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Cohesive behavior of single crystalline silicon carbide scribing by nanosecond laser 纳秒激光刻划单晶碳化硅的内聚行为
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-22 DOI: 10.1007/s10704-024-00801-7
Pei Chen, Shaowei Li, Rui Pan, Senyu Tu, Fei Qin

The existing mechanical dicing process of single crystalline Silicon Carbide (SiC) is one of the main factors limiting the development of semiconductor process, which could be replaced by laser scribing potentially. To achieve efficient and low-damage SiC separation, the cracking behavior of SiC after laser grooving should be well understood and controllable. Since the laser grooving including thermal ablation and meltage solidification, the cracking behavior of the scribed SiC would be different to the original single crystal SiC. In this paper, cohesive zone model (CZM) is used to quantitively represent the cracking behavior of the nano-laser scribed SiC. The separation after scribing was conducted in a three-point bending (3 PB) fixture to characterize the cracking behavior. Therefore, by inverting the load–displacement curves of 3 PB with CZM embedded finite element model, the cohesive behavior is characterized by bilinear traction–separation law, which illustrated the whole cracking process numerically. The methodology established in current paper gives way to understand the SiC scribing and cracking process with quantitative cohesive parameters.

现有的单晶碳化硅(SiC)机械切割工艺是限制半导体工艺发展的主要因素之一,而激光划槽有可能取代这一工艺。为实现高效、低损伤的碳化硅分离,应充分了解和控制激光划槽后碳化硅的开裂行为。由于激光划槽包括热烧蚀和熔融凝固,因此划线后的碳化硅的开裂行为将不同于原始单晶碳化硅。本文采用内聚区模型(CZM)来定量表示纳米激光划线碳化硅的开裂行为。划线后的分离在三点弯曲(3 PB)夹具中进行,以表征开裂行为。因此,通过用 CZM 嵌入式有限元模型反演三点弯曲的载荷-位移曲线,用双线性牵引-分离定律来表征内聚行为,从而用数值说明了整个开裂过程。本文所建立的方法有助于理解具有定量内聚参数的 SiC 划线和开裂过程。
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引用次数: 0
Construction of Kitagawa–Takahashi diagrams as a function of applied stress ratio 根据外加应力比绘制北川高桥图
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-13 DOI: 10.1007/s10704-024-00800-8
R. Sunder

Construction of the Kitagawa–Takahashi (K–T) diagram requires inputs of two material properties, namely, endurance limit and threshold stress intensity range, ΔKth. Both are sensitive to applied stress ratio. The effect of stress ratio on endurance limit is well known. Unfortunately, crack closure, associated with the nature of conventional testing practice obscures the effect of stress ratio on intrinsic, closure free ΔKth that would apply to natural crack like defects and short cracks. This study was made possible by the development of a new test method to characterize closure free threshold conditions under controlled near-tip residual stress conditions that essentially determine near-tip stress ratio at threshold. A procedure is described to construct the K–T diagram, using ΔKth values corrected for stress ratio and applicable to pre-existing defects and short cracks at notches that are unlikely to see closure. As a case study, a K–T diagram valid for different applied stress ratios is constructed for titanium alloy Ti-6Al-4V.

构建北川-高桥(K-T)图需要输入两个材料属性,即耐久极限和阈值应力强度范围 ΔKth。这两项属性对应用应力比都很敏感。应力比对耐久极限的影响众所周知。遗憾的是,与传统测试实践性质相关的裂纹闭合问题掩盖了应力比对本征无闭合 ΔKth 的影响,而这种影响适用于自然裂纹(如缺陷和短裂纹)。这项研究之所以能够进行,是因为开发了一种新的测试方法,可以在受控的近端残余应力条件下表征无闭合阈值条件,基本上确定了阈值处的近端应力比。本文介绍了构建 K-T 图的程序,该程序使用根据应力比校正的 ΔKth 值,适用于缺口处不太可能出现闭合的预先存在的缺陷和短裂纹。作为案例研究,为钛合金 Ti-6Al-4V 绘制了不同应用应力比下有效的 K-T 图。
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引用次数: 0
The tearing energy threshold of crack growth in rubber exposed to ozone: an experimental–numerical approach 暴露于臭氧中的橡胶裂纹生长的撕裂能量阈值:一种实验-数值方法
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-13 DOI: 10.1007/s10704-024-00799-y
Ondřej Peter, Martin Stěnička, Gert Heinrich, Christopher G. Robertson, Jakub Pawlas, Radek Stoček, Jan Ondrík

