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Cohesive behavior of single crystalline silicon carbide scribing by nanosecond laser 纳秒激光刻划单晶碳化硅的内聚行为
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-22 DOI: 10.1007/s10704-024-00801-7
Pei Chen, Shaowei Li, Rui Pan, Senyu Tu, Fei Qin

The existing mechanical dicing process of single crystalline Silicon Carbide (SiC) is one of the main factors limiting the development of semiconductor process, which could be replaced by laser scribing potentially. To achieve efficient and low-damage SiC separation, the cracking behavior of SiC after laser grooving should be well understood and controllable. Since the laser grooving including thermal ablation and meltage solidification, the cracking behavior of the scribed SiC would be different to the original single crystal SiC. In this paper, cohesive zone model (CZM) is used to quantitively represent the cracking behavior of the nano-laser scribed SiC. The separation after scribing was conducted in a three-point bending (3 PB) fixture to characterize the cracking behavior. Therefore, by inverting the load–displacement curves of 3 PB with CZM embedded finite element model, the cohesive behavior is characterized by bilinear traction–separation law, which illustrated the whole cracking process numerically. The methodology established in current paper gives way to understand the SiC scribing and cracking process with quantitative cohesive parameters.

现有的单晶碳化硅(SiC)机械切割工艺是限制半导体工艺发展的主要因素之一,而激光划槽有可能取代这一工艺。为实现高效、低损伤的碳化硅分离,应充分了解和控制激光划槽后碳化硅的开裂行为。由于激光划槽包括热烧蚀和熔融凝固,因此划线后的碳化硅的开裂行为将不同于原始单晶碳化硅。本文采用内聚区模型(CZM)来定量表示纳米激光划线碳化硅的开裂行为。划线后的分离在三点弯曲(3 PB)夹具中进行,以表征开裂行为。因此,通过用 CZM 嵌入式有限元模型反演三点弯曲的载荷-位移曲线,用双线性牵引-分离定律来表征内聚行为,从而用数值说明了整个开裂过程。本文所建立的方法有助于理解具有定量内聚参数的 SiC 划线和开裂过程。
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引用次数: 0
Construction of Kitagawa–Takahashi diagrams as a function of applied stress ratio 根据外加应力比绘制北川高桥图
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-13 DOI: 10.1007/s10704-024-00800-8
R. Sunder

Construction of the Kitagawa–Takahashi (K–T) diagram requires inputs of two material properties, namely, endurance limit and threshold stress intensity range, ΔKth. Both are sensitive to applied stress ratio. The effect of stress ratio on endurance limit is well known. Unfortunately, crack closure, associated with the nature of conventional testing practice obscures the effect of stress ratio on intrinsic, closure free ΔKth that would apply to natural crack like defects and short cracks. This study was made possible by the development of a new test method to characterize closure free threshold conditions under controlled near-tip residual stress conditions that essentially determine near-tip stress ratio at threshold. A procedure is described to construct the K–T diagram, using ΔKth values corrected for stress ratio and applicable to pre-existing defects and short cracks at notches that are unlikely to see closure. As a case study, a K–T diagram valid for different applied stress ratios is constructed for titanium alloy Ti-6Al-4V.

构建北川-高桥(K-T)图需要输入两个材料属性,即耐久极限和阈值应力强度范围 ΔKth。这两项属性对应用应力比都很敏感。应力比对耐久极限的影响众所周知。遗憾的是,与传统测试实践性质相关的裂纹闭合问题掩盖了应力比对本征无闭合 ΔKth 的影响,而这种影响适用于自然裂纹(如缺陷和短裂纹)。这项研究之所以能够进行,是因为开发了一种新的测试方法,可以在受控的近端残余应力条件下表征无闭合阈值条件,基本上确定了阈值处的近端应力比。本文介绍了构建 K-T 图的程序,该程序使用根据应力比校正的 ΔKth 值,适用于缺口处不太可能出现闭合的预先存在的缺陷和短裂纹。作为案例研究,为钛合金 Ti-6Al-4V 绘制了不同应用应力比下有效的 K-T 图。
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引用次数: 0
Integrating atomistics and experiments in gaining deeper insights into fatigue crack propagation in silver 将原子学与实验相结合,深入了解银的疲劳裂纹扩展过程
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-12 DOI: 10.1007/s10704-024-00796-1
Yinan Xie, Xiaoli Hao, Zumin Wang, Yuan Huang

