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Intracellular vacuoles induced by hypo-osmotic stress visualized by coherent anti-Stokes Raman scattering (CARS) spectroscopic imaging 通过相干反斯托克斯拉曼散射(CARS)光谱成像观察低渗透压诱导的细胞内空泡
Pub Date : 2024-07-16 DOI: 10.35848/1882-0786/ad63f0
Zuliang Hu, Kyota Shirane, Kota Aramaki, Philippe Leproux, Akihito Inoko, Hideaki KANO, Ayami Matsushima
We analyzed the effects of a hypo-osmotic environment on rat Schwann cells, a type of glial cell surrounding neurons, using ultra-broadband multiplex coherent anti-Stokes Raman scattering (CARS) microscopy. After hypo-osmotic treatment, we detected vacuole-like components in the cytoplasm using both bright-field and CARS spectroscopic imaging. An approach integrating both morphological examination and a spectroscopic analysis based on multiple vibrational bands revealed that these structures are predominantly water-filled, and their characteristics closely resembled those of the vacuoles observed in plant cells.  
我们使用超宽带多重相干反斯托克斯拉曼散射(CARS)显微镜分析了低渗透环境对大鼠许旺细胞(神经元周围的一种神经胶质细胞)的影响。经过低渗处理后,我们利用明视野和 CARS 光谱成像技术检测了细胞质中的空泡样成分。综合形态学检查和基于多个振动波段的光谱分析,我们发现这些结构主要充满水,其特征与在植物细胞中观察到的液泡非常相似。
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引用次数: 0
Facile preparation of graphene-graphene oxide liquid cells and their application in liquid-phase STEM imaging of Pt atoms 石墨烯-氧化石墨烯液态电池的简便制备及其在铂原子液相 STEM 成像中的应用
Pub Date : 2024-07-16 DOI: 10.35848/1882-0786/ad63f2
Masaki Takeguchi, K. Mitsuishi, A. Hashimoto
Graphene-graphene oxide (GO) hybrid liquid cells (LCs) for liquid-phase scanning transmission electron microscopy (STEM) were fabricated using a facile method with commercial graphene on a polymethyl methacrylate sheet and GO on a TEM grid. LCs containing Pt nanoparticles (NPs) and pure water were efficiently produced and observed via STEM. Their composition and thickness were characterized by STEM-electron energy-loss spectroscopy. High-resolution (HR) STEM revealed slow-moving Pt NPs’ atomic structures and fast-moving single Pt atoms at the LC’s thin edges. Minimal damage during HR STEM indicated stable LCs because of their excellent electrical and thermal conductivities and radiolysis species scavenging ability.
采用一种简便的方法,在聚甲基丙烯酸甲酯片上制造了商用石墨烯,在 TEM 网格上制造了 GO,从而制造出了用于液相扫描透射电子显微镜(STEM)的石墨烯-氧化石墨烯(GO)混合液体电池(LCs)。含有铂纳米颗粒(NPs)和纯水的液相沉积物被有效地制造出来,并通过 STEM 进行观察。它们的成分和厚度是通过 STEM-电子能量损失光谱来表征的。高分辨率(HR)STEM 显示了缓慢移动的 Pt NPs 原子结构以及 LC 薄边缘处快速移动的单个 Pt 原子。在高分辨率 STEM 过程中,由于 LC 具有出色的导电性、导热性和清除放射性物质的能力,因此损伤极小,这表明 LC 非常稳定。
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引用次数: 0
Neural-network-based transfer learning for predicting cryo-CMOS characteristics from small datasets 基于神经网络的迁移学习,从小型数据集预测低温-CMOS 特性
Pub Date : 2024-07-16 DOI: 10.35848/1882-0786/ad63f1
T. Inaba, Yusuke Chiashi, Minoru Ogura, H. Asai, H. Fuketa, H. Oka, S. Iizuka, K. Kato, S. Shitakata, T. Mori
Transfer learning was examined to predict current-voltage (I-V) characteristics of MOSFETs at cryogenic temperatures. An experimental dataset was obtained from approximately 800 silicon-on-insulator MOSFETs using an automated cryogenic wafer prober to pre-train a 3-hidden-layer neural network (NN) model. Transfer learning based on the NN model was then conducted using another small dataset from 2 bulk MOSFETs. The transfer learning NN model predicted more realistic I-V characteristics and threshold voltages than a control NN model trained using only the small dataset. This study demonstrates cryogenic MOSFET characteristics prediction from a small dataset to reduce time and financial costs.
