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Influence of sodium nitrite microcapsules on the physicochemical properties, microbiological stability, and mathematical modeling during the shelf life of mortadella 亚硝酸钠微胶囊对肉酱保质期内理化性质、微生物稳定性和数学模型的影响
IF 1.4 3区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY Pub Date : 2023-09-27 DOI: 10.1007/s00003-023-01459-4
Roberto Verlindo, Julia Lisboa Bernardi, Bruna Maria Saorin Puton, Greice Maria Ostrowski, Lucas Henrique do Nascimento, Patrícia Fonseca Duarte, Jamile Zeni, Geciane Toniazzo Backes, Eunice Valduga, Rodrigo Schwert, Rogério Luis Cansian, Alexander Junges

Since large amounts of sodium nitrite (NaNO2) are reduced during the shelf life of meat products, and given the difficulty in maintaining its stability in these products, the use of encapsulation techniques increases the action time of this additive to guarantee food safety. Thus, since NaNO2 is a mandatory food additive in mortadella formulations, the objective of the study was to evaluate different wall materials for the microencapsulation of NaNO2 in a spray dryer for further evaluation and monitoring of the agent encapsulated in mortadella during 60 days of storage at room temperature (25 ± 2 °C). The spray drying process was performed via atomization, testing 4 different compositions using porcine collagen, gum arabic (GA), and maltodextrin (MD) with NaNO2. The 10% GA + NaNO2 and 5% GA + 5% MD + NaNO2 samples had encapsulated NaNO2 yields of 46% and 42% (w/w), respectively. The application of microencapsulated materials on mortadella gave the product a better stability in the NaNO2 reduction reaction, remaining until the 50th day with NaNO2 residues above 50 mg/kg, while the control sample reached this level after 30 days of shelf life. Therefore, the application of NaNO2 capsules in mortadella can be an alternative for promotion of physicochemical and microbiological stability and is of fundamental importance for industrial applications.

Graphical abstract

由于大量亚硝酸钠(NaNO2)会在肉类产品的保质期内减少,而且很难保持其在这些产品中的稳定性,因此使用封装技术可以延长这种添加剂的作用时间,从而保证食品安全。因此,由于 NaNO2 是肉酱配方中必须使用的食品添加剂,本研究的目的是评估在喷雾干燥机中对 NaNO2 进行微胶囊化的不同壁材,以便进一步评估和监测肉酱在室温(25 ± 2 °C)下贮存 60 天期间所封装制剂的情况。喷雾干燥过程通过雾化进行,使用猪胶原蛋白、阿拉伯树胶(GA)和麦芽糊精(MD)与 NaNO2 进行了 4 种不同成分的测试。10% GA + NaNO2 和 5% GA + 5% MD + NaNO2 样品的封装 NaNO2 产率分别为 46% 和 42%(重量比)。在灰肉酱中使用微胶囊材料使产品在 NaNO2 还原反应中具有更好的稳定性,直到第 50 天,NaNO2 的残留量仍高于 50 毫克/千克,而对照样品在保质期 30 天后就达到了这一水平。因此,NaNO2 胶囊在熏肉中的应用可作为促进理化和微生物稳定性的替代方法,对工业应用具有重要意义。
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引用次数: 0
Anwendung des Vorsorgeprinzips nach Artikel 7 der Verordnung (EG) Nr. 178/2002: Allgemeine Grundsätze und Bewertung von Cannabidiol in Lebensmitteln 根据第175 /2002号条例第7条适用预防原则:食品中大麻迪奥的一般原则和评估
IF 2.4 3区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY Pub Date : 2023-09-26 DOI: 10.1007/s00003-023-01457-6
Constanze Sproll, Stephan G. Walch, Dirk W. Lachenmeier

Zusammenfassung

Das Vorsorgeprinzip ist in der Rechtsprechung und Gesetzgebung der Europäischen Union (EU) fest verankert. Im Lebensmittelrecht wurde das Vorsorgeprinzip in Art. 7 der Lebensmittel-Basisverordnung (EG) Nr. 178/2002 (BasisVO) etabliert. Dennoch findet das Vorsorgeprinzip sowohl in der Überwachungspraxis als auch in der nationalen Rechtsprechung nicht die angemessene Beachtung. Neben der historischen Entwicklung und der Anwendung in der nationalen und europäischen Rechtsprechung werden in diesem Beitrag die Möglichkeiten und Grenzen der Anwendung des Vorsorgeprinzips nach Art. 7 BasisVO am Beispiel von cannabidiolhaltigen (CBD) Produkten beleuchtet. Im Ergebnis wird festgestellt, dass die Behörden im Sinne des Vorsorgeprinzips aufgrund eines wahrscheinlichen Gesundheitsrisikos prioritäre Schutzmaßnahmen ergreifen können, die über die ohnehin erforderlichen Maßnahmen der Novel Food-Verordnung hinausgehen.

