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Modifying the Microstructure and Mechanical Properties of Non-Heat Treated HPDC AlSi10MnMg Foundry Alloy via Incorporation of TiB2 Particles and Sc 通过加入 TiB2 粒子和 Sc 改变非热处理 HPDC AlSi10MnMg 铸造合金的微观结构和力学性能
Pub Date : 2024-05-14 DOI: 10.4028/p-dsd17k
Nisha Shareef, Xiang Ting Liu, Kai Zhao, Muhammad Saqib Shahzad, Jing Tao Zhang, E. Guo, Hui Jun Kang, Zhi Gang Hao, Jie Hua Li, Cun-shan Wang, Zong Ning Chen, Tongzhen Wang
The demand for structural lightweight in a variety of industries, particularly the automobile industry, has driven the development of heat-free die-cast aluminum alloys with excellent properties. Utilizing lightweight materials, such as Al-Si alloys has several benefits, including higher overall performance in automobiles and other industries, increased heat resistance efficiency, decreased emissions, and reduced weight. The purpose of this study is to modify the microstructure and enhance the mechanical properties of high-pressure die-casting (HPDC) AlSi10MnMg foundry alloy by incorporation of TiB2 and Sc without any heat treatment. The results showed that the HPDC process significantly refines the grain structure and AlSiMnFe intermetallic compounds, transforming the eutectic morphology from sharp to rounded, and 93% enhancement in elongation at the optimum content (0.018 wt.%) of TiB2. While the hardness of the alloy was improved by 15.7% with the addition of 0.03wt.% TiB2. TiB2 incorporation refines the grain structure and AlSiMnFe phases, while depressing externally solidified crystals (ESCs). The HPDC process refines Al3Sc phases as well as AlSiMnFe phases while increasing yield strength due to Al3Sc strengthening effects. After 0.5wt.% Sc addition in 0.018wt.% TiB2-AlSi10MnMg alloy, the YS, and EL reached the maximum of 196MPa and 9.93% respectively.
各行各业,尤其是汽车行业对结构轻量化的需求,推动了具有优异性能的无热压铸铝合金的发展。使用铝硅合金等轻质材料有多种好处,包括提高汽车和其他行业的整体性能、提高耐热效率、减少排放和减轻重量。本研究的目的是在不进行任何热处理的情况下,通过加入 TiB2 和 Sc 来改变高压压铸 (HPDC) AlSi10MnMg 铸造合金的微观结构并提高其机械性能。结果表明,高压压铸工艺显著细化了晶粒结构和 AlSiMnFe 金属间化合物,使共晶形态从尖锐变为圆润,在 TiB2 的最佳含量(0.018 wt.%)下,伸长率提高了 93%。加入 0.03 重量百分比的 TiB2 后,合金的硬度提高了 15.7%。TiB2 的加入细化了晶粒结构和 AlSiMnFe 相,同时抑制了外部凝固晶体 (ESC)。HPDC 工艺细化了 Al3Sc 相和 AlSiMnFe 相,同时由于 Al3Sc 的强化效应提高了屈服强度。在 0.018 重量百分比的 TiB2-AlSi10MnMg 合金中添加 0.5 重量百分比的 Sc 后,YS 和 EL 分别达到 196MPa 和 9.93% 的最大值。
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引用次数: 0
Effect of Picosecond Laser Irradiation on the Properties of Nanostructured Zinc Oxide Thin Films 皮秒激光辐照对纳米结构氧化锌薄膜性能的影响
Pub Date : 2024-05-14 DOI: 10.4028/p-djtw4k
Muhammed Naziruddin Khan, A. Almohammedi
In this article, a picosecond laser source was employed to irradiate the nanostructured ZnO thin film prepared by the sol-gel method. The impact of laser irradiation on the characteristics of a nanostructured ZnO thin film was investigated. Analysis using X-ray diffraction, scanning electron microscopy, and Fourier transform infrared spectroscopy confirmed a significant influence on the structure of the ZnO thin film. As the duration of laser irradiation (the number of laser pulses) increased, there was a remarkable decrease in both the electronic and photoluminescence intensities of the nanostructured film. Tauc's plot indicates a noticeable change in the optical band gaps of the thin film with the increase in irradiation time. The morphological image suggests that the laser irradiation energy induces both degradation and modification of the film surface, consequently causing changes in the structural, absorption, and photoluminescence properties of nanostructured ZnO. The observed effects are attributed to alterations in the crystal structure and size of the nanostructured ZnO film, as confirmed by XRD. The reduction in photoluminescence intensity observed over the laser irradiation times may be a result of potential degradation in the crystalline structure of the nanostructured ZnO film.
