Pub Date : 2025-11-25DOI: 10.1007/s10443-025-10402-9
Tanner C. Garrett, Quentin S. Allen, Andrew R. George
Carbon fiber reinforced parts are utilized by the transportation industry due to being strong yet lightweight. The highest quality parts are made using carbon fiber (CF) pre-impregnated with resin processed in an autoclave to reduce void content. The autoclave process is expensive and takes up a large amount of space, so resin transfer molding (RTM), a form of liquid composite molding (LCM), is a less expensive alternative. The parts produced using RTM can be manufactured to rival the mechanical performance of parts made with pre-preg in an autoclave, but concerns remain over voids. Most research pertaining to void formation has been done ex-situ by either micro-CT or ultrasound, but valuable information can be obtained by monitoring void formation in-situ using a UV-sensitive dye mixed with resin. The objective of this research is to validate in-situ void formation observation methods for more complex fiber reinforcements beyond unidirectional. While previous work has established the validity of such observation for unidirectional fiber samples, this research focuses on preformed ply stacks alternating between 0 and 90 degrees.
{"title":"In-Situ Void Formation During Liquid Composite Molding for Preformed Warp, Weft, and Alternating Orientation RTM Samples","authors":"Tanner C. Garrett, Quentin S. Allen, Andrew R. George","doi":"10.1007/s10443-025-10402-9","DOIUrl":"10.1007/s10443-025-10402-9","url":null,"abstract":"<div><p>Carbon fiber reinforced parts are utilized by the transportation industry due to being strong yet lightweight. The highest quality parts are made using carbon fiber (CF) pre-impregnated with resin processed in an autoclave to reduce void content. The autoclave process is expensive and takes up a large amount of space, so resin transfer molding (RTM), a form of liquid composite molding (LCM), is a less expensive alternative. The parts produced using RTM can be manufactured to rival the mechanical performance of parts made with pre-preg in an autoclave, but concerns remain over voids. Most research pertaining to void formation has been done <i>ex-situ</i> by either micro-CT or ultrasound, but valuable information can be obtained by monitoring void formation in-situ using a UV-sensitive dye mixed with resin. The objective of this research is to validate in-situ void formation observation methods for more complex fiber reinforcements beyond unidirectional. While previous work has established the validity of such observation for unidirectional fiber samples, this research focuses on preformed ply stacks alternating between 0 and 90 degrees.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"33 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-11-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145612397","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2025-11-25DOI: 10.1007/s10443-025-10401-w
A. S. Ibrahim Mamane, S. Giljean, B. Gachet, C. François, G. L’Hostis, M.-J. Pac
The incremental hole drilling method is widely used to determine residual stresses in materials. For fiber-reinforced composites, the drilling-induced heat can create measurement errors that are not taken into account in the calculations. Even if the drilling parameters (cutting and feed speeds, type of cutter, etc.) are optimized to provide correct machining results and more reliable residual stress measurement, thermal effects remain relatively poorly understood and analyzed for fiber-reinforced composites. The purpose of this work is to investigate the effects of drilling-induced heat on the local chemical properties of unidirectional carbon/epoxy laminates that have undergone different curing cycles and to discuss the consequences on residual stresses. First, the thermal field generated by drilling was characterized using an infra-red camera. The measurements showed that relatively high temperatures were reached depending on the increment depth. Then, Modulated Differential Scanning Calorimetry before and after drilling were performed to investigate the effects of the produced heat on the chemical properties. The results showed a local increase in the degree of cure and the glass transition temperature (Tg) of the matrix. It is assumed that these mechanisms are responsible for the apparent residual stresses obtained when large increment depths are used during the process. The main conclusion of this study is that the heat generated during the drilling step of the incremental hole drilling method causes a progression of the cure reaction in the vicinity of the hole, leading to Tg-dependent residual stresses which are higher for low-Tg composites.
{"title":"Measurement of Residual Stresses in Fiber-Reinforced Composites by the Incremental Hole Drilling Method: Effect of the Drilling-Induced Heating","authors":"A. S. Ibrahim Mamane, S. Giljean, B. Gachet, C. François, G. L’Hostis, M.-J. Pac","doi":"10.1007/s10443-025-10401-w","DOIUrl":"10.1007/s10443-025-10401-w","url":null,"abstract":"<div><p>The incremental hole drilling method is widely used to determine residual stresses in materials. For fiber-reinforced composites, the drilling-induced heat can create measurement errors that are not taken into account in the calculations. Even if the drilling parameters (cutting and feed speeds, type of cutter, etc.) are optimized to provide correct machining results and more reliable residual stress measurement, thermal effects remain relatively poorly understood and analyzed for fiber-reinforced composites. The purpose of this work is to investigate the effects of drilling-induced heat on the local chemical properties of unidirectional carbon/epoxy laminates that have undergone different curing cycles and to discuss the consequences on residual stresses. First, the thermal field generated by drilling was characterized using an infra-red camera. The measurements showed that relatively high temperatures were reached depending on the increment depth. Then, Modulated Differential Scanning Calorimetry before and after drilling were performed to investigate the effects of the produced heat on the chemical properties. The results showed a local increase in the degree of cure and the glass transition temperature (Tg) of the matrix. It is assumed that these mechanisms are responsible for the apparent residual stresses obtained when large increment depths are used during the process. The main conclusion of this study is that the heat generated during the drilling step of the incremental hole drilling method causes a progression of the cure reaction in the vicinity of the hole, leading to Tg-dependent residual stresses which are higher for low-Tg composites.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"33 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-11-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145612337","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}