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Electrospinning of smart nanofibers based on PVP/PDA for wound dressing applications 基于PVP/PDA的智能纳米纤维静电纺丝在伤口敷料中的应用
4区 工程技术 Q2 Agricultural and Biological Sciences Pub Date : 2023-10-16 DOI: 10.1080/00405000.2023.2268828
Faezeh Bahrami, Niloofar Eslahi, Reza Jahanmardi
AbstractIn the present study, electrospinning of polyvinylpyrrolidone (PVP) and polydiacetylene (PDA) with pomegranate peel (PG) extract was investigated for the preparation of smart and antibacterial nanofibers. Briefly, PDA-PVP solutions were firstly prepared at two different ratios and electrospun under different conditions. Based on the SEM results, the 1:3 ratio of PDA:PVP nanofibers, with an average fiber diameter of 130 ± 40 nm, electrospun at a voltage of 15 kV, feeding rate of 0.5 ml/h and collector distance of 15 cm was selected as the optimal conditions. The addition of PG resulted in an increase in the diameter of the fibers. The color of the electrospun fibers was altered from blue to red due to changes in either temperature or pH or exposure to different solvents. The antibacterial test showed high antimicrobial activity of the fibers loaded with PG extract against both S. aureus and E. coli. MTT assay and cell attachment also validated the biocompatibility of the fabricated nanofibers. Thus, the prepared smart PG-loaded nanofibers had a high potential to be used in wound dressing applications.Keywords: Polydiacetylenepolyvinylpyrrolidonepomegranate peel extractelectrospun nanofiberswound dressing Disclosure statementNo potential conflict of interest was reported by the author(s).
摘要本研究以石榴皮(PG)提取物为原料,对聚乙烯吡咯烷酮(PVP)和聚二乙炔(PDA)静电纺丝制备智能抗菌纳米纤维进行了研究。简单地说,首先以两种不同的比例制备了PDA-PVP溶液,并在不同的条件下进行了静电纺丝。基于SEM结果,选择了PDA:PVP纳米纤维的比例为1:3,平均纤维直径为130±40 nm,电纺丝电压为15 kV,加料速度为0.5 ml/h,集电极距离为15 cm的最佳条件。PG的加入使纤维直径增大。由于温度或pH值或暴露于不同溶剂的变化,静电纺纤维的颜色从蓝色变为红色。抑菌试验表明,负载PG提取物的纤维对金黄色葡萄球菌和大肠杆菌均有较高的抑菌活性。MTT实验和细胞贴壁也验证了制备的纳米纤维的生物相容性。因此,所制备的智能聚乙二醇负载纳米纤维在伤口敷料中具有很高的应用潜力。关键词:聚二乙炔聚乙烯吡咯烷酯石榴皮提取物电纺纳米纤维超声敷料披露声明作者未报告潜在利益冲突。
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引用次数: 0
Prediction of the lifespan of C-9 parachute canopy using scale-down approach and mathematical modeling C-9降落伞伞盖的缩比方法和数学模型寿命预测
4区 工程技术 Q2 Agricultural and Biological Sciences Pub Date : 2023-10-14 DOI: 10.1080/00405000.2023.2266949
Gyana Ranjan Behera, Arunangshu Mukhopadhyay, Monica Sikka
AbstractLife prediction of the parachute canopy is an important consideration before multiple parachute jumps which can prevent unnecessary catastrophic scenarios for skydivers. The present research emphasized the prediction of the life as well as the reliability of the C-9 parachute canopy using a scale-down approach and mathematical modeling. In the research, a rectangular form of small stitched specimens was prepared from ripstop and plain-woven parachute canopy fabric where the seam angle was kept at 45°. Initially, the specimens were subjected to 5, 10, 15, 20, and 25 cycles of tensile impact force considering the critical situation of the C-9 parachute, and subsequently strength loss data was noted. In the results, it was found that, unlike plain-woven, the ripstop fabric specimen increased in strength and work of rupture up to 10 impact load cycles before dropping. Meanwhile, the breaking elongation decreases for both fabric specimens with the impact load cycles. Furthermore, the strength-loss data was extrapolated to assess the life of specimen and thereafter Weibull distribution was used determine the reliability of the specimen. Reliability results indicate that the plain-woven fabric is less reliable, has a faster rate of degradation, and will have a shorter service life than the ripstop fabric. The research revealed that the life of the parachute canopy is expected to be two times more in ripstop than in plain-woven fabric and hence the ripstop canopies may be preferred over plain-woven fabric for long-run applications.Keywords: Parachute canopytensile impact loadwork of rupturedegradationWeibull distribution Disclosure statementNo potential conflict of interest was reported by the authors.
