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Enhanced fracture toughness of additively manufactured Ti-6Al-4V ELI 增材制备Ti-6Al-4V ELI的断裂韧性增强
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-27 DOI: 10.1007/s10704-025-00863-1
Saurabh Kumar Gupta, Pranjal Singh, Kaushik Chatterjee, Satyam Suwas

This study investigates the enhancement of fracture toughness in Ti-6Al-4V ELI, fabricated via laser powder bed fusion (LPBF), through a tailored cyclic heat treatment applied below the β-transus temperature to transform the martensitic microstructure into a bimodal configuration. Fracture toughness experiments were conducted using fatigue pre-cracked four-point bend specimens at room temperature, evaluating two orientations in additively manufactured (AM), heat-treated (HT) and wrought (WR) conditions. The findings reveal that stress-relieved AM samples demonstrated good ductility without compromising strength in uniaxial tension tests. However, they exhibited poor fracture toughness and pronounced anisotropy in crack initiation along directions parallel and perpendicular to the build orientation. This behavior is attributed to the (text{Widmanst}ddot{text{a}}text{tten}) microstructure and residual prior (upbeta ) grain boundaries. The cyclic heat treatment significantly enhanced fracture toughness in both orientations. This improvement is attributed to the larger colony size and higher initial strain hardening rate observed in the HT condition, achieving fracture toughness values comparable to wrought Ti-6Al-4V ELI. Fractographic analysis identified void-sheeting as the primary deformation mechanism governing crack propagation across all conditions. EBSD analysis further revealed that hard crystallographic orientations hindered crack initiation and propagation in HT samples. Additionally, ET1 twinning activity near the crack tip played a critical role in improving fracture toughness by blunting the crack tip and limiting its progression. This study offers valuable insights into the microstructural determinants of fracture toughness in additively manufactured Ti-6Al-4V ELI and underscores the potential of strategic heat treatments to achieve mechanical properties comparable to those of wrought materials.

本研究研究了通过激光粉末床熔合(LPBF)制造的Ti-6Al-4V ELI,通过低于β-横截面温度的定制循环热处理,将马氏体组织转变为双峰结构,从而提高断裂韧性。在室温下,使用疲劳预裂四点弯曲试样进行断裂韧性实验,评估了增材制造(AM)、热处理(HT)和变形(WR)条件下的两种取向。研究结果表明,应力释放的AM样品在单轴拉伸试验中表现出良好的延展性,而不影响强度。然而,它们表现出较差的断裂韧性和明显的各向异性沿平行和垂直于构建方向的裂纹起裂。这种行为归因于(text{Widmanst}ddot{text{a}}text{tten})微观结构和残留的(upbeta )晶界。循环热处理显著提高了两个方向的断裂韧性。这种改善是由于在高温条件下观察到更大的菌落尺寸和更高的初始应变硬化率,达到与变形Ti-6Al-4V ELI相当的断裂韧性值。断口分析表明,在所有条件下,空洞片化是控制裂纹扩展的主要变形机制。EBSD分析进一步表明,高温试样中坚硬的晶体取向阻碍了裂纹的萌生和扩展。此外,裂纹尖端附近的ET1孪晶活动通过钝化裂纹尖端并限制其扩展,在提高断裂韧性方面发挥了关键作用。这项研究为增材制造Ti-6Al-4V ELI断裂韧性的微观结构决定因素提供了有价值的见解,并强调了战略热处理的潜力,以实现与变形材料相当的机械性能。
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引用次数: 0
Revisiting Dynamic Fracture in PMMA: The Interplay Between Local and Global Methods 重新审视PMMA的动态断裂:局部和全局方法之间的相互作用
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-27 DOI: 10.1007/s10704-025-00865-z
Vincent Fournier, Jérémie Girardot, Jean-Benoit Kopp

