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Utilizing artificial-intelligence image recognition systems to assist in the quality control analysis of 3D printing chocolate appearance and styling after oleogel adding 利用人工智能图像识别系统,辅助3D打印巧克力添加油凝胶后外观和造型的质量控制分析
IF 2.701 Pub Date : 2025-02-04 DOI: 10.1007/s13197-025-06210-5
Jeremiah Hao Ran Huang, GiGi Chin Wen Lim, Ching-Hui Su, Jhih-Ying Ciou

Chocolate is often used in 3D food printing, however in 3D food printing cold extrusion systems, chocolate often faces the issue of temperature-induced clumping. To address this texture alteration, the method of adding oleogels is employed. This study examines the impact of monoglycerides (MAG), sucrose fatty acid ester (SE) and hydroxypropyl methylcellulose (HPMC) oleogels on the thermal and textural properties of 3D printed white and dark chocolates. It compares the effects of adding MAG, SE, and HPMC to dark and white chocolate for 3D printing. Thermal analysis shows distinct melting points: white chocolate with MAG peaks at 29.53 °C, 32.46 °C and 37.08 °C, while dark chocolate with SE peaks at 29.79 °C and 31.78 °C. Texture analysis indicates that white chocolate with 2% SE is harder than with 2% MAG, correlating with their respective melting points. AI image recognition effectively identifies shape variations and defects, achieving recognition rates over 90% for ideal shapes and flagging incomplete extrusions and structural issues. These findings highlight 3D printing's potential in chocolate manufacturing for precise customization and quality control, supported by AI inspection systems. Besides, the method offers a simpler approach for future applications for non-thermal extrusion. Future research could optimize oleogel formulations and expand AI applications to enhance production efficiency and product consistency.

巧克力经常用于3D食品打印,然而在3D食品打印冷挤压系统中,巧克力经常面临温度诱导结块的问题。为了解决这种纹理变化,采用了添加油凝胶的方法。本研究考察了单甘油酯(MAG)、蔗糖脂肪酸酯(SE)和羟丙基甲基纤维素(HPMC)油凝胶对3D打印白巧克力和黑巧克力的热学和质地性能的影响。它比较了在黑巧克力和白巧克力中添加MAG、SE和HPMC的效果。热分析表明,白巧克力的MAG峰在29.53°C、32.46°C和37.08°C,黑巧克力的SE峰在29.79°C和31.78°C。质地分析表明,含2% SE的白巧克力比含2% MAG的白巧克力更硬,这与它们各自的熔点有关。人工智能图像识别有效识别形状变化和缺陷,对理想形状的识别率超过90%,并标记不完整的挤压和结构问题。这些发现突出了3D打印在巧克力制造中的潜力,在人工智能检测系统的支持下,可以进行精确定制和质量控制。此外,该方法为未来非热挤压的应用提供了一种更简单的方法。未来的研究可以优化油凝胶配方,扩大人工智能应用,以提高生产效率和产品一致性。
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引用次数: 0
Effect of propolis extracted and basil gum addition on physicochemical, rheological, sensory, and antioxidant properties of low-fat yogurt 蜂胶萃取及罗勒胶加入对低脂酸奶理化、流变、感官及抗氧化性能的影响
IF 2.701 Pub Date : 2025-01-27 DOI: 10.1007/s13197-025-06208-z
Mina Noshadi, Mostafa Karami, Masoumeh Arab, Mahdi Taheri, Vahid Ghasemzadeh-Mohammadi

Dairy products such as yogurt are nutritious food sources. Propolis is formed by mixing tree secretions with pollen and bee enzymes and has some functional properties. Basil seed is a rich source of hydrocolloids with outstanding functional properties. It gum has excellent potential for use as a fat substitute in yogurt. Pasteurized milk containing 2% w/v starter was investigated with different propolis extract and basil seed mixtures. Then, on days 1, 3, 6, 14, and 21, the yogurt samples’ physiological, rheological, sensory, and antioxidant properties were investigated. Propolis significantly increased (p < 0.05) the antioxidant activity, phenolic compounds, and color index; nonetheless, it reduced sensory acceptability. The basil seed gum significantly increased (p < 0.05) textural and rheological characteristics, acidity, brightness, and sensory acceptability. The sample containing propolis and basil gum exhibited the highest water-holding capacity, the highest level of antioxidant activity and phenolic compounds, and the lowest acidity.

