首页 > 最新文献

2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)最新文献

英文 中文
Gas sensing oxide materials and methods - past, present and future 气敏氧化物材料和方法——过去、现在和未来
Pub Date : 2012-03-07 DOI: 10.1109/ISPTS.2012.6260964
G. Kale
Metal oxides in different length scales have been used as sensing materials for designing gas sensors for several years. A number of sensor architectures have been explored for developing selective gas sensors that are capable of discriminating between reducing and oxidising gases as well as amongst the gases that are either reducing or oxidising. There is an immense drive towards developing highly selective gas sensors for continuous environmental monitoring and in-line process control in both benign and hostile conditions. Some of the desirable essential features of a typical gas sensor are (1) the ability to discriminate between gases in a real mixture of gases at all temperatures, (2) fast response, (3) rapid recovery, (4) high sensitivity, (5) size, (6) manufacturability, (7) cost effectiveness, (8) signal reproducibility, (9) robustness of signal, (10) compatibility with data logging system and (11) wireless communication. Many of these aspects strongly depend on the synthetic chemistry, crystal structure, film thickness, particle size, porosity, morphology, composition and catalytic properties of the sensing material.This paper will attempt to illustrate how gas sensors research has evolved over the number of years with the advancement in physics and chemistry of materials and what does the future holds for the technology.
近年来,不同长度尺度的金属氧化物被用作气体传感器的传感材料。已经探索了许多传感器架构,用于开发能够区分还原性和氧化性气体以及还原性或氧化性气体的选择性气体传感器。在良好和恶劣条件下,开发高选择性气体传感器用于连续环境监测和在线过程控制是一个巨大的动力。典型气体传感器的一些理想基本特征是:(1)能够在所有温度下区分真实气体混合物中的气体,(2)快速响应,(3)快速恢复,(4)高灵敏度,(5)尺寸,(6)可制造性,(7)成本效益,(8)信号可再现性,(9)信号鲁棒性,(10)与数据记录系统兼容,(11)无线通信。这些方面很大程度上取决于传感材料的合成化学、晶体结构、薄膜厚度、粒度、孔隙度、形貌、组成和催化性能。本文将试图说明气体传感器的研究是如何随着材料的物理和化学的进步而发展的,以及该技术的未来。
{"title":"Gas sensing oxide materials and methods - past, present and future","authors":"G. Kale","doi":"10.1109/ISPTS.2012.6260964","DOIUrl":"https://doi.org/10.1109/ISPTS.2012.6260964","url":null,"abstract":"Metal oxides in different length scales have been used as sensing materials for designing gas sensors for several years. A number of sensor architectures have been explored for developing selective gas sensors that are capable of discriminating between reducing and oxidising gases as well as amongst the gases that are either reducing or oxidising. There is an immense drive towards developing highly selective gas sensors for continuous environmental monitoring and in-line process control in both benign and hostile conditions. Some of the desirable essential features of a typical gas sensor are (1) the ability to discriminate between gases in a real mixture of gases at all temperatures, (2) fast response, (3) rapid recovery, (4) high sensitivity, (5) size, (6) manufacturability, (7) cost effectiveness, (8) signal reproducibility, (9) robustness of signal, (10) compatibility with data logging system and (11) wireless communication. Many of these aspects strongly depend on the synthetic chemistry, crystal structure, film thickness, particle size, porosity, morphology, composition and catalytic properties of the sensing material.This paper will attempt to illustrate how gas sensors research has evolved over the number of years with the advancement in physics and chemistry of materials and what does the future holds for the technology.","PeriodicalId":6431,"journal":{"name":"2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)","volume":"33 1","pages":"1-1"},"PeriodicalIF":0.0,"publicationDate":"2012-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76552637","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Preparation and nitrogen sorption characteristics of Silica aerogel suitable for sensor applications 传感器用二氧化硅气凝胶的制备及氮吸附特性研究
Pub Date : 2012-03-07 DOI: 10.1109/ISPTS.2012.6260889
K. Stanly Jacob, P. A. Abraham, N. Rani Panicker, N. C. Pramanik
Mesoporous silicates have been investigated extensively in recent years for use in sensor systems. Silica aerogels are remarkable for their unique and exceptional properties like high surface area, high meso porosity, low density and tunable pore size and finds potential application in the field of sensor fabrication. Silica gels were prepared through sol-gel process and converted into silica aerogel through super critical drying method using isopropyl alcohol as a solvent. The surface area, pore size distribution, micropore analysis, was carried out using BET method. Low density silica aerogel with 0.30 g/cm3-density and surface area of 350–650 m2/g were prepared.