欧盟的欧盟法律和立法充斥着预防原则。由此产生了《食物基本条例》(简称EG) 97 /2002年,由此产生了预防性原则。然而,无论在监测措施还是在国家司法实践中,预防性原则都没有得到适当的重视。除了历史发展和在国家和欧洲司法实践中应用之外,本论文还通过种植草本植物产品的例子,亮点了采用预防性原则的可能性和局限性。由此产生的结果是,由于潜在的健康风险产生了一个风险,并由此产生了一个紧急的保护措施,由此产生的管理当局可以采取比Novel食品法已经需要的更大的步骤来预防犯罪。
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引用次数: 0
Contaminants in honey: an analysis of EU RASFF notifications from 2002 to 2022 蜂蜜中的污染物:2002年至2022年欧盟RASFF通报分析
IF 2.4 3区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY Pub Date : 2023-09-21 DOI: 10.1007/s00003-023-01460-x
Fawzy Eissa, El-Kazafy A. Taha

Honey is regarded as natural and healthy. However, a variety of contaminants could be present in the areas of production. The study aimed to identify the top hazard categories in Rapid Alert System for Food and Feed (RASFF) notifications for honey from 2002 to 2022, taking into account the notification year and type, country of origin, notifying country, risk decision, and actions taken. All RASFF notifications were processed in Pivot tables using Microsoft Excel. Out of 388 notifications for honey in the last 21 years 309 (79.64%) concerned the unauthorized residues of veterinary medicinal products hazard category, followed by adulteration/fraud (5.15%), foreign bodies (2.83%), pesticide residues (2.58%), and poor or insufficient controls (2.58%). China was the most frequently notified country of origin (25.77%), followed by Turkey (6.44%), Ukraine (6.19%), Argentina (6.19%), and Bulgaria (5.67%). Germany was the most frequently notifying country (16.49%), followed by the UK (16.24%), Spain (13.40%), Italy (10.82%), and Belgium (7.99%). Among all notifications, 22.68% were alerted and 12.37% were border rejected. The notification frequency (%) and mean concentration ± standard deviation (SD) (μg/kg) of the most frequently reported contaminants in the honey were as follows: chloramphenicol (25.26%, 172.10 ± 827.92 μg/kg), followed by streptomycin (12.11%, 104.94 ± 209.44 μg/kg), sulfathiazole (9.54%, 52.31 ± 52.62 μg/kg), tylosin (4.90%, 9.03 ± 11.23 μg/kg), and sulfadimidine (4.64%, 254.99 ± 587.00 μg/kg), respectively, due to their application by beekeepers to control infectious diseases of bees. Strict restrictions must be put in place to reduce the risk posed by these contaminants in honey.

蜂蜜被认为是天然和健康的。然而,各种污染物可能存在于生产区域。该研究旨在确定2002年至2022年期间食品和饲料快速警报系统(RASFF)蜂蜜通报中的最高危害类别,同时考虑到通报年份和类型、原产国、通报国、风险决策和采取的行动。所有RASFF通知都使用Microsoft Excel在数据透视表中处理。在近21年的388份蜂蜜通报中,309份(79.64%)涉及兽药残留危害类别,其次是掺假/欺诈(5.15%)、异物(2.83%)、农药残留(2.58%)和控制不良或不充分(2.58%)。中国是最频繁通报的原产国(25.77%),其次是土耳其(6.44%)、乌克兰(6.19%)、阿根廷(6.19%)和保加利亚(5.67%)。德国是最频繁通报的国家(16.49%),其次是英国(16.24%)、西班牙(13.40%)、意大利(10.82%)和比利时(7.99%)。检出率为22.68%,检出率为12.37%。蜂蜜中报告频率最高的污染物为氯霉素(25.26%,172.10±827.92 μg/kg),其次为链霉素(12.11%,104.94±209.44 μg/kg)、磺胺噻唑(9.54%,52.31±52.62 μg/kg)、泰络菌素(4.90%,9.03±11.23 μg/kg)和磺胺嘧啶(4.64%,254.99±587.00 μg/kg),主要是养蜂人用于防治蜜蜂传染病。严格的限制措施必须到位,以减少蜂蜜中这些污染物带来的风险。
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引用次数: 0
91. Arbeitstagung des ALTS 91. ALTS的实质性会议
IF 2.4 3区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY Pub Date : 2023-09-19 DOI: 10.1007/s00003-023-01456-7
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引用次数: 0
Whole-genome sequencing of Salmonella serotypes recovered longitudinally from broiler production, processing, and retailing in Trinidad and Tobago 特立尼达和多巴哥肉鸡生产、加工和零售中纵向恢复的沙门氏菌血清型的全基因组测序
IF 2.4 3区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY Pub Date : 2023-09-11 DOI: 10.1007/s00003-023-01455-8
Anisa S. Khan, Rian Ewald Pierneef, Woubit Abebe, Abiodun A. Adesiyun