研究人员利用迁移学习预测低温条件下 MOSFET 的电流-电压 (I-V) 特性。实验数据集来自约 800 个硅-绝缘体 MOSFET,使用自动低温晶圆探测仪对 3 个隐藏层神经网络 (NN) 模型进行预训练。然后,使用来自 2 块 MOSFET 的另一个小型数据集,在 NN 模型的基础上进行迁移学习。与仅使用小型数据集训练的对照神经网络模型相比,迁移学习神经网络模型预测的 I-V 特性和阈值电压更为真实。这项研究展示了利用小型数据集预测低温 MOSFET 特性的方法,从而减少了时间和财务成本。
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引用次数: 0
Influence of fixed charges and trapped electrons on free electron mobility at 4H-SiC(0001)/SiO2 interfaces with gate oxides annealed in NO or POCl3 在 NO 或 POCl3 中退火的 4H-SiC(0001)/SiO2 界面栅极氧化物上的固定电荷和捕获电子对自由电子迁移率的影响
Pub Date : 2024-07-16 DOI: 10.35848/1882-0786/ad63ef
Koji Ito, Hajime Tanaka, M. Horita, J. Suda, Tsunenobu Kimoto
Free electron mobility (µ free) in 4H-SiC(0001) metal-oxide-semiconductor field-effect transistors (MOSFETs) with gate oxides annealed in NO or POCl3 was calculated in a wide range of effective normal field (E eff) from 0.02 to 2 MV cm−1, taking account of scattering by fixed charges and trapped electrons. The present calculation indicates that the Hall mobility in the high-E eff region experimentally obtained for NO-annealed MOSFETs (14 cm2 V−1 s−1 at 1.1 MV cm−1) is much lower than that for POCl3-annealed MOSFETs (41 cm2 V−1 s−1) due to severe Coulomb scattering by electrons trapped at a very high density of interface states.
考虑到固定电荷和捕获电子的散射,在 0.02 至 2 MV cm-1 的宽有效法向场 (E eff) 范围内计算了栅极氧化物在 NO 或 POCl3 中退火的 4H-SiC(0001) 金属氧化物半导体场效应晶体管 (MOSFET) 中的自由电子迁移率 (µ free)。本计算表明,在高 E eff 区域,NO 退火 MOSFET 实验获得的霍尔迁移率(1.1 MV cm-1 时为 14 cm2 V-1 s-1)远低于 POCl3 退火 MOSFET 的霍尔迁移率(41 cm2 V-1 s-1),这是由于被困在极高密度界面态的电子产生了严重的库仑散射。
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引用次数: 0
Dynamic wide gamut color generation using highly lossy metal-based metal-dielectric-metal structure 利用高损耗金属基金属-电介质-金属结构生成动态广色域色彩
Pub Date : 2024-07-12 DOI: 10.35848/1882-0786/ad62d3
Y. Takashima, Kentaro Nagamatsu, M. Haraguchi, Y. Naoi
Dynamic structural color control across a wide spectral range was experimentally achieved via phase retardation between orthogonal polarization states in a Ni/SiO2/Ni-subwavelength grating (SWG) structure. The fabricated Ni/SiO2/Ni-SWG structure exhibited spectrally broadened resonant reflection dips due to the optical damping of Ni. The resonances induced a large phase retardation between the p- and s-polarizations over a wide spectral range, and the retardation changed the reflected polarization states depending on the wavelength. The rotation of the analyzing polarizer enabled the dynamic variation of the reflected structural color from the sample across the wide visible color gamut.