摘要伞篷寿命预测是多次跳伞前需要考虑的重要问题,可以防止跳伞者发生不必要的灾难。本研究着重利用缩尺方法和数学模型对C-9降落伞伞篷的寿命和可靠性进行预测。在本研究中,以防撕裂平编伞盖织物为材料,在接缝角为45°的情况下,制备了矩形的小缝样。首先,考虑C-9降落伞的临界情况,对试件进行了5、10、15、20和25次循环的拉伸冲击,并记录了随后的强度损失数据。结果发现,与平纹织物不同,止裂织物试样在下降前的10次冲击载荷循环中强度和断裂功都有所增加。同时,两种织物试样的断裂伸长率随冲击载荷循环次数的增加而减小。此外,外推强度损失数据来评估试样的寿命,然后使用威布尔分布来确定试样的可靠性。可靠性结果表明,与防撕裂织物相比,平纹织物可靠性差,降解速度快,使用寿命短。研究表明,防撕裂伞的使用寿命是平纹织物的两倍,因此,在长期应用中,防撕裂伞可能比平纹织物更受欢迎。关键词:伞盖拉伸冲击载荷破裂退化威布尔分布披露声明作者未报告潜在利益冲突。
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引用次数: 0
Development and performance analysis of flame-retardant polylactic acid elastic bands for thermal protective clothing 热防护服用阻燃聚乳酸松紧带的研制及性能分析
4区 工程技术 Q2 Agricultural and Biological Sciences Pub Date : 2023-10-14 DOI: 10.1080/00405000.2023.2265628
Junwu Chen, Yuzheng Lu, Fengxin Sun
AbstractThe burning and melting of elastic fastening bands in high-temperature environments are major contributors to empyrosis and ambustion owing to their snug fit to human body parts in practical usage. Conventionally fabricated fastening bands show poor degradation, negative environmental impact, and poor flame-retardant performance. Herein, we report an ecofriendly cyclic phosphate ester-based flame-retardant polylactic acid (PLA) elastic band prepared using an impregnation-baking process, and experimental investigation was conducted on the optimized finishing process. The band was characterized using scanning electron microscopy, energy-dispersive spectroscopy, and thermogravimetry. The band exhibited a damage length of 3.9 cm after vertical combustion and self-extinguishing effect after being removed from the fire source without generating molten droplets. The cross-linking phenomenon between the modified PLA fibers was beneficial in improving the flame retardancy of the PLA elastic band in the condensed phase. The strength loss of the band was <5%. Thus, the prepared band can be widely used in real-world applications.Keywords: Antidrippingbakingblast dryercross-linkinggraphitizationorganophosphorus Disclosure statementThe authors report there are no competing interests to declare.Additional informationFundingThis work was supported by the National Key Research and Development Program of China under Grant number 2019YFA0706900 and Jiangsu Provincial Policy Guidance Programme-International Cooperation Projects under Grant number BZ2020010.