This study was conducted within 2 months by sampling chicken batches from a broiler farm, a plant processing plant, and supermarket retail. The overall frequency of isolation of Salmonella was 50% (16/32), 17.5% (7/40), and 40% (4/10) for the samples collected from the broiler farm, processing plant, and retail outlet, respectively. Serovar Infantis was the predominantly isolated serovar at the 3 sampling sites. Resistance genes aac(3)IV, aph(4)Ia, blaCTX-M65, and qacEdelta1 were detected in 84.6% (11/13) of the isolates subjected to whole genome sequencing. S. Infantis strains were clustered within and across the 3 sampling sites. This study demonstrates a direct measure of the transmission dynamics of Salmonella during a farm-to-fork approach.

这项研究是在两个月内通过对肉鸡农场、植物加工厂和超市零售的鸡肉批次进行抽样进行的。在肉鸡养殖场、加工厂和零售店采集的样品中,沙门氏菌的分离率分别为50%(16/32)、17.5%(7/40)和40%(4/10)。3个采样点分离的血清型主要为婴儿血清型。经全基因组测序,84.6%(11/13)的菌株检出耐药基因aac(3)IV、aph(4)Ia、blaCTX-M65和qacEdelta1。3个采样点内及采样点间均有婴幼儿链球菌聚集。这项研究证明了在农场到餐桌的方法中沙门氏菌传播动力学的直接测量。
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引用次数: 0
Evidence for an accumulation of mineral oil saturated hydrocarbons (MOSH) in human tissues: a re-evaluation of biopsy and autopsy data 矿物油饱和碳氢化合物(MOSH)在人体组织中积累的证据:对活检和尸检数据的重新评估
IF 1.4 3区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY Pub Date : 2023-09-07 DOI: 10.1007/s00003-023-01458-5
Ralph Pirow, Nicole Concin, Koni Grob

Consumers are exposed to mineral oil hydrocarbons (MOH) e.g. through foodstuffs and cosmetics. Upon ingestion, MOH follow the absorption pathway of dietary lipids. Analytical chemistry has revealed the presence of the main fraction, designated as mineral oil saturated hydrocarbons (MOSH), in mesenteric lymph nodes (MLNs), liver, spleen, and adipose tissue. Recent results from animal studies raised concerns about a long-term, possibly irreversible accumulation of some MOSH in humans. To address this issue, we performed a statistical re-analysis of published biopsy and autopsy data regarding the age-dependence of MOSH levels in human tissue. MOSH concentrations in MLNs and adipose tissue showed a 1.2–1.4-fold increase per decade, pointing to very long-term accumulation in both tissues. There was no evidence for age-dependent MOSH concentrations in liver and spleen. There was no sex difference in the MOSH concentrations in MLNs, suggesting a similar oral exposure for men and women. On average, women had a 2.2–2.5-fold higher MOSH concentration in the liver, spleen and adipose tissue compared to men. This finding may point to a sex difference in metabolism, in line with animal data. The use of certain cosmetics was a relevant predictor in addition to age. Women that used cosmetics like lipstick, hand cream, and sun cream had an average 2.1-fold higher MOSH concentration in abdominal subcutaneous fat than non-users.