The global rubber industry is seeking alternatives to the widely-used antiozonant, N-(1,3-dimethylbutyl)-N′-phenyl-p-phenylenediamine (6PPD), due to its environmental toxicity concerns when used in automobile tires. These substantial research and development efforts on new antiozonants for rubber are hindered by a general inability to characterize the fundamental physical parameter of ozone-induced tearing energy threshold for crack growth, which underlies the practical ozone resistance of rubber products. Therefore, this paper presents, for the first time, a novel experimental–numerical combined approach to determine the tearing energy threshold in rubber exposed to ozone, which is a key criterion for assessing the resistance of rubber to ozone crack growth. The approach is based on in-situ optical analysis of ozone crack growth on the rubber surface and the determination of the crack growth rate when the rubber is stretched. Subsequently, the growth rates form the basis for calculating the energy release rates at the crack tips using the finite element method in Ansys software. By comparing the calculated energy release rates and experimentally measured crack growth rates, the energy release rate interval corresponding to the threshold tearing energy is determined. Based on this approach, the tearing energy threshold for carbon black reinforced natural rubber exposed to ozone was found to be a maximum of 2.12 J/m2. This value is 96% lower than the threshold for the non-ozone-exposed specimens. In conclusion, this novel methodology was able to determine the ozone threshold tearing energy and represents a powerful, unique tool for an efficient future development of environmentally friendly antiozonants.

全球橡胶工业正在寻找广泛使用的抗臭氧剂N-(1,3-二甲基丁基)-N ' -苯基-对苯二胺(6PPD)的替代品,因为它在汽车轮胎中使用时存在环境毒性问题。橡胶抗臭氧剂的大量研究和开发工作受到阻碍,因为人们普遍无法确定臭氧引起的裂缝生长的撕裂能量阈值的基本物理参数,这是橡胶产品实际抗臭氧性的基础。因此,本文首次提出了一种新的实验-数值相结合的方法来确定橡胶在臭氧作用下的撕裂能阈值,这是评估橡胶抗臭氧裂纹扩展能力的关键标准。该方法是基于橡胶表面臭氧裂纹扩展的原位光学分析和橡胶拉伸时裂纹扩展速率的测定。随后,利用Ansys软件中的有限元法计算裂纹尖端的能量释放率,以此作为扩展速率的基础。通过计算的能量释放率与实验测量的裂纹扩展率的比较,确定了阈值撕裂能对应的能量释放率区间。基于该方法,炭黑增强天然橡胶在臭氧作用下的撕裂能阈值最大值为2.12 J/m2。该值比非臭氧暴露标本的阈值低96%。总之,这种新方法能够确定臭氧阈值撕裂能量,为未来高效开发环境友好型抗臭氧剂提供了强大而独特的工具。
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引用次数: 0
Integrating atomistics and experiments in gaining deeper insights into fatigue crack propagation in silver 将原子学与实验相结合,深入了解银的疲劳裂纹扩展过程
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-12 DOI: 10.1007/s10704-024-00796-1
Yinan Xie, Xiaoli Hao, Zumin Wang, Yuan Huang