摘要:弹性扣带在实际使用中由于与人体部位贴合较紧,在高温环境中极易发生燃烧、熔化等现象,是造成烧伤和伏击的主要原因。传统制造的紧固带具有较差的降解性、对环境的负面影响和较差的阻燃性能。本文报道了采用浸渍-烘烤法制备环保型环磷酸酯基阻燃聚乳酸(PLA)弹性带,并对优化后的整理工艺进行了实验研究。利用扫描电子显微镜、能量色散光谱和热重法对其进行了表征。垂直燃烧后条带损伤长度为3.9 cm,离开火源后条带具有自熄作用,且不产生熔滴。改性PLA纤维之间的交联现象有利于提高PLA弹性带在缩合相的阻燃性。带强度损失<5%。因此,制备的带可以广泛应用于实际应用中。关键词:防滴漏;烘培;鼓风干燥机;交联;本研究得到国家重点研发计划项目(资助号:2019YFA0706900)和江苏省政策指导计划国际合作项目(资助号:BZ2020010)的支持。
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引用次数: 0
Enhanced dyeing properties of gardenia yellow on cotton with siloxane-based medium 硅氧烷增强栀子黄在棉花上的染色性能
4区 工程技术 Q2 Agricultural and Biological Sciences Pub Date : 2023-10-14 DOI: 10.1080/00405000.2023.2267353
Jingzhi Li, Chendi Xie, Ling Gao, Huan Qi, Lili Feng, Yiping Qiu, Yangyi Chen
AbstractDecamethyl cyclopentasiloxane (D5) was devoted to the medium in the dyeing process of gardenia yellow on cotton fabric to improve the dyeing properties. The effects of D5 percentages and mordants, dyes dosage as well as dyeing temperature and time on dyeing properties were investigated. The results show that optimal dyeing processes of gardenia yellow on cotton in a siloxane-based medium are as follows: D5 percentages 94%vol, dye dosage 2% (o.w.f), alum as mordant dosage 3% (o.w.f), dyeing temperature 80 °C, dyeing time 40 min. Compared with water dyeing, cotton fabrics dyeing with D5/water present enhanced color strength (K/S value) and fine levelness. By fitting the dyeing curves, it is found that dyeing mechanism of gardenia yellow on cotton in D5 follows a pseudo-second-order kinetics model, which is alike to the dyeing kinetics in water. Owing to the hatred of D5, gardenia yellow is rapidly absorbed on the cotton fiber in initial dyeing process, then diffuses and reacts with cotton, which is drived by the diffusive force inducing by the concentration differences of dyes between dye liquor and fiber. In addition, the color fastness of cotton fabrics dyeing with D5/water is equal to that dyeing with water. This dyeing technique that immensely reduces dyeing wastewater has potential application in natural dyestuffs.Keywords: Gardenia yellowD5dyeing kineticscolor strengthcolor fastness AcknowledgmentsThe authors are grateful for the financial support provided by Fujian External Cooperation project of Natural Science Foundation (No. 2022I0042), Fujian Young and Middle-aged Teachers Education research project (No. JT180376), and Quanzhou City Science & Technology Program of China (No. 2019C014R).Disclosure statementNo potential conflict of interest was reported by the authors.
摘要将十甲基环五硅氧烷(D5)加入到棉织物栀子黄染色过程中,以改善其染色性能。考察了D5用量、媒染剂用量、染色温度和染色时间对染色性能的影响。结果表明,棉织物在硅氧烷基介质上的最佳染色工艺为:D5用量94%vol,染料用量2% (o.w.f),明矾为媒染剂用量3% (o.w.f),染色温度80℃,染色时间40 min。与水染色相比,D5/水染色棉织物的色强(K/S值)和细度均有所提高。通过对染色曲线的拟合,发现栀子黄在D5中对棉花的染色机理符合准二级动力学模型,与在水中的染色动力学相似。由于D5的存在,栀子黄在初始染色过程中迅速吸附在棉纤维上,然后在染料液与纤维之间染料浓度差异所产生的扩散力的驱动下与棉纤维发生扩散反应。此外,棉织物用D5/水染色的色牢度与用水染色的色牢度相等。该染色技术极大地减少了染色废水,在天然染料中具有潜在的应用前景。本文作者感谢福建省自然科学基金对外合作项目(No. 2022I0042)、福建省中青年教师教育研究项目(No. 2022I0042)的资助。JT180376),泉州市科技计划项目(2019C014R)。披露声明作者未报告潜在的利益冲突。
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引用次数: 0
Evaluation on thermal and wet comfort properties of hygroscopic exothermic knitted fabric based on moisture diffused-transmission mechanism 基于水分扩散传递机理的吸湿放热针织物热湿舒适性评价
4区 工程技术 Q2 Agricultural and Biological Sciences Pub Date : 2023-10-11 DOI: 10.1080/00405000.2023.2266610
Limin Zhang, Longdi Cheng, Ruiyun Zhang, Wenliang Xue, Wanwan Ma, Xueqing Han
AbstractThis paper aims to study the hygroscopic exothermic behavior of fabrics, exploring the feasibility of achieving much slower and more even hygroscopic heating process by strengthened moisture transmission control. Based on the model of coupled heat and moisture transfer, the moisture diffused-transmission, ‘type-ladder’ mechanism was proposed, and then different moisture-absorbing and heating knitted fabrics were prepared by dissimilar finishing. The result showed that the mechanism of ‘type-ladder’ had the feasibility and advantages in retarding, extending and uniforming the moisture absorption and heat