介孔硅酸盐近年来在传感器系统中的应用得到了广泛的研究。二氧化硅气凝胶具有高表面积、高介孔率、低密度和可调孔径等独特的性能,在传感器制造领域具有潜在的应用前景。采用溶胶-凝胶法制备硅胶,以异丙醇为溶剂,采用超临界干燥法制备硅胶气凝胶。采用BET法进行了比表面积、孔径分布、微孔分析。制备了密度为0.30 g/cm3,表面积为350 ~ 650 m2/g的低密度二氧化硅气凝胶。
{"title":"Preparation and nitrogen sorption characteristics of Silica aerogel suitable for sensor applications","authors":"K. Stanly Jacob, P. A. Abraham, N. Rani Panicker, N. C. Pramanik","doi":"10.1109/ISPTS.2012.6260889","DOIUrl":"https://doi.org/10.1109/ISPTS.2012.6260889","url":null,"abstract":"Mesoporous silicates have been investigated extensively in recent years for use in sensor systems. Silica aerogels are remarkable for their unique and exceptional properties like high surface area, high meso porosity, low density and tunable pore size and finds potential application in the field of sensor fabrication. Silica gels were prepared through sol-gel process and converted into silica aerogel through super critical drying method using isopropyl alcohol as a solvent. The surface area, pore size distribution, micropore analysis, was carried out using BET method. Low density silica aerogel with 0.30 g/cm3-density and surface area of 350–650 m2/g were prepared.","PeriodicalId":6431,"journal":{"name":"2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)","volume":"15 1","pages":"96-97"},"PeriodicalIF":0.0,"publicationDate":"2012-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"90755403","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Gold-graphene nanocomposite based ultrasensitive electrochemical glucose sensor 基于金-石墨烯纳米复合材料的超灵敏电化学葡萄糖传感器
Pub Date : 2012-03-07 DOI: 10.1109/ISPTS.2012.6260947
R. K. Gangwar, V. Dhumale, Arvind Kumar, P. Alegaonkar, Rishi Sharma, Suwarna Datar
Gold-graphene (Au-G) nanocomposite has been synthesized by wet chemical method. Synthesized Au-G nanocomposite was examined under the UV-vis spectroscopy and transmission electron microscopy (TEM). Further Au-G nanocomposite was drop casted onto the glassy carbon electrode (GCE) by immobilizing glucose oxidase (GOx) into it for the electrochemical detection of glucose. Fabricated sensor demonstrates good linear response to glucose in the range 3 to 18 mM with linearity coefficient 0.964.
