性微结构和(b)组成纤维的材料属性,研究了具有不同次级纤维的单向纤维混合 S 玻璃/环氧层压板,以评估这些几何和材料变化对均质化弹性层压板属性和层内微应力场的影响。结果表明,层内纤维杂化对弹性层特性和微应力场有显著影响。值得注意的是,次生纤维的存在会显著增加或减少基体内和纤维-基体界面上的应力场(即法向应力和剪切应力成分)--这取决于次生纤维的微观结构和刚度--这可用于控制破坏模式,从而改变能量耗散机制。
{"title":"On the Micro-Stress Fields in Fibre-Hybrid Polymer Composite Laminae with Periodic Microstructure Under Transverse Tension and Transverse Shear Loading","authors":"G. Romano, Y. N. Rao, C. Liu, K. B. Katnam, Z. Zou, P. Potluri","doi":"10.1007/s10443-024-10213-4","DOIUrl":"10.1007/s10443-024-10213-4","url":null,"abstract":"<div><p>This paper investigates the effect of intra-laminar fibre hybridisation, <i>i.e.,</i> primary and secondary fibres within a matrix, on the homogenised properties and micro-stress fields in uni-directional polymer composite laminae. The study is focused on S-glass/epoxy laminae which are hybridised with secondary fibres (<i>e.g.,</i> polypropylene). Two-dimensional repeating unit cells (2D RUCs) with periodic microstructures are developed to conduct the micro-mechanical analyses under transverse tensile and transverse shear loading conditions. Uni-directional fibre-hybrid S-glass/epoxy laminae with different secondary fibres are studied by varying (a) the periodic microstructure and (b) the material properties of the constituent fibres to assess the effect of such geometric and material variations on the homogenised elastic lamina properties and intra-lamina micro-stress fields. The results show that intra-laminar fibre hybridisation significantly affects the elastic lamina properties and micro-stress fields. Notably, the presence of the secondary fibres significantly increases or reduces the stress fields in the matrix and at the fibre-matrix interfaces (i.e. normal and shears stress components)–depending on the microstructure and the stiffness of the secondary fibres–which could be explored to manipulate the damage modes and thus energy dissipation mechanisms. </p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"31 6","pages":"1967 - 1989"},"PeriodicalIF":2.3,"publicationDate":"2024-03-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s10443-024-10213-4.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140098700","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-06DOI: 10.1007/s10443-024-10214-3
Xuda Qin, Gongbo Feng, Xianming Meng, Sai Zhang, Shipeng Li, Hao Li
In this paper, the effects of interference-fit sizes and service environment temperature on the preload and relaxation of CFRP bolted joints are investigated based on an ultrasonic monitoring method. Specimens of different interference-fit sizes were subjected to insertion, preloading and preloading force monitoring for up to 200 h. To describe the preloading relaxation response of CFRP bolted joints, a comprehensive relaxation mechanics model is proposed. Experimental results demonstrate that this model accurately describe the variations in bolted preloading force under interference-fit conditions and thermal-oxygen environments. During the preloading process, a portion the axial force in interference-fit bolted joints is dissipated by interfacial frictional force and the magnitude of the frictional force is influenced by the interference-fit sizes. The interference-fit will lead to a tightly coupled interface, causing interface friction between the bolt-shank and the joint-holes, which can lead to a weakening transformation ability from tightening torque to axial force. Compared to clearance-fit condition, interference-fit can suppress the preloading relaxation effect of CFRP bolted joints to a certain extent. With an increase in interference-fit percentage (from 0% to 1.2%), the preloading relaxation coefficient rises from 94.4% to 95.7%. The additional interfacial friction effectively suppresses the creep deformation of composites. However, with an increase in the service temperature, the relaxation behavior of preloading forces in CFRP bolted joint significantly intensifies. As the environmental temperature rises from 25 ℃ to 150 ℃, the preloading relaxation coefficient decreases from 95.0% to 79.8%. High-temperature environments can lead changes in the material properties of composite and interface friction characteristics, even potentially leading to damage.