Polymethyl methacrylate (PMMA) is a benchmark brittle material for dynamic crack propagation studies. Despite extensive research, significant inconsistencies persist in reported fracture parameter values, complicating the establishment of a consensus on their sensitivity to the cracking regime. This study aims to rigorously determine these properties while identifying the origins of these discrepancies. To minimize microbranching effects that can strongly influence fracture surface roughness, crack propagation was restricted to subcritical velocities using a strip-band-specimen (SBS) geometry and a dedicated experimental setup. This approach ensured a quasi-steady propagation regime with minimal inertial effects. Dynamic toughness was evaluated using resistance curves constructed from Williams series expansion and displacement fields obtained via digital image correlation (DIC). Fracture energy was assessed through two complementary methods: a global energy balance and an indirect analytical approach based on Irwin’s generalized relation. Two distinct propagation regimes were identified: a stable regime (90 – 180 (hbox {m}.hbox {s}^{-1})) with smooth fracture surfaces and an unstable regime (180 – 320 (hbox {m}.hbox {s}^{-1})) characterized by the emergence of conical microstructures, followed by a transition to fully disrupted propagation beyond 320 (hbox {m}.hbox {s}^{-1}), marking the onset of microbranches. A key outcome of this study is the validation of global fracture energy estimation through the local approach, and vice versa, allowing the derivation of one fracture property from the other – an unprecedented achievement for PMMA in dynamic crack propagation. This was made possible by the experimental setup and specimen geometry, which effectively minimized parasitic effects such as inertia and microbranching. Additionally, the findings confirm a strong correlation between surface roughness and the evolution of fracture energy from the earliest stages of dynamic propagation.

聚甲基丙烯酸甲酯(PMMA)是动态裂纹扩展研究的基准脆性材料。尽管进行了广泛的研究,但报道的断裂参数值仍然存在显著的不一致性,这使得它们对开裂状态的敏感性的共识的建立变得复杂。本研究旨在严格确定这些属性,同时确定这些差异的起源。为了最大限度地减少可能严重影响断裂表面粗糙度的微分支效应,使用带状带试样(SBS)几何形状和专用实验装置将裂纹扩展限制在亚临界速度。这种方法保证了准稳定的传播状态,并具有最小的惯性效应。利用Williams级数展开和数字图像相关(DIC)得到的位移场构建的阻力曲线对材料的动态韧性进行了评价。通过整体能量平衡和基于Irwin广义关系的间接分析两种互补的方法来评估裂缝能量。发现了两种不同的扩展状态:稳定状态(90 - 180 (hbox {m}.hbox {s}^{-1})),具有光滑的断裂表面;不稳定状态(180 - 320 (hbox {m}.hbox {s}^{-1})),其特征是出现圆锥形微观结构,随后过渡到完全中断的扩展,超过320 (hbox {m}.hbox {s}^{-1}),标志着微分支的开始。本研究的一个关键成果是通过局部方法验证了全局断裂能估计,反之亦然,允许从一种断裂性质推导另一种断裂性质- PMMA在动态裂纹扩展方面取得了前所未有的成就。这是通过实验设置和标本几何结构实现的,有效地减少了寄生效应,如惯性和微分支。此外,研究结果证实了表面粗糙度与动态扩展早期断裂能的演变之间存在很强的相关性。
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引用次数: 0
Phase-field modeling of fracture via homogenization 均匀化裂缝相场模拟
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-18 DOI: 10.1007/s10704-025-00861-3
Gerard Villalta, Alex Ferrer, Fermin Otero

This study presents a novel phase-field modeling approach for brittle fracture that incorporates computational homogenization techniques to characterize the microstructural degradation of the material. Traditional phase-field models often implement degradation and dissipation functions in terms of the phase-field variable that, despite offering satisfactory results, their physical interpretation and their extension to anisotropic fracture behavior is not always clear. To address this challenge, we develop a framework inspired by the nucleation, growth, and coalescence of microstructural voids to model macroscopic fracture. The proposed approach employs homogenization techniques to calculate the effective material properties when introducing voids of varying sizes and shapes. By solving the homogenization problem for different void geometries, we obtain degradation functions that relate the size of microstructural voids to the homogenized constitutive tensor. These degradation functions provide a direct link between microscale damage mechanisms and macroscale fracture behavior. Comparative analyses with conventional AT1 and AT2 models reveal strong correlations between their response and those obtained via homogenization techniques. This relationship highlights the ability of homogenized models to not only replicate established results but also provide a new understanding of the phase-field variable.

