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Hydrogen embrittlement properties of several stainless steels 几种不锈钢的氢脆特性
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-14 DOI: 10.1007/s10704-024-00809-z
Mitsuhiro Okayasu, Hisanobu Matsuura

The hydrogen embrittlement (HE) characteristics of various stainless steels were investigated. In this study, as-received, heated (1100 °C, 15 h), and cold-rolled (30% strain) γ-austenite (AS), α-ferrite (FS), α′-martensite (MS), and γα duplex (DS) stainless steels were employed. For as-received stainless steels, severe HE occurred for DS and MS with static tensile loading, while no clear and weak HE was observed for AS and FS, respectively. This could be attributed to the different extent of hydrogen diffusivity in the stainless steel. A large amount of hydrogen penetrated to (i) lattice vacancy with low atomic density for body-centered cubic FS, DS, and MS, compared to that for face-centered cubic (AS); (ii) the phase boundary between γ-austenite and α-ferrite for DS; and (iii) the boundary between the Cr base precipitate and the martensite matrix for MS. HE also occurred strongly for heated-DS owing to the grain growth, i.e., a high hydrogen concentration in grain and phase boundaries. Although no clear HE was detected in as-received AS with static loading, HE occurred in cold-rolled AS, where hydrogen penetrated lattice vacancies and α′-martensite formed through strain-induced martensite. Owing to strain-induced martensite created during cyclic loading, HE was detected even for as-received AS, which is dissimilar to the result of the tensile test. Details of HE characteristics of the strainless steels were examined using the four stainless steels with different microstructures, diferent strain level and oxide layer. Moreover, those were investigated under different loading conditions, such as constant, static, and cyclic loading.

研究了各种不锈钢的氢脆(HE)特性。这项研究采用了γ-奥氏体(AS)、α-铁素体(FS)、α′-马氏体(MS)和γ-α双相(DS)不锈钢的原样、加热(1100 °C,15 小时)和冷轧(30% 应变)。对于刚收到的不锈钢,DS 和 MS 在静态拉伸载荷下会出现严重的 HE,而 AS 和 FS 则分别没有观察到明显和微弱的 HE。这可能是由于氢在不锈钢中的扩散程度不同。与面心立方(AS)相比,大量氢渗透到:(i) 体心立方 FS、DS 和 MS 的低原子密度晶格空位;(ii) DS 的γ-奥氏体和 α-铁素体之间的相界;(iii) MS 的铬基沉淀和马氏体基体之间的边界。由于晶粒生长(即晶粒和相边界氢浓度较高),加热-DS 也发生了强烈的氢化反应。虽然在静态加载的未接收 AS 中未检测到明显的 HE,但在冷轧 AS 中却出现了 HE,氢渗透到晶格空位中,通过应变诱导马氏体形成了 α′-马氏体。由于在循环加载过程中产生了应变诱导马氏体,因此即使是成品 AS 也能检测到 HE,这与拉伸试验的结果不同。使用四种具有不同微观结构、不同应变水平和氧化层的不锈钢,对无应变钢的高热特性进行了详细研究。此外,还在恒定、静态和循环加载等不同加载条件下对这些特性进行了研究。
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引用次数: 0
A computational approach for phase-field model of quasi-brittle fracture under dynamic loading 动态加载下准脆性断裂相场模型的计算方法
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-05 DOI: 10.1007/s10704-024-00806-2
Roman Vodička

A computational model is formulated for studying dynamic crack propagation in quasi-brittle materials exposed to time-dependent loading conditions. Under such conditions, inertial effects of structural components play an important role in modelling crack propagation problems. The computational model is proposed within the theory of regularised cracks which uses a damage-like internal variable. Here, fracture considers phase-field damage which gives rise to a material degradation in a narrow material strip defining the regularised crack. Based on the energy formulation using the Lagrangian of the system, the proposed computational approach introduces a staggered scheme adopted to solve the coupled system and providing it in a variational form within the time stepping procedure. The numerical data are obtained by quadratic programming algorithms implemented together with a finite element code.

