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Effect of Fiber Weight Ratio and Fiber Modification on Flexural Properties of Posidonia-Polyester Composites 纤维重量比和纤维改性对波希多尼-聚酯复合材料抗弯性能的影响
Pub Date : 2016-07-01 DOI: 10.4236/OJCM.2016.63007
S. Zannen, Lassaad Ghali, M. Halimi, M. Hassen
The main objective of this research is to study the effect of fiber weight ratio and chemical fiber modification on flexural properties of composites reinforced with Posidonia fiber. An unsaturated polyester matrix reinforced with untreated and treated Posidonia fibers was fabricated under various fiber weight ratios. Results showed that the combined chemical treatment provided better mechanical properties of composites in comparison with untreated fiber. The fiber weight ratio influenced the flexural properties of composites. Indeed, a maximum value of flexural modulus was observed for 10% fiber weight ratio for composites reinforced with treated fibers. SEM photographs revealed a different fracture surface between Posidonia fibers reinforced polyester composites.
本研究的主要目的是研究纤维重量比和化学纤维改性对波西多尼纤维增强复合材料抗弯性能的影响。在不同的纤维重量比下,制备了未经处理和处理的波西多尼亚纤维增强的不饱和聚酯基体。结果表明,复合化学处理使复合材料的力学性能优于未经处理的纤维。纤维重量比影响复合材料的弯曲性能。事实上,当处理过的纤维增强复合材料的纤维重量比为10%时,其弯曲模量达到最大值。扫描电镜照片显示,Posidonia纤维增强聚酯复合材料之间的断裂表面不同。
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引用次数: 10
Experimental Investigation of the Impact of Compression on the Petro-Physical and Micromechanical Properties of Wellbore Cement Containing Salt 压缩对含盐井眼水泥岩石物理和微观力学性能影响的实验研究
Pub Date : 2016-07-01 DOI: 10.4236/OJCM.2016.63006
A. Oyibo, M. Radonjic
In this study, we investigated the effect of compression on the micromechanical and the petro- physical properties of salted wellbore cement systems. The experiments were conducted using a customized bench scale model, which utilized an expandable tubulars simulating the compression of a previously cemented casing under field-like conditions. The “mini-wellbore model” sample consisted of a pipe inside pipe assembly with a cemented annulus. The cement samples were cured in a water bath for 28 days prior to the compression experiments to allow adequate hydration. The impact of compression on the cement’s petro-physical and mechanical properties was quantified by measuring the porosity, permeability and hardness of salt cement cores drilled parallel to the orientation of the pipe from the compacted cement sheath. Permeability (Core-flood) experiments were conducted at 21℃, 10,342 kPa confining pressure for a period of 120 minutes. During the core-flood experiments, conducted using Pulse-decay method, deionized water was flowed through cement cores to determine the permeability of the cores. The results obtained from these experiments confirmed that the compression of the cement positively impacted the cements ability to provide long term zonal isolation, shown by the effective reduction in porosity and permeability. Furthermore, the results confirm reduction in the detrimental effect of salt on the strength and stiffness in post-compression cement.