通过在 Ni/SiO2/Ni 亚波长光栅(SWG)结构中正交偏振态之间的相位延迟,实验实现了宽光谱范围内的动态结构颜色控制。由于镍的光学阻尼作用,制备的镍/二氧化硅/镍-亚波长光栅结构显示出光谱拓宽的谐振反射凹陷。共振在很宽的光谱范围内引起了 p 极化和 s 极化之间的较大相位延迟,这种延迟会根据波长改变反射的极化状态。分析偏振片的旋转使样品的反射结构颜色在广泛的可见光色域内发生动态变化。
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引用次数: 0
Deep-subwavelength and hydrostatic-pressure-resistant meta-absorber for broadband low-frequency underwater sound 用于宽带低频水下声学的深亚波长和抗静水压力元吸收器
Pub Date : 2024-07-11 DOI: 10.35848/1882-0786/ad622e
Yanni Zhang, Manlin Tong, Xiaoting Rui, Guoping Wang, Fufeng Yang
By embedding center-supported graded-circular-plates (CS-GCPs) into an elastomer, a deep-subwavelength and hydrostatic-pressure-resistant meta-absorber was designed and manufactured for sound absorption (SA) under hydrostatic pressure. The meta-absorber exhibits excellent SAs (>0.842, 0.927 on average) within 500-2000 Hz and quasi-perfect SA (>0.94) within 500-700 Hz with thickness 2% of the sound wavelength. This excellent SA (0.91 on average) is verified experimentally within 1-10 kHz, and maintained high (0.84 on average) under hydrostatic pressure of 1.0 MPa. The exotic functionality arises from enriched local-dynamics by the CS-GCPs and pressure-resistance of the center-support, and provides an effective solution for ultra-broadband low-frequency underwater sound control.
通过在弹性体中嵌入中心支撑分级圆板(CS-GCP),设计并制造了一种深亚波长、耐静水压的元吸声体,用于在静水压力下吸声(SA)。这种元吸声材料在 500-2000 Hz 范围内具有极佳的吸声性能(大于 0.842,平均值为 0.927),在 500-700 Hz 范围内具有准完美的吸声性能(大于 0.94),厚度为声波长的 2%。在 1-10 kHz 的频率范围内,实验验证了这一优异的 SA 值(平均 0.91),并在 1.0 MPa 的静水压力下保持较高的 SA 值(平均 0.84)。这种奇特的功能源于 CS-GCP 丰富的局部动力学和中心支撑的抗压性,为超宽带低频水下声控提供了有效的解决方案。
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引用次数: 0
Theory for electromigration at metal nanocontacts driven by kinetic energy transfer from “lucky electrons” 由 "幸运电子 "动能转移驱动的金属纳米接触点电迁移理论
Pub Date : 2024-07-10 DOI: 10.35848/1882-0786/ad61ba
Yue Tian, Guangtai Lu, Shaoqing Du, K. Kuroyama, K. Hirakawa
We have developed a theory for electromigration at metal nanocontacts. In the proposed theory, a metal atom is removed by kinetic energy transfer from a “lucky electron” that ballistically traverses a metal nanocontact, when the applied voltage exceeds the surface self-diffusion potential of the metal. The histogram of the critical voltage, Vc, at which metal atoms are removed, depends on the temperature as well as the probability for an atom being removed by collision with a lucky electron. The histograms of Vc for Au, Ni, Pd are well explained by the present theory.
我们提出了金属纳米触点电迁移理论。在提出的理论中,当施加的电压超过金属表面自扩散电位时,金属原子会通过动能转移从弹道穿越金属纳米接触的 "幸运电子 "上移除。金属原子被移除的临界电压 Vc 直方图取决于温度以及原子与幸运电子碰撞而被移除的概率。本理论可以很好地解释金、镍、钯的 Vc 直方图。
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引用次数: 0
Pulsed laser deposition and structural analysis of Ba2Ti6O13 epitaxial thin film on the (210) surface of SrTiO3 single crystal SrTiO3 单晶 (210) 表面上的 Ba2Ti6O13 外延薄膜的脉冲激光沉积和结构分析
Pub Date : 2024-07-08 DOI: 10.35848/1882-0786/ad605d
Ryuta Kono, Kohei Hieda, T. Tokunaga, Ryoma Tamura, Ryotaro Masamura, yasuyuki hikita, Kazuhiko Kano, Takahisa Yamamoto
A single crystalline thin film of Ba2Ti6O13 was grown on the (210) surface of a SrTiO3 single-crystal substrate by pulsed laser deposition. Scanning transmission electron microscopy shows that the Ba2Ti6O13 thin film grew epitaxially with the a-plane, and the b-/c-axes of Ba2Ti6O13 parallel to the (210) plane and the [00-1]/[-120] directions of SrTiO3, respectively. The electrical conductance of the Ba2Ti6O13 film was approximately one order larger than that of reduced SrTiO3-δ single crystal with oxygen deficiency of roughly δ = 0.05. Electronic structure calculations predict that δ is an n-type degenerate semiconductor with spin-split states primarily of Ti 3d orbital.