酸奶等乳制品是营养丰富的食物来源。蜂胶是由树木分泌物与花粉和蜜蜂酶混合而成,具有一些功能特性。罗勒籽含有丰富的水胶体,具有优异的功能特性。它在酸奶中作为脂肪替代品的潜力很大。以含有2% w/v发酵剂的巴氏奶为原料,用不同的蜂胶提取物和罗勒籽混合物进行了研究。然后,在第1、3、6、14和21天,研究酸奶样品的生理、流变、感官和抗氧化性能。蜂胶显著提高了抗氧化活性、酚类化合物含量和显色指数(p < 0.05);然而,它降低了感官上的可接受性。罗勒种子胶显著提高了(p < 0.05)质地和流变特性、酸度、亮度和感官接受度。含有蜂胶和罗勒胶的样品具有最高的保水能力,最高的抗氧化活性和酚类化合物水平,最低的酸度。
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引用次数: 0
Watermelon juice microfiltration: optimization to maximize antioxidant compounds and influence mineral content 西瓜汁微过滤:优化,最大限度地提高抗氧化化合物和影响矿物质含量
IF 2.701 Pub Date : 2025-01-27 DOI: 10.1007/s13197-025-06202-5
Frederico Lovato, Jussara Kowaleski, Sabrine Zambiazi da Silva, Luciana Bill Mikito Kottwitz, Clayton Antunes Martin, Tatiana Shioji Tiuman, Ricardo Fiori Zara

Traditional methods for fruit juice preservation use high temperatures, which degrade beneficial compounds like vitamins and antioxidants. Membrane filtration provides a gentler alternative, preserving nutrients through mild operating temperatures. This study assessed the temperature and pressure influence on watermelon juice microfiltration, focusing on permeated flow, lycopene, sugars, phenolic compounds, and flavonoids. Using a 22 composite design with central values, optimal conditions were determined by the desirability function, with pressure at 1.0 bar and temperature at 37ºC, maximizing these response variables. Resistance to permeated flux was primarily due to fouling, with an initial 25% flux reduction. The process effectively concentrated lycopene, sugars, phenolic compounds, and flavonoids, although mineral content decreased in both concentrated and permeated juice, with potassium being the most abundant mineral. The concentrated juice showed greater mineral loss than pasteurized due to retention during microfiltration. Under optimized conditions, microbial load reduction allowed the concentrated juice a shelf life comparable to pasteurized juice (14 days). Sensory analysis showed strong consumer acceptance, with 64% of tasters expressing purchase intent. These results suggest commercial viability for the concentrated juice; moreover, its high carotenoid retention could serve as an industrial ingredient for functional foods.

传统的果汁保存方法使用高温,这会降解维生素和抗氧化剂等有益化合物。膜过滤提供了一个更温和的选择,通过温和的操作温度保存营养物质。本研究评估了温度和压力对西瓜汁微滤的影响,重点是渗透流量、番茄红素、糖、酚类化合物和类黄酮。采用22个具有中心值的复合设计,根据期望函数确定最佳条件,压力为1.0 bar,温度为37ºC,最大限度地提高这些响应变量。对渗透通量的阻力主要是由于污垢,初始通量减少了25%。这一过程有效地浓缩了番茄红素、糖、酚类化合物和类黄酮,尽管浓缩汁和渗透汁的矿物质含量都有所下降,其中钾是含量最高的矿物质。浓缩果汁由于微滤期间的滞留,矿物质损失比巴氏灭菌果汁大。在优化条件下,微生物负荷减少使浓缩果汁的保质期与巴氏灭菌果汁相当(14天)。感官分析显示,消费者接受度很高,64%的品尝者表达了购买意愿。这些结果表明浓缩果汁具有商业可行性;此外,它的高类胡萝卜素保留率可以作为功能性食品的工业成分。
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引用次数: 0
Does fixed oil impart more antioxidant potential to spices than essential oils? A comparative study with seed (nutmeg) and aril (mace) oil from the spice myristica fragrans 固定油比精油赋予香料更多的抗氧化潜力吗?香料肉豆蔻种子油和假种皮油的比较研究
IF 2.701 Pub Date : 2025-01-27 DOI: 10.1007/s13197-024-06164-0
Salony Azam Sheikh, Vallamkondu Manasa, Palak Daga, Ajay W. Tumaney