{"title":"The Investigation of Preload Relaxation Behavior of CFRP Bolted Joints Under Thermal-Oxygen Environment: Modeling and Experiments","authors":"Xuda Qin, Gongbo Feng, Xianming Meng, Sai Zhang, Shipeng Li, Hao Li","doi":"10.1007/s10443-024-10214-3","DOIUrl":"10.1007/s10443-024-10214-3","url":null,"abstract":"<div><p>In this paper, the effects of interference-fit sizes and service environment temperature on the preload and relaxation of CFRP bolted joints are investigated based on an ultrasonic monitoring method. Specimens of different interference-fit sizes were subjected to insertion, preloading and preloading force monitoring for up to 200 h. To describe the preloading relaxation response of CFRP bolted joints, a comprehensive relaxation mechanics model is proposed. Experimental results demonstrate that this model accurately describe the variations in bolted preloading force under interference-fit conditions and thermal-oxygen environments. During the preloading process, a portion the axial force in interference-fit bolted joints is dissipated by interfacial frictional force and the magnitude of the frictional force is influenced by the interference-fit sizes. The interference-fit will lead to a tightly coupled interface, causing interface friction between the bolt-shank and the joint-holes, which can lead to a weakening transformation ability from tightening torque to axial force. Compared to clearance-fit condition, interference-fit can suppress the preloading relaxation effect of CFRP bolted joints to a certain extent. With an increase in interference-fit percentage (from 0% to 1.2%), the preloading relaxation coefficient rises from 94.4% to 95.7%. The additional interfacial friction effectively suppresses the creep deformation of composites. However, with an increase in the service temperature, the relaxation behavior of preloading forces in CFRP bolted joint significantly intensifies. As the environmental temperature rises from 25 ℃ to 150 ℃, the preloading relaxation coefficient decreases from 95.0% to 79.8%. High-temperature environments can lead changes in the material properties of composite and interface friction characteristics, even potentially leading to damage.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"31 4","pages":"1323 - 1342"},"PeriodicalIF":2.3,"publicationDate":"2024-03-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140057390","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Internal delamination damage in carbon fibre reinforced polymer (CFRP) composites occurs easily after a fastener is installed. To determine the internal delamination damage in CFRPs with a fastener under lightning strike conditions, an experiment was conducted with different lightning channel gaps, fastener diameters, and fitting conditions. On the basis of the experimental findings and the results of a coupled thermal–electrical simulation model, a circuit model for CFRPs with a fastener was established to explore the current path, delamination properties and internal damage in CFRP specimens. The factors influencing the correlations between the generation and development of internal delamination damage under multiple conditions were proposed to clarify the lightning damage mechanism of the CFRP composites. The results indicated that internal delamination damage was mainly caused by resin pyrolysis and pyrolysis gas expansion; in addition, the thermal–electrical coupling effect of the contact interface had a significant impact on the internal delamination damage. For example, at approximately 50 kA, the damage area of the specimen with a 6 mm diameter fastener was 28.5% smaller than that of the specimen with a 4 mm diameter fastener. This work provides a basis for understanding the propagation of delamination in CFRP composites with a fastener and for reducing the delamination damage under lightning strike environment.