本文采用皮秒激光源辐照溶胶-凝胶法制备的纳米结构氧化锌薄膜。研究了激光辐照对纳米结构氧化锌薄膜特性的影响。利用 X 射线衍射、扫描电子显微镜和傅立叶变换红外光谱进行的分析表明,激光辐照对氧化锌薄膜的结构有显著影响。随着激光照射时间(激光脉冲数)的增加,纳米结构薄膜的电子强度和光致发光强度都显著下降。陶克曲线图表明,随着辐照时间的增加,薄膜的光带隙发生了明显变化。形态图像表明,激光辐照能量会引起薄膜表面的降解和改性,从而导致纳米结构 ZnO 的结构、吸收和光致发光特性发生变化。经 XRD 证实,观察到的效应归因于纳米结构氧化锌薄膜晶体结构和尺寸的改变。激光照射时间越长,光致发光强度越低,这可能是纳米结构氧化锌薄膜晶体结构退化的结果。
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引用次数: 0
Evaluation of Fatigue Limit Improvement and Harmless Crack Size of Maraging Steel Using Shot Peening 利用喷丸强化评估马氏体时效钢的疲劳极限改善和无害裂纹尺寸
Pub Date : 2024-05-14 DOI: 10.4028/p-ucz3th
Seo Hyun Yun, Ho Seok Nam, Ki Woo Nam
The fatigue strength of maraging steel, which is an ultra-high-strength steel, is relatively low, compared to that of conventional high-strength steel. The fatigue life of a structure is highly dependent on the surface conditions, because fatigue cracks generally start at the surface of the material. In particular, surface cracks considerably degrade the fatigue limit. To expand the application range of maraging steel, it is necessary to improve the fatigue limit, and render the surface cracks harmless. This study aims to investigate the effect of shot peening (SP) on the fatigue strength of maraging steel with surface cracks. The SP application introduced a compressive residual stress from the specimen surface to a depth of 170 μm, and increased the fatigue limit by 77 %. The estimated crack size that can be rendered harmless, based on fracture mechanics, is (0.170 − 0.202) μm in the range As = (1.0 − 0.1). The intersections of the harmless crack sizes were determined at depth. A semicircular surface crack below this value is harmless in terms of fatigue limit. The usefulness of non-destructive inspection (NDI) and non-damaging technology was evaluated in relation to ahml, aNDI, a25,50, and As. Thus, the SP process can improve the reliability of the maraging steel. Compressive residual stress is the dominant factor to improve fatigue strength and render the surface crack harmless.
马氏体时效钢是一种超高强度钢,与传统的高强度钢相比,其疲劳强度相对较低。结构的疲劳寿命在很大程度上取决于表面条件,因为疲劳裂纹通常始于材料表面。尤其是表面裂纹会大大降低疲劳极限。为了扩大马氏体时效钢的应用范围,有必要提高其疲劳极限,并使表面裂纹无害化。本研究旨在探讨喷丸强化(SP)对带有表面裂纹的马氏体时效钢疲劳强度的影响。喷丸强化从试样表面到 170 μm 的深度引入了压缩残余应力,使疲劳极限提高了 77%。根据断裂力学估算,在 As = (1.0 - 0.1) 范围内,可实现无害化的裂纹尺寸为 (0.170 - 0.202) μm。无害裂缝尺寸的交叉点是在深度上确定的。就疲劳极限而言,低于该值的半圆形表面裂纹是无害的。根据 ahml、aNDI、a25、50 和 As 对无损检测(NDI)和无损技术的有用性进行了评估。因此,SP 工艺可以提高马氏体时效钢的可靠性。压缩残余应力是提高疲劳强度和使表面裂纹无害化的主要因素。
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引用次数: 0
In Situ Measurement of Twist Propagation and Yarn Tension with Superconducting Magnetic Bearing Twisting Element for Ring Spinning Process 利用环锭纺工艺中的超导磁性轴承加捻元件现场测量捻度传播和纱线张力
Pub Date : 2024-03-27 DOI: 10.4028/p-6a6cti
M. Hossain, A. Abdkader, Chokri Cherif, Mostafa Baloochi, Ruben Hühne, Yves Jesus Perez Delgado, Michael Beitelschmidt