To understand their importance, we performed a comparative study on fixed, total, and essential oils from the seed and aril of Myristica fragrans. The total, essential, and fixed oils content of nutmeg (34.47%, 5.95%, and 26.43%, respectively) and mace (22.55%, 8.79%, and 23.73%, respectively) showed varied oil content. The major fatty acid in mace fixed oil (MFO) and mace total oil (MTO) was palmitic acid (33.30% and 33.11%. respectively), whereas, in nutmeg fixed oil (NFO) and nutmeg total oil (NTO), it was myristic acid (62.52% and 58.20%, respectively). MTO exhibited the highest total phenolic (~ 4596 mg gallic acid equivalent/100 g) content. The phenolics and the flavonoids (mg/100 g), such as catechin (25.40 ± 16.11) and quercetin (13.86 ± 2.34), were high in MFO. Rutin (20.61 ± 3.91) and gallic acid (10.69 ± 1.58) were highest in MTO. Ferulic acid (8.26 ± 0.49) was highest in NTO, and synergic acid (24.72 ± 3.41) in NFO. The MFO showed the highest antioxidant activity (53% radical scavenging activity by DPPH; 34 M Trolox equivalent/ 100 g of oil by TEAC assay; 104 M Trolox equivalent/ 100 g of oil by FRAP assay), correlating with the polyphenols content. The fixed oils showed higher overall antioxidant activity than essential oils.

为了了解它们的重要性,我们对肉豆蔻种子和假种皮的固定油、总油和精油进行了比较研究。肉豆蔻(34.47%,5.95%,26.43%)和豆蔻(22.55%,8.79%,23.73%)的总油含量、挥发油含量和固定油含量各不相同。豆蔻固定油(MFO)和豆蔻总油(MTO)的主要脂肪酸为棕榈酸(33.30%和33.11%)。肉豆蔻固定油(NFO)和肉豆蔻总油(NTO)中肉豆蔻酸含量最高,分别为62.52%和58.20%。MTO的总酚含量最高(~ 4596 mg没食子酸当量/100 g)。多酚类化合物中儿茶素(25.40±16.11)、槲皮素(13.86±2.34)含量较高,黄酮类化合物含量较高(mg/100 g)。芦丁(20.61±3.91)和没食子酸(10.69±1.58)在MTO中含量最高。阿魏酸(8.26±0.49)在NTO组最高,协同酸(24.72±3.41)在NFO组最高。与多酚含量相关,MFO具有最高的抗氧化活性(DPPH清除自由基活性为53%,TEAC测定为34 M Trolox当量/ 100 g油,FRAP测定为104 M Trolox当量/ 100 g油)。固定油的整体抗氧化活性高于精油。
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引用次数: 0
Experimental and mechanism analysis of vacuum cooling for high temperature liquid food 高温液态食品真空冷却实验及机理分析
IF 2.701 Pub Date : 2025-01-27 DOI: 10.1007/s13197-025-06215-0
Yu Yang, Tonghua Zou, Bin Chen, Youxian Du, Baomin Dai

To minimize the liquid splashing in vacuum cooling, the mass and temperature changes of liquid food were measured by changing the conditions such as the volume ratio of the solution to the container, the pore area, the initial temperature and the terminal temperature, and the effects of different conditions on the ineffective water loss rate were derived from the test results. When the opening area is 1.13cm2, the ineffective water loss rate is the largest. The higher the initial temperature, the smaller the ineffective water loss rate. The terminal temperature is 25 °C, the ineffective water loss rate is the lowest. By exploring the key factors of the splash of liquid droplets in the process of vacuum cooling liquid food, the effect of reducing the splash of liquid droplets in the process of vacuum cooling is realized.