本研究建立了一个计算模型,用于研究准脆性材料在随时间变化的加载条件下的动态裂纹扩展。在这种条件下,结构部件的惯性效应在模拟裂纹扩展问题中发挥着重要作用。计算模型是在正则化裂纹理论中提出的,该理论使用了类似损伤的内部变量。在这里,断裂考虑了相场损伤,这种损伤会在定义规则化裂缝的窄材料带中引起材料退化。基于使用系统拉格朗日的能量公式,所提出的计算方法引入了一种交错方案,用于求解耦合系统,并在时间步进程序中以变分形式提供。数值数据通过与有限元代码一起实施的二次编程算法获得。
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引用次数: 0
Prediction of crack growth in polycrystalline XH73M nickel-based alloy at thermo-mechanical and isothermal fatigue loading 多晶 XH73M 镍基合金在热机械和等温疲劳加载条件下的裂纹生长预测
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-29 DOI: 10.1007/s10704-024-00807-1
Aleksandr Sulamanidze, Valery Shlyannikov, Dmitry Kosov

The importance of developing simple relationships for interpreting crack growth rate test results and a practical approach to predicting crack propagation under thermo-mechanical fatigue conditions based on readily available data is emphasised by many authors. In this study, a damage impact parameter was introduced to predict the crack growth rate and durability under isothermal and thermo-mechanical fatigue conditions. To validate the model, we used a single-edge notched specimen made of polycrystalline coarse-grained nickel-based alloy XH73M. The specimen was subjected to loading conditions that included in-phase and out-of-phase thermo-mechanical fatigue at a temperature range of 400–650 °C, as well as isothermal fatigue at 26 °C, 400 °C and 650 °C. A numerical analysis was used to simulate the material deformation behaviour at the crack tip according to a nonlinear kinematic hardening model. Numerical and experimental stress–strain state parameters based on strain energy density were used to formulate and estimate the damage impact parameter. Based on the correlation between the crack growth rate and the introduced damage impact parameter, a method for predicting crack propagation is proposed. The accuracy of the proposed method was experimentally validated.

许多学者都强调了建立简单关系来解释裂纹生长率测试结果的重要性,以及根据现成数据预测热机械疲劳条件下裂纹扩展的实用方法。在这项研究中,我们引入了一个损伤影响参数来预测等温和热机械疲劳条件下的裂纹生长率和耐久性。为了验证模型,我们使用了由多晶粗粒镍基合金 XH73M 制成的单边缺口试样。试样承受的加载条件包括 400-650 °C 温度范围内的相内和相外热机械疲劳,以及 26 °C、400 °C 和 650 °C 温度范围内的等温疲劳。数值分析根据非线性运动硬化模型模拟了裂纹尖端的材料变形行为。基于应变能密度的数值和实验应力应变状态参数被用于制定和估算损伤影响参数。根据裂纹增长率与引入的损伤冲击参数之间的相关性,提出了一种预测裂纹扩展的方法。实验验证了所提方法的准确性。
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引用次数: 0
Isogeometric multilayer thin-shell analysis of failure in composite structures with hygrothermal effects 具有湿热效应的复合材料结构失效的等时多层薄壳分析
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-27 DOI: 10.1007/s10704-024-00808-0
Weican Li, Hoang Nguyen, Yuri Bazilevs

We develop a computational framework to model damage and delamination in laminated polymer composite structures incorporating the effects of temperature and moisture content. The framework is founded on a recently developed comprehensive multi-layer thin-shell formulation based on Isogeometric Analysis, which includes continuum damage, plasticity and cohesive-interface models. To incorporate hygrothermal effects in the modeling, we propose a scaling law that is based on the Arrhenius equation and material glass transition temperature that establishes the dependence of the intra- and interlaminar material properties on the temperature and moisture content. We compute several classical test cases using a combination of environmental conditions and demonstrate that the resulting modeling approach shows a good agreement with the experimental data, both in terms of failure loads reached as well as failure modes predicted.