The twisting of yarn in one of the most widely used conventional ring spinning processes is based on the ring/traveler system. The existing limitation of productivity in the ring spinning process lies on the prevailing force relation between ring, traveler and yarn as well as the frictional heat between traveler and ring, principally in the ring traveler system. Recently, a frictional free twisting element based on a superconducting magnetic bearing (SMB) was developed to increase the productivity of ring spinning drastically, which was patented by ITM and Leibniz IFW Dresden. This SMB consists of a circular superconductor and a permanent magnet (PM) ring. In the superconducting state, the PM ring levitates and can freely rotate even up to an angular speed of 50.000 rpm. It is connected with the spindle via the yarn through a guide attached to the PM ring to impart yarn twist. Through the rotation of the PM ring, the twist propagates to the nip point of the delivery rollers. The twist propagation rate depends on different parameters, e.g., spindle speed, balloon geometry, and friction between yarn and yarn guides. A change in the level of twist affects the process, yarn tension, yarn breakage rate, and yarn properties. Hence, it is important to investigate the twist distribution to derive effective measures for improving the twist propagation especially at higher angular spindle speeds and thus eliminate weak points to increase process stability and yarn quality. The aim of these measurements is to analyze the twist distribution along the yarn path to understand the causes of yarn breakages. In this study, the yarn path was traced at different regions by in-situ measuring the helix angle of twisted yarn using a high-speed camera. From the recorded images, the number of twists per unit length was determined using the image processing software ‘Image J’. Thus, the measurement method allows a new insight into the problem of yarn breakages originating from twist propagation in order to take optimized measures at higher angular spindle speeds.
在应用最广泛的传统环锭纺纱工艺中,纱线的加捻是以钢领/钢丝圈系统为基础的。目前,环锭纺纱工艺的生产率主要受限于钢领、钢丝圈和纱线之间普遍存在的力的关系,以及钢丝圈和钢领之间的摩擦热。最近,ITM 和 Leibniz IFW Dresden 共同开发了一种基于超导磁轴承 (SMB) 的无摩擦加捻元件,以大幅提高环锭纺的生产率。这种 SMB 由一个圆形超导体和一个永磁环组成。在超导状态下,永磁环悬浮并可自由旋转,角速度最高可达 50.000 rpm。它通过连接到永磁环上的导纱器与纱锭相连,以传递纱线捻度。通过永磁环的旋转,捻度传播到输纱罗拉的压捻点。捻度传播速度取决于不同的参数,如锭子速度、气球几何形状以及纱线和纱线导纱器之间的摩擦力。捻度的变化会影响工艺、纱线张力、断纱率和纱线特性。因此,有必要对捻度分布进行研究,以便采取有效措施改善捻度传播,尤其是在锭子角速度较高的情况下,从而消除薄弱环节,提高工艺稳定性和纱线质量。这些测量的目的是分析纱线路径上的捻度分布,以了解断纱的原因。在这项研究中,通过使用高速摄像机现场测量加捻纱线的螺旋角,在不同区域追踪纱线路径。根据记录的图像,使用图像处理软件 "Image J "确定了单位长度上的捻数。因此,通过这种测量方法,可以对因捻度传播而导致的断纱问题有一个新的认识,从而在更高的锭子角速度下采取优化措施。
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引用次数: 0
Fabrication of Liquid-Metal Printed 2D Tin Oxide Nanosheets for Optoelectronic Applications 制作用于光电应用的液态金属印刷二维氧化锡纳米片
Pub Date : 2024-03-27 DOI: 10.4028/p-clz1kt
Shunjiro Fujii
Liquid-metal printed processes have been recently developed as a novel strategy to grow ultrathin 2D oxide materials, which are transferred from liquid-metal surfaces to substrates. In this study, we fabricated liquid-metal printing 2D tin oxide (SnO) nanosheets on SiO2/Si and glass substrates. A large lateral-sized 2D SnO nanosheets of >100 µm and a thickness of approximately 6.3 nm was fabricated. The 2D SnO nanosheets exhibited a strong optical absorption in the ultraviolet and violet region and its bandgap was estimated to be approximately 2.9 eV. The 2D SnO nanosheets on glass substrates with patterned gold electrodes generated a photocurrent under ultraviolet (UV) light irradiation, demonstrating a potential for optoelectronic applications such as UV detectors.