在本研究中,我们研究了压缩对盐井筒水泥体系微观力学和石油物理性质的影响。实验采用定制的台式模型进行,该模型利用可膨胀管模拟在类似现场条件下之前固井套管的压缩。“迷你井眼模型”样品由一根管内管组合组成,环空为胶结环空。在压缩实验之前,将水泥样品在水浴中固化28天,以使其充分水化。压缩对水泥的岩石物理和力学性能的影响是通过测量从压实水泥环平行于管柱方向钻取的盐水泥岩心的孔隙度、渗透率和硬度来量化的。渗透率(岩心-注水)实验在21℃、10342 kPa围压条件下进行,持续120分钟。在岩心驱替实验中,采用脉冲衰减法,将去离子水流过水泥岩心,以确定岩心的渗透率。这些实验的结果证实,水泥的压缩对水泥提供长期层间隔离的能力有积极的影响,这可以通过有效降低孔隙度和渗透率来证明。此外,研究结果证实了盐对后压缩水泥强度和刚度的不利影响。
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引用次数: 1
Out of Plane Thermal Conductivity of Carbon Fiber Reinforced Composite Filled with Diamond Powder 金刚石粉填充碳纤维增强复合材料的面外导热性能
Pub Date : 2016-04-06 DOI: 10.4236/OJCM.2016.62005
M. Srinivasan, P. Maettig, K. Glitza, B. Sanny, A. Schumacher, M. Duhovic, J. Schuster
Highly conductive fillers have a strong influence on improving the poor out of plane thermal conductivity of carbon fiber reinforced composites. The objective of this study has been to investigate the role of the diamond powder (DP) in enhancing the out-of-plane thermal conductivity of the woven composites. Samples of the standard modulus T300 carbon fiber composite with 44% and 55% fiber volume fraction and the high modulus YS90A carbon fiber composite with 50% volume fraction were fabricated with their matrices comprising of neat epoxy and different loading of diamond powder within epoxy resin. Steady state thermal conductivity measurements were carried out and it was found from the measurements that the out of plane thermal conductivity of the standard modulus composite increased by a factor of 2.3 with 14% volume fraction of diamond powder in the composite while the out of plane thermal conductivity of the high modulus composite increased by a factor of 2.8 with 12% volume fraction of diamond powder in the composite. Finite Element Modeling (FEM) with the incorporation of microstructural characteristics is presented and good consistency between the measurements and FEM results were observed.
高导电性填料对改善碳纤维增强复合材料的面外导热性能有重要作用。本研究的目的是研究金刚石粉(DP)在提高机织复合材料的面外导热性能中的作用。制备了纤维体积分数为44%和55%的标准模量T300型碳纤维复合材料和50%体积分数的高模量YS90A型碳纤维复合材料,其基体为纯环氧树脂和环氧树脂内不同载荷的金刚石粉。对稳态导热系数进行了测量,结果表明,当金刚石粉的体积分数为14%时,标准模量复合材料的面外导热系数增加了2.3倍;当金刚石粉的体积分数为12%时,高模量复合材料的面外导热系数增加了2.8倍。提出了结合微观结构特征的有限元模拟方法,结果与有限元模拟结果吻合较好。
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引用次数: 9
On the Impact of Manufacturing Uncertainty in Structural Health Monitoring of Composite Structures: A Signal to Noise Weighted Neural Network Process 复合材料结构健康监测中制造不确定性的影响:一种信噪加权神经网络处理方法
Pub Date : 2016-01-22 DOI: 10.4236/OJCM.2016.61004
H. Teimouri, A. Milani, R. Seethaler, A. Heidarzadeh
This article investigates the potential impact of manufacturing uncertainty in composite structures here in the form of thickness variation in laminate plies, on the robustness of commonly used Artificial Neural Networks (ANN) in Structural Health Monitoring (SHM). Namely, the robustness of an ANN SHM system is assessed through an airfoil case study based on the sensitivity of delamination location and size predictions, when the ANN is imposed to noisy input. In light of the observed poor performance of the original network, even when its architecture was carefully optimized, it had been proposed to weigh the input layer of the ANN by a set of signal-to-noise (SN) ratios and then trained the network. Both damage location and size predictions of the latter SHM approach were increased to above 90%. Practical aspects of the proposed robust SN-ANN SHM have also been discussed.