我们开发了一个计算框架,用于模拟层状聚合物复合材料结构中的损伤和分层,其中包含温度和含水量的影响。该框架建立在最近开发的基于等距分析法的综合多层薄壳模型基础上,其中包括连续损伤、塑性和内聚界面模型。为了将湿热效应纳入建模,我们提出了一个基于阿伦尼乌斯方程和材料玻璃化转变温度的比例定律,该定律确定了层内和层间材料特性对温度和含水量的依赖性。我们利用各种环境条件计算了几个经典测试案例,结果表明,无论是在达到的破坏载荷方面,还是在预测的破坏模式方面,建模方法都与实验数据显示出良好的一致性。
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引用次数: 0
Failure assessment of eccentric circular holes under compressive loading 压缩荷载下偏心圆孔的失效评估
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-17 DOI: 10.1007/s10704-024-00805-3
Francesco Ferrian, Alberto Sapora, Rafael Estevez, Aurélien Doitrand

The present work aims to investigate the failure size effect on flattened disks containing an eccentric circular hole under mode I loading conditions. For this purpose, uniaxial compression tests are carried out on polymethyl methacrylate (PMMA) samples with holes. Depending on the hole radius and eccentricity, the energy release rate is either an increasing or decreasing function of the crack length, thus affecting the stability of crack propagation. Experimental results are interpreted and discussed through the coupled stress and energy criterion of Finite Fracture Mechanics. The approach lies on the assumption of a finite crack advance and it is implemented through the numerical estimation of the stress field and the Incremental Energy Release Rate functions. Finally, stability and crack speed propagation are discussed under the assumption of Linear Elastic Fracture Mechanics. Theoretical predictions reveal in agreement with experimental results thus demonstrating that the Coupled Criterion effectively captures the failure condition.

本研究旨在探讨在模式 I 载荷条件下,含有偏心圆孔的扁平圆盘的破坏尺寸效应。为此,对带孔的聚甲基丙烯酸甲酯(PMMA)样品进行了单轴压缩试验。根据孔的半径和偏心率,能量释放率是裂纹长度的递增或递减函数,从而影响裂纹扩展的稳定性。实验结果通过有限断裂力学的应力和能量耦合准则进行解释和讨论。该方法基于有限裂纹前进的假设,并通过应力场和增量能量释放率函数的数值估计来实现。最后,讨论了线性弹性断裂力学假设下的稳定性和裂纹速度传播。理论预测结果与实验结果一致,从而证明耦合准则有效地捕捉了失效条件。
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引用次数: 0
Dissipation during crack growth in a viscoelastic material from a cohesive model for a finite specimen 从有限试样的内聚模型看粘弹性材料裂纹增长过程中的耗散
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-08 DOI: 10.1007/s10704-024-00803-5
M. Ciavarella

In the present paper, we extend results recently given by Ciavarella et al. (J Mech Phys Solids 169:105096, 2022) to show some actual calculations of the viscoelastic dissipation in a crack propagation at constant speed in a finite size specimen. It is usually believed that the cohesive models introduced by Knauss and Schapery and the dissipation-based theories introduced by de Gennes and Persson-Brener give very similar results for steady state crack propagation in viscoelastic materials, where usually only the asymptotic singular field is used for the stress. We show however that dissipation and the energy balance never reach a steady state, despite the constant propagation crack rate and stress intensity factor. Our loading protocol permits a rigorous solution, and implies a short phase with constant specimen elongation rate, but then possibly a very long phase of constant or decreasing elongation, which differs from typical experiments. For the external work we are therefore unable to use the de Gennes and Persson-Brener theories which suggested that the increase of effective fracture energy would go up to the ratio of instantaneous to relaxed modulus, at very fast rates. We show viscoelastic dissipation is in general a transient quantity, which can vary by orders of magnitude while the stress intensity factor is kept constant, and is largely affected by dissipation in the bulk rather than at the crack tip. The total work to break a specimen apart is found also to be possibly arbitrarily large for quite a large range of intermediate crack growth rates.