本研究提出了一种新的脆性断裂相场建模方法,该方法结合了计算均匀化技术来表征材料的微观结构退化。传统的相场模型通常采用相场变量的退化和耗散函数,尽管给出了令人满意的结果,但它们的物理解释及其对各向异性断裂行为的推广并不总是很清楚。为了应对这一挑战,我们开发了一个受微观结构孔隙成核、生长和聚并启发的框架来模拟宏观断裂。所提出的方法采用均质化技术来计算引入不同尺寸和形状的空隙时的有效材料性能。通过求解不同孔洞几何形状的均质化问题,得到了微观结构孔洞尺寸与均质化本构张量之间的退化函数。这些退化函数提供了微观尺度损伤机制和宏观尺度断裂行为之间的直接联系。与传统的AT1和AT2模型的比较分析表明,它们的响应与通过均质技术获得的响应之间存在很强的相关性。这种关系突出了均质化模型不仅能够复制已建立的结果,而且还提供了对相场变量的新理解。
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引用次数: 0
Tensile fracture initiation and propagation of granite and gneiss at wedge splitting tests: Part 1—Effect of notch type on tensile crack initiation and fracture mechanics results 楔形劈裂试验中花岗岩和片麻岩的拉伸裂纹萌生和扩展:第1部分:缺口类型对拉伸裂纹萌生和断裂力学结果的影响
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-16 DOI: 10.1007/s10704-025-00857-z
Lars Jacobsson, Johan Sandström, Linus Brander, Mathias Flansbjer

Wedge splitting tests were conducted on a granite and a gneiss with similar mineralogy but different microstructure. The basic properties of the two rock types were characterized by petrographic analyses and mechanical tests. The granite specimens were split in one material direction, perpendicular to the rift plane, and the gneiss specimens were split in three different material directions, parallel and perpendicular to the foliation (and along and across a lineation). The effect of having a large blunt versus a sharp notch on the crack initiation was studied in the granite. The wedge splitting tests are unconventional for testing rocks and allowed to study the crack initiation and propagation under mode I loading condition in the quasi-brittle granite and brittle gneiss. The fracture energy and strain energy release rate were calculated. The strain energy release rate for gneiss, when splitting along and across the foliation, was around 45% and 60% of the values for the structurally isotropic granite. The fracture toughness was calculated from the strain energy release rate and was larger than corresponding values obtained from linear elastic fracture mechanics (LEFM). There was an effect on the early cracking stages by using a sharp notch compared with using a large blunt notch on the granite specimens, but the required largest force to split the specimens remained the same for the two notch types. The crack initiation started at a splitting force corresponding to 78% and 90% of the maximum splitting force on the specimens with a sharp notch and a large blunt notch, respectively. The results with a full force-displacement response during the crack propagation obtained for the brittle gneiss are unique. Most fracture mechanics results on rock materials are obtained from standard tests and LEFM and not via the measured strain energy release rate.

对矿物学相似但微观结构不同的花岗岩和片麻岩进行了楔形劈裂试验。通过岩石学分析和力学试验对两种岩石的基本性质进行了表征。花岗岩在垂直于裂谷面的一个物质方向上分裂,片麻岩在平行于和垂直于片理的三个不同物质方向上分裂(沿着和穿过一条线理)。在花岗岩中,研究了大钝口和尖口对裂纹起裂的影响。楔形劈裂试验是一种非常规的岩石试验方法,可用于研究准脆性花岗岩和脆质片麻岩在I型加载条件下的裂纹萌生和扩展。计算了断裂能和应变能释放率。片麻岩沿片理和跨片理分裂时的应变能释放率约为结构各向同性花岗岩的45%和60%。断裂韧性是根据应变能释放率计算得出的,它比线弹性断裂力学(LEFM)的相应值要大。在花岗岩试样上使用锋利的缺口与使用大钝的缺口对早期开裂阶段有影响,但两种缺口类型劈裂试样所需的最大力保持相同。裂纹萌生的劈裂力分别相当于有尖锐缺口和较大钝缺口试样最大劈裂力的78%和90%。在脆片麻岩裂纹扩展过程中获得了完整的力-位移响应,这是唯一的结果。大多数岩石材料的断裂力学结果是通过标准试验和LEFM得到的,而不是通过测量的应变能释放率得到的。
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引用次数: 0
Strain based finite fracture mechanics for fatigue life prediction of additively manufactured samples 基于应变的有限断裂力学增材试样疲劳寿命预测
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-12 DOI: 10.1007/s10704-025-00855-1
A. M. Mirzaei, A. H. Mirzaei, A. Sapora, P. Cornetti

A novel failure criterion, named Strain-based Finite Fracture Mechanics, is proposed to predict the fatigue life of additively manufactured notched components under uniaxial loading conditions. The model relies on the simultaneous fulfillment of two conditions: a non-local strain requirement and the discrete energy balance. The inputs of the model are strain and the stress intensity factor at failure, which depend on the number of cycles according to power law equations. The inputs can be obtained based on strain-life and stress intensity factor-life data from plain and notched specimens. The present approach is comprehensively validated against experimental datasets on additively manufactured samples from the literature for different materials, raster angles, notch geometries and loading conditions. Predictions by other approaches, such as Finite Fracture Mechanics (in its original stress formulation) and the Theory of Critical Distances, are also considered, for the sake of completeness. Results show that, in general, the proposed strain-based model is more accurate and provides consistently precise predictions across different cases.