采用湿化学方法合成了金-石墨烯纳米复合材料。利用紫外可见光谱和透射电子显微镜对合成的金- g纳米复合材料进行了表征。通过固定葡萄糖氧化酶(GOx),进一步将Au-G纳米复合材料滴铸在玻碳电极(GCE)上,用于葡萄糖的电化学检测。该传感器对葡萄糖在3 ~ 18 mM范围内具有良好的线性响应,线性系数为0.964。
{"title":"Gold-graphene nanocomposite based ultrasensitive electrochemical glucose sensor","authors":"R. K. Gangwar, V. Dhumale, Arvind Kumar, P. Alegaonkar, Rishi Sharma, Suwarna Datar","doi":"10.1109/ISPTS.2012.6260947","DOIUrl":"https://doi.org/10.1109/ISPTS.2012.6260947","url":null,"abstract":"Gold-graphene (Au-G) nanocomposite has been synthesized by wet chemical method. Synthesized Au-G nanocomposite was examined under the UV-vis spectroscopy and transmission electron microscopy (TEM). Further Au-G nanocomposite was drop casted onto the glassy carbon electrode (GCE) by immobilizing glucose oxidase (GOx) into it for the electrochemical detection of glucose. Fabricated sensor demonstrates good linear response to glucose in the range 3 to 18 mM with linearity coefficient 0.964.","PeriodicalId":6431,"journal":{"name":"2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)","volume":"12 1","pages":"282-285"},"PeriodicalIF":0.0,"publicationDate":"2012-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85189216","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Analysis, fabrication and testing of ultra high pressure microchannels using LTCC technology 超高压微通道的LTCC技术分析、制造和测试
Pub Date : 2012-03-07 DOI: 10.1109/ISPTS.2012.6260930
R. Hatwar, P. Gandhi, M. D. Atre, Chandrakant Patel, V. Giramkar, S. Joseph, G. Phatak
Several MEMS applications including microturbines, engines, and micro heat exchangers demand ultra high pressure and temperature withstanding microchannels. This paper focuses on design and analysis of such microchannels fabricated using LTCC technology. Extensive FE simulations and analysis are carried out to characterize various design parameters enabling their proper selection. An empirical model with nondimensional variables is proposed to extend applicability of results to high-pressure microchannels of other materials and a typical range of dimensions. Several microchannels are fabricated and tested to pressures upto 8 MPa. Results show that the radius at the corners of microchannels is a significant governing parameter.
包括微型涡轮机、发动机和微型热交换器在内的一些MEMS应用需要超高压和耐温的微通道。本文着重对采用LTCC技术制作的微通道进行了设计和分析。进行了广泛的有限元模拟和分析,以表征各种设计参数,使其能够正确选择。提出了一个无量纲变量的经验模型,将结果的适用性扩展到其他材料的高压微通道和典型的尺寸范围。制作了几个微通道,并在高达8 MPa的压力下进行了测试。结果表明,微通道转角半径是一个重要的控制参数。
{"title":"Analysis, fabrication and testing of ultra high pressure microchannels using LTCC technology","authors":"R. Hatwar, P. Gandhi, M. D. Atre, Chandrakant Patel, V. Giramkar, S. Joseph, G. Phatak","doi":"10.1109/ISPTS.2012.6260930","DOIUrl":"https://doi.org/10.1109/ISPTS.2012.6260930","url":null,"abstract":"Several MEMS applications including microturbines, engines, and micro heat exchangers demand ultra high pressure and temperature withstanding microchannels. This paper focuses on design and analysis of such microchannels fabricated using LTCC technology. Extensive FE simulations and analysis are carried out to characterize various design parameters enabling their proper selection. An empirical model with nondimensional variables is proposed to extend applicability of results to high-pressure microchannels of other materials and a typical range of dimensions. Several microchannels are fabricated and tested to pressures upto 8 MPa. Results show that the radius at the corners of microchannels is a significant governing parameter.","PeriodicalId":6431,"journal":{"name":"2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)","volume":"489 1","pages":"224-227"},"PeriodicalIF":0.0,"publicationDate":"2012-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77782818","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
PEM fuel cells as a power source for wireless sensor networks PEM燃料电池作为无线传感器网络的电源
Pub Date : 2012-03-07 DOI: 10.1109/ISPTS.2012.6260943
V. Devaraj, S. Dinil, M.S. Diju, S. Vineeth, A. Jose, M. Jyothy, M. Neethu
Wireless sensor networks are considered to be one of the key technologies of 21st century. A wireless sensor network consists of spatially distributed sensors used to monitor physical and environmental conditions. The application of wireless sensor networks includes battle field surveillance, industrial process monitoring, environmental pollution monitoring etc. A wireless sensor network generally consists of tens/hundreds of sensor nodes. Each sensor network node consists of a radio transceiver with an antenna, a microcontroller, an electronic circuit for interfacing with the sensors and an energy source. A microcontroller require 1.8mW, transceiver require 67 mW while transmitting and 60 mW while receiving and sensing will require 1.8 mW. Total power needed will come around 75 mW. Here a compact PEM fuel cell is designed which can meet the above power requirements and a typical power generation system is proposed.