在本文中,我们扩展了 Ciavarella 等人最近给出的结果(J Mech Phys Solids 169:105096, 2022),展示了在有限尺寸试样中匀速裂纹扩展过程中粘弹性耗散的一些实际计算结果。人们通常认为,Knauss 和 Schapery 引入的内聚模型与 de Gennes 和 Persson-Brener 引入的基于耗散的理论对粘弹性材料中的稳态裂纹扩展给出了非常相似的结果,而粘弹性材料中的应力通常只使用渐近奇异场。然而,我们的研究表明,尽管裂纹扩展速率和应力强度因子恒定,但耗散和能量平衡从未达到稳定状态。我们的加载协议允许严格的求解,并意味着试样伸长率恒定的短阶段,但随后可能是伸长率恒定或递减的很长阶段,这与典型的实验不同。因此,在外部工作中,我们无法使用 de Gennes 和 Persson-Brener 的理论,这两个理论认为有效断裂能的增加会以非常快的速度达到瞬时模量与松弛模量之比。我们的研究表明,粘弹性耗散通常是一个瞬态量,在应力强度因子保持不变的情况下,其变化幅度可以达到几个数量级,并且主要受体积耗散而非裂纹尖端耗散的影响。研究还发现,在相当大的中间裂纹增长率范围内,使试样断裂的总功可能非常大。
{"title":"Dissipation during crack growth in a viscoelastic material from a cohesive model for a finite specimen","authors":"M. Ciavarella","doi":"10.1007/s10704-024-00803-5","DOIUrl":"10.1007/s10704-024-00803-5","url":null,"abstract":"<div><p>In the present paper, we extend results recently given by Ciavarella et al. (J Mech Phys Solids 169:105096, 2022) to show some actual calculations of the viscoelastic dissipation in a crack propagation at constant speed in a finite size specimen. It is usually believed that the cohesive models introduced by Knauss and Schapery and the dissipation-based theories introduced by de Gennes and Persson-Brener give very similar results for steady state crack propagation in viscoelastic materials, where usually only the asymptotic singular field is used for the stress. We show however that dissipation and the energy balance never reach a steady state, despite the constant propagation crack rate and stress intensity factor. Our loading protocol permits a rigorous solution, and implies a short phase with constant specimen elongation rate, but then possibly a very long phase of constant or decreasing elongation, which differs from typical experiments. For the external work we are therefore unable to use the de Gennes and Persson-Brener theories which suggested that the increase of effective fracture energy would go up to the ratio of instantaneous to relaxed modulus, at very fast rates. We show viscoelastic dissipation is in general a transient quantity, which can vary by orders of magnitude while the stress intensity factor is kept constant, and is largely affected by dissipation in the bulk rather than at the crack tip. The total work to break a specimen apart is found also to be possibly arbitrarily large for quite a large range of intermediate crack growth rates.</p></div>","PeriodicalId":590,"journal":{"name":"International Journal of Fracture","volume":"248 1-3","pages":"95 - 108"},"PeriodicalIF":2.2,"publicationDate":"2024-07-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s10704-024-00803-5.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141575115","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
On the loci of exactness for truncated Williams crack-tip stress expansions 关于截断威廉姆斯裂缝尖端应力扩展的精确性位置
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-03 DOI: 10.1007/s10704-024-00802-6
Gaëtan Hello

Williams asymptotic expansions are widely used to represent mechanical fields at the vicinity of crack-tips in plane elastic media. For practical applications, series solutions have to be truncated and it is believed that a better accuracy can be achieved by retaining more terms in the summations. The influence of the truncation on the accuracy can be quantified comparing truncated closed-form Williams series solutions available for some fracture configurations to their corresponding complex exact counterparts. The computation of 2D absolute error fields reveals astonishing patterns in which appear points with numerically zero error implying the existence of loci where truncated series can provide exact results. These loci of exactness gather on curves emanating from the crack-tips and pointing towards the outside of series convergence disks. An analytical investigation of this phenomenon allows to relate the number and tangency angle at the crack-tip of these curves to the number and values of the zeros of Williams series angular eigenfunctions. Beyond its analytical interest in the understanding of Williams series framework, this property of exactness for truncated series can also help to improve the accuracy of experimental and computational techniques based on Williams series.

威廉斯渐近展开法被广泛用于表示平面弹性介质裂纹尖端附近的机械场。在实际应用中,必须对数列求解进行截断,相信通过在求和中保留更多的项可以获得更高的精度。截断对精度的影响可以通过比较某些断裂构造的截断闭式威廉斯序列解与相应的复杂精确对应解来量化。二维绝对误差场的计算揭示了惊人的模式,其中出现了数值误差为零的点,这意味着存在截断序列可以提供精确结果的位置。这些精确点聚集在从裂缝尖端发出的曲线上,并指向序列收敛盘的外部。通过对这一现象的分析研究,可以将这些曲线裂缝尖端的数量和切角与威廉斯数列角特征函数零点的数量和值联系起来。除了对理解威廉斯数列框架有分析意义之外,截断数列的精确性还有助于提高基于威廉斯数列的实验和计算技术的准确性。
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引用次数: 0
Introduction to the special issue on structural integrity 结构完整性特刊导言
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1007/s10704-024-00804-4
Viswanath Chinthapenta, Shailendra Joshi, Srinivasan Chandrasekar
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引用次数: 0
Cohesive behavior of single crystalline silicon carbide scribing by nanosecond laser 纳秒激光刻划单晶碳化硅的内聚行为
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-22 DOI: 10.1007/s10704-024-00801-7
Pei Chen, Shaowei Li, Rui Pan, Senyu Tu, Fei Qin