Graphical Abstract

为了最大限度地减少真空冷却过程中液体的飞溅,通过改变溶液与容器的体积比、孔面积、初始温度和终端温度等条件,测量了液态食品的质量和温度变化,并从试验结果中得出了不同条件对无效失水率的影响。当开口面积为1.13cm2时,无效失水率最大。初始温度越高,无效失水速率越小。终端温度为25℃时,无效失水率最低。通过探索真空冷却液态食品过程中液滴飞溅的关键因素,实现了减少真空冷却过程中液滴飞溅的效果。图形抽象
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引用次数: 0
Physical and chemical properties of exopolysaccharide obtained from whey fermentation by Lactiplantibacillus plantarum DF60Mi 植物乳杆菌DF60Mi发酵乳清所得胞外多糖的理化性质
IF 2.701 Pub Date : 2025-01-25 DOI: 10.1007/s13197-025-06201-6
J. H. P. Lopes Neto, S. Soares, R. E. Santos, K. S. Leite, M. I. F. Campos, C. V. B. Grisi, J. E. S. Ribeiro, M. T. Cavalcanti, C. M. Silva, M. Iacomini, H. R. Cardarelli

The use of whey as an alternative culture medium for fermentation by lactic bacteria enables generating new products exopolysaccharide (EPS) and avoids environmental and economic damage. This work aimed to characterize the exopolysaccharide obtained from whey fermentation (EPS-LN60) by Lactiplantibacillus plantarum DF60Mi to identify its physical and chemical properties. The EPS was characterized in terms of total sugar, protein, yield, FTIR, thermogravimetry, calorimetry, monosaccharide composition, optical microscopy and SEM. High EPS yield (777 mg/L) and sugar content (43.78%) were obtained, as well as, as expected, low protein content (1.82%). The monosaccharides found in EPS-LN60 were galactose (51.1%), mannose (22.9%), glucose (20.8%) and rhamnose (5.2%). The EPS-LN60 spectrogram showed the same bonds and functional groups to the identity of polysaccharides and the thermogram showed high thermal stability (310 °C). The EPS showed a porous surface and leaf shape, indicating its potential application for rheological changes in foods. Therefore, the results confirmed the presence of a heteropolysaccharide with high thermal stability from whey fermentation whose use can be envisioned as a potential ingredient to be explored by the food industry.

Graphical abstract

乳清作为乳酸菌发酵的替代培养基,可以产生新产品外多糖(EPS),避免对环境和经济造成损害。本研究旨在对植物乳杆菌DF60Mi发酵乳清获得的多糖(EPS-LN60)进行理化性质鉴定。通过总糖、蛋白、产率、红外光谱、热重、量热、单糖组成、光学显微镜和扫描电镜对EPS进行了表征。获得了较高的EPS产量(777 mg/L)和糖含量(43.78%),蛋白质含量(1.82%)如预期的那样低。在EPS-LN60中发现的单糖为半乳糖(51.1%)、甘露糖(22.9%)、葡萄糖(20.8%)和鼠李糖(5.2%)。EPS-LN60谱图显示出与多糖相同的键和官能团,热图显示出高的热稳定性(310°C)。EPS具有多孔的表面和叶片形状,表明其在食品流变学变化方面的潜在应用。因此,结果证实了乳清发酵中具有高热稳定性的杂多糖的存在,其用途可以设想为食品工业探索的潜在成分。图形抽象
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引用次数: 0
Current trends in the determination of microbiological indicators of dairy products 乳制品微生物指标测定的最新趋势
IF 2.701 Pub Date : 2025-01-22 DOI: 10.1007/s13197-025-06207-0
A. A. Shuba, E. V. Bogdanova, E. P. Anokhina, R. U. Umarkhanov

Milk and dairy products are the most common and widely consumed foods. At the same time, milk is often contaminated with pathogenic microorganisms by endo- and exogenous ways, which can cause various defects in raw materials and finished products. Recently, new techniques have been developed for monitoring microbiological indicators of milk, which are characterized by simplicity, ease of use and high reliability. In addition, the analysis time using the new techniques is significantly reduced compared to traditional ones. The review considers the microflora of milk and ways of its contamination with pathogenic microorganisms, as well as new methods for monitoring microbiological indicators that will be useful for specialists in the dairy industry.