无线传感器网络被认为是21世纪的关键技术之一。无线传感器网络由空间分布的传感器组成,用于监测物理和环境条件。无线传感器网络的应用包括战场监视、工业过程监测、环境污染监测等。无线传感器网络通常由数十/数百个传感器节点组成。每个传感器网络节点由带天线的无线电收发器、微控制器、用于与传感器接口的电子电路和能源组成。微控制器需要1.8兆瓦,收发器在发射时需要67兆瓦,接收和传感时需要60兆瓦,需要1.8兆瓦。所需的总功率约为75兆瓦。本文设计了一种能够满足上述功率要求的小型PEM燃料电池,并提出了一种典型的发电系统。
{"title":"PEM fuel cells as a power source for wireless sensor networks","authors":"V. Devaraj, S. Dinil, M.S. Diju, S. Vineeth, A. Jose, M. Jyothy, M. Neethu","doi":"10.1109/ISPTS.2012.6260943","DOIUrl":"https://doi.org/10.1109/ISPTS.2012.6260943","url":null,"abstract":"Wireless sensor networks are considered to be one of the key technologies of 21st century. A wireless sensor network consists of spatially distributed sensors used to monitor physical and environmental conditions. The application of wireless sensor networks includes battle field surveillance, industrial process monitoring, environmental pollution monitoring etc. A wireless sensor network generally consists of tens/hundreds of sensor nodes. Each sensor network node consists of a radio transceiver with an antenna, a microcontroller, an electronic circuit for interfacing with the sensors and an energy source. A microcontroller require 1.8mW, transceiver require 67 mW while transmitting and 60 mW while receiving and sensing will require 1.8 mW. Total power needed will come around 75 mW. Here a compact PEM fuel cell is designed which can meet the above power requirements and a typical power generation system is proposed.","PeriodicalId":6431,"journal":{"name":"2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)","volume":"115 1","pages":"269-273"},"PeriodicalIF":0.0,"publicationDate":"2012-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91493529","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
Design and characterization of magneto-electric sensors. What are the limits? 磁电传感器的设计与表征。限制是什么?
Pub Date : 2012-03-07 DOI: 10.1109/ISPTS.2012.6260932
A. Axelsson, F. Aguesse, M. Valant, N. Alford
Multi-functional materials can respond to more than one external stimulus. Here we will present a magneto-electric system, which couples two switchable states; polarization and magnetisation. In magneto-electric materials, magnetic domains can be tuned by the application of an external electric field and electric domains are switched by a magnetic field via a magneto-electric coupling (ME) across the oxide interface. This two-order coupling can be effectively utilized in the development of multiple state memory elements, tuneable magneto-electric inductors where the electric field tunes the permeability in a voltage variable self-inductance device or as magnetic sensors where the magnetic field produces an electric signal. In the case of magnetic field sensors, their sensitivity, room temperature operation and zero power consumption are particularly attractive. In the area of power electronics such materials show potential as high-quality variable inductors, where miniaturisation of the inductors could enable small, lightweight products.