液态金属印刷工艺是最近发展起来的一种生长超薄二维氧化物材料的新策略,这种材料可以从液态金属表面转移到基底上。在这项研究中,我们在二氧化硅/硅和玻璃基底上制作了液态金属印刷二维氧化锡(SnO)纳米片。制备的二维氧化锡纳米片横向尺寸大于 100 µm,厚度约为 6.3 nm。这种二维氧化锡纳米片在紫外和紫光区有很强的光吸收,其带隙估计约为 2.9 eV。玻璃基底上的二维氧化锡纳米片带有图案化的金电极,在紫外线(UV)照射下可产生光电流,显示了紫外线探测器等光电应用的潜力。
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引用次数: 0
The Effect of Drying Temperature Variation on the Production of Porang Starch Bioplastics with Sorbitol Plasticizer on Mechanical and Thermal Properties 干燥温度变化对使用山梨醇增塑剂生产波朗淀粉生物塑料的机械和热性能的影响
Pub Date : 2024-03-27 DOI: 10.4028/p-d9dpe4
A. Maghfirah, Sudiati Sudiati, M. Z. Sofyan, Nurul Adila Damanik, Yoseva Hia
The objective of this work is in order to investigate how the mechanical properties of bioplastics synthesized from chitosan and porang starch with sorbitol plasticizer are affected by varying drying temperatures. According to the study's findings, changes in drying temperatures significantly affect the mechanical properties of these bioplastics. This research provides valuable insights for developing environmentally friendly packaging alternatives of various drying temperatures starting from 50°C, 55°C, 60°C, 65°C, 70°C. The results of mechanical characterization show that at 50°C with 40% sorbitol, the plastic possesses a 17.32% elongation and 2.66 MPa tensile strength. At 50°C with 60% sorbitol, the tensile strength reaches 1.34 MPa and elongation is 34.43%. Meanwhile, at 65°C with 80% sorbitol, the tensile strength is 1.59 MPa and elongation reaches 37.80%. The plastic is also thermally tested using TGA-DTA, morphologically tested using SEM and its functional divisions are analyzed using FTIR to obtain further data about its properties.
这项工作的目的是研究壳聚糖和茯苓淀粉与山梨醇增塑剂合成的生物塑料的机械性能如何受到不同干燥温度的影响。研究结果表明,干燥温度的变化会显著影响这些生物塑料的机械性能。这项研究为开发不同干燥温度(从 50°C、55°C、60°C、65°C 到 70°C)的环保型包装替代品提供了宝贵的见解。机械表征结果表明,在 50°C 温度下,如果山梨醇含量为 40%,塑料的伸长率为 17.32%,拉伸强度为 2.66 兆帕。在 50°C 时,山梨醇含量为 60%,拉伸强度达到 1.34 兆帕,伸长率为 34.43%。同时,在 65°C 时,山梨醇含量为 80%,拉伸强度为 1.59 兆帕,伸长率为 37.80%。此外,还使用 TGA-DTA 对该塑料进行了热测试,使用 SEM 对其进行了形貌测试,并使用傅立叶变换红外光谱对其功能分区进行了分析,以获得有关其性能的更多数据。
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引用次数: 0
Effect Evaluation of Repeated Compression for Tactile Hardening of Cotton Pile Towel by Indentation Test 通过压痕测试评估重复压缩对棉绒毛巾触觉硬化的影响
Pub Date : 2024-03-27 DOI: 10.4028/p-qxq4ws
Shenglin Cui, Atsushi Sakuma, Tsuyoshi Morita, Hideo Matsui
Pile has a textured structure that contains voids and cavities, and the texture hardens with repeated use. It is advantageous to numerically evaluate the hardening characteristics of the pile texture for the development of the products such as towels. Then, the objective of this study is to establish an objective method for evaluating the hardening of the pile due to repeated use. In particular, to determine product specifications, it is necessary to define the conditions under which measurement results are stable. Therefore, for proper design of pile products, objective test methods for repeat use of the pile must be identified. This article reports the effect of repeated indentation testing with a spherical probe on towel samples folded in two to form four layers. A contact theory based on Hertzian theorem is used to evaluate the stiffening of the towel due to repeated indentation. For the properties evaluated in this extended contact theorem, the stiffening behavior is discussed by comparing the changes in the results of 20 repeated tests. In this discussion, the critical times of the indentation test are analyzed to quantify the characteristics of the stiffening behavior of the cotton towels. Analyzing the indentation times shows that critical conditions for the number of tests can be defined.