牛奶和奶制品是最常见和最广泛消费的食物。与此同时,牛奶经常受到内源性和外源性致病微生物的污染,导致原料和成品出现各种缺陷。近年来,牛奶微生物指标监测新技术的发展具有简单、易用、可靠性高的特点。此外,与传统技术相比,使用新技术的分析时间显着减少。这篇综述考虑了牛奶中的微生物群及其被致病微生物污染的途径,以及监测微生物指标的新方法,这将对乳制品行业的专家有用。
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引用次数: 0
Pyrodextrin powder production from sorghum beer residue: optimisation of spray drying parameters for improved conservation properties 高粱啤酒渣制焦糊精粉:优化喷雾干燥参数以提高保存性能。
IF 2.701 Pub Date : 2025-01-22 DOI: 10.1007/s13197-025-06198-y
María Agostina Bianchi, Laura Cecilia Gómez Pamies, María del Rosario Acquisgrana, María Mercedes Lataza Rovaletti, Fernanda Micaela Quiroga, Pablo Daniel Ribotta, Diego Libkind Frati, Elisa Inés Benítez

Pyrodextrins are polysaccharides with the potential to be used as food additives, standing out for their nutritional interest associated with their behaviour as soluble dietary fiber. Being isolated from a gluten-free cereal, it is possible to add them to products suitable for individuals with coeliac disease. In the present study, the impact of the spray drying process of sorghum pyrodextrins obtained by pyroconversion of beer mashing residues, is investigated. The operating conditions for laboratory-scale drying are optimised to produce a stable powdered material for storage. The response surface methodology was used for different drying air inlet temperatures (150–250 °C), feed flow rates (20–80%) and drying airflow rates (20–80%). To characterise the spray-dried sorghum pyrodextrins, their water activity, moisture content, colour, particle size distribution and glass transition temperature were analysed. It was verified that the operational variables evaluated had an impact on the characteristic parameters of sorghum pyrodextrin powders. The optimal drying conditions determined a drying air temperature of 181.9 °C, feed flow rate at 23% and drying airflow rate at 78%, allowing powders with stability suitable for conservation to be obtained. The utilisation of a substantial waste from another process enhances efficiency and contributes to sustainability.

焦糊精是一种多糖,具有用作食品添加剂的潜力,其作为可溶性膳食纤维的行为与其营养价值相关。从无麸质谷物中分离出来,可以将它们添加到适合乳糜泻患者的产品中。本文研究了啤酒醪渣热转化所得高粱焦糊精喷雾干燥工艺的影响。优化了实验室规模干燥的操作条件,以生产稳定的粉末材料用于存储。响应面法用于不同的干燥空气入口温度(150-250°C)、进料流量(20-80%)和干燥气流速率(20-80%)。对喷雾干燥高粱焦糊精的水活度、水分含量、颜色、粒度分布和玻璃化转变温度进行了表征。结果表明,所评价的操作变量对高粱焦糊精粉的特性参数有影响。最佳干燥条件为:干燥空气温度为181.9℃,进料流量为23%,干燥气流为78%,可获得稳定性适合保存的粉体。利用另一个过程产生的大量废物可提高效率并有助于可持续发展。
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引用次数: 0
Biomass production optimization and quality assessment of Saccharomyces eubayanus starter cultures for their application in the craft brewing industry 真贝酵母发酵剂生物质产量优化及品质评价及其在精酿工业中的应用
IF 2.701 Pub Date : 2025-01-21 DOI: 10.1007/s13197-025-06203-4
Julieta Amalia Burini, Andrea Trochine, Diego Libkind Frati

The wild yeast Saccharomyces eubayanus (parental of the lager brewing hybrid yeast) has been intensively studied for brewing applications since its discovery in Patagonia (Argentina), and then in other parts of the world. In this work, cultures of this non-conventional yeast in different physiological conditions were tested in terms of viability and vitality, to understand its behavior and provide tools for biomass quality assessment for brewing. Four dyes were analyzed, and alkaline methylene violet turned out to be the most accurate for S. eubayanus viability measurements. Regarding vitality, cultures in exponential and stationary phases presented shorter lag phase and greater acidification power, indicating a better metabolic state; contrary to what was observed in cultures under starvation and refrigerated for 30 days (stressed); however, these presented the highest subsequent fermentation rate. In addition, culture medium for propagation was optimized from malt extract. Plackett–Burman design allowed identifying the most influential factors for biomass production: yeast extract and acid casein peptone, which were optimized by applying a CCD-RSM. Finally, scaling-up (20 L) allowed the obtention of S. eubayanus starter cultures with an adequate biomass quantity and quality for being transferred to the brewing industry.