This research utilizes both single crystal and polycrystalline models to probe the fatigue crack propagation mechanism in pure silver via molecular dynamics (MD) simulations. A comprehensive validation approach at both micro and macro scales, incorporating transmission electron microscopy (TEM), electron backscatter diffraction (EBSD), and compact tension (CT) specimen fatigue testing, is developed to verify the reliability of simulation models and results. Simulation findings indicate that the initial crack orientation significantly influences crack propagation. As the crack advances within the crystal, two primary crack propagation mechanisms are discerned: (1) nano-voids appear at the crack tip, and the crack propagates by continuously aggregating with the nano-voids ahead; (2) the formation of Stair-rod dislocations and V-shape stacking faults due to dislocation reactions and slip band movements impedes crack propagation, accompanied by the dislocation reaction of Shockley partial dislocations ((tfrac{1}{6}) <112>) generating Hirth dislocations ((tfrac{1}{6}) <110>). The dislocation reaction is verified through the dislocation analysis of the crack tip area of the CT specimen after fatigue experiment by using TEM. In addition, the results of this study show that the angle between the direction of crack propagation and the grain boundary affects the fatigue crack propagation, e.g. when the angle is less than 60°, the crack rapidly propagates along the grain boundary. The orientation distribution function (ODF) results of EBSD can verify that the polycrystalline model containing 30 grains is a reliable model for the MD simulation of behavior of the crack tip of CT specimen. Lastly, the Paris law constants for pure silver are determined as m = 3.72 and lg C = − 10.77, providing a reference for the fatigue analysis and life prediction of silver components or silver soldering pots in engineering applications.

本研究利用单晶和多晶模型,通过分子动力学(MD)模拟探究纯银的疲劳裂纹扩展机制。研究开发了一种微观和宏观尺度的综合验证方法,结合了透射电子显微镜(TEM)、电子反向散射衍射(EBSD)和紧密拉伸(CT)试样疲劳测试,以验证模拟模型和结果的可靠性。模拟结果表明,初始裂纹取向对裂纹扩展有很大影响。随着裂纹在晶体内的扩展,可发现两种主要的裂纹扩展机制:(1) 在裂纹尖端出现纳米空洞,裂纹通过不断与前方的纳米空洞聚集而扩展;(2)由于位错反应和滑移带运动形成的Stair-rod位错和V形堆叠断层阻碍了裂纹的扩展,同时伴随着Shockley部分位错的位错反应((tfrac{1}{6} <112>)产生了Hirth位错((tfrac{1}{6} <110>)。通过使用 TEM 对疲劳实验后 CT 试样的裂纹尖端区域进行位错分析,验证了位错反应。此外,研究结果表明,裂纹扩展方向与晶界之间的夹角会影响疲劳裂纹的扩展,例如当夹角小于 60°时,裂纹会沿着晶界迅速扩展。EBSD 的取向分布函数(ODF)结果可以验证包含 30 个晶粒的多晶模型是对 CT 试样裂纹尖端行为进行 MD 模拟的可靠模型。最后,确定了纯银的帕里斯定律常数为 m = 3.72 和 lg C = - 10.77,为工程应用中银元件或银焊锅的疲劳分析和寿命预测提供了参考。
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引用次数: 0
Enhanced solid element model with embedded strong discontinuity for representation of mesoscale quasi-brittle failure 用于表示中尺度准脆性破坏的嵌入式强不连续性增强型固体元素模型
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-05 DOI: 10.1007/s10704-024-00797-0
Matej Šodan, Andjelka Stanić, Mijo Nikolić

This article presents a novel two-dimensional quadrilateral solid finite element model, enhanced by incompatible modes and embedded strong discontinuity for simulation of localized failure in quasi-brittle heterogeneous multi-phase materials. The focus of interest lies in the development of discontinuities and cracks induced by both tensile and compressive loads, considering mesoscale material constituents and very complex meshes. Multiple cracks are initiated within elements using local Gauss-point criteria for crack initiation. Rankine and Maximum shear stress criteria control the crack initiation, location, and orientation depending solely on the stress state within the finite element. The model identifies distinct clusters of cracked elements and merges them into continuous cracks. A tracking algorithm ensures crack continuity, eliminating spurious cracks ahead of the crack tip to prevent crack arrest and stress locking. This approach ensures the formation of various types of cracks within the constituents of composite materials and their spontaneous coalescence forming the final failure mechanisms. The constitutive model for the crack representation is the damage softening model, which accounts for opening and sliding behavior. The efficacy of the proposed model is demonstrated through numerical simulations of heterogeneous 3-phase and 4-phase composites subjected to both tensile and compressive load cases.