多功能材料可以对一种以上的外界刺激作出反应。这里我们将提出一个磁电系统,它耦合了两个可切换状态;极化和磁化。在磁电材料中,磁畴可以通过外加电场调谐,而电畴可以通过磁场通过氧化物界面上的磁电耦合(ME)来切换。这种二阶耦合可以有效地用于开发多状态存储元件,可调谐磁电电感器,其中电场可调谐电压可变自感器件中的磁导率,或作为磁场产生电信号的磁传感器。就磁场传感器而言,其灵敏度、室温操作和零功耗特别具有吸引力。在电力电子领域,这种材料显示出作为高质量可变电感器的潜力,其中电感器的小型化可以实现小而轻的产品。
{"title":"Design and characterization of magneto-electric sensors. What are the limits?","authors":"A. Axelsson, F. Aguesse, M. Valant, N. Alford","doi":"10.1109/ISPTS.2012.6260932","DOIUrl":"https://doi.org/10.1109/ISPTS.2012.6260932","url":null,"abstract":"Multi-functional materials can respond to more than one external stimulus. Here we will present a magneto-electric system, which couples two switchable states; polarization and magnetisation. In magneto-electric materials, magnetic domains can be tuned by the application of an external electric field and electric domains are switched by a magnetic field via a magneto-electric coupling (ME) across the oxide interface. This two-order coupling can be effectively utilized in the development of multiple state memory elements, tuneable magneto-electric inductors where the electric field tunes the permeability in a voltage variable self-inductance device or as magnetic sensors where the magnetic field produces an electric signal. In the case of magnetic field sensors, their sensitivity, room temperature operation and zero power consumption are particularly attractive. In the area of power electronics such materials show potential as high-quality variable inductors, where miniaturisation of the inductors could enable small, lightweight products.","PeriodicalId":6431,"journal":{"name":"2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)","volume":"22 8","pages":"1-1"},"PeriodicalIF":0.0,"publicationDate":"2012-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91439661","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Application of machine learning (reinforcement learning) for routing in Wireless Sensor Networks (WSNs) 机器学习(强化学习)在无线传感器网络路由中的应用
Pub Date : 2012-03-07 DOI: 10.1109/ISPTS.2012.6260967
Kaveri Kadam, Navin Srivastava
Traditionally, protocols and applications in the networking domain have been designed to work in large-scale heterogeneous, hierarchically organized networks with low failure rate. In a Wireless Sensor Network (WSN) scenario, new problems arise and traditional routing protocols cannot be successfully applied. Additionally, in energy-restricted environments like WSNs the overhead of keeping routing information fresh becomes unbearable. In this problem context problem context, many researchers have turned their attention to the domain of machine learning (ML). The goal of this paper is to analyze the application of the Reinforcement Learning (specifically Q-learning) for an energy- aware routing scenario.
传统上,网络领域的协议和应用程序被设计为在大规模异构、分层组织的低故障率网络中工作。在无线传感器网络(WSN)场景中,出现了新的问题,传统的路由协议无法成功应用。此外,在像wsn这样的能源限制环境中,保持路由信息新鲜的开销变得难以忍受。在这种问题语境下,许多研究者将注意力转向了机器学习领域。本文的目标是分析强化学习(特别是q -学习)在能量感知路由场景中的应用。
{"title":"Application of machine learning (reinforcement learning) for routing in Wireless Sensor Networks (WSNs)","authors":"Kaveri Kadam, Navin Srivastava","doi":"10.1109/ISPTS.2012.6260967","DOIUrl":"https://doi.org/10.1109/ISPTS.2012.6260967","url":null,"abstract":"Traditionally, protocols and applications in the networking domain have been designed to work in large-scale heterogeneous, hierarchically organized networks with low failure rate. In a Wireless Sensor Network (WSN) scenario, new problems arise and traditional routing protocols cannot be successfully applied. Additionally, in energy-restricted environments like WSNs the overhead of keeping routing information fresh becomes unbearable. In this problem context problem context, many researchers have turned their attention to the domain of machine learning (ML). The goal of this paper is to analyze the application of the Reinforcement Learning (specifically Q-learning) for an energy- aware routing scenario.","PeriodicalId":6431,"journal":{"name":"2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)","volume":"46 1","pages":"349-352"},"PeriodicalIF":0.0,"publicationDate":"2012-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83669120","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 9