安装紧固件后,碳纤维增强聚合物(CFRP)复合材料很容易发生内部分层损坏。为了确定带紧固件的 CFRP 在雷击条件下的内部分层损坏情况,实验采用了不同的雷击通道间隙、紧固件直径和安装条件。在实验结果和热电耦合模拟模型结果的基础上,建立了带紧固件的 CFRP 电路模型,以探索 CFRP 试样的电流路径、分层特性和内部损伤。提出了多种条件下内部分层损伤产生和发展的相关影响因素,以阐明 CFRP 复合材料的雷击损伤机理。结果表明,内部分层损伤主要由树脂热解和热解气体膨胀引起;此外,接触界面的热电耦合效应对内部分层损伤也有显著影响。例如,在大约 50 kA 的电流下,直径为 6 mm 的紧固件试样的损坏面积比直径为 4 mm 的紧固件试样的损坏面积小 28.5%。这项研究为了解带有紧固件的 CFRP 复合材料的分层扩展以及减少雷击环境下的分层损坏提供了依据。
{"title":"Assessment of Delamination Damage in Carbon Fibre Reinforced Polymer Composites with a Fastener Under Multiple Lightning Strike Conditions","authors":"Xiangyu Tian, Jinru Sun, Wei Sun, Xueling Yao, Xianchao Xu, Shu Li, Jingliang Chen","doi":"10.1007/s10443-024-10212-5","DOIUrl":"10.1007/s10443-024-10212-5","url":null,"abstract":"<div><p>Internal delamination damage in carbon fibre reinforced polymer (CFRP) composites occurs easily after a fastener is installed. To determine the internal delamination damage in CFRPs with a fastener under lightning strike conditions, an experiment was conducted with different lightning channel gaps, fastener diameters, and fitting conditions. On the basis of the experimental findings and the results of a coupled thermal–electrical simulation model, a circuit model for CFRPs with a fastener was established to explore the current path, delamination properties and internal damage in CFRP specimens. The factors influencing the correlations between the generation and development of internal delamination damage under multiple conditions were proposed to clarify the lightning damage mechanism of the CFRP composites. The results indicated that internal delamination damage was mainly caused by resin pyrolysis and pyrolysis gas expansion; in addition, the thermal–electrical coupling effect of the contact interface had a significant impact on the internal delamination damage. For example, at approximately 50 kA, the damage area of the specimen with a 6 mm diameter fastener was 28.5% smaller than that of the specimen with a 4 mm diameter fastener. This work provides a basis for understanding the propagation of delamination in CFRP composites with a fastener and for reducing the delamination damage under lightning strike environment.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"31 4","pages":"1155 - 1172"},"PeriodicalIF":2.3,"publicationDate":"2024-03-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140034012","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-04DOI: 10.1007/s10443-024-10211-6
Ming Cai, Jiwei Liu, Xian Zhang, Qihua Ma, Dazhong Wang, Geoffrey I. N. Waterhouse, Baozhong Sun
Hybrid composites containing carbon fibers and ramie fibers in an epoxy polymer matrix were prepared (denoted as CRFRP), after which the composites were immersed in distilled water at three different temperatures (20, 40, and 60 °C) for a period up to 2 months. Water absorption tests and static (tensile and flexural) and dynamic (low-velocity impact) mechanical tests were then conducted on the hygrothermally-treated composites to explore their hydrothermal aging mechanism. Results show that water uptake by CRFRP composites was enhanced by increasing the hygrothermal treatment temperature or aging time, with the water uptake obeying a Fickian diffusion model. Hygrothermal aging decreased the tensile strength, tensile modulus, flexural strength and flexural modulus of the CRFRP composites, though enhanced the impact absorption energy since the ramie fibers had greater plasticity and deformability after aging. Based on the experimental findings, a plausible mechanism was developed for the hydrothermal aging of the hybrid composites. Importantly, CRFRP composites were lighter than carbon fiber-reinforced composites (CFRP), whilst offering similar all-round performance, suggesting CRFRP composites may be useful in applications where CFRP composites have traditionally been used.