The existing mechanical dicing process of single crystalline Silicon Carbide (SiC) is one of the main factors limiting the development of semiconductor process, which could be replaced by laser scribing potentially. To achieve efficient and low-damage SiC separation, the cracking behavior of SiC after laser grooving should be well understood and controllable. Since the laser grooving including thermal ablation and meltage solidification, the cracking behavior of the scribed SiC would be different to the original single crystal SiC. In this paper, cohesive zone model (CZM) is used to quantitively represent the cracking behavior of the nano-laser scribed SiC. The separation after scribing was conducted in a three-point bending (3 PB) fixture to characterize the cracking behavior. Therefore, by inverting the load–displacement curves of 3 PB with CZM embedded finite element model, the cohesive behavior is characterized by bilinear traction–separation law, which illustrated the whole cracking process numerically. The methodology established in current paper gives way to understand the SiC scribing and cracking process with quantitative cohesive parameters.

现有的单晶碳化硅(SiC)机械切割工艺是限制半导体工艺发展的主要因素之一,而激光划槽有可能取代这一工艺。为实现高效、低损伤的碳化硅分离,应充分了解和控制激光划槽后碳化硅的开裂行为。由于激光划槽包括热烧蚀和熔融凝固,因此划线后的碳化硅的开裂行为将不同于原始单晶碳化硅。本文采用内聚区模型(CZM)来定量表示纳米激光划线碳化硅的开裂行为。划线后的分离在三点弯曲(3 PB)夹具中进行,以表征开裂行为。因此,通过用 CZM 嵌入式有限元模型反演三点弯曲的载荷-位移曲线,用双线性牵引-分离定律来表征内聚行为,从而用数值说明了整个开裂过程。本文所建立的方法有助于理解具有定量内聚参数的 SiC 划线和开裂过程。
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引用次数: 0
Construction of Kitagawa–Takahashi diagrams as a function of applied stress ratio 根据外加应力比绘制北川高桥图
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-13 DOI: 10.1007/s10704-024-00800-8
R. Sunder

Construction of the Kitagawa–Takahashi (K–T) diagram requires inputs of two material properties, namely, endurance limit and threshold stress intensity range, ΔKth. Both are sensitive to applied stress ratio. The effect of stress ratio on endurance limit is well known. Unfortunately, crack closure, associated with the nature of conventional testing practice obscures the effect of stress ratio on intrinsic, closure free ΔKth that would apply to natural crack like defects and short cracks. This study was made possible by the development of a new test method to characterize closure free threshold conditions under controlled near-tip residual stress conditions that essentially determine near-tip stress ratio at threshold. A procedure is described to construct the K–T diagram, using ΔKth values corrected for stress ratio and applicable to pre-existing defects and short cracks at notches that are unlikely to see closure. As a case study, a K–T diagram valid for different applied stress ratios is constructed for titanium alloy Ti-6Al-4V.

构建北川-高桥(K-T)图需要输入两个材料属性,即耐久极限和阈值应力强度范围 ΔKth。这两项属性对应用应力比都很敏感。应力比对耐久极限的影响众所周知。遗憾的是,与传统测试实践性质相关的裂纹闭合问题掩盖了应力比对本征无闭合 ΔKth 的影响,而这种影响适用于自然裂纹(如缺陷和短裂纹)。这项研究之所以能够进行,是因为开发了一种新的测试方法,可以在受控的近端残余应力条件下表征无闭合阈值条件,基本上确定了阈值处的近端应力比。本文介绍了构建 K-T 图的程序,该程序使用根据应力比校正的 ΔKth 值,适用于缺口处不太可能出现闭合的预先存在的缺陷和短裂纹。作为案例研究,为钛合金 Ti-6Al-4V 绘制了不同应用应力比下有效的 K-T 图。
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引用次数: 0
期刊
International Journal of Fracture
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