本文提出了一种新的二维四边形实体有限元模型,该模型通过不相容模态和嵌入强不连续增强,用于模拟准脆性非均质多相材料的局部破坏。考虑到中尺度材料成分和非常复杂的网格,关注的焦点在于由拉伸和压缩载荷引起的不连续和裂纹的发展。采用局部高斯点裂纹萌生准则,在单元内萌生多个裂纹。朗肯和最大剪切应力准则控制裂纹的萌生、位置和方向,这完全取决于有限元中的应力状态。该模型识别出不同的裂纹单元簇,并将它们合并为连续的裂纹。跟踪算法确保裂纹连续性,在裂纹尖端之前消除虚假裂纹,防止裂纹止裂和应力锁定。这种方法保证了复合材料成分中各种类型裂纹的形成和它们的自发合并形成最终的破坏机制。裂纹表示的本构模型为损伤软化模型,考虑了开裂和滑动行为。通过对非均相3相和4相复合材料在拉伸和压缩载荷下的数值模拟,验证了该模型的有效性。
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引用次数: 0
Microstructure based fatigue life prediction of polycrystalline materials using SFEM and CDM 利用 SFEM 和 CDM 基于微观结构预测多晶材料的疲劳寿命
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-29 DOI: 10.1007/s10704-024-00795-2
Deepak Sharma, I. V. Singh, Jalaj Kumar, Shahnawaz Ahmed

Accurate fatigue life prediction of polycrystalline materials is crucial for many engineering applications. In polycrystalline materials, a significant portion of life is spent in the crack nucleation phase at the microstructural scale. Hence, the total fatigue life shows high sensitivity to the local microstructure. To predict fatigue life accurately, the microstructure models of polycrystalline material i.e., titanium alloy are virtually generated with the help of the Voronoi tessellation technique. These models incorporate critical microstructural features such as grain size, grain shape, and the volume fraction of different phases within the material. To efficiently predict microstructure sensitive fatigue life, the smooth finite element method (SFEM) is coupled with continuum damage mechanics (CDM). The SFEM provides flexibility in the meshing of complex microstructure geometries as it alleviates the need to use only triangular and quadrilateral elements. Moreover, there is no need of isoparametric mapping and explicit form of shape function derivatives in SFEM, hence it requires less computation time. To obtain the fatigue life (in number of cycles), jump in cycles algorithm is implemented using SFEM-CDM. The numerical results of fatigue life data obtained from simulations are compared with experimental data, which reveals the validity of the present approach. This approach is useful to find out the scatter in fatigue life data of polycrystalline materials along with the source of scatter.

精确预测多晶材料的疲劳寿命对许多工程应用至关重要。在多晶材料中,很大一部分寿命是在微结构尺度的裂纹成核阶段度过的。因此,总疲劳寿命对局部微观结构非常敏感。为了准确预测疲劳寿命,我们利用 Voronoi 镶嵌技术虚拟生成了多晶材料(即钛合金)的微观结构模型。这些模型包含了关键的微观结构特征,如晶粒尺寸、晶粒形状和材料中不同相的体积分数。为了有效预测对微观结构敏感的疲劳寿命,平滑有限元法(SFEM)与连续损伤力学(CDM)相结合。SFEM 可以灵活地对复杂的微观结构几何形状进行网格划分,因为它无需只使用三角形和四边形元素。此外,SFEM 不需要等参数映射和明确的形状函数导数形式,因此计算时间更短。为了获得疲劳寿命(循环次数),使用 SFEM-CDM 实现了循环跳跃算法。模拟得到的疲劳寿命数值结果与实验数据进行了比较,结果表明本方法是有效的。这种方法有助于找出多晶材料疲劳寿命数据的散点以及散点的来源。
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引用次数: 0
The effect of crack orientation on the mode I fracture resistance of pinewood 裂纹走向对松木 I 型断裂抗力的影响
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-29 DOI: 10.1007/s10704-024-00798-z
Marek Romanowicz, Maciej Grygorczuk