This research utilizes both single crystal and polycrystalline models to probe the fatigue crack propagation mechanism in pure silver via molecular dynamics (MD) simulations. A comprehensive validation approach at both micro and macro scales, incorporating transmission electron microscopy (TEM), electron backscatter diffraction (EBSD), and compact tension (CT) specimen fatigue testing, is developed to verify the reliability of simulation models and results. Simulation findings indicate that the initial crack orientation significantly influences crack propagation. As the crack advances within the crystal, two primary crack propagation mechanisms are discerned: (1) nano-voids appear at the crack tip, and the crack propagates by continuously aggregating with the nano-voids ahead; (2) the formation of Stair-rod dislocations and V-shape stacking faults due to dislocation reactions and slip band movements impedes crack propagation, accompanied by the dislocation reaction of Shockley partial dislocations ((tfrac{1}{6}) <112>) generating Hirth dislocations ((tfrac{1}{6}) <110>). The dislocation reaction is verified through the dislocation analysis of the crack tip area of the CT specimen after fatigue experiment by using TEM. In addition, the results of this study show that the angle between the direction of crack propagation and the grain boundary affects the fatigue crack propagation, e.g. when the angle is less than 60°, the crack rapidly propagates along the grain boundary. The orientation distribution function (ODF) results of EBSD can verify that the polycrystalline model containing 30 grains is a reliable model for the MD simulation of behavior of the crack tip of CT specimen. Lastly, the Paris law constants for pure silver are determined as m = 3.72 and lg C = − 10.77, providing a reference for the fatigue analysis and life prediction of silver components or silver soldering pots in engineering applications.

本研究利用单晶和多晶模型,通过分子动力学(MD)模拟探究纯银的疲劳裂纹扩展机制。研究开发了一种微观和宏观尺度的综合验证方法,结合了透射电子显微镜(TEM)、电子反向散射衍射(EBSD)和紧密拉伸(CT)试样疲劳测试,以验证模拟模型和结果的可靠性。模拟结果表明,初始裂纹取向对裂纹扩展有很大影响。随着裂纹在晶体内的扩展,可发现两种主要的裂纹扩展机制:(1) 在裂纹尖端出现纳米空洞,裂纹通过不断与前方的纳米空洞聚集而扩展;(2)由于位错反应和滑移带运动形成的Stair-rod位错和V形堆叠断层阻碍了裂纹的扩展,同时伴随着Shockley部分位错的位错反应((tfrac{1}{6} <112>)产生了Hirth位错((tfrac{1}{6} <110>)。通过使用 TEM 对疲劳实验后 CT 试样的裂纹尖端区域进行位错分析,验证了位错反应。此外,研究结果表明,裂纹扩展方向与晶界之间的夹角会影响疲劳裂纹的扩展,例如当夹角小于 60°时,裂纹会沿着晶界迅速扩展。EBSD 的取向分布函数(ODF)结果可以验证包含 30 个晶粒的多晶模型是对 CT 试样裂纹尖端行为进行 MD 模拟的可靠模型。最后,确定了纯银的帕里斯定律常数为 m = 3.72 和 lg C = - 10.77,为工程应用中银元件或银焊锅的疲劳分析和寿命预测提供了参考。
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引用次数: 0
Microstructure based fatigue life prediction of polycrystalline materials using SFEM and CDM 利用 SFEM 和 CDM 基于微观结构预测多晶材料的疲劳寿命
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-29 DOI: 10.1007/s10704-024-00795-2
Deepak Sharma, I. V. Singh, Jalaj Kumar, Shahnawaz Ahmed