绒毛具有包含空隙和空洞的纹理结构,反复使用会使纹理硬化。对绒毛质地的硬化特性进行数值评估有利于毛巾等产品的开发。因此,本研究的目的是建立一种客观的方法,用于评估重复使用导致的绒毛硬化。特别是,为了确定产品规格,有必要确定测量结果稳定的条件。因此,为了正确设计桩产品,必须确定桩重复使用的客观测试方法。本文报告了用球形探头对折叠成两层形成四层的毛巾样品进行重复压痕测试的效果。以赫兹定理为基础的接触理论被用来评估毛巾因重复压痕而产生的刚度。对于该扩展接触定理所评估的特性,通过比较 20 次重复试验结果的变化来讨论变硬行为。在讨论中,分析了压痕测试的临界时间,以量化棉质毛巾的硬化行为特征。对压痕时间的分析表明,可以定义测试次数的临界条件。
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引用次数: 0
Intelligent Identification of Chinese and Australian Merino Wool Fibers Based on Image Recognition 基于图像识别的中国和澳大利亚美利奴羊毛纤维的智能识别
Pub Date : 2024-03-27 DOI: 10.4028/p-o96bar
Xiao Bo Wang, Zhan Xia Chen, Li Jing Wang, Xue Lei Shan, Zi Li Xie, Yun Long Shi, Xiao Ming Qian
In order to promote the sustainable growth of the wool industry and protect consumers' legitimate rights, rapid identification of the country of origin for wool of the same type is deemed crucial. This research presents a computer graphic recognition training model that utilizes median and Wiener filtering techniques to effectively reduce noise in the raw wool fiber images. Employing a support vector machine as the classifier and integrating a polynomial kernel function, this model achieves swift and accurate identification of Chinese and Australian Merino wool fibers. Experimental results underscore that following image recognition training, the model attains an impressive 92.5% comprehensive and precise identification rate for Chinese and Australian Merino wool fibers, effectively distinguishing the origin of wool from the same category. This approach not only provides a valuable reference for identifying the origin of similar wool types but also holds the potential to standardizing the wool fibre material market and assuring the consumer’s confidence on wool products.
为了促进羊毛产业的可持续发展,保护消费者的合法权益,快速识别同类羊毛的原产国至关重要。本研究提出了一种计算机图形识别训练模型,利用中值滤波和维纳滤波技术有效降低羊毛纤维原始图像中的噪声。该模型采用支持向量机作为分类器,并集成了多项式核函数,可快速准确地识别中国和澳大利亚的美利奴羊毛纤维。实验结果表明,经过图像识别训练后,该模型对中国和澳大利亚美利奴羊毛纤维的综合精确识别率高达 92.5%,有效区分了同类羊毛的产地。这种方法不仅为识别同类羊毛的产地提供了有价值的参考,而且有望规范羊毛纤维材料市场,确保消费者对羊毛产品的信心。
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引用次数: 0
Neural Network Based Determination of the Degree of Fiber Mixing in Hybrid Yarns and Composites 基于神经网络确定混合纱线和复合材料中的纤维混合度
Pub Date : 2024-03-27 DOI: 10.4028/p-x2keu5
Matthias Overberg, Alexander Dams, A. Abdkader, Chokri Cherif
A deep understanding on the intermixing of components in hybrid yarn or composite structures is decisive in order to develop hybrid structures with desired properties. This paper presents the development of a versatile procedure for the determination of the degree of fiber mixing in yarns and composites based on microscopy images auto-segmented by a neural network. The procedure is based on the quantification of blend irregularity values and blend homogeneity. For this purpose, functions of spatial point patterns analysis have been used to investigate the blend uniformity of yarn and composite cross sectional areas. The results show that the trained neural network model for segmentation of images has an accuracy of 92 %, indicating that the method is capable of accurately assessing the location of fibers in hybrid struc-tures. The results of the spatial point patterns analysis reveals a correlation between the blend value and the properties of yarns and composites. The proposed method provides a fast and reliable way to evaluate the hybrid structures, which could be used as a tool for quality control and process optimization.