提出了一种基于应变的有限断裂力学准则,用于预测单轴加载条件下增材制造缺口构件的疲劳寿命。该模型依赖于同时满足两个条件:非局部应变要求和离散能量平衡。模型的输入是应变和破坏时的应力强度因子,它们根据幂律方程取决于循环次数。输入可以根据平原和缺口试样的应变寿命和应力强度因子寿命数据获得。本文针对文献中不同材料、光栅角度、缺口几何形状和加载条件的增材制造样品的实验数据集进行了全面验证。为了完整起见,还考虑了其他方法的预测,例如有限断裂力学(在其原始应力公式中)和临界距离理论。结果表明,总体而言,提出的基于菌株的模型更准确,并且在不同的病例中提供一致的精确预测。
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引用次数: 0
Identifying simple shear in plane stress states 识别平面应力状态下的简单剪切
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-10 DOI: 10.1007/s10704-025-00856-0
Lilia Schuster, Sebastian Münstermann

Modern phenomenological damage models use Lode parameter L and triaxiality (eta ) to describe the stress state of an isotropic material. Value pairs in the region between (L, eta = (0, 0)) and (L, eta = (0, frac{1}{sqrt{3}})) in plane stress condition can lead to ambiguous descriptions of the deformation. The case of simple shear is not defined separately. By using the difference in angles between the principal strain and principal stress axes, cases of coaxial stretch superposed with simple shear can be distinguished from cases of coaxial stretch without simple shear. In the case of anisotropic material or large elements, the distinction between these ambiguous cases can be utilized to optimize failure models. This study proposes a method to recover the deformation gradient and shear direction for proportional and non-proportional loading with an elastoplastic von Mises material. The deformation gradient is suitable for distinguishing stress states with simple shear from stress states without simple shear in plane stress condition.

现代现象学损伤模型使用Lode参数L和三轴性(eta )来描述各向同性材料的应力状态。平面应力条件下(L, eta = (0, 0))和(L, eta = (0, frac{1}{sqrt{3}}))之间区域的值对可能导致变形描述不明确。单剪情况没有单独定义。利用主应变轴与主应力轴夹角之差,可以区分单纯剪切叠加的共轴拉伸与单纯剪切叠加的共轴拉伸。在各向异性材料或大单元的情况下,可以利用这些模糊情况之间的区别来优化失效模型。本研究提出了一种恢复von Mises弹塑性材料在比例和非比例加载下的变形梯度和剪切方向的方法。在平面应力条件下,变形梯度适用于区分有单剪和无单剪的应力状态。
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引用次数: 0
Stress intensity factor determination along a kinked crack path by DIC analyses 弯曲裂纹路径应力强度因子的DIC分析
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-10 DOI: 10.1007/s10704-025-00862-2
T. Corre, F. Hild, V. Lazarus

Sharp kinks may be observed under shear loading or in materials containing weak directions, such as those produced by additive manufacturing. A better understanding of the fracture of these materials, both theoretically and experimentally, is required to deploy them in structural applications. This study focuses on the measurement of stress intensity factors (SIFs) around a sharp kink using digital image correlation (DIC). The performances of two DIC-based techniques, namely, integrated-DIC and post-processing of DIC-measured displacement fields, are assessed on a benchmark test using fused deposit modeling capabilities, and are compared to a reference finite element solution. It is shown that Williams’ expansion remains valid on a large enough region around the crack to extract reliable SIFs even very close to the crack kink. Both techniques are very trustworthy, provided the SIF identification zone is carefully defined to exclude the kink zone of influence.

在剪切载荷下或在含有弱方向的材料中,例如通过增材制造生产的材料中,可以观察到尖锐的扭结。在理论和实验上更好地理解这些材料的断裂,需要在结构应用中部署它们。本研究的重点是使用数字图像相关(DIC)测量尖锐扭结周围的应力强度因子(SIFs)。基于dic的两种技术,即集成dic和dic测量位移场的后处理,在使用熔融沉积建模能力的基准测试中进行了评估,并与参考有限元解决方案进行了比较。结果表明,Williams展开在裂纹周围足够大的区域内仍然有效,即使非常接近裂纹扭结,也可以提取可靠的SIFs。如果仔细定义SIF识别区以排除扭结影响区,这两种技术都是非常值得信赖的。
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引用次数: 0
Fatigue life prediction method based on polynomial chaotic expansion and Weibull distribution 基于多项式混沌展开和威布尔分布的疲劳寿命预测方法
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-05 DOI: 10.1007/s10704-025-00858-y
GaoFei Ji, LingHui Hu