Accurate fatigue life prediction of polycrystalline materials is crucial for many engineering applications. In polycrystalline materials, a significant portion of life is spent in the crack nucleation phase at the microstructural scale. Hence, the total fatigue life shows high sensitivity to the local microstructure. To predict fatigue life accurately, the microstructure models of polycrystalline material i.e., titanium alloy are virtually generated with the help of the Voronoi tessellation technique. These models incorporate critical microstructural features such as grain size, grain shape, and the volume fraction of different phases within the material. To efficiently predict microstructure sensitive fatigue life, the smooth finite element method (SFEM) is coupled with continuum damage mechanics (CDM). The SFEM provides flexibility in the meshing of complex microstructure geometries as it alleviates the need to use only triangular and quadrilateral elements. Moreover, there is no need of isoparametric mapping and explicit form of shape function derivatives in SFEM, hence it requires less computation time. To obtain the fatigue life (in number of cycles), jump in cycles algorithm is implemented using SFEM-CDM. The numerical results of fatigue life data obtained from simulations are compared with experimental data, which reveals the validity of the present approach. This approach is useful to find out the scatter in fatigue life data of polycrystalline materials along with the source of scatter.

精确预测多晶材料的疲劳寿命对许多工程应用至关重要。在多晶材料中,很大一部分寿命是在微结构尺度的裂纹成核阶段度过的。因此,总疲劳寿命对局部微观结构非常敏感。为了准确预测疲劳寿命,我们利用 Voronoi 镶嵌技术虚拟生成了多晶材料(即钛合金)的微观结构模型。这些模型包含了关键的微观结构特征,如晶粒尺寸、晶粒形状和材料中不同相的体积分数。为了有效预测对微观结构敏感的疲劳寿命,平滑有限元法(SFEM)与连续损伤力学(CDM)相结合。SFEM 可以灵活地对复杂的微观结构几何形状进行网格划分,因为它无需只使用三角形和四边形元素。此外,SFEM 不需要等参数映射和明确的形状函数导数形式,因此计算时间更短。为了获得疲劳寿命(循环次数),使用 SFEM-CDM 实现了循环跳跃算法。模拟得到的疲劳寿命数值结果与实验数据进行了比较,结果表明本方法是有效的。这种方法有助于找出多晶材料疲劳寿命数据的散点以及散点的来源。
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引用次数: 0
The effect of crack orientation on the mode I fracture resistance of pinewood 裂纹走向对松木 I 型断裂抗力的影响
IF 2.5 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-29 DOI: 10.1007/s10704-024-00798-z
Marek Romanowicz, Maciej Grygorczuk

The fracture resistance of pinewood under mode I loading is investigated experimentally for different crack plane orientations and the crack propagation direction parallel to longitudinal cells. Experiments are conducted on double cantilever beams using a digital image correlation system to evaluate the crack tip opening displacement. The compliance based beam method is used to determine the energy release rate at various crack lengths. The decomposition of crack propagation into the pre-peak and post-peak propagations is proposed to find the fracture energy contributions from individual toughening mechanisms in pinewood. The cohesive strengths measured in the experiments are confirmed by comparison with the tensile strengths obtained from separate tests performed on pinewood. An analytical model for evaluating the fracture process zone is used to validate the experimental results. The difference between the fracture energy values in different crack propagation systems is explained by using X-ray microtomography images of the fracture surfaces.