The fracture resistance of pinewood under mode I loading is investigated experimentally for different crack plane orientations and the crack propagation direction parallel to longitudinal cells. Experiments are conducted on double cantilever beams using a digital image correlation system to evaluate the crack tip opening displacement. The compliance based beam method is used to determine the energy release rate at various crack lengths. The decomposition of crack propagation into the pre-peak and post-peak propagations is proposed to find the fracture energy contributions from individual toughening mechanisms in pinewood. The cohesive strengths measured in the experiments are confirmed by comparison with the tensile strengths obtained from separate tests performed on pinewood. An analytical model for evaluating the fracture process zone is used to validate the experimental results. The difference between the fracture energy values in different crack propagation systems is explained by using X-ray microtomography images of the fracture surfaces.

通过实验研究了松木在模式 I 载荷作用下的抗断裂性能,包括不同的裂纹平面方向和平行于纵向单元的裂纹扩展方向。使用数字图像相关系统对双悬臂梁进行了实验,以评估裂纹尖端张开位移。基于顺应性的梁法用于确定不同裂缝长度下的能量释放率。提出了将裂纹扩展分解为前峰和后峰扩展的方法,以找出松木中各个增韧机制的断裂能量贡献。实验中测得的内聚强度通过与松木单独测试获得的拉伸强度进行比较得到了证实。评估断裂过程区的分析模型用于验证实验结果。通过断裂表面的 X 射线显微层析成像,解释了不同裂纹扩展系统中断裂能量值之间的差异。
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引用次数: 0
Assessing the fracture toughness of Zircaloy-4 fuel rod cladding tubes: impact of delayed hydride cracking 评估 Zircaloy-4 燃料棒包壳管的断裂韧性:延迟氢化物裂纹的影响
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-17 DOI: 10.1007/s10704-024-00781-8
Pierrick François, Tom Petit, Quentin Auzoux, David Le Boulch, Isabela Zarpellon Nascimento, Jacques Besson

Delayed hydride cracking (DHC) is a hydrogen embrittlement phenomenon that may potentially occur in Zircaloy-4 fuel claddings during dry storage conditions. An experimental procedure has been developed to measure the toughness of this material in the presence of DHC by allowing crack propagation through the thickness of a fuel cladding. Notched C-ring specimens, charged with 100 wppm of hydrogen, were used and pre-cracked by brittle fracture of a hydrided zone at the notch root at room temperature. The length of the pre-crack was measured on the fracture surface or cross-sections. Additionally, a finite element model was developed to determine the stress intensity factor as a function of the crack length for a given loading. Two types of tests were conducted independently to determine the fracture toughness with and without DHC, (K_{I_text {DHC}}) and (K_{I_text {C}}), respectively: (i) constant load tests at 150 (^{circ })C, 200 (^{circ })C, and 250 (^{circ })C; (ii) monotonic tests at 25 (^{circ })C, 200 (^{circ })C, and 250 (^{circ })C. The results indicate the following: (1) there is no temperature influence on the DHC toughness of Zircaloy-4 between 150 and 250 (^{circ })C ((K_{I_text {DHC}} in left[ 7.2;9.2right] ) MPa(sqrt{text {m}})), (2) within this temperature range, the fracture toughness of Zircaloy-4 is halved by DHC ((K_{I_text {C}} in left[ 16.9;19.7 right] ) MPa(sqrt{text {m}})), (3) the crack propagation rate decreases with decreasing temperature and (4) the time before crack propagation increases as the temperature and loading decrease.