消费者会通过食品和化妆品等途径接触到矿物油碳氢化合物 (MOH)。摄入后,矿物油烃会通过膳食脂质的吸收途径被人体吸收。化学分析显示,肠系膜淋巴结(MLN)、肝脏、脾脏和脂肪组织中存在主要的矿物油饱和碳氢化合物(MOSH)。最近的动物研究结果引发了人们对某些 MOSH 在人体中长期积累(可能是不可逆的)的担忧。为了解决这个问题,我们重新对已发表的活检和尸检数据进行了统计分析,以了解人体组织中的 MOSH 水平与年龄的关系。MLN和脂肪组织中的MOSH浓度每十年增加1.2-1.4倍,这表明这两种组织中的MOSH长期积累。没有证据表明肝脏和脾脏中的 MOSH 浓度与年龄有关。MLN中的MOSH浓度没有性别差异,这表明男性和女性的口服暴露量相似。与男性相比,女性肝脏、脾脏和脂肪组织中的 MOSH 浓度平均高出 2.2-2.5 倍。这一发现可能表明在新陈代谢方面存在性别差异,这与动物实验数据一致。除年龄外,使用某些化妆品也是一个相关的预测因素。使用口红、护手霜和防晒霜等化妆品的女性腹部皮下脂肪中的 MOSH 浓度平均比不使用化妆品的女性高 2.1 倍。
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引用次数: 0
Listeria monocytogenes detection on food contact surfaces: suitability of different swab materials 食品接触表面单核增生李斯特菌检测:不同拭子材料的适用性
IF 2.4 3区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY Pub Date : 2023-09-01 DOI: 10.1007/s00003-023-01454-9
Nadja Hillig, Ahmad Hamedy, Martin Koethe

The high binding capacity of Listeria monocytogenes to food contact surfaces increases the risk of cross-contamination in food. In addition to appropriate cleaning and disinfection procedures, a suitable sampling plan and technique for the earliest possible detection are necessary for prevention. This paper evaluates the sensitivity of 3 swab materials (cotton, viscose and nylon-flocked) for the qualitative and quantitative detection of L. monocytogenes on food contact surfaces (100 cm2). A L. monocytogenes cocktail of 3 serotypes (IIa, IIb and IVb) was applied to stainless steel, polyvinyl chloride, polytetrafluoroethylene and high-density polyethylene surfaces at a concentration of approx. 1.0 × 101-1.0 × 102 CFU/100 cm2 and approx. 4.0 × 104 CFU/100 cm2. The surfaces were sampled after 15 min of incubation by 3 different swabs using the double-swab technique, and then stored for 4 and 24 h until processing. The results of the qualitative and quantitative tests showed a few statistically significant differences in the detectability of L. monocytogenes by different swab materials, which implies that the detection rate of L. monocytogenes on a certain food contact surfaces can be increased by using the respective most suitable swab.

单核细胞增生李斯特菌对食品接触面的高结合能力增加了食品中交叉污染的风险。除了适当的清洁和消毒程序外,适当的取样计划和尽早发现的技术是预防的必要条件。本文评价了3种棉签材料(棉、粘胶和尼龙绒)对食品接触表面(100 cm2)单核细胞增生乳杆菌的定性和定量检测的灵敏度。将3种血清型(IIa、IIb和IVb)的单核细胞增生乳杆菌混合物以约为浓度分别施用于不锈钢、聚氯乙烯、聚四氟乙烯和高密度聚乙烯表面。1.0 × 101-1.0 × 102 CFU/100 cm2。4.0 × 104 CFU/100 cm2。用3种不同的拭子(双拭子技术)孵育15 min后对表面取样,然后分别保存4和24 h待处理。定性和定量试验结果显示,不同拭子材料对单核增生乳杆菌的检出率有统计学差异,说明使用各自最合适的拭子可提高特定食品接触面上单核增生乳杆菌的检出率。
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引用次数: 0
120. ALS-Sitzung
IF 2.4 3区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY Pub Date : 2023-08-23 DOI: 10.1007/s00003-023-01452-x
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引用次数: 0
Identification of representative sampling sites for the investigation of aerial longer distances transport of pesticides in Germany 德国农药空中长途运输调查代表性采样点的确定
IF 2.4 3区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY Pub Date : 2023-08-18 DOI: 10.1007/s00003-023-01448-7
Roland Kubiak, Anna Peters, Achim Gathmann, Karsten Hohgardt, Christine Kula, Daniela Marutzky, Lucas Streib, Kai Thomas, Matthias Trapp

Aerial transport of pesticides during and after their application both over medium range distances and long distance may lead to residues on plants and soil far away from agricultural treatments. Therefore, the Federal Office of Consumer Protection and Food Safety carried out a Germany-wide geographical analysis to identify monitoring sites which could be used for a representative German-wide monitoring. The identified sites reflect climate areas with different meteorological conditions, land coverage and pesticide use. By using a geographical information system, five different areas were identified representing the climatic and agricultural conditions of pesticide use in Germany. Since the required measuring technique needed a certain infrastructure, using already existing measuring sides was considered to be most efficient in order to use them for a German-wide monitoring. In a second step, agro-meteorological weather stations with distances of < 100 m, 100–1000 m and > 1 km in the main wind direction from treated fields were identified within these areas. The identified areas reflect the main different conditions for aerial pesticide transport along with suitable weather stations to monitor pesticide residues in the air and its deposition on plants and soil all over Germany.