本文研究了复合材料结构中制造不确定性对结构健康监测(SHM)中常用的人工神经网络(ANN)鲁棒性的潜在影响,即层压层厚度变化。也就是说,通过一个基于分层位置和尺寸预测敏感性的机翼型案例研究,当人工神经网络被施加到噪声输入时,评估了一个人工神经网络SHM系统的鲁棒性。鉴于观察到原始网络的性能较差,即使对其结构进行了精心优化,也有人提出通过一组信噪比对人工神经网络的输入层进行加权,然后对网络进行训练。后一种方法的损伤位置和尺寸预测均提高到90%以上。本文还讨论了所提出的稳健SN-ANN SHM的实际方面。
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引用次数: 12
The Thermal and Crystallization Studies of Luffa Fiber Reinforced Poly Lactic Acid Composites 丝瓜纤维增强聚乳酸复合材料的热晶化研究
Pub Date : 2016-01-01 DOI: 10.4236/OJCM.2016.61001
C. Parida, S. K. Dash, P. Chaterjee
Poly lactic acid (PLA)—chemically treated fiber of Luffa cylindrica (LC) composites were fabricated by micro-compounding followed by injection molding method. Before reinforcement, LC fibers were exposed to chemical treatment like alkali treatment, bleaching and acid hydrolysis. The chemically treated LC fibers were then modified with Ca salts to explore their uses in bio medical industries. Thermal stability of chemically extracted cellulose fibers of LC and PLA composites reinforced with 2 wt%, 5 wt% and 10 wt% LC fibers were studied by thermo gravimetric analysis (TGA) in the temperature range from 30℃ to 700℃. Better interfacial bonding between fiber and matrix was evidenced by increased thermal stability of composites due to incorporation of fiber. Crystallization and melting behavior of PLA composites were studied in the temperature range from 30℃ to 170℃ at heating rate of 10°/minute. The crystallization temperature and crystallization enthalpy increased up to 2 wt% of LC fiber content and gradually decreased with further increase of fiber content in the composites. Double melting peaks were observed for all composite samples and possible explanations were suggested on the basis of different crystalline structure of PLA and melt crystallization phenomena.
采用微复配后注射成型的方法制备了聚乳酸-化学处理的丝瓜复合材料。增强前,LC纤维经过碱处理、漂白、酸水解等化学处理。然后用Ca盐对经过化学处理的LC纤维进行改性,以探索其在生物医学工业中的应用。采用热重分析(TGA)研究了2 wt%、5 wt%和10 wt% LC纤维增强LC和PLA复合材料的热稳定性,温度范围为30 ~ 700℃。纤维的加入使复合材料的热稳定性得到提高,表明纤维与基体之间的界面结合更好。在30 ~ 170℃的温度范围内,以10°/min的升温速率研究了PLA复合材料的结晶和熔融行为。结晶温度和结晶焓在LC纤维含量为2 wt%时升高,随着纤维含量的进一步增加而逐渐降低。所有复合材料样品均出现双熔融峰,并根据PLA不同的晶体结构和熔融结晶现象提出了可能的解释。
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引用次数: 9
3D Printing of Continuous Carbon Fibre Reinforced Thermo-Plastic (CFRTP) Tensile Test Specimens 连续碳纤维增强热塑性塑料(CFRTP)拉伸试样的3D打印
Pub Date : 2016-01-01 DOI: 10.4236/OJCM.2016.61003
F. V. D. Klift, Y. Koga, A. Todoroki, M. Ueda, Y. Hirano, R. Matsuzaki
A study was conducted to evaluate the current production capabilities of the Mark One® 3D printer in printing carbon fibre reinforced thermoplastic (CFRTP) tensile test specimens according to the JIS K 7073 by making use of fused deposition modelling. Several different types of CFRTP tensile test specimens are printed and are tensile tested in the longitudinal direction to obtain an overview of the mechanical properties of 3D printed CFRTP material. These properties are compared with the literature values known for composite materials to see if these agree. The main goal of this research is to increase the knowledge of the 3D printing process of CFRTP and to later use this knowledge to further improve the 3D printing process to obtain stronger 3D printed CFRTP materials.