延迟氢化物开裂(DHC)是一种氢脆现象,在干燥储存条件下可能发生在锆合金-4 燃料包壳中。我们开发了一种实验程序,通过允许裂纹在燃料包层厚度上扩展来测量这种材料在出现 DHC 时的韧性。使用带凹口的 C 型环试样,充入 100 wppm 的氢气,在室温下通过在凹口根部的水化物区的脆性断裂预裂纹。在断裂表面或横截面上测量预裂纹的长度。此外,还开发了一个有限元模型,以确定在给定加载条件下应力强度因子与裂纹长度的函数关系。为了确定有 DHC 和无 DHC 时的断裂韧性,分别进行了两种类型的测试,即 (K_{I_text {DHC}}) 和 (K_{I_text {C}})(i) 150 C、200 C 和 250 C 的恒载试验;(ii) 25 C、200 C 和 250 C 的单调试验。结果表明(1) 在 150 和 250 (^{circ })C 之间,温度对 Zircaloy-4 的 DHC 韧性没有影响((K_{I_text {DHC}} in left[ 7.2;9.2right] ) MPa(sqrttext {m}})), (2) 在这个温度范围内,Zircaloy-4 的断裂韧性被 DHC 减半 ((K_{I_text {C}} in left[ 16.9;19.7(右))MPa((sqrttext {m}})),(3)裂纹扩展速率随温度的降低而降低,(4)裂纹扩展前的时间随温度和载荷的降低而增加。
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引用次数: 0
Introduction to the special issue on failure mechanism in advanced materials and structures 先进材料和结构的失效机理特刊简介
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-17 DOI: 10.1007/s10704-024-00793-4
Zengtao Chen, Minghao Zhao, Cunfa Gao, Efstathios Theotokoglou
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引用次数: 0
Fatigue crack growth behavior of a nickel-based superalloy under turbine standard spectrum loads 涡轮机标准频谱载荷下镍基超级合金的疲劳裂纹增长行为
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-17 DOI: 10.1007/s10704-024-00794-3
Sharanagouda G. Malipatil, N. Nagarajappa, Ramesh Bojja, N. Jagannathan, Anuradha N. Majila, D. Chandru Fernando, M. Manjuprasad, C. M. Manjunatha

In this investigation, the growth behavior of a crack in a nickel-based superalloy under a turbine standard load sequence was determined by experimental, analytical, and computational methods. In the first experimental approach, ASTM standard compact tension (CT) test specimens were fabricated and fatigue crack growth (FCG) tests were conducted in a universal test machine under cold-TURBISTAN, a turbine standard spectrum load sequence. In the second analytical method, after rain-flow cycle counting of the cold-TURBISTAN sequence, the crack growth was estimated for each counted cycle from the crack growth law. The accumulated crack extension for each block of loading was thus estimated to determine the FCG behavior. In the third computational approach, a CT specimen containing an initial crack was modeled and the FCG behavior was predicted under cold-TURBISTAN spectrum load sequence using FRANC3D. The FCG trend predicted by analytical and computational methods was almost similar to the observed experimental behavior. The predicted FCG life was conservative with a life ratio ranging from 0.9 to 0.95.

本研究通过实验、分析和计算方法确定了镍基超合金在涡轮机标准载荷序列下的裂纹生长行为。在第一种实验方法中,制作了 ASTM 标准紧凑拉伸(CT)试样,并在通用试验机中进行了涡轮机标准频谱载荷序列冷-湍流(cold-TURBISTAN)下的疲劳裂纹生长(FCG)试验。在第二种分析方法中,在对冷-TURBISTAN 序列进行雨流循环计数后,根据裂纹增长规律估算每个计数循环的裂纹增长。由此估算出每个加载块的累计裂纹扩展量,从而确定 FCG 行为。在第三种计算方法中,使用 FRANC3D 对包含初始裂纹的 CT 试样进行建模,并预测冷-TURBISTAN 频谱加载序列下的 FCG 行为。分析和计算方法预测的 FCG 趋势与观察到的实验行为几乎相似。预测的 FCG 寿命比较保守,寿命比在 0.9 至 0.95 之间。
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引用次数: 0
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International Journal of Fracture
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