通过实验研究了松木在模式 I 载荷作用下的抗断裂性能,包括不同的裂纹平面方向和平行于纵向单元的裂纹扩展方向。使用数字图像相关系统对双悬臂梁进行了实验,以评估裂纹尖端张开位移。基于顺应性的梁法用于确定不同裂缝长度下的能量释放率。提出了将裂纹扩展分解为前峰和后峰扩展的方法,以找出松木中各个增韧机制的断裂能量贡献。实验中测得的内聚强度通过与松木单独测试获得的拉伸强度进行比较得到了证实。评估断裂过程区的分析模型用于验证实验结果。通过断裂表面的 X 射线显微层析成像,解释了不同裂纹扩展系统中断裂能量值之间的差异。
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引用次数: 0
Assessing the fracture toughness of Zircaloy-4 fuel rod cladding tubes: impact of delayed hydride cracking 评估 Zircaloy-4 燃料棒包壳管的断裂韧性:延迟氢化物裂纹的影响
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-17 DOI: 10.1007/s10704-024-00781-8
Pierrick François, Tom Petit, Quentin Auzoux, David Le Boulch, Isabela Zarpellon Nascimento, Jacques Besson

Delayed hydride cracking (DHC) is a hydrogen embrittlement phenomenon that may potentially occur in Zircaloy-4 fuel claddings during dry storage conditions. An experimental procedure has been developed to measure the toughness of this material in the presence of DHC by allowing crack propagation through the thickness of a fuel cladding. Notched C-ring specimens, charged with 100 wppm of hydrogen, were used and pre-cracked by brittle fracture of a hydrided zone at the notch root at room temperature. The length of the pre-crack was measured on the fracture surface or cross-sections. Additionally, a finite element model was developed to determine the stress intensity factor as a function of the crack length for a given loading. Two types of tests were conducted independently to determine the fracture toughness with and without DHC, (K_{I_text {DHC}}) and (K_{I_text {C}}), respectively: (i) constant load tests at 150 (^{circ })C, 200 (^{circ })C, and 250 (^{circ })C; (ii) monotonic tests at 25 (^{circ })C, 200 (^{circ })C, and 250 (^{circ })C. The results indicate the following: (1) there is no temperature influence on the DHC toughness of Zircaloy-4 between 150 and 250 (^{circ })C ((K_{I_text {DHC}} in left[ 7.2;9.2right] ) MPa(sqrt{text {m}})), (2) within this temperature range, the fracture toughness of Zircaloy-4 is halved by DHC ((K_{I_text {C}} in left[ 16.9;19.7 right] ) MPa(sqrt{text {m}})), (3) the crack propagation rate decreases with decreasing temperature and (4) the time before crack propagation increases as the temperature and loading decrease.

延迟氢化物开裂(DHC)是一种氢脆现象,在干燥储存条件下可能发生在锆合金-4 燃料包壳中。我们开发了一种实验程序,通过允许裂纹在燃料包层厚度上扩展来测量这种材料在出现 DHC 时的韧性。使用带凹口的 C 型环试样,充入 100 wppm 的氢气,在室温下通过在凹口根部的水化物区的脆性断裂预裂纹。在断裂表面或横截面上测量预裂纹的长度。此外,还开发了一个有限元模型,以确定在给定加载条件下应力强度因子与裂纹长度的函数关系。为了确定有 DHC 和无 DHC 时的断裂韧性,分别进行了两种类型的测试,即 (K_{I_text {DHC}}) 和 (K_{I_text {C}})(i) 150 C、200 C 和 250 C 的恒载试验;(ii) 25 C、200 C 和 250 C 的单调试验。结果表明(1) 在 150 和 250 (^{circ })C 之间,温度对 Zircaloy-4 的 DHC 韧性没有影响((K_{I_text {DHC}} in left[ 7.2;9.2right] ) MPa(sqrttext {m}})), (2) 在这个温度范围内,Zircaloy-4 的断裂韧性被 DHC 减半 ((K_{I_text {C}} in left[ 16.9;19.7(右))MPa((sqrttext {m}})),(3)裂纹扩展速率随温度的降低而降低,(4)裂纹扩展前的时间随温度和载荷的降低而增加。
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引用次数: 0
Introduction to the special issue on failure mechanism in advanced materials and structures 先进材料和结构的失效机理特刊简介
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-17 DOI: 10.1007/s10704-024-00793-4
Zengtao Chen, Minghao Zhao, Cunfa Gao, Efstathios Theotokoglou
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引用次数: 0
Fatigue crack growth behavior of a nickel-based superalloy under turbine standard spectrum loads 涡轮机标准频谱载荷下镍基超级合金的疲劳裂纹增长行为
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-17 DOI: 10.1007/s10704-024-00794-3
Sharanagouda G. Malipatil, N. Nagarajappa, Ramesh Bojja, N. Jagannathan, Anuradha N. Majila, D. Chandru Fernando, M. Manjuprasad, C. M. Manjunatha