generation. Moreover, it was found that the inner layer of the composite finishing fabric was much more sensitive to the moisture with a faster diffusion and a closer water-fiber interaction through the analysis of the moisture transmission. By means of finishing to obtain the variation both in moisture state and diffusion, caused the fabric heating up much slowly in the continuous high-humidity micro-environment and evenly in the micro-environment with the moisture increasing until high-humidity significantly, which is further proven by the heat of desorption. These results demonstrated that hygroscopic exothermic fabric on ‘type-ladder’ mechanism might provide a new option fit to the actual thermal and humid comfort requirements.Keywords: Hygroscopic exothermic fabric‘type-ladder’ diffused-transmission mechanismuniform and slow moisture absorption and heat generationcoupled heat and moisture transfer Disclosure statementNo potential conflict of interest was reported by the authors.Table 1. The materials of the fabric.Download CSVDisplay TableAdditional informationFundingThe author(s) would like to acknowledge the following financial support for the research: This research was funded by the National Key R&D Program of China: No. 2017YFB0309100.
摘要本文旨在研究织物的吸湿放热行为,探讨通过加强吸湿控制,实现更慢更均匀的吸湿加热过程的可行性。在热湿耦合传递模型的基础上,提出了湿扩散传递的“阶梯式”机理,并采用不同整理工艺制备了不同吸湿增温针织织物。结果表明,“阶梯式”机理在延缓、延长和均匀吸湿生热方面具有可行性和优越性。此外,通过对复合整理织物的水分传递分析发现,复合整理织物内层对水分更为敏感,扩散速度更快,水-纤维相互作用更紧密。通过整理得到织物在连续高湿微环境中受热缓慢,在微环境中受热均匀,随着湿度的增加,直至高湿显著,解吸热进一步证明了这一点。这些结果表明,“梯型”机制的吸湿放热织物可能提供一种适合实际热湿舒适要求的新选择。关键词:吸湿放热织物“梯型”扩散传输机制均匀缓慢吸湿产热耦合热湿传递披露声明作者未报告潜在利益冲突。表1。织物的材料。作者感谢对本研究的资金支持:本研究由国家重点研发计划(2017YFB0309100)资助。
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引用次数: 0
Evaluation on dyeable, antibacterial and antioxidant properties of cotton fabric dyed with spent coffee grounds 用废咖啡渣染色棉织物的可染性、抗菌性和抗氧化性评价
4区 工程技术 Q2 Agricultural and Biological Sciences Pub Date : 2023-10-11 DOI: 10.1080/00405000.2023.2265620
Tuan Anh Nguyen, Duyen Nguyen Thi Hong, Thuy Nguyen Thi, Khoa Tran Dang
AbstractAlmost, spent coffee grounds are discarded to landfill, causing bad impacts on natural environment and generating a great waste because of removing beneficial bioactive compounds. This study investigated effects of dyeing techniques (exhaustion and pad-dry), types of mordants, sequences of adding mordants, temperature, exhausting time and concentration on dyeability of coffee extracts for cotton fabric in terms of color strength (K/S) and color difference (ΔE), thereby proposing a suitable treatment procedure. The experimental results showed that K/S and ΔE values were highest when mordanting with FeSO4.7H2O and CuSO4.5H2O. Simultaneously, highly antioxidant and antibacterial properties of treated cotton were quantitatively evaluated by UV-vis spectroscopy, scanning electronic microscopy, microbiologicalmethod and mechanical experiments. The content of polyphenols and tannins as well as the bacteriostatic activity of gram-positive and gram-negative species on treated cotton fabrics with coffee extracts were promising in future applications. Particularly, the total amounts of polyphenols and tannins, which could demonstrate antioxidant activity, were examined as 3.01 g/L (GAE) and 0.57 g/L (TAE), respectively. Especially, high reduction of E. coli bacteria and S. aureus bacteria on dyed specimens accounted for 78% and 80% as mordanting with CuSO4.5H2O, and it could be sustained to 75% and 48% after a washing cycle, respectively.Keywords: Antioxidant abilityantibacterial activityspent coffee groundsdyeabilitymordanting method AcknowledgementsThe authors would like to thank for support from Faculty of Mechanical Engineering at Ho Chi Minh City University of TechnologyDisclosure statementWe all commit that there are no conflicts of interest among authors as well as others and this manuscript has not been published to other journals before.Additional informationFundingThis work belongs to the project grant No: T2022-73 funded by Ho Chi Minh City University of Technology and Education, Vietnam.