Nanoporous materials for energy related and sensing applications 用于能源相关和传感应用的纳米多孔材料
Pub Date : 2012-03-07 DOI: 10.1109/ISPTS.2012.6260972
A. Vinu
Nanoporous non-siliceous materials such as carbons, nitrides, and phosphides have attracted much attention in the recent years due to their enormous applications in the fields of adsorption, catalysis, and fuel cells. However, the incorporation of hetero atoms such as boron and nitrogen in the non-siliceous materials can significantly change their electronic and semi-conducting properties. Firstly I will present some results about the discovery of the nanoporous carbon and nitride materials, and the basics and the mechanism behind the synthesis of various nanoporous nitride materials with different pore structure and textural parameters. Then, the preparation, characterization and the applications of one and three dimensional nanoporous carbon nitrides materials synthesized using various inorganic templates with the different pore structures (MCN-11,2 and MCN-23) through a simple polymerization reaction between ethylenediamine (EDA) and carbon tetrachloride (CTC) will be presented. Moreover, the methods to control the textural parameters and the nitrogen content of the nanoporous carbon nitride materials, which have been solely developed in my group, will also be discussed.4 Not only the powder materials but also the different ways for the fabrication of nanoporous carbon nitride nanoparticles and films with hierarchical ordered structure and morphology will be demonstrated. In addition, I will show some of the results on the preparation of nanoporous boron nitride (MBN) and boron carbon nitride (MBCN) which have been prepared by novel elemental substitution technique5 using nanoporous carbon as the template at very high temperature. In the last part of the talk, I briefly discuss about the different ways of preparing nanoporous carbon materials with various structure types, especially “Carbon Nanocage and Carbon Nanocoops”, and to tune the pore diameters and textural parameters. The applications of the materials including sensing of different molecules and biosensing will be discussed in detail.6−12
近年来,碳、氮化物、磷化物等纳米多孔非硅材料在吸附、催化和燃料电池等领域的广泛应用引起了人们的广泛关注。然而,在非硅质材料中掺入硼和氮等杂原子会显著改变其电子和半导体性能。首先,我将介绍一些关于纳米多孔碳氮材料的发现,以及各种具有不同孔隙结构和结构参数的纳米多孔氮材料的合成基础和机理。然后介绍了以不同孔结构的无机模板(MCN-11、2和MCN-23)为原料,通过乙二胺(EDA)和四氯化碳(CTC)的简单聚合反应合成一维和三维纳米多孔氮化碳材料的制备、表征和应用。此外,还将讨论我课题组单独开发的纳米多孔氮化碳材料的结构参数和含氮量的控制方法不仅介绍了粉末材料,还介绍了制备纳米多孔氮化碳纳米颗粒和具有分层有序结构和形态的薄膜的不同方法。此外,我将展示一些用新型元素取代技术在高温下以纳米多孔碳为模板制备纳米多孔氮化硼(MBN)和氮化硼碳(MBCN)的结果。在讲座的最后部分,我简要讨论了不同结构类型的纳米多孔碳材料的不同制备方法,特别是“碳纳米笼和碳纳米笼”,以及孔径和结构参数的调整。将详细讨论材料的应用,包括不同分子的传感和生物传感。6−12
{"title":"Nanoporous materials for energy related and sensing applications","authors":"A. Vinu","doi":"10.1109/ISPTS.2012.6260972","DOIUrl":"https://doi.org/10.1109/ISPTS.2012.6260972","url":null,"abstract":"Nanoporous non-siliceous materials such as carbons, nitrides, and phosphides have attracted much attention in the recent years due to their enormous applications in the fields of adsorption, catalysis, and fuel cells. However, the incorporation of hetero atoms such as boron and nitrogen in the non-siliceous materials can significantly change their electronic and semi-conducting properties. Firstly I will present some results about the discovery of the nanoporous carbon and nitride materials, and the basics and the mechanism behind the synthesis of various nanoporous nitride materials with different pore structure and textural parameters. Then, the preparation, characterization and the applications of one and three dimensional nanoporous carbon nitrides materials synthesized using various inorganic templates with the different pore structures (MCN-11,2 and MCN-23) through a simple polymerization reaction between ethylenediamine (EDA) and carbon tetrachloride (CTC) will be presented. Moreover, the methods to control the textural parameters and the nitrogen content of the nanoporous carbon nitride materials, which have been solely developed in my group, will also be discussed.4 Not only the powder materials but also the