In this investigation, the growth behavior of a crack in a nickel-based superalloy under a turbine standard load sequence was determined by experimental, analytical, and computational methods. In the first experimental approach, ASTM standard compact tension (CT) test specimens were fabricated and fatigue crack growth (FCG) tests were conducted in a universal test machine under cold-TURBISTAN, a turbine standard spectrum load sequence. In the second analytical method, after rain-flow cycle counting of the cold-TURBISTAN sequence, the crack growth was estimated for each counted cycle from the crack growth law. The accumulated crack extension for each block of loading was thus estimated to determine the FCG behavior. In the third computational approach, a CT specimen containing an initial crack was modeled and the FCG behavior was predicted under cold-TURBISTAN spectrum load sequence using FRANC3D. The FCG trend predicted by analytical and computational methods was almost similar to the observed experimental behavior. The predicted FCG life was conservative with a life ratio ranging from 0.9 to 0.95.

本研究通过实验、分析和计算方法确定了镍基超合金在涡轮机标准载荷序列下的裂纹生长行为。在第一种实验方法中,制作了 ASTM 标准紧凑拉伸(CT)试样,并在通用试验机中进行了涡轮机标准频谱载荷序列冷-湍流(cold-TURBISTAN)下的疲劳裂纹生长(FCG)试验。在第二种分析方法中,在对冷-TURBISTAN 序列进行雨流循环计数后,根据裂纹增长规律估算每个计数循环的裂纹增长。由此估算出每个加载块的累计裂纹扩展量,从而确定 FCG 行为。在第三种计算方法中,使用 FRANC3D 对包含初始裂纹的 CT 试样进行建模,并预测冷-TURBISTAN 频谱加载序列下的 FCG 行为。分析和计算方法预测的 FCG 趋势与观察到的实验行为几乎相似。预测的 FCG 寿命比较保守,寿命比在 0.9 至 0.95 之间。
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引用次数: 0
Boundary element method: cells with embedded discontinuity modeling the fracture process zone in 3D failure analysis 边界元法:在三维失效分析中用嵌入式不连续单元模拟断裂过程区
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-16 DOI: 10.1007/s10704-024-00785-4
A. P. Chaves, R. G. Peixoto, R. P. Silva

Damage and failure in quasi-brittle materials such as rocks, concrete, and ceramics, have a complex non-linear behavior due to their heterogeneous character and the development of a fracture process zone (FPZ), formed by micro-cracking around the tip of an induced or pre-existing flaw. A softening behavior is observed in the FPZ, and the linear elastic fracture mechanic (LEFM) cannot correctly reproduce the stress field ahead of the crack tip. The existence of the FPZ may be the intrinsic cause of the size effect. An appropriate modeling of this process zone is mandatory to reproduce accurately the failure propagation and consequently, the structural behavior. Different from most of the domain numerical techniques, the boundary element method (BEM) requires (besides the boundary division into elements) only the discretization of a small region where dissipative effects occur. Cells with embedded continuum strong discontinuity approach (CSDA), placed in the region where the crack is supposed to occur, are capable of capturing the transition of regimes in the failure zone. Numerical bifurcation analysis, based on the singularity of the localization tensor, is used to determine the end of the continuum regime. Weak and strong discontinuity regimes are associated with diffuse micro-cracks (strain discontinuity) and macro-crack (displacement discontinuity). A variable bandwidth model is used during the weak discontinuity regime to represent the advance of micro-cracks density and their coalescence. Continuum and discrete cohesive isotropic damage models are used to describe the softening behavior. Analysis of three-dimensional problems with single crack in standard and mixed fracture modes, using this transitional approach and the BEM cells is firstly presented in this work. Experimental reference results are used to attest the capability of the approach in reproducing the structural behavior during crack propagation. Some necessary advances required for its applications for general complex structural problems are pointed out.