通过脉冲激光沉积法在 SrTiO3 单晶衬底的 (210) 表面生长出了 Ba2Ti6O13 单晶薄膜。扫描透射电子显微镜显示,Ba2Ti6O13 薄膜是外延生长的,Ba2Ti6O13 的 a 轴和 b/c 轴分别平行于 (210) 平面和 SrTiO3 的 [00-1]/[-120] 方向。Ba2Ti6O13 薄膜的电导率比缺氧约为δ = 0.05 的还原型 SrTiO3-δ 单晶大约大一个数量级。电子结构计算表明,δ 是一种 n 型变质半导体,主要具有钛 3d 轨道的自旋分裂态。
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引用次数: 0
Prediction of NdFe16-based permanent-magnet compounds with high magnetization 预测具有高磁化率的 NdFe16 基永磁化合物
Pub Date : 2024-07-05 DOI: 10.35848/1882-0786/ad5fd9
Insung Seo, Shimpei Tanaka, Mitsuru Endo, Y. Gohda
We find a candidate for new permanent-magnet materials with the 1-16 stoichiometry on the basis of first-principles calculations utilizing a materials database. An extremely iron-rich NdFe16 compound shows exceptionally high saturation magnetization with an adequate magnetocrystalline anisotropy energy and Curie temperature. Although it has an excessive formation energy in its binary composition, introducing interstitial light elements into NdFe16 successfully decreases the formation energy while maintaining its superior magnetic properties. The density of states explains the alteration of magnetization from incorporating light elements.
在利用材料数据库进行第一性原理计算的基础上,我们找到了具有 1-16 化学计量的新型永磁材料的候选材料。一种含铁量极高的 NdFe16 化合物显示出极高的饱和磁化率,并具有足够的磁晶各向异性能和居里温度。虽然钕铁硼在二元成分中具有过高的形成能,但在钕铁硼中引入间隙轻元素后,成功地降低了形成能,同时保持了其卓越的磁性能。状态密度解释了加入轻元素后磁化的变化。
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引用次数: 0
Nanometer-precision measurements of geometric fluctuations via momentum-filtered spectroscopy 通过动量滤波光谱对几何波动进行纳米级精确测量
Pub Date : 2024-07-03 DOI: 10.35848/1882-0786/ad5f0e
Wenping Hu, Yingjun Zhang, Weihang Zhou
In this work, we report ultra-sensitive detection of geometric fluctuations of semiconductor nanostructures using momentum-filtered spectroscopy. Our strategy is developed based on angle-resolved photoluminescence / absorption spectroscopic imaging technique. By filtering out signals with non-zero in-plane momentum using a confocal pinhole, ultra-sensitive detection of tiny geometric fluctuations with nanometer precision was made possible. In this way, we could optically detect geometric fluctuations of semiconductor nanostructures in real time with a spatial resolution as high as ~ 0.2 nm. Moreover, this technique is widely applicable to nanostructures where optical resonance can be formed.
在这项工作中,我们报告了利用动量滤波光谱技术对半导体纳米结构的几何波动进行超灵敏检测的情况。我们的策略是基于角度分辨光致发光/吸收光谱成像技术开发的。通过使用共焦针孔滤除非零平面动量信号,实现了纳米级精度的微小几何波动的超灵敏检测。通过这种方法,我们可以实时光学检测半导体纳米结构的几何波动,空间分辨率高达 ~ 0.2 nm。此外,这项技术还广泛适用于可形成光学共振的纳米结构。
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引用次数: 0
期刊
Applied Physics Express
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