根据JIS K 7073,通过使用熔融沉积建模,对Mark One®3D打印机打印碳纤维增强热塑性塑料(CFRTP)拉伸试件的当前生产能力进行了评估。打印几种不同类型的CFRTP拉伸试样,并在纵向上进行拉伸测试,以获得3D打印CFRTP材料的力学性能概述。将这些性能与已知复合材料的文献值进行比较,看看它们是否一致。本研究的主要目标是增加对CFRTP 3D打印工艺的了解,并在以后使用这些知识进一步改进3D打印工艺,以获得更强的3D打印CFRTP材料。
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引用次数: 404
Longitudinal Compressive Failure of Multiple-Fiber Model Composites for a Unidirectional Carbon Fiber Reinforced Plastic 单向碳纤维增强塑料多纤维模型复合材料纵向压缩破坏研究
Pub Date : 2016-01-01 DOI: 10.4236/OJCM.2016.61002
T. Jeong, M. Ueda
The longitudinal compressive failure of a unidirectional carbon fiber reinforced plastic (CFRP) was studied using multiple-fiber model composites. Aligned carbon fibers were embedded in an epoxy matrix and put on a rectangular beam. A compression test of the model composite was performed by means of a four point bending test of the rectangular beam. The number of carbon fibers was changed from one to several thousands, by which the effect on compressive failure modes was investigated. A compressive failure of a single-fiber model composite was fiber crush. The fiber crush strain was much higher than the compressive failure strain of the unidirectional carbon fiber reinforced plastic. By contrast, a compressive failure of a multiple-fiber model composite was kink-band. The longitudinal compressive failure mechanism shifted from fiber crush to kink-band due to an increasing number of fibers. Kink-band parameters i.e. kink-band angle and kink-band width were dependent on the number of closely-aligned carbon fibers.
采用多纤维模型复合材料对单向碳纤维增强塑料(CFRP)纵向压缩破坏进行了研究。排列整齐的碳纤维被嵌在环氧树脂基体中,并置于矩形梁上。通过矩形梁的四点弯曲试验,对模型复合材料进行了压缩试验。将碳纤维的数量从1根增加到数千根,研究了碳纤维对压缩破坏模式的影响。单纤维模型复合材料的压缩破坏是纤维粉碎。纤维的破碎应变远高于单向碳纤维增强塑料的压缩破坏应变。而多纤维模型复合材料的压缩破坏表现为扭结带。随着纤维数量的增加,纵向压缩破坏机制由纤维压碎向扭结带转变。扭结带参数,即扭结带角和扭结带宽度取决于紧密排列的碳纤维的数量。
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引用次数: 4
Supercapacitor Consisting of a Form Core Sandwich with Woven Carbon Fiber Skin 由编织碳纤维外壳构成的芯芯夹层超级电容器
Pub Date : 2015-09-16 DOI: 10.4236/OJCM.2015.54013
A. Todoroki, Tomohiro Sawada, Y. Mizutani, Yoshiro Suzuki
Structural capacitors are composite structures that function as energy storage capacitors. Parallel plate-type capacitors have the advantage of high voltage resistance, but are limited by low capacitance. An electric double-layer capacitor with a composite structure using a solid polymer electrolyte matrix with a glass fiber fabric separator has recently been developed. However, the solid polymer electrolyte caused the capacitor to possess high internal resistance. In the present study, a new design of supercapacitor using a form core sandwich with high water retention is proposed and experimentally investigated. Activated carbon sheets are used as electrodes on the form core sandwich to make a supercapacitor. Woven carbon fabric is used as lead wires of the supercapacitor. The resulting supercapacitor displays a low surface resistance of 810 Ωcm2 and high areal capacitance of 520 mF/cm2.
结构电容器是一种具有储能功能的复合结构电容器。并联板型电容器具有耐高压的优点,但受低电容的限制。本文研制了一种以固体聚合物电解质为基体,以玻璃纤维织物为分离器的复合结构双电层电容器。然而,固体聚合物电解质使电容器具有较高的内阻。本文提出了一种新型的高保水型芯夹芯超级电容器的设计方案,并进行了实验研究。活性炭片被用作芯芯夹层上的电极来制造超级电容器。编织碳织物用作超级电容器的引线。由此产生的超级电容器显示出810 Ωcm2的低表面电阻和520 mF/cm2的高面电容。
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引用次数: 1
Controllable Crack Propagation in Off-Axis Crushing of Stitched Composite Absorbers 缝接复合材料吸波器离轴破碎中的可控裂纹扩展
Pub Date : 2015-09-16 DOI: 10.4236/OJCM.2015.54012
N. Ghafari-Namini, H. Ghasemnejad
Crack growth resistance plays a different role in crashworthiness analysis since the progressive energy absorption is based on controllable fracture mechanisms. In this regard, the present paper studies the efficient crack growth resistance in off-axis crushing of composite tubular structures by implementing natural fiber yarns. One of the through-to-thickness reinforcement methods known as stitching has been chosen to influence the axial and off-axis crushing process. Improving the crack growth resistance and appropriate fiber breakage at different stages of crushing process can significantly improve the resistance force and consequently the energy absorption capability of composite absorbers in axial and off-axis crushing. This analysis will be applied to non-stitched and stitched CFRP composite boxes which showed brittle fracture and transverse shearing crushing modes under off-axis loading of 10 degrees. The analytical methods are also implemented to analysze the effect of various failure mechanisms such as bending, friction, bundle fracture, and interlaminar crack growth for the observed crushing modes. The proposed model is able to predict the crushing load and crush force efficiency in close agreement from experimental studies.