岩石、混凝土和陶瓷等准脆性材料的损伤和破坏具有复杂的非线性行为,这是因为它们具有异质性,而且在诱发或预先存在的缺陷尖端周围会产生微裂纹,从而形成断裂加工区(FPZ)。在 FPZ 中可观察到软化行为,线性弹性断裂力学(LEFM)无法正确再现裂纹尖端前方的应力场。FPZ 的存在可能是尺寸效应的内在原因。为了准确再现失效扩展,进而再现结构行为,必须对这一过程区进行适当建模。与大多数域数值技术不同,边界元法(BEM)只需要对发生耗散效应的一小块区域进行离散化(除了将边界划分为单元外)。嵌入式连续体强不连续方法(CSDA)的单元被放置在裂纹应该出现的区域,能够捕捉到失效区的过渡状态。基于局部张量奇异性的数值分岔分析被用来确定连续状态的终点。弱不连续和强不连续状态与弥散微裂缝(应变不连续)和宏观裂缝(位移不连续)有关。在弱不连续状态下,使用可变带宽模型来表示微裂缝密度的增加及其凝聚。连续和离散内聚各向同性损伤模型用于描述软化行为。本研究首次采用这种过渡方法和 BEM 单元,分析了标准和混合断裂模式下单个裂缝的三维问题。实验参考结果证明了该方法在裂纹扩展过程中再现结构行为的能力。同时还指出了该方法应用于一般复杂结构问题所需的一些必要改进。
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引用次数: 0
Analysis of a cracked harmonic substrate under a rigid punch 刚性冲床下的谐波裂纹基板分析
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-05-13 DOI: 10.1007/s10704-024-00782-7
Hailiang Ma, Yueting Zhou, Xu Wang, Xing Li, Shenghu Ding

The study of the mechanical action between a punch and a cracked substrate has some theoretical guidance for the material protection. So the coupling problem of a cracked semi-infinite harmonic substrate under the action of a rigid flat punch is studied. The mixed boundary value problem is transformed into the Riemann-Hilbert boundary value problem by applying the complex-variable method, and then converted into singular integral equation for a numerical solution. The stress intensity factors at the contact ends and crack tips and the Piola stresses of whole harmonic material can be expressed as complex functions. The results indicate that the stressed state of harmonic solid near the crack tip and contact ends have similar features as those in linear elastic solids. The crack causes an obvious impact on the stress distributions near the contact region. The study provides theoretical guidance for analyzing the damaged problems of some soft materials under small deformation.

研究冲头与开裂基体之间的机械作用对材料保护具有一定的理论指导意义。因此研究了刚性平冲头作用下裂纹半无限调和基体的耦合问题。应用复变法将混合边界值问题转化为黎曼-希尔伯特边界值问题,然后转化为奇异积分方程进行数值求解。接触端和裂纹尖端的应力强度因子以及整个谐波材料的皮奥拉应力都可以用复变函数表示。结果表明,谐波固体在裂纹尖端和接触端附近的受力状态与线性弹性固体的受力状态具有相似的特征。裂纹对接触区附近的应力分布有明显的影响。该研究为分析一些软材料在小变形下的损坏问题提供了理论指导。
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引用次数: 0
期刊
International Journal of Fracture
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