咖啡渣大多被丢弃到垃圾填埋场,对自然环境造成不良影响,并因去除有益的生物活性成分而产生巨大的浪费。本研究考察了染色工艺(滤干法和垫干法)、媒染剂种类、媒染剂添加顺序、温度、滤干时间和浓度对咖啡提取物棉织物染色强度(K/S)和色差(ΔE)的影响,从而提出了合适的处理工艺。实验结果表明,以FeSO4.7H2O和CuSO4.5H2O为介质时,K/S和ΔE值最高。同时,通过紫外-可见光谱、扫描电镜、微生物学和力学实验等方法,定量评价了处理后棉花的抗氧化和抗菌性能。咖啡提取物对棉织物的多酚和单宁含量以及革兰氏阳性和革兰氏阴性菌的抑菌活性具有广阔的应用前景。其中,具有抗氧化活性的多酚和单宁含量分别为3.01 g/L (GAE)和0.57 g/L (TAE)。其中,以CuSO4.5H2O为介质,染色标本上大肠杆菌和金黄色葡萄球菌的去除率分别为78%和80%,洗涤一个循环后,去除率分别可维持在75%和48%。关键字:抗氧化能力抗菌活性咖啡渣可降解性资助方法致谢作者感谢胡志明市工业大学机械工程学院的支持披露声明我们承诺作者和其他人之间不存在利益冲突,本文之前未在其他期刊上发表过。本工作属于越南胡志明城市技术与教育大学资助的项目批准号:T2022-73。
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引用次数: 0
Immobilization of Ag-NPs onto cellulose-containing fabrics using O 2 -plasma o2 -等离子体固定化Ag-NPs在含纤维素织物上的研究
4区 工程技术 Q2 Agricultural and Biological Sciences Pub Date : 2023-10-10 DOI: 10.1080/00405000.2023.2266133
Ghada Kadry
AbstractSilver nanocomposites (Ag-NPs/PVP) were synthesized through the reduction of Ag+ using Ethylene glycol (EG) and poly(N-vinylpyrrolidone) (PVP) as a protective agent in an alkaline medium. Characterization involved UV–Vis spectrum, and TEM image, confirming the well spread of the nanoparticles with a particle size of range 5–10 nm. Stability, assessed after three months, revealed a zeta potentialof −17 mV, identicating no agglomeration. . PVP role in decreasing the nanoparticle size was studied, attributed to the protective layer preventing aggregation. . The study enhanced the antibacterial activity of various cellulosic fabrics (cotton, linen, and viscose) by activating their surfaces through O2 plasma pretreatment at atmospheric pressure. Activation immobilized the fabric matrix by the extracting radicals fforming functional groups(C = O, –O–C = O, –COH, –COOH, and CH2–OH). Viscose demonstrated the highest effect. FTIR confirmed the formation of polar groups on the fabric surface. Activated cellulosic fabric was treated with Ag-NPs/PVP colloid solution and antibacterial activity was assessed against Staphylococcus aureus (S. aureus) andEscherichia coli (E. coli). Parameters such as: plasma exposure time, Ag-NPs/PVP concentration, and the pretreatment bath temperature were studied.SEM images and EDX spectra verified the presence of nitrogen and silver elements on the treated substrates surface .Keywords: Silver nanoparticlessurface activationO2-plasmaantibacterial activitycellulosic fiber Disclosure statementThe authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.