This study proposes a fatigue life prediction method combining small-sample data expansion with the Weibull distribution function, incorporating the first order reliability factor (FOSM) to improve accuracy. Using Generalized Polynomial Chaos Expansion (GPC) and Latin Hypercube Sampling (LHS), small-sample fatigue data is expanded, followed by enhancing the two-parameter Weibull model with FOSM. Results show the generalized polynomial chaotic expansion method and Latin hypercube sampling are used to obtain the probability density curve when the stress level is 350 MPa, and the original data are all on this probability density curve, indicating that the expansion method is more credible. High prediction precision within a 1.5 × error range, with logarithmic safety life linearly related to stress level and decreasing with higher failure probability.

本文提出了一种将小样本数据展开与威布尔分布函数相结合的疲劳寿命预测方法,并引入一阶可靠性因子(FOSM)来提高预测精度。采用广义多项式混沌展开(GPC)和拉丁超立方体采样(LHS)对小样本疲劳数据进行扩展,然后用FOSM对双参数威布尔模型进行增强。结果表明:采用广义多项式混沌展开法和拉丁超立方采样法得到应力水平为350 MPa时的概率密度曲线,原始数据均在该概率密度曲线上,表明展开法更可靠。在1.5 ×误差范围内具有较高的预测精度,安全寿命与应力水平呈对数线性相关,随着失效概率的增大而减小。
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引用次数: 0
Simulation of ductile failure of a notched-tension specimen of 3D printed 316L stainless steel 3D打印316L不锈钢缺口拉伸试样延性破坏模拟
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-05-28 DOI: 10.1007/s10704-025-00851-5
Jianing Xie, Krishnaswamy Ravi-Chandar

The rapid development of 3D printing of 316L stainless steel thin-walled structures obtained by direct energy deposition has generated an increased interest in the mechanical properties of such materials for use in applications; in particular, failure models are needed to ensure structural reliability. We consider the response of uniaxial tension specimens, with and without notches, to characterize the constitutive and failure behavior of the material. Specifically, we use numerical simulations of the notched tension experiment, achieved with a simple power-law strain hardening model and a failure criterion based on attaining a triaxiality-dependent critical strain-to-failure, to demonstrate that this model is capable of reproducing the material behavior accurately.

通过直接能量沉积获得的316L不锈钢薄壁结构的3D打印的快速发展使人们对此类材料的机械性能产生了越来越大的兴趣。特别是,为了保证结构的可靠性,需要建立失效模型。我们考虑单轴拉伸试样的响应,有和没有缺口,表征材料的本构和破坏行为。具体来说,我们使用了缺口拉伸实验的数值模拟,通过简单的幂律应变硬化模型和基于获得三轴相关临界应变到失效的破坏准则来实现,以证明该模型能够准确地再现材料的行为。
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引用次数: 0
Peridynamics based model of anticrack-type fracture in brittle foams 基于周动力学的脆性泡沫抗裂纹型断裂模型
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-05-28 DOI: 10.1007/s10704-025-00860-4
Shucheta Shegufta, Michael Zaiser

A particular failure mode of highly porous brittle materials consists in the propagation of cracks under uniaxial compressive loads. Such ’anticracks’ have been observed in a range of materials, from snow and porous sandstone to brittle foams. Here we present a computational model for the formation and propagation of anticrack-type failure in porous materials within the general computational framework of bond-based peridynamics. Random porosity is represented, on a scale well above the characteristic pore size, by random bond deletion (dilution disorder). We apply our framework to experimental data on anticrack propagation in silicate foams.

高孔隙脆性材料的一种特殊破坏模式是在单轴压缩载荷作用下裂纹的扩展。从雪、多孔砂岩到脆性泡沫,在一系列材料中都观察到了这种“裂缝”。在这里,我们提出了一个基于键基周动力学的通用计算框架下多孔材料抗裂纹型破坏的形成和扩展的计算模型。随机孔隙率在远高于特征孔径的尺度上由随机键缺失(稀释紊乱)表示。我们将该框架应用于硅酸盐泡沫中裂纹扩展的实验数据。
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引用次数: 0
期刊
International Journal of Fracture
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