由于渐进式能量吸收是基于可控断裂机制,裂纹扩展阻力在耐撞性分析中起着不同的作用。为此,本文采用天然纤维纱对复合材料管状结构的离轴破碎进行了有效的抗裂纹扩展研究。其中一种通过厚度的加固方法被称为拼接,以影响轴向和离轴破碎过程。在破碎过程的不同阶段提高抗裂纹扩展能力和适当的纤维断裂,可以显著提高复合材料在轴向和离轴破碎中的阻力,从而提高复合材料的吸能能力。该分析将应用于CFRP复合材料箱体在10度离轴载荷作用下表现为脆性断裂和横向剪切破碎模式的非缝合和缝合CFRP复合材料箱体。采用分析方法分析了弯曲、摩擦、束状断裂和层间裂纹扩展等破坏机制对观察到的破碎模式的影响。该模型能较好地预测破碎载荷和破碎力效率,与实验结果吻合较好。
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引用次数: 0
Physico-Mechanical Properties of Luffa aegyptiaca Fiber Reinforced Polymer Matrix Composite 埃及丝瓜纤维增强聚合物基复合材料的物理力学性能
Pub Date : 2015-09-16 DOI: 10.4236/OJCM.2015.54014
S. I. Ichetaonye, I. Madufor, M. Yibowei, D. N. Ichetaonye
This paper presents the study of moisture content, hardness, bulk density, apparent porosity, tensile and flexural characteristics of composite properties of Luffa aegyptiaca fiber. Luffa aegyptiaca reinforced epoxy composites have been developed by hand lay-up method with Luffa fiber untreated and treated conditions for 12 Hrs and 24 Hrs in different filler loading as in 2:1 ratio (5%, 10%, 15%, 20% and 25%). The effects of filler loading on the moisture content, hardness, bulk density, apparent porosity, tensile and flexural properties were studied. In general, the treated Luffa fibre composite for 24 Hrs showed better improvement properties via addition of modified Luffa fibre as reinforcement. However, tensile and flexural properties improved continuously with increasing filler loading up to 20% but decreasing at 25% due to weak interfacial bonding for both untreated and treated composite. The favourable results were obtained at 20% for treated composite at 24 Hrs especially at tensile and flexural characteristics and are suitable for mechanical applications.
本文研究了埃及丝瓜纤维复合性能的含水率、硬度、容重、表观孔隙率、拉伸和弯曲特性。采用手铺法制备了埃及丝瓜增强环氧复合材料,丝瓜纤维未经处理,填料配比为2:1(5%、10%、15%、20%和25%),处理时间分别为12小时和24小时。研究了填料载荷对材料含水率、硬度、容重、表观孔隙率、拉伸和弯曲性能的影响。总的来说,添加改性丝瓜纤维作为增强剂,处理24h后的丝瓜纤维复合材料的性能得到了更好的改善。然而,随着填料加载量的增加,拉伸和弯曲性能持续改善,但在25%时,由于未处理和处理的复合材料界面粘合较弱,拉伸和弯曲性能下降。处理后的复合材料在24小时内获得了20%的良好结果,特别是在拉伸和弯曲特性方面,适用于机械应用。
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引用次数: 17
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复合材料期刊(英文)
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