摘要以乙二醇(EG)和聚n -乙烯基吡咯烷酮(PVP)为保护剂,在碱性介质中还原银离子,合成银纳米复合材料Ag- nps /PVP。通过紫外可见光谱和透射电镜图像进行表征,证实纳米颗粒的扩散良好,粒径范围为5-10 nm。三个月后的稳定性评估显示,zeta电位为- 17 mV,未发现团聚。研究了PVP对减小纳米颗粒粒径的作用,认为PVP的保护层阻止了纳米颗粒的聚集。该研究通过在常压下进行O2等离子体预处理,激活各种纤维素织物(棉、麻和粘胶)的表面,从而增强了其抗菌活性。活化通过提取自由基形成官能团(C = O, -O-C = O, -COH, -COOH和CH2-OH)来固定织物基体。粘胶的效果最好。FTIR证实了织物表面极性基团的形成。用Ag-NPs/PVP胶体溶液对活化后的纤维素织物进行处理,并对金黄色葡萄球菌(S. aureus)和大肠杆菌(E. coli)进行抑菌活性评价。研究了血浆暴露时间、Ag-NPs/PVP浓度、预处理浴温度等参数。SEM图像和EDX光谱证实了氮和银元素在处理过的底物表面的存在。关键词:纳米银粒子表面活化o2等离子体抗菌活性纤维素纤维披露声明作者声明他们没有已知的竞争经济利益或个人关系可能会影响本文报道的工作。
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引用次数: 0
Understanding consumer face mask consumption: a MaxDiff-based cluster analysis 了解消费者口罩消费:基于maxff的聚类分析
4区 工程技术 Q2 Agricultural and Biological Sciences Pub Date : 2023-10-09 DOI: 10.1080/00405000.2023.2267408
Wenna Han, Yingjiao Xu, Jitong Li
AbstractThis study aims to develop a consumer typology based on the importance of product attributes in consumer face mask consumption during the COVID-19 pandemic. An online survey with a MaxDiff experiment was employed to measure the importance of eight face mask attributes. Data were collected from 563 U.S. consumers during April 2022. Hierarchical Bayes analysis, K-means clustering, Chi-square tests, and ANOVA were used for data analysis. Results suggested that protection and comfort were the most important attributes, while appearance and brand were the least important. Based on the tradeoffs made in their purchase decision-making process, three distinct groups of face mask consumers were identified, named protection-focused, utilitarian-driven, and eco-conscious consumers. A consumer profile was established for each group, reflecting their mask-wearing behaviors, mask type preferences, and demographics. This study provides implications for face mask manufacturers and retailers to develop effective production and target marketing strategies for future respiratory pandemics.Keywords: Face maskattribute importanceMaxDiffcluster analysismarket segmentation Disclosure statementNo potential conflict of interest was reported by the author(s).Data availability statementThe data that support the findings of this study are available from the corresponding author upon reasonable request.Permission to reproduce material from other sourcesThere are no excerpts from copyrighted works owned by third parties included in this study.Additional informationFundingThis work was supported by a grant from the NSRP program at North Carolina State University.