different ways for the fabrication of nanoporous carbon nitride nanoparticles and films with hierarchical ordered structure and morphology will be demonstrated. In addition, I will show some of the results on the preparation of nanoporous boron nitride (MBN) and boron carbon nitride (MBCN) which have been prepared by novel elemental substitution technique5 using nanoporous carbon as the template at very high temperature. In the last part of the talk, I briefly discuss about the different ways of preparing nanoporous carbon materials with various structure types, especially “Carbon Nanocage and Carbon Nanocoops”, and to tune the pore diameters and textural parameters. The applications of the materials including sensing of different molecules and biosensing will be discussed in detail.6−12","PeriodicalId":6431,"journal":{"name":"2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)","volume":"39 1","pages":"1-1"},"PeriodicalIF":0.0,"publicationDate":"2012-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88275056","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis and characterization of In doped ZnO thin films for LPG sensing LPG传感用In掺杂ZnO薄膜的合成与表征
Pub Date : 2012-03-07 DOI: 10.1109/ISPTS.2012.6260965
R. K. Kolhe, K. Kulkarni, K. Sonawane, M. More, S. Gosavi
Thin films of indium doped zinc oxide (In:ZnO) have been deposited onto glass substrates using a facile and inexpensive Spray Pyrolysis method. To reveal the effect of indium concentration on the gas sensing characteristics, thin films were synthesized using different concentration of indium in the precursor. X-ray diffraction (XRD) study indicates formation of crystalline phase of zinc oxide under the prevailing experimental conditions. The scanning electron microscope (SEM) images reveal uniform deposition on the entire substrate surface characterized by granular morphology. A careful observation of the SEM images reveals that nanocrystalline nature of the films, with average grain size ∼ 300 nm. The elemental composition obtained from the Energy Dispersive X-ray Analysis (EDAX) confirms presence of indium along with zinc and oxygen in the synthesized thin films. The gas sensing characteristics of the In-ZnO2 films were investigated for Liquefied Petroleum Gas (LPG) vapours at different operating temperatures in the range of 200 to 320 °C and various vapour concentration values. Interestingly, the In-ZnO thin films exhibited good sensor response in the operating temperature range. The response and recovery times are also in the range of few tens of second. The present results indicate that spray synthesized In-ZnO films have potential towards detection of LPG vapours
采用喷雾热解的方法在玻璃衬底上制备了铟掺杂氧化锌(In:ZnO)薄膜。为了揭示铟浓度对气敏特性的影响,在前驱体中加入不同浓度的铟,合成了薄膜。x射线衍射(XRD)研究表明,在现行的实验条件下,氧化锌形成了结晶相。扫描电子显微镜(SEM)图像显示整个衬底表面均匀沉积,具有颗粒状形貌。对扫描电镜图像的仔细观察表明,薄膜具有纳米晶的性质,平均晶粒尺寸为~ 300 nm。从能量色散x射线分析(EDAX)中获得的元素组成证实,在合成的薄膜中存在铟、锌和氧。研究了in - zno2薄膜在200 ~ 320℃不同工作温度和不同蒸气浓度下对液化石油气(LPG)蒸气的气敏特性。有趣的是,in - zno薄膜在工作温度范围内表现出良好的传感器响应。响应和恢复时间也在几十秒的范围内。本研究结果表明,喷雾合成的In-ZnO薄膜具有检测LPG蒸气的潜力
{"title":"Synthesis and characterization of In doped ZnO thin films for LPG sensing","authors":"R. K. Kolhe, K. Kulkarni, K. Sonawane, M. More, S. Gosavi","doi":"10.1109/ISPTS.2012.6260965","DOIUrl":"https://doi.org/10.1109/ISPTS.2012.6260965","url":null,"abstract":"Thin films of indium doped zinc oxide (In:ZnO) have been deposited onto glass substrates using a facile and inexpensive Spray Pyrolysis method. To reveal the effect of indium concentration on the gas sensing characteristics, thin films were synthesized using different concentration of indium in the precursor. X-ray diffraction (XRD) study indicates formation of crystalline phase of zinc oxide under the prevailing experimental conditions. The scanning electron microscope (SEM) images reveal uniform deposition on the entire substrate surface characterized by granular morphology. A careful observation of the SEM images reveals that nanocrystalline nature of the films, with average grain size ∼ 300 nm. The elemental composition obtained from the Energy Dispersive X-ray Analysis (EDAX) confirms presence of indium along with zinc and oxygen in the synthesized