深入了解混合纱线或复合材料结构中各组分的混合情况,对于开发具有所需性能的混合结构至关重要。本文介绍了一种多功能程序的开发,该程序基于神经网络自动分割的显微镜图像,用于确定纱线和复合材料中的纤维混合程度。该程序基于混纺不规则值和混纺均匀性的量化。为此,使用了空间点模式分析函数来研究纱线和复合材料横截面积的混纺均匀性。结果显示,训练有素的神经网络图像分割模型的准确率达到 92%,表明该方法能够准确评估混合结构中纤维的位置。空间点模式分析结果表明,混纺值与纱线和复合材料的特性之间存在相关性。所提出的方法为评估混合结构提供了一种快速可靠的方法,可用作质量控制和工艺优化的工具。
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引用次数: 0
Enhanced Electrical Conductivity of Graphene-Incorporated Copper Wire and its Performances on Coaxial Cable Application at Sub 6 GHz 增强石墨烯包裹铜线的导电性及其在 6 千兆赫以下同轴电缆应用中的性能
Pub Date : 2024-03-27 DOI: 10.4028/p-vy3zb7
Yi Chun Jin, Han Chang Pan, Shih Hong Chen
Intensive global research is focused on advanced conductive materials to meet the electrical requirements of the telecommunication and power industry. The primary aim is to enhance electrical conductivity, resulting of improved current-carrying capacity and reduced energy loss during transmission. Copper and its composites are vital for power transmission and telecommunications due to their electrical, thermal, and mechanical qualities. However, current methods have drawbacks, such as compromised conductivity with alloying. Graphene, an extraordinary carbon allotrope with exceptional properties and high conductivity, offers promising opportunities for the development of superior materials; such as graphene-incorporated copper (GrCu). The incorporation of graphene into copper wire holds significant potential for various industries, including electronics, energy transmission, and telecommunications, where high conductivity and reliability are paramount. This study investigates GrCu characteristics through mixing graphene and copper, vacuum melting, fine copper wire drawing, and GrCu coaxial cable manufacturing. Graphene infusion enhances conductivity and mechanical properties, altering microstructure and inducing twin boundaries in copper grains. Graphene's disruption during wire drawing triggers this effect, elevating wire conductivity to 103.5% by IACS. GrCu coaxial cable demonstrates performance coherence with HFSS simulation up to 6 GHz. Graphene's inclusion offers tailored material properties. Ongoing research promises further optimization and advancement of graphene-copper composites, paving the way for novel technological progress.
全球正在集中精力研究先进的导电材料,以满足电信和电力行业的电气要求。主要目的是增强导电性,从而提高载流能力,减少传输过程中的能量损耗。铜及其复合材料因其电气、热和机械特性,对电力传输和电信至关重要。然而,目前的方法存在一些缺点,例如合金化会影响导电性。石墨烯是一种非凡的碳同素异形体,具有优异的性能和高导电性,为开发优质材料(如石墨烯结合铜(GrCu))提供了良好的机遇。在铜线中加入石墨烯为电子、能源传输和电信等对高导电性和可靠性要求极高的各行各业带来了巨大的发展潜力。本研究通过石墨烯与铜的混合、真空熔炼、精细铜线拉伸和 GrCu 同轴电缆制造,对 GrCu 的特性进行了研究。石墨烯注入可增强导电性和机械性能,改变微观结构并在铜晶粒中形成孪生边界。在拉丝过程中,石墨烯的扰动触发了这一效应,通过 IACS 将线缆导电率提高到 103.5%。GrCu 同轴电缆与 HFSS 仿真的性能一致性高达 6 GHz。石墨烯的加入提供了量身定制的材料特性。正在进行的研究有望进一步优化和提高石墨烯-铜复合材料的性能,为新的技术进步铺平道路。
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引用次数: 0
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