{"title":"Mechanical Stability of Carbon/Ramie Fiber Hybrid Composites Under Hygrothermal Aging","authors":"Ming Cai, Jiwei Liu, Xian Zhang, Qihua Ma, Dazhong Wang, Geoffrey I. N. Waterhouse, Baozhong Sun","doi":"10.1007/s10443-024-10211-6","DOIUrl":"https://doi.org/10.1007/s10443-024-10211-6","url":null,"abstract":"<p>Hybrid composites containing carbon fibers and ramie fibers in an epoxy polymer matrix were prepared (denoted as CRFRP), after which the composites were immersed in distilled water at three different temperatures (20, 40, and 60 °C) for a period up to 2 months. Water absorption tests and static (tensile and flexural) and dynamic (low-velocity impact) mechanical tests were then conducted on the hygrothermally-treated composites to explore their hydrothermal aging mechanism. Results show that water uptake by CRFRP composites was enhanced by increasing the hygrothermal treatment temperature or aging time, with the water uptake obeying a Fickian diffusion model. Hygrothermal aging decreased the tensile strength, tensile modulus, flexural strength and flexural modulus of the CRFRP composites, though enhanced the impact absorption energy since the ramie fibers had greater plasticity and deformability after aging. Based on the experimental findings, a plausible mechanism was developed for the hydrothermal aging of the hybrid composites. Importantly, CRFRP composites were lighter than carbon fiber-reinforced composites (CFRP), whilst offering similar all-round performance, suggesting CRFRP composites may be useful in applications where CFRP composites have traditionally been used. </p>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"80 1","pages":""},"PeriodicalIF":2.3,"publicationDate":"2024-03-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140034104","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
The primary objective of this study is to conduct a comprehensive experimental investigation into the impact of yarn reduction on the damage mechanisms and progression of 3D woven composites under bending loads, utilizing a combination of micro-XCT and digital image correlation (DIC) techniques. Typical bending behaviors of 3D woven composites have been discussed through load–displacement curves combining camera photography techniques. The influence of yarn reduction on strain distribution during bending deformation can be obtained by utilizing DIC techniques. Additionally, the final failure mode analysis of three-dimensional woven composite materials was conducted using micro-XCT techniques.
{"title":"Research on the Influence of Yarn Reduction on the Bending Performance of Three-dimensional Woven Composites","authors":"Chao Li, Haili Zhou, Yang Sun, Fangfang Sun, Zhiyan Liu, Jian Huang, Liquan Zhang, Chengming Yue, Qian Zhao, Shoufu Yu, Guangming Zhou","doi":"10.1007/s10443-024-10206-3","DOIUrl":"10.1007/s10443-024-10206-3","url":null,"abstract":"<div><p>The primary objective of this study is to conduct a comprehensive experimental investigation into the impact of yarn reduction on the damage mechanisms and progression of 3D woven composites under bending loads, utilizing a combination of micro-XCT and digital image correlation (DIC) techniques. Typical bending behaviors of 3D woven composites have been discussed through load–displacement curves combining camera photography techniques. The influence of yarn reduction on strain distribution during bending deformation can be obtained by utilizing DIC techniques. Additionally, the final failure mode analysis of three-dimensional woven composite materials was conducted using micro-XCT techniques.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"31 3","pages":"1069 - 1082"},"PeriodicalIF":2.3,"publicationDate":"2024-02-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140001903","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-02-29DOI: 10.1007/s10443-024-10209-0
Massinissa Grabi, Ahmed Chellil, Samir Lecheb, Hocine Grabi, Abdelkader Nour
Luffa cylindrical (LC) has an exceptionally multipartite architecture, a hierarchical and light structure, and a low density. Such a structure is potentially suitable to replace conventional porous-type composites for low-energy absorption and material reinforcement applications. This paper presents an experimental study of the impact behavior of four different luffa/epoxy composites, named (A), (B), (C), and (D) subjected to low-velocity impact (LVI) at energies ranging from barely visible impact damage (BVID) to perforation (5,15, and 20J). Acoustic emission (AE), scanning electron microscopy (SEM), and digital image correlation (DIC) were introduced to the indentation test to offer additional information on damage mechanisms and on strain and displacement fields since the LVI test has a short duration and real-time damage monitoring is not always achievable. The results showed that the values of the peak force of laminates (A), (B), and (D) are relatively lower compared to laminates (C). In the case of perforation impact energy (20J), the Coefficients of Restitution (CoR) of composites (A), (B), and (D) are equal to 0, which indicates that the nature of the impact is completely plastic, except for composite (C) had a value of 0.11, and a lower degree of damage at all impact energies. Composites (C) exhibit the highest impact resistance, followed by composites (A), while composites (D) display the highest energy absorption, followed by composites (B). Multivariable statistical analysis of the AE signals identified four classes of damage: matrix cracking, fiber-matrix debonding, delamination, and fiber breakage. The damage modes found by AE are well presented and proven by SEM analysis. The luffa fiber-reinforced composite has better impact properties than other natural fiber-reinforced composites.