thin films. The gas sensing characteristics of the In-ZnO2 films were investigated for Liquefied Petroleum Gas (LPG) vapours at different operating temperatures in the range of 200 to 320 °C and various vapour concentration values. Interestingly, the In-ZnO thin films exhibited good sensor response in the operating temperature range. The response and recovery times are also in the range of few tens of second. The present results indicate that spray synthesized In-ZnO films have potential towards detection of LPG vapours","PeriodicalId":6431,"journal":{"name":"2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)","volume":"62 1","pages":"346-348"},"PeriodicalIF":0.0,"publicationDate":"2012-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"79153783","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
Quartz crystal microbalance sensors for discrimination of black tea 用于红茶鉴别的石英晶体微天平传感器
Pub Date : 2012-03-07 DOI: 10.1109/ISPTS.2012.6260906
Prolay Sharma, Arunangshu Ghosh, B. Tudu, R. Bandyopadhyay, N. Bhattacharyya, A. Chatterjee
The quality evaluation of black tea is based on organoleptic methods of “Tea- tasters”. However the present quality estimation involving Tea-tasters is not a very reliable method as professional acumen, mood and other personal factors affect the judgment of tea quality. Electronic nose consists of an array of gas sensors with overlapping selectivity patterns, signal handling and classifier modules. An array of quartz crystal microbalance (QCM) sensors has been developed to differentiate among different tea samples. The important volatile components responsible for aroma of tea have been considered and the corresponding sensing materials have been identified. Five AT-cut 10 MHz Quartz crystal blanks coated with different sensing materials have been used to differentiate the aroma of orthodox and cut-tear-curl (CTC) tea samples. The developed sensors can distinguish not only between the orthodox and CTC tea but distinct clusters are also obtained for the four different tea-samples, as visualized through principal component analysis (PCA).
红茶的品质评价以“品茶师”的感官方法为基础。然而,目前由品茶者参与的品茶质量评价方法并不十分可靠,因为专业敏誉度、心情等个人因素会影响品茶者对茶叶质量的判断。电子鼻由一系列具有重叠选择模式、信号处理和分类模块的气体传感器组成。研制了一种石英晶体微天平(QCM)传感器阵列,用于区分不同茶叶样品。研究了茶叶香气的重要挥发性成分,并确定了相应的传感材料。用5个at切割的10 MHz石英晶体毛坯包覆不同的传感材料,对传统茶和切割茶的香气进行了区分。所开发的传感器不仅可以区分正统茶和CTC茶,而且可以通过主成分分析(PCA)对四种不同的茶样品进行可视化分析,得到不同的聚类。
{"title":"Quartz crystal microbalance sensors for discrimination of black tea","authors":"Prolay Sharma, Arunangshu Ghosh, B. Tudu, R. Bandyopadhyay, N. Bhattacharyya, A. Chatterjee","doi":"10.1109/ISPTS.2012.6260906","DOIUrl":"https://doi.org/10.1109/ISPTS.2012.6260906","url":null,"abstract":"The quality evaluation of black tea is based on organoleptic methods of “Tea- tasters”. However the present quality estimation involving Tea-tasters is not a very reliable method as professional acumen, mood and other personal factors affect the judgment of tea quality. Electronic nose consists of an array of gas sensors with overlapping selectivity patterns, signal handling and classifier modules. An array of quartz crystal microbalance (QCM) sensors has been developed to differentiate among different tea samples. The important volatile components responsible for aroma of tea have been considered and the corresponding sensing materials have been identified. Five AT-cut 10 MHz Quartz crystal blanks coated with different sensing materials have been used to differentiate the aroma of orthodox and cut-tear-curl (CTC) tea samples. The developed sensors can distinguish not only between the orthodox and CTC tea but distinct clusters are also obtained for the four different tea-samples, as visualized through principal component analysis (PCA).","PeriodicalId":6431,"journal":{"name":"2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)","volume":"8 1","pages":"153-156"},"PeriodicalIF":0.0,"publicationDate":"2012-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76317004","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
期刊
2012 1st International Symposium on Physics and Technology of Sensors (ISPTS-1)
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1