野生酵母真酵母(酿酒杂交酵母的亲本)自从在巴塔哥尼亚(阿根廷)被发现以来,一直被广泛研究用于酿酒的应用,然后在世界其他地区。本研究通过对该酵母在不同生理条件下培养物的生存力和活力进行测试,了解其行为,为酿酒生物质的质量评价提供工具。对四种染料进行了分析,结果表明碱性亚甲基紫是测定真丝酵母活力最准确的染料。在活力方面,指数期和稳定期的培养物滞后期较短,酸化能力较大,代谢状态较好;与在饥饿和冷藏30天(压力)的培养中观察到的相反;然而,这些品种的后续发酵率最高。此外,还以麦芽提取物为主要原料,对培养培养基进行了优化。Plackett-Burman设计确定了对生物质生产影响最大的因素:酵母提取物和酸性酪蛋白蛋白胨,并通过CCD-RSM对其进行了优化。最后,扩大规模(20 L)可以获得具有足够生物量和质量的真巴芽孢杆菌发酵剂,以便转移到酿造业。
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引用次数: 0
Potential application of seaweed extract in tomato to improve bioactive compounds during postharvest storage 海藻提取物在番茄采后贮藏中提高生物活性成分的潜在应用
IF 2.701 Pub Date : 2025-01-17 DOI: 10.1007/s13197-024-06196-6
Vinícius Villa e Vila, Roberto Rezende, Patricia Angélica Alves Marques, Bianka Rocha Saraiva, Gustavo Soares Wenneck, Paula Toshimi Matumoto-Pintro

Seaweed extract has been applied in many crops to improve plant growth, mitigate plant stress, and enhance fruit quality. Ascophyllum nodosum is a macroalgae that is source of phytohormones, minerals, polysaccharides and antioxidant compounds. These elements can enhance food nutritional value, contributing to human health. The objective was to analyze the potential of Ascophyllum nodosum extract (ANE) applications in tomato, to improve physicochemical and bioactive compounds during storage. Tomato plants were cultivated divided into three treatments, foliar and soil applications of ANE (0.2%), and control. Intermediate fruits were harvested and stored for 16 days at 10 ± 1 °C and 90 ± 5% RH to evaluate some postharvest parameters. At harvest, ANE applications increased bioactive compounds, including total polyphenols content (TPC), lycopene, vitamin C and antioxidant activity (AA), as well as chemical parameters like soluble solids and pH. During storage, color parameters, β-carotene, total acidity and firmness tended to decrease as storage time increased. However, TPC, lycopene, vitamin C, AA and weight loss increased during storage. Tomatoes were positively affected by ANE applications on almost every day of storage evaluated, improving their postharvest physiology. Therefore, ANE can be used to extend tomato shelf life and is a great source of beneficial compounds, which are responsible for increasing tomato quality.

海藻提取物已被应用于许多作物中,以促进植物生长,减轻植物胁迫,提高果实品质。藤蔓是一种大型藻类,是植物激素、矿物质、多糖和抗氧化化合物的来源。这些元素可以提高食物的营养价值,有利于人体健康。目的是分析藤茎提取物(Ascophyllum nodosum extract, ANE)在番茄中的应用潜力,以改善其在贮藏过程中的理化和生物活性成分。番茄植株栽培分为叶面和土壤施用ANE(0.2%)和对照3个处理。采集中间果实,在10±1℃、90±5% RH条件下保存16天,评价采后的一些参数。在收获时,施用ANE增加了生物活性成分,包括总多酚含量(TPC)、番茄红素、维生素C和抗氧化活性(AA),以及可溶性固形物和ph等化学参数。在储存期间,颜色参数、β-胡萝卜素、总酸度和硬度随着储存时间的增加而降低。TPC、番茄红素、维生素C、AA和减重均在贮藏期间增加。施用ANE对番茄在贮藏期间几乎每天都有积极影响,改善了番茄采后生理机能。因此,ANE可以用来延长番茄的保质期,并且是有益化合物的重要来源,这些化合物负责提高番茄的品质。
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引用次数: 0
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