农药施用期间和施用后的空中运输,无论是中距离还是长距离,都可能导致农药残留在远离农业处理的植物和土壤上。因此,联邦消费者保护和食品安全办公室进行了一项全德国的地理分析,以确定可用于具有代表性的全德国监测的监测点。确定的地点反映了具有不同气象条件、土地覆盖和农药使用的气候区域。通过使用地理信息系统,确定了代表德国农药使用的气候和农业条件的五个不同区域。由于所需的测量技术需要一定的基础设施,使用现有的测量侧被认为是最有效的,以便将它们用于全德国的监测。第二步,在这些区域内确定距离处理田主风向分别为100米、100 - 1000米和1公里的农业气象气象站。确定的区域反映了空中农药运输的主要不同条件,以及适合监测空气中农药残留及其在德国各地植物和土壤上沉积的气象站。
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引用次数: 0
Antimicrobial susceptibility profile and detection of E. coli O157:H7 from slaughterhouses and butcher shops in Ethiopia 埃塞俄比亚屠宰场和肉店O157:H7大肠杆菌的抗菌药敏谱和检测
IF 2.4 3区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY Pub Date : 2023-08-14 DOI: 10.1007/s00003-023-01449-6
Fufa Abunna, Muhaba Yimana, Hika Waketole, Takele Beyene, Tsedale Teshome, Bekele Megersa

A cross-sectional study was carried out on 352 samples (120 fecal, 92 beef cut, and 140 environmental swabs) to investigate the occurrence of E. coli O157:H7 in raw beef and to assess its antimicrobial susceptibility profile in slaughterhouses and butcher shops in Bishoftu town, Ethiopia. The samples were enriched by modified tryptone soy broth supplemented with novobiocin (mTSB + N) at the ratio of 1:9 BPW to mTSB + N and incubated overnight at 41.5 ± 0.5 ̊C (24 h). Latex agglutination was performed for confirmation of E. coli O157:H7 using an RIM E. coli O157:H7 latex test kit. The isolates were further tested for their resistance against antimicrobial susceptibility to 13 antimicrobials using the Kirby–Bauer disk diffusion method. Out of 352 samples, 14 (4.0%) were positive for E. coli O157:H7 serotype; of which, 28.6% (4/14), 21.4% (3/14), and 50% (7/14) were from fecal, beef, and environmental swab samples, respectively. A significant difference in the occurrences of the pathogen was observed among the sources of samples (p < 0.05). The antimicrobial susceptibility test revealed high resistance to 3 commonly used drugs: tetracycline (100%), erythromycin (92.8%), and ampicillin (64.3%). All E. coli O157 isolates were susceptible to azithromycin, cefotaxime, and chloramphenicol. However, of 14 isolates, 12 (85.8%) were resistant to ≥ 3 classes of antimicrobial agents. The current study warrants the need to implement appropriate hygienic measures in slaughterhouses and butcher shops to safeguard public health.

对352份样本(120份粪便、92份牛肉切片和140份环境棉子)开展了一项横断面研究,以调查生牛肉中O157:H7大肠杆菌的发生情况,并评估埃塞俄比亚Bishoftu镇屠宰场和肉店中O157:H7大肠杆菌的抗菌敏感性。用添加新生物素(mTSB + N)的改良色氨酸豆汤(BPW与mTSB + N的比例为1:9)对样品进行富集,并在41.5±0.5℃(24 h)下孵育过夜。使用RIM大肠杆菌O157:H7乳胶检测试剂盒进行乳胶凝集,确认大肠杆菌O157:H7。采用Kirby-Bauer纸片扩散法检测分离菌株对13种抗菌素的耐药性。352份样本中,14份(4.0%)O157:H7大肠杆菌血清型阳性;其中,28.6%(4/14)、21.4%(3/14)和50%(7/14)来自粪便、牛肉和环境拭子样本。不同样品来源间病原菌的发生率差异有统计学意义(p < 0.05)。药敏试验显示对常用药物四环素(100%)、红霉素(92.8%)、氨苄西林(64.3%)耐药较高。所有大肠杆菌O157分离株均对阿奇霉素、头孢噻肟和氯霉素敏感。14株中有12株(85.8%)对≥3类抗菌药物耐药。目前的研究表明,有必要在屠宰场和肉店实施适当的卫生措施,以保障公众健康。
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引用次数: 0
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Journal of Consumer Protection and Food Safety
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