{"title":"Impact Behavior Analysis of Luffa/Epoxy Composites Under Low-Velocity Loading","authors":"Massinissa Grabi, Ahmed Chellil, Samir Lecheb, Hocine Grabi, Abdelkader Nour","doi":"10.1007/s10443-024-10209-0","DOIUrl":"https://doi.org/10.1007/s10443-024-10209-0","url":null,"abstract":"<p>Luffa cylindrical (LC) has an exceptionally multipartite architecture, a hierarchical and light structure, and a low density. Such a structure is potentially suitable to replace conventional porous-type composites for low-energy absorption and material reinforcement applications. This paper presents an experimental study of the impact behavior of four different luffa/epoxy composites, named (A), (B), (C), and (D) subjected to low-velocity impact (LVI) at energies ranging from barely visible impact damage (BVID) to perforation (5,15, and 20J). Acoustic emission (AE), scanning electron microscopy (SEM), and digital image correlation (DIC) were introduced to the indentation test to offer additional information on damage mechanisms and on strain and displacement fields since the LVI test has a short duration and real-time damage monitoring is not always achievable. The results showed that the values of the peak force of laminates (A), (B), and (D) are relatively lower compared to laminates (C). In the case of perforation impact energy (20J), the Coefficients of Restitution (CoR) of composites (A), (B), and (D) are equal to 0, which indicates that the nature of the impact is completely plastic, except for composite (C) had a value of 0.11, and a lower degree of damage at all impact energies. Composites (C) exhibit the highest impact resistance, followed by composites (A), while composites (D) display the highest energy absorption, followed by composites (B). Multivariable statistical analysis of the AE signals identified four classes of damage: matrix cracking, fiber-matrix debonding, delamination, and fiber breakage. The damage modes found by AE are well presented and proven by SEM analysis. The luffa fiber-reinforced composite has better impact properties than other natural fiber-reinforced composites.</p>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"27 1","pages":""},"PeriodicalIF":2.3,"publicationDate":"2024-02-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140002093","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
A novel 3D printing method for continuous carbon fiber-reinforced thermosetting epoxy resin composites (CCFRTC) was proposed, including CCFRTC prepreg filament manufacturing, secondary impregnation, printing and curing stages. Through the addition of an impregnation stage before printing, this method ensures a close interface bond and uniform distribution of fibers and resin. After testing, the average tensile strength and tensile modulus of the uncured pre-impregnated continuous filaments were found to be 968 MPa and 58.6 GPa, respectively. Mechanical testing of the specimens revealed that the maximum tensile strength and flexural strength of the CCFRTC specimens reached 825 MPa and 557 MPa, with tensile and flexural modulus measuring 157 GPa and 185 GPa. Furthermore, scanning electron microscopy (SEM) examination of the cross-sections indicated a highly uniform impregnation of both the filaments and printed specimens. In conclusion, the method proposed in this study enables the preparation and printing of continuous fiber-reinforced thermosetting resin composite materials, addressing the issues of inadequate impregnation and poor interfacial bonding performance in continuous carbon fiber-reinforced thermosetting resin composite materials. These findings may broaden the potential applications of 3D printing CCFRTC in the aerospace, defense, and automotive industries.