摘要本研究旨在建立基于产品属性在COVID-19大流行期间消费者口罩消费中的重要性的消费者类型。采用在线问卷调查和MaxDiff实验来衡量8种口罩属性的重要性。该研究收集了2022年4月期间563名美国消费者的数据。采用层次贝叶斯分析、k均值聚类、卡方检验和方差分析进行数据分析。结果表明,保护和舒适是最重要的属性,而外观和品牌是最不重要的。基于他们在购买决策过程中所做的权衡,我们确定了三个不同的口罩消费者群体,分别是保护型、功利型和生态意识型消费者。每个群体都建立了一个消费者档案,反映了他们的口罩佩戴行为、口罩类型偏好和人口统计数据。这项研究为口罩制造商和零售商制定有效的生产和目标营销策略提供了启示,以应对未来的呼吸道流行病。关键词:人脸;属性重要性;模糊聚类分析;数据可得性声明支持本研究结果的数据可根据通讯作者的合理要求获得。从其他来源复制材料的许可本研究中没有从第三方拥有的版权作品中摘录。本研究得到了北卡罗莱纳州立大学NSRP项目的资助。
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引用次数: 0
Preparation and characterization of zeolite A-basalt fiber composite 沸石a -玄武岩纤维复合材料的制备与表征
4区 工程技术 Q2 Agricultural and Biological Sciences Pub Date : 2023-10-09 DOI: 10.1080/00405000.2023.2265117
Ling Guo, Ruonan Su, Shitan Miao, Zhao Yuan, Chuncheng Yang, Hongchao Li, Changjiang Liu
AbstractBy adjusting n(Na2O)/n(SiO2) and crystallization time, zeolite A - basalt fiber composite was successfully prepared by direct loading method under the system composition of n(SiO2)/n(Al2O3)=2, n(H2O)/n(SiO2)=125, n(Na2O)/n(SiO2)=2.1. The samples were determined by XRD, SEM, FTIR and calcium ion exchange. The results show that the composite of fiber and zeolite A is a combination of structure, and the crystallization time will affect the morphology of zeolite and composite effect. After crystallization for 6h, zeolite A with high crystallinity and moderate particle size can be obtained. At the same time, the loading ratio of zeolite on the fiber surface reaches the maximum, but the alkaline environment will reduce the fiber strength.Keywords: zeolite Abasalt fiberzeolite A- basalt fiber compositeion exchange Disclosure statementNo potential conflict of interest was reported by the authors.Additional informationFundingThis work was financially supported by the Fund from the Innovation Capacity Grant Project for Master Degree Candidate in Hebei province (CXZZSS2022019), the science and technology project of Hebei Education Department (BJK2023040), and the Central Government Guide Local for Scientific and Technological Development (206Z1501G).
摘要通过调整n(Na2O)/n(SiO2)和结晶时间,在n(SiO2)/n(Al2O3)=2、n(H2O)/n(SiO2)=125、n(Na2O)/n(SiO2)=2.1的体系组成下,采用直接负载法制备了沸石A -玄武岩纤维复合材料。采用XRD、SEM、FTIR、钙离子交换等方法对样品进行了表征。结果表明,纤维与A型沸石的复合是一种组合结构,而结晶时间会影响沸石的形态和复合效果。结晶6h后可得到结晶度高、粒度适中的A型沸石。同时,沸石在纤维表面的负载比达到最大,但碱性环境会降低纤维强度。关键词:沸石玄武岩纤维沸石A-玄武岩纤维成分交换披露声明作者未报道潜在利益冲突。项目资助:河北省硕士研究生创新能力资助项目(CXZZSS2022019)、河北省教育厅科技项目(BJK2023040)、中央政府科技发展指导地方项目(206Z1501G)。
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引用次数: 0
Effect of carbon nanotubes on the dielectric properties of spandex fabric 碳纳米管对氨纶纤维介电性能的影响
4区 工程技术 Q2 Agricultural and Biological Sciences Pub Date : 2023-10-06 DOI: 10.1080/00405000.2023.2262807
Prabir K. Mukherjee, Sajal Barman, Sudipta S. Mahish
AbstractEffect of carbon nanotubes (CNTs) on the dielectric properties of spandex fabric is studied theoretically. The frequency and CNTs dependence of the real and imaginary part of the complex dielectric permittivity are calculated and compared with experimental results of spandex fabric. An appreciable change in the dielectric permittivity has been observed for CNTs doped spandex fabric. Good agreement between theoretical and experimental results is observed.Keywords: Textilespandex fabricdielectric permittivitydielectric losscarbon nanotubes Disclosure statementThe authors declare no conflict of interest, financial or otherwise.
摘要从理论上研究了碳纳米管对氨纶织物介电性能的影响。计算了复介电常数实部和虚部的频率和碳纳米管的依赖关系,并与氨纶织物的实验结果进行了比较。对于碳纳米管掺杂的氨纶织物,介电常数发生了明显的变化。理论与实验结果吻合较好。关键词:纺织纤维织物介电常数介电损耗碳纳米管披露声明作者声明无利益冲突,经济或其他。
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引用次数: 0
期刊
Journal of the Textile Institute
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